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DOTD TR 202-08

Rev. 08/08
Page 1 of 11
Method A

Method of Test for


AIR CONTENT OF FRESHLY MIXED CONCRETE
DOTD Designation: TR 202-08

METHOD A - VOLUMETRIC METHOD

I. Scope 1. The bowl and top sections shall be of


sufficient thickness and rigidity to
A. This method of test covers the procedure withstand rough field use. The
for determining the air content of freshly material shall not be attacked by high
mixed concrete with a slump of 1 in. (25 pH cement paste, deform when
mm) or greater by determining the stored at high temperatures in closed
volumetric displacement of air with water spaces, or become brittle or crack at
after thorough agitation. This method low temperatures. A watertight seal
should not be used with aggregates must be obtained when the top
greater than 1.5 inch. This is the section is attached to the bowl.
appropriate method to use when the 2. Bowl - shall have a diameter equal to
concrete contains lightweight or highly 1 to 1.25 times the height and be
porous aggregates. This is the only constructed with a flange at or near
method allowed for concrete with the top surface. Bowls shall not have
aggregate absorption of 4.0% or greater. a capacity of less than 0.075 ft3 (0.002
m3).
Note A-1: When the concrete contains aggregates larger 3. Top section - shall have a capacity at
than 1.5 inch, wet sieve over the 1in. sieve, least 20% larger than the bowl and
discard the larger aggregates, and then shall be equipped with a flexible
proceed with the slump test. gasket and a device to attach the top
section to the bowl. The top section
B. Reference Documents shall be equipped with a transparent
1. DOTD S301 - Sampling Fresh scale, graduated in increments (not
Concrete greater than 0.5%) from 0 at the top to
2. DOTD TR 640 – Calibration of 9% or more, of the volume of the
Measures Used to Determine Unit bowl. The upper end of the neck shall
Weights have a watertight cap that will
3. ASTM C 173-07 – Air Content of maintain a watertight seal when the
Freshly Mixed Concrete by the meter is inverted and rolled.
Volumetric Method

Note A-2: ASTM C173-07 may be used in lieu of this


method.

II. Apparatus

A. Air meter – consisting of a bowl and a top


section conforming to the following
requirements. (Figure 1) Figure 1
DOTD 202-08
Rev. 08/08
Page 2 of 11
Method A

B. Funnel - with a spout of a size J. Glass plate - at least ½ in. (13 mm)
permitting it to be inserted through thick with a length and width at least
the neck of the top section and long 2 in. (50 mm) greater than the
enough to extend to a point just above diameter of the bowl.
the bottom of the top section. The K. Mallet – (with a rubber or rawhide
discharge end of the spout shall be so head) with a mass approximately
constructed that when water is added 1.25±0.5 lb. (600 ±200 g).
to the container there will be a L. Paper Towel
minimum disturbance of the concrete. M. Applicable Documentation
C. Tamping rod - a round, smooth 1. Batch Certification for Portland
straight ⅝ ± 1/16 in. [16 ± 2 mm] Cement Concrete (DOTD 03-22-
diameter rod at least 12 in [300 mm] 4028)
long with both ends rounded to a 2. Structural Concrete Tests (DOTD
hemispherical tip of the same 03-22-0740, Figure 2)
diameter. The rod shall be made of 3. Portland Cement Concrete Report
steel, high-density polyethylene, or (DOTD 03-22-4035)
other plastic of equal or greater 4. Approved computer generated
abrasion resistance. forms or spreadsheets.
D. Strike-off Bar - a flat, straight steel
bar at least ⅛x¾x12 in. [3x20x300 III. Health Precautions
mm] or a flat, straight high-density
polyethylene bar, or other plastic of A. Protect against potential injury by
equal or greater abrasion resistance, avoiding skin contact with fresh concrete
at least ¼x¾x12 in. [6x20x300 mm]. by wearing appropriate protective clothing
E. Calibrated cup - a metal or plastic and eye wear.
cup either having a capacity of or B. If the freshly mixed concrete should
being graduated in increments equal contact skin or eyes, immediately flush
to 1.00 ± 0.04% of the volume of the with water for a minimum of 5 minutes. If
bowl of the air meter. symptoms continue, consult a physician
F. Syringe - a small rubber bulb syringe immediately.
C. Observe all precautions as specified by the
having a capacity of at least that of
manufacturer before handling fresh
the calibrated cup.
concrete.
G. Pouring vessel (for water) - a
container having a capacity of
IV. Calibration of Apparatus
approximately 1 qt (1 L).
H. Scoop - a small metal scoop
A. Calibrate the meter and calibrated cup
I. Isopropyl alcohol - 70% by volume
initially and annually or whenever there is
isopropyl alcohol (approximately 65%
reason to suspect damage or deformation
by weight).
of the meter or calibrated cup.
B. Determine the volume of the bowl with an
Note A-3: 70% isopropyl alcohol is commonly available as
accuracy of at least 0.1%. Follow the
rubbing alcohol. More concentrated grades can be
diluted with water to obtain the required calibration procedure in accordance with
concentration. DOTD TR 640.
DOTD TR 202-08
Rev. 08/08
Page 3 of 11
Method A

C. Determine the volume of the calibrated Note A-4: After tapping the final layer, a slight excess of
cup using water in accordance with DOTD concrete, ⅛ in. (3 mm) or less, above the rim
TR 640. A quick check can be made by is acceptable. Add or remove a representative
adding one or more calibrated cups of sample of concrete if necessary to obtain the
water to the assembled apparatus and required amount of concrete.
observing the increase in the height of the
water column after filling to a given level. F. Strike off excess concrete with the strike-
D. Determine the accuracy of the graduations off bar until the surface is flush with the
on the neck of the top section of the air top of the bowl and free of voids. Wipe
meter by filling the assembled measuring the flange of the bowl clean.
bowl and top section with water to the G. Wet the inside of the top section of the
level of the mark for highest air content meter, including the gasket, and attach the
graduation. top section to the bowl.
E. Add water in increments of 1.0% of the H. Insert the funnel and add water until it
volume of the bowl to check accuracy appears in the neck.
throughout the graduated range of air I. Remove the funnel and adjust the water
content. The error at any point throughout level, using the rubber syringe, until the
the graduated range shall not exceed 0.1% bottom of the meniscus is level with zero
of air. mark.
J. Attach and tighten the cap.
V. Sample K. Invert the meter, shake the base
horizontally, and return the meter to the
Obtain the sample of mixed concrete in upright position.
accordance with DOTD S301 of the Materials
Sampling Manual and meet the minimum Note A-5: To prevent the aggregate from lodging in the
sample quantity of 0.25 cu. ft. (0.01 cu. meters). neck of the unit, do not keep it inverted for
more than 5 seconds at a time.
VI. Procedure
L. Repeat the inversion and shaking process
A. Wet the inside of the bowl and dry it to a for a minimum of 45 seconds and until the
damp, but not shiny appearance. concrete has broken free and the aggregate
B. Using the scoop, fill the bowl with mixed can be heard moving in the meter as it is
concrete in two equal layers of equal inverted.
depth. M. Place one hand on the neck of the meter
C. Rod after each layer 25 times with the and the other on the flange. Using the
tamping rod. Do not forcibly strike the hand on the neck, tilt the top of the meter
bottom of the bowl when rodding the first approximately 45° from the vertical
layer. position with the bottom edge of the base
D. When rodding the second layer, penetrate of the meter resting on the floor or on the
the prior layer approximately 1 in. work surface. Maintain this position
(25mm). through the procedures described in this
E. After each layer is rodded, tap the sides of section.
the bowl 10 to 15 times with the mallet to N. Using the hand on the flange to rotate the
close any voids left by the tamping rod meter; vigorously roll the meter ¼ to ½
and to release any large bubbles of air that turn forward and back several times,
may have been trapped. quickly starting and stopping the roll.
DOTD 202-08
Rev. 08/08
Page 4 of 11
Method A

O. Turn the base of the meter about ⅓ turn VII. Calculations


and repeat the rolling procedure as stated
previously. Calculate the total air content (TA) of the
P. Continue the turning and rolling concrete in the measuring bowl to the nearest
procedures for approximately 1 minute. 0.25 percent by using the following formula.

Note A-6: The aggregate must be heard sliding in the TA = R1 + R2


meter during this process.
where:
Note A-7: If, at any time during the inversion and
rolling procedures liquid is found to be leaking R1 = reading directly in the neck, after
from the meter, the test is invalid and a new the alcohol was added.
test shall be started as in Section V. R2 = number of cups filled with alcohol
used.
Q. Set the unit upright and allow the meter to
stand while the air rises to the top and example:
until the liquid level stabilizes. The liquid
level is considered stable when no further R1 = 4.25%
drop in the water column is observed. R2 = 2.0
R. When all the air has been removed from
the concrete and allowed to rise to the top TA = 4.25 + 2.0
of the apparatus, remove the screw cap. = 6.25%
S. Using the syringe, add sufficient isopropyl
alcohol in calibrated cup increments to VIII. Report
dispel the foamy mass on the surface of
the water. Record the number of Round and report air content to the nearest
calibrated cups used on the back of DOTD 0.1%.
Form 03-22-0740 (Figure 2).
T. Make a direct reading of the liquid in the IX. Normal Test Reporting Time
neck, reading to the bottom of the
meniscus and estimate to the nearest The normal test reporting time is 15 minutes.
(0.25%) of air.
DOTD TR 202-08
Rev. 08/08
Page 5 of 11
Method A

Figure 2
DOTD 202-08
Rev. 08/08
Page 6 of 11
Method B

DOTD Designation: TR 202-08


METHOD B – PRESSURE METHOD

I. Scope

A. This method of test covers the concrete sample. The dial on the pressure
determination the air content of freshly gage shall be calibrated in terms of percent
mixed concrete for all ranges of slump but air for the observed pressure at which
not for nonplastic concrete such as is equalization takes place. (Figure 3)
commonly used in the manufacture of 1. Measuring bowl - a flanged or
pipe and concrete masonry units. This is otherwise constructed cylindrical
the only method allowed for concrete bowl, made of hard metal not readily
containing aggregates greater than 1.5 attacked by cement paste, having a
inch. This method shall only be used for diameter equal to 0.75 to 1.25 times
concrete containing aggregates with the height and a capacity of at least
absorption less than 4.0%. If aggregate 0.20 ft3 (0.006 m3).
absorption is 4.0% or greater, use Method 2. Cover assembly - shall be made of
A. This method is not applicable to hard metal or other hard material not
concrete made with lightweight readily attacked by the cement paste.
aggregates or air-cooled blast furnace slag. It shall have smoothly machined
interior surfaces contoured to provide
B. Reference Documents an air space above the level of the top
1. DOTD TR 201 - Mass Per Cubic of the measuring bowl. It shall be
Meter, Yield, and Air Content flanged or otherwise constructed such
(Gravimetric) of Concrete that the cover and the measuring
2. DOTD S301 - Sampling Fresh bowl can be fitted together into a
Concrete pressure-tight assembly. The cover
3. DOTD TR 640 – Calibration of shall be fitted with a gage for
Measures Used to Determine Unit obtaining a direct reading of air
Weights content. The graduations for a
4. ASTM C192-06 – Standard Practice suitable range in air content shall be
for making and Curing Concrete Test within 0.1%. The cover shall be fitted
Specimens for the Laboratory with an air bleeder valve for venting
5. ASTM C 231-04 – Air Content of of the air chamber, a main air valve,
Freshly Mixed Concrete by the and petcocks for bleeding off water as
Pressure Method required. Suitable means of clamping
the cover to the bowl shall be
II. Apparatus provided to make a pressure-tight
seal without entrapping air at the
A. Air meter - consisting of a measuring bowl joint between the flanges of the cover
and cover assembly conforming to the and bowl. A suitable hand pump
requirements shown below. The operating shall be provided with the cover,
principle of this meter consists of either as an attachment or as an
equalizing a known volume of air at a accessory.
known pressure in a sealed air chamber
with the unknown volume of air in the
DOTD TR 202-08
Rev. 08/08
Page 7 of 11
Method B

kg) for use with measures larger than 0.5


ft3 (14 m3).
G. Strike-off Bar - a flat, straight steel bar at
least ⅛x¾x12 in. [3x20x300 mm] or a flat,
straight high-density polyethylene bar, or
other plastic of equal or greater abrasion
resistance, at least ¼x¾x12 in. [6x20x300
mm].
H. Strike-off Plate – a flat, rectangular metal
plate at least ¼ in. (6 mm) thick or a glass
or acrylic plate at least ½ in. (12 mm) thick
with a length and width at least 2 in. (50
mm) greater than the diameter of the
Figure 3 measure with which it is to be used. The
edges of the plate shall be straight and
B. Calibration Vessel - a measure having an smooth within a tolerance of 1/16 in. (1.5
internal volume equal to an even (whole) mm).
percentage of the volume of the measuring I. Vibrator with Power Source – (when
bowl corresponding to the approximate required) as described in ASTM C192-06.
percent of air in the concrete to be tested; J. Container - having a ½ or 1 gal. (2 or 4 L)
or, if smaller, it shall be possible to check capacity as required shall be provided to
calibration of the meter indicator at the fill the assembled air meter with water
approximate percent of air in the concrete from the top of the concrete to overflow at
to be tested by repeated filling of the the petcock.
measure. K. Scoop - a small metal scoop
C. Syringe – a small rubber bulb syringe L. Scale - of sufficient capacity to determine
D. Calibration Tubes - auxiliary calibration the weights of fine and coarse aggregates
tubes of approximate diameters provided required for the determination of the
either as an integral part of the cover aggregate correction factor in Step IV.O.
assembly or separately, shall be M. Paper Towel, Towel or Sponge
constructed to assist in adding and N. Personal protective equipment- rubber
removing water from the container during boots, gloves, eye and ear protection, etc.
the aggregate correction factor O. Applicable Documentation
determination. 1. Batch Certification for Portland
E. Tamping Rod – shall be a round, straight Cement Concrete (DOTD 03-22-4028)
steel rod, ⅝ in. (16 mm) in diameter and 2. Structural Concrete Tests (DOTD 03-
not less than 16 in. (400 mm) in length, 22-0740)
having the tamping end rounded to a 3. Portland Cement Concrete Report
hemispherical tip the diameter ⅝ in. (16 (DOTD 03-22-4035)
mm). 4. Approved computer generated forms
F. Mallet - with a rubber or rawhide head, or spreadsheets
weighing 1.25± 0.50 lb. (0.57 ± 0.23 kg) for
use with measures of 0.5 ft3 (14 m3) or III. Health Precautions
smaller, and a mallet weighing A. Protect against potential injury by
approximately 2.25 ± 0.50 lb (1.02 ± 0.23 avoiding skin contact with fresh concrete
DOTD 202-08
Rev. 08/08
Page 8 of 11
Method B

by wearing appropriate protective measuring bowl with water. Screw the


clothing and eye wear. short piece of tubing or pipe furnished
B. If the freshly mixed concrete should with the apparatus into the threaded
contact skin or eye(s), immediately flush petcock hole on the underside of the cover
with water for a minimum of 5 minutes. If assembly. Assemble the apparatus. Close
symptoms continue, consult a physician the air valve between the air chamber and
immediately. the measuring bowl and open the two
C. Observe all precautions as specified by the petcocks on holes through the cover
manufacturer before handling fresh assembly. Add water through the petcock
concrete. on the cover assembly having the
extension below until all air is expelled
IV. Calibration from the second petcock.
F. Pump air into the air chamber until the
Note B-1: Rough handling will affect the calibration of pressure reaches the indicated initial
pressure-type apparatus for the determination pressure line.
of air content. Should the accuracy of the air G. Allow a few seconds for the compressed
meter be questioned, it should be returned to air to cool to normal temperature.
the Materials and Testing Section for a Stabilize the gage hand at the initial
calibration check. pressure line by pumping or bleeding off
air as necessary tapping the gage lightly.
A. Calibration Vessel – Determine the weight Close the petcock opposite the tube or pipe
of water, Τ, required to fill the calibration extension on the under side of the cover.
vessel in accordance with DOTD TR 640 H. Remove water from the assembly to the
Steps III(a) to III(c). calibrating vessel controlling the flow.
B. Measuring Bowl – Determine the weight of
water, W, required to fill the measuring Note B-2: Depending on the particular meter design, by
bowl, in accordance with DOTD TR 640 opening the petcock provided with the tube or
Steps III(a) to III(c). pipe extension and opening the air valve
C. Effective Volume of the Calibration Vessel – between the air chamber and the measuring
The constant R, represents the effective bowl, or by opening the air valve and using
volume of the calibration vessel expressed the petcock to control flow.
as a percentage of the volume of the
measuring bowl: I. Perform the calibration at an air content
which is within the normal range of use.
R, % = 100 x (ω W )
where, Note B-3: If the calibration vessel has a capacity within
Τ = weight of water required to fill the normal range of use, remove exactly that
calibration vessel amount of water.
W = weight of water required to fill
measuring bowl J. With some meters, the calibrating vessel is
quite small and it will be necessary to
D. Initial Pressure Line Calibration – Follow the remove several times that volume to
manufacturer’s recommendations for obtain air content within the norm range
obtaining the initial pressure line. of use. In this instance, carefully collect
E. Calibration Test to Check the Air Content the water in an auxiliary container and
Graduations on the Pressure Gage – Fill the determine the amount removed by
DOTD TR 202-08
Rev. 08/08
Page 9 of 11
Method B

weighing to the nearest 0.1%. Calculate de-aerated water which can be obtained by
the correct air content, R. cooling hot water to room temperature.
K. Release the air from the apparatus at the
petcock not used for filling the calibration O. Determine the aggregate correction factor, G,
vessel. on a combined sample of fine and coarse
aggregated as follows:
Note B-4: If the apparatus employs an auxiliary tube for
filling the calibration container, open the 1. Mix representative samples of fine
petcock to which the tube is connected to drain aggregate of weight, Fs, and coarse
the tube back into the measuring bowl. aggregate of weight, Cs, and place in
the measuring bowl.
Note B-5: At this point, the measuring bowl contains the 2. Fill the bowl ⅓ full of water.
percentage of air determined by the calibration 3. Add the mixed aggregate a small
test of the calibrating vessel. amount at a time until all of the
aggregate is covered with water.
K. Pump air into the air chamber until the 4. Add each scoopful in a manner that
pressure reaches the initial pressure line will entrap as little air as possible and
marked on the pressure gage, close both remove accumulations of foam
petcocks in the cover assembly, and then promptly.
open the valve between the air chamber 5. Tap the sides of the bowl and lightly
and the measuring bowl. rod the upper inch (25mm) of the
aggregate about 10 times and stir
Note B-6: Refer to manufacturer’s directives to after each addition of aggregate to
determine and verify the initial pressure line. eliminate entrapped air.
6. When all aggregate has been placed
L. If two or more determinations show the in the bowl and allowed to soak for at
same variation from the correct air content, least 5 minutes, strike off all foam and
reset the dial hand to the correct air excess water.
content and repeat the test until the gage 7. Thoroughly clean the flanges of both
reading corresponds to the calibrated air the bowl and conical cover so that
content within 0.1%. when the cover is clamped in place, a
M. If the dial hand was reset to obtain the pressure-tight seal will be obtained.
correct air content, recheck the initial 8. Attach the cover assembly to the
pressure mark. measuring bowl.
N. If a new initial pressure reading is 9. With both petcocks open, pump air
required, repeat the calibration to check into the air chamber until the
the accuracy of the graduation on the predetermined initial pressure line is
pressure gage described earlier in Step reached.
IV.D. 10. Close both petcocks and open the
main air valve between the air
Note B-7: If difficulty is encountered in obtaining chamber and measuring bowl.
consistent readings, check for leaks, for the 11. Read the air content scale and record
presence of water inside the air chamber, or as the aggregate correction factor, G.
the presence of air bubbles clinging to the 12. See Steps VII.A. for calculations for
inside surfaces of the meter from the use of determination of Fs and Cs.
cool aerated water. In this latter instance, use
DOTD 202-08
Rev. 08/08
Page 10 of 11
Method B

Note B-8: Ensure all petcocks and bleeder valves are F. Using a syringe, inject water through one
closed to prevent water from entering pump petcock until water emerges from the
chamber. opposite petcock.
G. Place a thumb over one petcock and tilt
Note B-9: The aggregate correction factor must be slightly to expel air bubbles from this same
determined for each portland cement concrete petcock. Turn to original position and
mix design, at the beginning of each project, readjust water.
or whenever there is a change in the aggregate
properties. Note B-10: If water level changes, there is a leak.

V. Sample H. Close the air bleeder valve on the air


chamber and pump air into the air
Obtain a representative sample of the concrete chamber until the gage hand is on the
to be tested in accordance with DOTD S 301 initial pressure line. Allow a few seconds
and meet the minimum sample quantity of 0.50 for the compressed air to cool to normal
cu. ft. (0.01 cu. meters). temperature.
I. Stabilize the gage hand at the initial
VI. Procedure pressure line by pumping or bleeding-off
air as necessary, taping the gage lightly.
A. Place the concrete in the measuring bowl J. Close both petcocks and open the main air
in three layers of approximately equal valve between the air chamber and the
volume. Consolidate each layer of measuring bowl. Tap the sides of the
concrete by 25 strokes of the tamping rod measuring bowl sharply to relieve local
evenly distributed over the cross section. restraints. Lightly tap the pressure gage to
B. After each layer is rodded, strike the sides stabilize the gage and read the percentage
of the measure 10 to 15 times with the of air, A1, on the dial of the pressure gage.
mallet to close any voids left by the K. Make sure the main air valve is closed and
tamping rod and to release any large release the pressure by opening both
bubbles of air that may have been trapped. petcocks before removing the cover.
C. Rod the bottom layer throughout its depth, L. Determine air content, A, in accordance
taking care not to allow the rod to forcibly with Step VII.B.
strike the bottom of the measure. In
rodding the second and final layers, use VII. Calculations
only enough force to cause the rod to
penetrate the surface of the previous layer A. Determination of Aggregate Correction
about 1 in. (25 mm). When adding the Factor
final layer of concrete, be careful not to
overfill the measure. 1. Calculate the weights of fine and
D. After consolidating the concrete, strike off coarse aggregate present in the
the excess concrete with the strike-off bar volume, S, of the sample of fresh
until the surface is flush with the top of the concrete whose air content is to be
bowl. Wipe the flange of the bowl clean. determined, as follows:
E. Assemble the apparatus, close the main air
valve between the air chamber and the S
Fs = x Fb
measuring bowl and open both petcocks. B
DOTD TR 202-08
Rev. 08/08
Page 11 of 11
Method B

S B. Calculate the air content, A, of the concrete


Cs = x Cb
B to the nearest 0.1 % by using the following
formula:

where: A = A1 - G

Fs = weight of fine aggregate in concrete where:


sample under test, lb (kg)
S = volume of concrete sample (same A = air content, percentage by volume of
as volume of measuring bowl of concrete
apparatus), ft3 (m3) A1 = apparent air content of the sample,
B = volume of concrete produced per percentage by volume of concrete
batch (Note B-9), ft3 (m3) G = aggregate correction factor,
Fb = total weight of fine aggregate in percentage by volume of concrete, (see
batch, lb (kg) Step IV. O.)
Cs = weight of coarse aggregate in
concrete sample under test, lb (kg) example:
Cb = total weight of coarse aggregate in
batch, lb (kg) A1 = 7.2%
G = 0.2%
Note B-11: The volume of concrete produced per batch
can be determined in accordance with DOTD A = 7.2 - 0.2
TR 201 part 6(b). = 7.0%

example:
VIII. Report
S = 0.25 ft3
B = 217.8 ft3 Report the air content to the nearest 0.1%.
Fb = 10,848 lb
Cb = 13,627 lb IX. Normal Test Reporting Time

0.25 The normal test reporting time is 15 minutes.


Fs = × 10848
217.8

= 12.45 lb

0.25
Cs = × 13627
217.8

= 15.64 lb

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