A.

Apparatus and Chemicals

1. Apparatus
a. Round flask 500 mL 1 piece
b. Beaker glass 500 mL 1 piece
c. Beaker glass 250 mL 4 pieces
d. Beaker glass 100 mL 1 piece
e. Graduated cylinder 50 mL 1 piece
f. Graduated cylinder 10 mL 1 piece
g. Soxhlet 1 piece
h. Buchner funnel 1 piece
i. Funnel 1 piece
j. Spatula 1 piece
k. Stir bar 1 piece
l. Evaporating dish 2 pieces
m. Separation funnel 250 mL 1 piece
n. Lighter 1 piece
o. Stative 2 pieces
p. Clamp 2 pieces
q. Analytical balance 1 piece
r. Tripod 1 piece
s. Gauze 1 piece
t. Spiritus burner 1 piece
u. Hot plate 2 pieces
v. Wood clamp 2 pieces
w. Drop pipette 3 pieces
x. Soft cloth 3 pieces
y. Spray bottle 1 piece
z. Vacuum pump 1 piece
aa. Stopwatch 1 piece
bb. Scissors 1 piece
cc. Oven 1 piece
 dd. Water bath 1 piece
ee. Filtering flask 1 piece
ff. Minichiller 1 piece
gg. Hose 2 pieces
hh. Reflux condenser 1 piece
2. Chemicals
a. Ethanol (C2H5OH)
b. Sulphuric acid dilute (H2SO4)
c. Chloroform (CHCl3)
d. Magnesium oxide (MgO)
e. Aquadest (H2O)
f. Sodium hydroxide (NaOH)
g. Aluminium foil (Al2O3(s))
h. Ice (H2O(s))
i. Vaseline
j. Tea
k. Whatman filter paper
l. Filter paper
m. Cotton
n. Tissue
o. Boiling stone
p. Thread

Data Analysis

Known,
Mass of sample (tea) = 25 grams
Mass of caffeine crystal = 0 grams
Asked,
% rendament of caffeine = …?
Solution,
4%
Mass of theory = × 25 grams
100 %
= 1 grams
mass of experiment
% rendament of caffeine = ×100 %
mass of theory
0 grams
= ×100 %
1 grams
=0%