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Impact Behavior of Hybrid Glass/Carbon Epoxy Composites: M. J. Pe Rez-Martı N
Impact Behavior of Hybrid Glass/Carbon Epoxy Composites: M. J. Pe Rez-Martı N
Pérez-Martı́n1
Department of Materials Science,
E.T.S.I. Caminos,
Canales y Puertos,
Universidad Politécnica de Madrid (UPM),
28040, Madrid, Spain
Impact Behavior of Hybrid
e-mail: mariajesus.perez@mater.upm.es
Glass/Carbon Epoxy Composites
A. Enfedaque
Department of Civil Engineering: Construction, The high velocity impact performance in hybrid woven carbon and S2 and E glass fab-
E.T.S.I. Caminos, ric laminates manufactured by resin transfer molding (RTM) was studied. Specimens
Canales y Puertos, with different thicknesses and glass-fiber content were tested against 5.5 mm spherical
Universidad Politécnica de Madrid (UPM), projectiles with impact velocities ranging from 300 to 700 m/s to obtain the ballistic
28040, Madrid, Spain limit. The resulting deformation and fracture micromechanisms were studied. Several
impacts were performed on the same specimens to identify the multihit behavior of such
W. Dickson laminates. The results of the fracture analysis, in conjunction with those of the impact
Massachusetts Institute of Technology (MIT), tests, were used to describe the role played by glass-fiber hybridization on the fracture
Cambridge, MA 02139 micromechanisms and on the overall laminate performance under high velocity impact.
[DOI: 10.1115/1.4023344]
F. Gálvez
Department of Materials Science, Keywords: impact behavior, multihit behavior, hybrid composites, fracture
E.T.S.I. Caminos, micromechanisms
Canales y Puertos,
Universidad Politécnica de Madrid (UPM),
28040, Madrid, Spain
to compare the performance of the glass fibers with the behavior be seen in the shots made at 400 m/s and above. The results of
aforementioned. these tests form a straight line and therefore the increment of the
All the laminates were ultrasonically inspected after manufac- residual speed is proportional to that of the impact speed.
turing and were free of macroscopic defects. The actual thickness Once the first test was conducted a second shot was performed
of each laminate was determined as the average of eight measure- in order to study the multihit behavior of the laminates. The
ments carried out with a 0.01 mm resolution micrometer. Areal results of these tests are represented as hollow symbols in
density was computed by weighting the plate with a balance with the Fig. 2, whereas the distance between the center of the first and
a resolution of 0.01 g and using the thickness previously obtained. the second impact is shown in millimetres. The hollow symbols
Square specimens of 50 50 mm were obtained from the lami- are plotted near or right on top of the full ones, except the projec-
nates. The samples were tested on a SABRE A1þ gas gun. The tile that impacted at 6.3 mm. Comparing the residual velocity of
projectiles used were 5.5 mm ball of high strength steel using a this second impact (V0 ¼ 393 m/s, Vr ¼ 257 m/s) with the nearest
sabot to fit on a 7.62 barrel. They were fired using air compressed first one result (V0 ¼ 393 m/s, Vr ¼ 216 m/s) there is a 41 m/s ve-
or helium, with both varying the pressure from 50 bar to 200 bar locity increment. Based in these results it can be stated that if the
and achieving projectile velocities ranging from 300 m/s to 700 m/s. second impact is closer than 6.3 mm from the first one, then the
Samples were placed on the impact chamber without using any loss of ballistic performance in not negligible, while if it is further
fixture. This decision was taken in order to avoid any forces than 7.5 mm from the first one there is no decrease in the ballistic
applied on the specimen, excepting those coming from the projec- efficiency.
tile. Such a process allows computation of the energy impact, the The results obtained when shooting the H-18/21S specimens
energy transferred to the specimen, and the projectile residual (made of an 18-layer hybrid composite with 21% of S2 glass fiber
energy without any dissipation through any specimen mounting distributed among six different layers) is shown in Fig. 3. The
system. Impact velocity was obtained using two infrared window results of the first impacts made in the samples are represented as
frames, as well as a Phantom V12 video camera. The images were full squares, while the second impacts are plotted as hollow
recorded at a frame rate of 80,000 fps (leading a period of 12.5 ls squares. The V50 of the composite is slightly higher than the one
among frames), a resolution of 512 128 pixels, and an exposure obtained in the carbon laminate, with it being 354 m/s. The two
time of 9.35 ls. The measurements taken from the video camera trends previously observed in the carbon laminate are reproduced
were used to compute the impact velocity, the residual velocity of again. The first one starts at V50 and finishes around 420 m/s; and
the projectile, and the residual velocity of the target if any. the second one comprises higher speeds. However, the slope of
Through these measurements and weighting, the projectile and the the first straight trend is less steep when compared with the carbon
tested specimens, the energy balance was obtained. laminate. This different slope shows that slight changes in the
impact velocities are accompanied by reductions of the residual
velocity in contrast to that observed in the composites without
3 Results hybridization.
The results of the velocities of the test campaign were obtained The second trend shown is similar to the one obtained for car-
using the recordings of the tests taken by means of a high-speed bon fiber composites. The increments of impact velocities cause a
camera. The velocity of the projectile before and after the impact proportional increment of the residual velocities of the projectile.
was obtained using a fixed distance and knowing the time between The second impacts in the samples showed no different behav-
two different frames of the video. All tests were performed with a ior. Most of the points of Fig. 3 that appear in hollow squares are
normal impact. In addition, the trajectories of the projectile before in contact with previous results of samples tested only once. Not
and after the tests were stable. only did this event take place, but also some of the second impacts
A sequence of images taken from an impact is shown in Fig. 1. performed showed better behavior than the first ones. However,
The images show the projectile, the frame and a carbon laminate this cannot be related with the material properties because the dis-
(C-16/0), which is in contact to the frame without any attachment tances between impacts were larger than those previously regis-
system. Those images were taken at times 112 ls, 37 ls, 76 ls tered in the case of the carbon fiber laminates.
and 201 ls from the impact instant. Given that the images reveal The influence of the amount of hybridization was studied by test-
that the residual velocity of the target is almost negligible, it can ing hybrid laminates with smaller amounts of glass fibers. These
be considered that the latter is not moving after the impact. Meas- tests were performed in a hybrid laminate named H-20/12S. This
urements taken from this video give an initial velocity of 700 m/s composite was manufactured with the same S2 glass fibers as H-18/
and residual velocity of 537 m/s. 21S, though the fibers were placed in two layers placed close to the
The results of the test performed in the quasi-isotropic carbon free surfaces of the laminate. The results obtained can be seen in
laminate are shown in Fig. 2. Some specimens were impacted Fig. 4. Laminate H-20/12S has a measured ballistic limit of V50 of
twice to study the multihit behavior; in this figure the first shot on 399 m/s. In this laminate, the trends shown in Figs. 2 and 3 cannot
the specimen is represented as a full symbol, while the second be seen so clearly. However, it seems that the slope of the first part
shot is represented as hollow symbols. of the graph is steeper than the one shown in Fig. 3, but less steep
The ballistic limit obtained V50 was 348 m/s. The behavior of than the one in Fig. 2. The first trend ends close to 400 m/s. In the
the laminate at speeds above the ballistic limit shows two types of second part of Fig. 4, as in the previous laminates, there is propor-
trend. One such trend comprises the tests performed at speeds tionality between any increment of the impact velocity and the re-
slightly higher than V50. In this zone, any increment of the impact sidual velocity.
velocity of the projectile causes a total penetration in the sample. The results obtained after shooting in the samples already tested
For instance, a change of 5 m/s in the impact velocity generates an can be seen in hollow symbols. As happens in H-18/21S, there are
increment of the residual speed of 125 m/s. The second trend can no great differences between the first and second impacts in the
Fig. 2 Residual velocity versus impact velocity of the projec- Fig. 3 Residual velocity versus impact velocity of the projec-
tile for laminates C-16/0. Distance between first and second tile for laminate H-18/21S. Distance between first and second
impact shown next to the test result. impact shown close to the test result.
V50 (m/s) n
energy absorbed by the sample. This expression can be developed type S. These dots are close to those obtained in the composites
in the following one, assuming that the kinetic energy of rotation with three layers of glass fibers type E. The laminate that absorbed
of the sample after the impact can be neglected when comparing it most energy was the laminate manufactured with two plies of
with the rest of the energies obtained. Therefore, the previous glass fibers type S. It is also noticeable that the energy absorbed
equation will be expressed as: per mm of thickness of the carbon laminate was constant between
the ballistic limit and 250 m/s. On the other hand, the hybrid lami-
1 1 1 nates absorbed more energy as the residual speed grew. Besides,
mp v20 ¼ mp v2rp þ ms v2rs þ Eabs (3)
2 2 2 the increment in the energy absorbed by the H-20/12S laminate is
higher than those observed in the rest of the hybrid laminates.
In the latter equation all the data needed has been obtained in the This is important, given that this behavior appears in the laminates
tests and thus the energy balance is complete. manufactured with E glass fibers and S glass fibers alike.
A comparison between the behavior of the composite materials According to Fig. 8, it seems that the position of the most flexi-
was studied, relating how much energy absorbed by the samples ble plies of glass fibers is more important than the amount of
in contrast to the impact energy. However, direct comparison hybridization. The glass fiber plies closest to the middle of the
between materials cannot be made because the results shown in sample might not contribute to the sample impact strength and,
Fig. 7 are influenced by the thicknesses of the composites. due to their distant position, are not able to spread the damaged
According to the thicknesses that appear in Table 1, only a direct inflicted by the projectile, this is what happens in samples H-18/
comparison between H-18/21S and C-16/0 can be made. The 21S and H-22/15E. Conversely, the glass fiber plies that are near
amount of energy absorbed in relation to the energy before the the free surfaces of the sample are capable of distributing the dam-
impact is higher in H-18/21S than in C-16/0, even though the car- age to the outer plies and, instead of breaking these plies, massive
bon laminate is thicker than the hybrid one. delamination appears near the glass fiber plies. To check this hy-
Laminate H-22/15E absorbs more energy than C-16/0 or H-18/ pothesis, a closer look at the tested samples was taken.
21S, though it is probable that the differences between H-22/15E Figure 9 shows pictures of nonhybrid composites. On the left
and H-18/21S might be caused because H-22/15E is 0.37 mm part of Fig. 9 a sample tested below 400 m/s is shown. This sam-
thicker than H-18/21S. The differences between C-16/0 and H- ple corresponds to the first trend that appears in Fig. 2. On the
22/15E are noticeable, and the thickness differences between the right part of Fig. 9, a sample tested at a higher velocity can be
two laminates thickness is only 0.21 mm. The different results seen. In these two pictures the damage patterns of the laminate are
between these two composites are sound; this suggests that they similar. There are no delaminated areas, either in the first sample
could be partially caused by a better behavior of the hybrid or in the second sample. The main failure mechanism of the mate-
material. Above all, the best performance of all laminates was rial in both tests is crushing in the ply that the projectile impacts
achieved with H-20/12S. These results were expected, due to first and shear stresses in the opposite plies.
the differences in the number of plies, and thus in thickness of
H-20/12S.
However, direct comparison between the behavior of the com-
posites is still not possible due to their different thicknesses. To
solve this problem the energy absorbed by the samples was di-
vided by their thicknesses and plotted versus the residual speed of
the projectile. This plot can be seen in Fig. 8 which shows the test
results for all laminates. As can be clearly seen, there is no cross-
ing between the data of the laminates. The dots obtained by test-
ing the carbon laminate appear in the lowest part of the curve,
whereas the hybrid laminates appear right above them. The dots
closest to the carbon laminate results are those obtained for the Fig. 9 C-16/0 samples tested at different velocities. No visible
hybrid laminate manufactured with three layers of glass fiber delamination appears in any sample.