0

2  
// ++

 000  3)( +(*), (+( /,+/) KS0 
(1 */*1
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&
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// ((
HS0  )*33
&) (+ 3(( +3
(+ R 201 R 202 A/B

 00
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 005
/ )(/*+
- 1
- 4--4
PASSIVATION AIR 14 90 (.)
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 005
*+*
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00
1 45
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   /0 5420
1 -,
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NATURAL GAS FEED E 204-2 & 17..
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&
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1

1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello

0 04/09/2011 First Issue HTAS Cedrati Agnello
#"- >9000> >9090> >90:<> >90=<> >9/0<> >9330> >=/00> This PFD is valid 1).
REV. DATE DESCRIPTION PREPARED
for UnitCHECKED
11(Train APPROVED
&)-( %?  @ %?  @ %?  @ %?  @ %?  @ %?  @ %?  @ Identical PFD is valid for Unit 21 (Train 2)
 /0 0 20 /0 0 09 /0 </ ;03 0 9= =33 0 3. 29;< / 02
&9: 29<9 < <2 29<9 < 9/ DWG. No.: 11-GD-4E-06900
&2; 30< / <. 30< / .<
&./0 2=0 0 :2 2=0 0 <3 
 
  


 

       

 
 
   
   


 
 
Sh. 1 of. 8
&</9 /00 0 /= /00 0 /: 17/10/13 Final Issue Acerbi Covelli Covelli
&:/. =/ 0 /9 =/ 0 // DANGOTE FERTILIZER LIMITED
&=/: :< 0 // :< 0 /0 Job: 032124
&. <03.3 ;: :< 2/ 0 30 <03;0 ;/ =0 92/:9 // <= //3. 0 .0 00-GD-E-06900
DANGOTE FERTILIZER PROJECT
&) 9 9/;<. /0 39 .9;/3 /. 2. * Discontinuous
&)9 93=< < 0: #"* !"&#()%
0 1 !" !#$% &"&' ((#
2/.: < 0. 9//;= /0 <3 999/: = .. 9< 0 02 2=<0: // =/ NIGERIA
Pressure kg/cm² g  Rev.
9 9<99 =. 0; 9<.3 . 0; /293:9 :: .2 /:.90/ << 09  GI%M

Normal Operation Case
%9 //9 0 /3 ;./ 9. =9 3<3 / <. 3<3 0 .; :=9:2 99 <2 ::20. =; 0. 9=932: ;< /; Duty Gcal/h  
 L6%I!
Process Flow Diagram ""," +%
)9 /=;22 90 33 :::3 9 0; Flow kg/h SCALE:
Desulphurization and Reforming
&'GI! 
9) : /;;:=; /20=.9 /.23.= </0 ;3;39 Flow Nm³/h %-"
&'JI!  ! "#
$
!#8
DRY <;=33 /00 00 2.0. /00 00 :9.0= /00 00 900/2. /00 00 93;<02 /00 00 ;.3:/ /00 00 29023= /00 00 Lower Heating Value kcal/Nm³ %&'
Rev. IN REPLACEMENT &/(4!0/1# 
5
OF:
TOTAL 1'2
Issuer Specific number G%IJ/ !)&+-"%!
)6 <;=33 2./0 9</0;< 220;=: ..9..3 ;<.=/ ./09;; 1
Temperature °C  F (.//0/102/33 /
MOLE WEIGHT
-)6"$"7 /3 92 ; =0 /; /3 /2 ;0 /< 30 9; 30 9= .< 
1 REPLACED BY:
  



This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
 11-V-208 Waste Heat Boiler
Steam Drum Package in
common for 11- Ammonia unit
from Convection bank
E-208, 11-E-210 including
51
& 8
,3 +-3+(
*33 &+ and 11-E-501 11-V-201
*33
&
 (
11-E-208
11-E-210
+
2S0  3/ /,+/) 11-E-501
&+ */
*/ )*
 3O
V 201 /,,,-
. 0 

BL *3-
LS STEAM

158
all these boilers produce saturated
1824 steam with 120 KG/CM2g and
3(., 3/.,
320 oC.
188 3/ /,,+ 3, (
*/+
*/+ ++ +/(
188
0C0  V 203 R 204 R 205
CONTINUOUS 2 1
ATM BLOWDOWN O

O

DRUM -( -(

+)/+ +**(/
*3) *3,(

--)%6))(
{4<|
1 E 501 E 502

V 206 3(.3, 3.3

INTERMITTENT
BLOWDOWN DRUM
/3, -
4++(4 +(
CW

E 218 
3+
CBD COOLER E 211
 2 
3/

52 

+,
BL
BLOW DOWN +(
.+

&
 3++ 33.)
3/
3,

 0060 + //)* +,+ 
 0060
+( &+ +, &3
4+(4 +3( 4+,4
&

3  3
gas flow 442,449 Nm3/h +*./ +(.(+ +., +-.,
H2 37.11 vol% E 208 E 210 E 212 -1/2/3 E 213 -1/2
N2 15.20 vol% 80 2  80 2  &8
2 
&8
2 

CO 9.68 vol% 51

.+ 51
. .+ +)( .
CO2 5.02 vol% 3(,*(/
Ar 0.18 vol%
CH4 0.27 vol% *3/
H2O 32.53 vol%
Total 100.00

51
& 8
130 (,*(/
*3(1
*3(
&
7&8

1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello

0 04/09/2011 First Issue HTAS Cedrati Agnello
REV. DATE This PFD is valid
DESCRIPTION PREPARED 11(Train 1).
for UnitCHECKED APPROVED
Identical PFD is valid for Unit 21 (Train 2)
DWG. No.: 11-GD-4E-06900


 
  


 

       

 
 
2 8
   
   


 
 
Sh. of.
17/10/13 Final Issue Acerbi Covelli Covelli
#"- >9/0<> >9//<> >9/:0> DANGOTE FERTILIZER LIMITED
&)-( %?  @ %?  @ %?  @ Job: 032124
 ;03 0 9= ;03 0 9< ;03 0 9. DANGOTE FERTILIZER PROJECT
&. //3. 0 .0 //3. 0 2: //3. 0 2<
0 1
&) .9;/3 /. 2. //<// 2 .3 ///9 0 22 #"* !"&#()% !" !#$% &"&' ((#
NIGERIA
&)9 999/: = .. <2<9. /: 92 :2399 /; =3  Rev.
Normal Operation 
Case
9 /:.90/ << 09 /3<<03 <3 9; 90<303 :0 <9 Pressure kg/cm² g  GI%M  
Process Flow Diagram SCALE: ""," +%
%9 :=9:2 99 <2 :=9:2 90 23 :=9:2 /3 ==
Duty Gcal/h  L6%I!
CO Conversion 
9) /.23.= //9:23 /099.0 %-"
&'GI! 07 5
N
!#8
DRY 93;<02 /00 00 293;// /00 00 2.0903 /00 00 Flow kg/h
%&'
Rev. IN REPLACEMENT OF: &/(4!091

TOTAL Flow Nm³/h &'JI!
Issuer Specific number / !)&+-"%!
)6 ..9..3 ..9..3 ..9..3 1
Temperature °C  F 102/33 (.//09 /
MOLE WEIGHT
-)6"$"7 /< 30 /< 30 /< 30 
1 REPLACED BY:
  



22
This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
 CUSTOMER JOB UNIT No.
DANGOTE FERTILIZER LIMITED 032154 11

PLANT LOCATION
NIGERIA SPC No. 11-RA-E-06614
PROJECT / UNIT Rev.
DANGOTE FERTILIZER PROJECT Sh 14 of 16 0 1

Sketch No. 1: Normal Operation

This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal
provisions of the law. It shall neither be disclosed to third parties nor used for purposes other than those for which it has been disclosed.
 ,.3

.( )3 &10260

5R5 /
V 303  &+
1 ( 44
4(4 
 E 306 
&

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0 
 
LP FLASH GAS 2 

.,/ 3.*
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 0060
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C 301 ,.,- V 301 C 302
0
5
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 0

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.*, 3-3) &) )+
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0
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)+ 
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)/

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51

E 301
01 52  E 303
R26
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+ 1


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8
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 33

,(
4+)/4
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015 0
 0 51  V 304
 01 5 )+ 
 0060
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8
2 
/
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 00.
1 &/ -
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-*31 ,(
-*3
&
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 00.


 5 P 703 A/B -, &)
-,
8 + 0
5

CONDENSATE
1 -,+ PUMP NO. 2
-,+
 
 
P 305 A/B

 00
 0
CO2 COMPRESSOR .
General Revision after Client's Comments
1 05/01/2012 HTAS Cedrati Agnello
0 04/09/2011
This PFD is valid for
First Issue HTAS
Unit 11(Train
Cedrati
1). Agnello
INTERSTAGE P 323A/B valid for Unit 21 (Train 2)
REV. DATE DESCRIPTION
Identical PFD isPREPARED CHECKED APPROVED
CONDENSATE 2640 45 ATM CO2 COMPRESSOR INTERSTAGE
BL CONDENSATE PUMP DWG. No.: 11-GD-4E-06900
FROM UREA UNIT T 323
1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello
COMPRESSOR INTERSTAGE 0 04/09/2011 First Issue HTAS Cedrati Agnello

 
  


 

       

 
 
REV. DATE DESCRIPTION
3 PREPARED CHECKED
8
   
   


 
 
Sh. of. APPROVED
17/10/13 Final Issue Acerbi Covelli Covelli
#"- >9/:0> >9/;.> >9900> >999<> >99<0>
CONDENSATE TANK DANGOTE FERTILIZER LIMITED DWG. No.: 11-GD-4E-06900
&)-( %?  @ %?  @ %?  @ %?  @ %?  @ Job: 032124
 ;03 0 9. ;03 0 9. ;03 0 93 Pressure kg/cm² g DANGOTE FERTILIZER PROJECT Sh. of.
&. //3. 0 2< //3. 0 2< < 0 9/ //;; 0 .2  GI%M
Alt DANGOTE FERTILIZER LIMITED0 1
&) ///9 0 22 ///9 0 22 . 0 /: //0; 0 .0 #"* !"&#()% !" !#$% &"&' ((#
Pressure kg/cm² g  NIGERIA Job: 032124
&)9 :2399 /; =3 :2=.; /; =< /:./ :. =< :/3=/ 33 ;< /2; 0 0<  GI%M DANGOTE PROJECT
 FERTILIZERRev.

Normal Operation Case 0 1
9 90<303 :0 <9 90<;;9 :0 << =<. 93 =; ;= 0 /. 90<0./ =. .: Duty Gcal/h
NIGERIA
 
Process Flow Diagram
 L6%I! SCALE: ""," +%
Rev.
%9 :=9:2 /3 == :=9<= /3 =; /93 < /0 : /00 :=/9/ 9. 2= Flow kg/h
&'GI! Normal Operation Case
MDEA CO2 Removal
9) /099.0 9<3= /;9 2/2; /02/ Alt  %-" SCALE:
Flow tons/h &'I!  
N
!#8
DRY 2.0903 /00 00 2.0009 /00 00 9<22 /00 00 :90:. /00 00 9=<.0< /00 00 Rev. IN REPLACEMENT OF:&/(4!021-!"
%&'
Flow Nm³/h &'JI!
Issuer Specific number / !)&+-"%! Rev. IN REPLACEMENT OF:
TOTAL
)6 ..9..3 2.9<33 9=/< :<909 9=:.2: Issuer Specific number 1 /
Temperature °C  F 102/331 (.//02 1 /
-)6"$"7
MOLE WEIGHT /< 30 /< 9; 93 =: .9 =0 ; :; 
REPLACED BY:
  
REPLACED BY:


This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
 1- Relative hemudity is zero but during start up is 1000
2- During Normal operation the anti surge valve should not exceed 75% , and it should be a low noise type.
3- Vendor must select "O" ring material in dry gas seal to take into account possible traces of NH3 in Make-Up Gas due to anti-surge opening
4- The steam turbine rated power should be 110% of compressor rated power at normal extraction flow.
5-

N2 =22,01 mol%
H2= 66,02 mol%
Argon= 2,08 mol%
CH4= 5,92 mol%
NH3= 3,97 mol%
MW= 9,97 Kmol/kg
+-,
/ -3)3
5
1 560
3.+ // &(
//
 (3
3
K 431
*(
0C 2 05060

00

d&e R 301
E 211  2 

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5
1 560
.+
&( /3(
4/3(4
&
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7 O
+))
/ ,**, 0C 2 05060
3( &(
43(4
5
Compressability factor =1,09 0C 2 0501
MW= 8,7 Kmol/kg
E 431 E 432
3+ E 433 N2 =24,72 mol%
1st INTERSTAGE 2nd INTERSTAGE H2= 74.08 mol%
/ 3rd INTERSTAGE
3 3) *+)3 COOLER FOR COOLER FOR Argon= 0,3 mol%
(( ) 43(4 COOLER FOR CH4= 0,9 mol%
K-431 K-431 NH3= -
K-431
E 311-1/2 V 433
3.* 60O60

 0060 ( *,/3, R26

( &3 3rd INTERSTAGE

4(4
&
3 +.(- SEPARATOR FOR
8 8 8
V 431 K-431
1st INTERSTAGE V 432
SEPARATOR FOR 2nd INTERSTAGE
**
)( K-431 SEPARATOR FOR
V 311
E 312 &5160 K-431 INTERSTAGE
&511
0 
 

423 CONDENSATE
/3

3)(
2385 F8
2385
3.-3 TO C-701
8


 00 1
 0 / +/+(
&3 - (+.(
// 3/+
C1 2
-
3/  &+

2C
6  5
P
P 311 A/B
702 A/B
(1) The Specified minimum conditions refer to 100% plant load. At reduced load the temperature will
 decrease. The compressor/turbine should be able to operate continuously at 60% compressor load at
 0 0 5 601005 (/
.+ &
 O 
00
c
steam temperature of 465°C. The manufacturer should give minimum steam temperatures at 3)

inlet for continuous operation and for temporary operation. The manufacturer has to confirm that the
maximum extraction steam temperature will not be exceeded during running up of the turbine and 1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello
during operation at reduced load, provided the steam conditions at inlet are "normal". 0 04/09/2011 First Issue HTAS Cedrati Agnello
REV. DATE DESCRIPTION PREPARED CHECKED APPROVED
6 (2) Inlet Temperature =36.3°C. Outlet Temperature = 49°C. Max Pressure Drop =0.7 kg/cm2
This PFD is valid for Unit 11(Train 1).
7 (3) At the rated point the turbine must develop not less than 110% of compressor rated power DWG.
Identical PFD is valid 11-GD-4E-06900
No.:for Unit 21 (Train 2)
continuosly at normal steam header conditions. General Revision after Client's Comments
1 05/01/2012 HTAS Cedrati Agnello
8 (4) Normal, maximum and minimum extraction temperature to be defined by vendor. 0 04/09/2011 First Issue HTAS Cedrati Agnello

 
  


 

       

 
 
REV. DATE DESCRIPTION
Sh. 4
   
   


 
 
PREPARED
of.CHECKED
8 APPROVED
#"- >99<0> >920<> >92<9> >9.2<>
&)-( %?  @ %?  @ %?  @ %?  @ 9 (5) For data refer to Ammonia Synthesis Gas/Recirculation Compressor (See spc 11-MA-E-06593) 17/10/13
DANGOTE FERTILIZER
Final Issue LIMITED Acerbi Covelli Covelli
DWG. No.: 11-GD-4E-06900
 ;03 0 93 ;03 0 20 =3= 0 20 /3/;< 9 0; Job: 032124
&. //;; 0 .2 9.2. 0 30 9233 0 30 <.::9 < 39 DANGOTE FERTILIZER PROJECT Sh. of.
&) //0; 0 .0
DANGOTE FERTILIZER LIMITED0 1
&)9 /2; 0 0< #"* !"&#()% !" !#$% &"&' ((#
NIGERIA Job: 032124
9 90<0./ =. .: 90//:: =. 0; /3;9.9 =. 0; :03.<0 :: 09 DANGOTE PROJECT
 FERTILIZERRev.
Normal 
Operation Case 0 1
%9 :=/9/ 9. 2= :=/9/ 9. =9 ::/.= 9. =9 902/<0 99 0/ Pressure kg/cm² g  GI%M NIGERIA
 
%2 2::2: 2 3= Process Flow Diagram SCALE: Rev.""," +%
Duty Gcal/h Methanation
 L6%I! Normal Operation Case
and Compression
9) /02/ :<2 /9/ 
%-"
SCALE:
&'GI! !#
!#8
DRY 9=<.0< /00 00 9=/<20 /00 00 9:=<;: /00 00 3920;2 /00 00 Flow kg/h OF:
%&'
Rev. IN REPLACEMENT&/(4!0.1- ~&
TOTAL
E 432 E 433 Flow Nm³/h &'JI!
Issuer Specific number / !)&+-"%! Rev. IN REPLACEMENT OF:
)6 431 9=:.2: 9=9/;2 9:==0: 3920;2 Issuer Specific number 1 /
 F 102/33 1
(.//0. /
-)6"$"7
MOLE WEIGHT ; :; ; =0 ; :3 3 3< Temperature °C REPLACED REPLACED BY:
BY:

  


1

This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
V 432 V 433
third parties nor used for purposes other than those for which it has been disclosed.
 /.*
51
& 8
-( +)/+ * 3--* % 2
23de
& *3) /+, &,
*3) /+,
0 
 ()

+ .*
0  3/ O/ *( % 2
23de
& *-+ 11-E-506 /+) &,
*-+ /+)
0 
 (*

Ammonia In =3.97 mol%, Out 19.6 mol% +)*.(

 ,+++ 
6 60
Construcation material is 1.25 Cr, 0.5 Mo +(( &*
4+((4
Converter basket & 1st IHE, 2nd IHE= SS321 5
,/- %2
*+3 %2


C
1st bed catalyst type = KM1R, Volume 21,7 m3 /+* /+*,
2nd bed catalyst type = KM1, Volume 25,3 m3
3rd bed catalyst type = KM1, Volume 38 m3
V 514
E 514 
6 60
Alloys Specs; 
6 60 0 
 

+-( 2511

Heat resistant & Cooling Rate resistant A1 Tube inlet

hydrogen service 33 B1 Tube outlet ++ 

4//(4 A3 Shell inlet (+ (

A2 Shell outlet .

R 501
5 B2 Shell vapour outlet


D Drain
1st IHE
780 tubes +)*
Favor with High TL =4,6 m

Pressure & Low 3-+ % 2
Pressure /( (3
2nd IHE V 501
949 tubes E 501 E 502 E 503 E 504 E 505 E 506 E 508 5
TL =4,6 m 180 1&8 2 HEAT 8
1
1 +0 5 5 0 
 

+-3 2  51

2 
EXCHANGER R26
2511
2511

/(( 3/ ,3 , 3) / ++ + 

4/,4 /,( /* /*( /) /)( /- ( /+( /
3(.3, 3.3 ,.3+ +,.*- +.*) )./- TEMA type DKU *.(*
No. of U-tubes = 930 8
CW flow 3,382 m3 No. of tubes = 3723 tube
No. of tubes = 5540 No. of tubes = 3360, length = 5.7 m No. of U-tubes = 1,300 tubes
tube length = 16.2 m Lenght 11,8 m Design differential pressure,
3H2+N2= 2NH3+ Heat (22 Kcal/mol) shell/tube side: 20 kg/cm².
OD = 25,4 mm, IN = 19,86 mm
Tube lenght = 4530 mm
+-, +),
the choice of temperature should be based on a compromise material = CS
/ 3/
between the theoretical equilibrium conversion and the
// /3(
approach to equilibrium
 -),( % 2

 5
, &,
4,4
(
K 431
7+
O/  % 2
23de
67$*(
/+- &,
/+-
(3
d&/e

51
8
Temperature 7 oC /(3( +  23de
%2 % 2
& &, /(
/+* /(
&
0 
 &
((

51
& 8
+)( +)/+
* +)+ % 2
23de
*3*( &
*3*( /+-+ 1
&
 +3 /+-+


7 O 6
1 5
+))
0C 2 05060 / ,**, Saturated with water 0.05%, trace of CO, CO2 7 oC
3( &/
43(4 +- *)3+ 23de
&
0C60 4,7 Kg/cm2 % 2

00
And it will be removed by absorbtion in ammonia liquid &, /+
/+
&
 (+

1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello

0 04/09/2011 This PFD is valid for
First Issue Unit 11(Train
HTAS Cedrati 1). Agnello
REV. DATE Identical PFD
DESCRIPTION valid for Unit
is PREPARED 21 (Train
CHECKED 2)
APPROVED

DWG. No.: 11-GD-4E-06900

1 17/10/13 Final Issue Acerbi Covelli Covelli


 
  


 

       

 
 
   
   


 
 
Sh. 5 of. 8
#"- >92<9> >9..<> >9.:0> >9:00> >/9<0<> DANGOTE FERTILIZER LIMITED
&)-( %?  @ %?  @ %?  @ %?  @ %?  @ Job: 032124
 =3= 0 20 /3/;< 9 0; /3/;< 9 23 <2 0 0. =.. 9 ;< DANGOTE FERTILIZER PROJECT
&. 9233 0 30 <.::9 < 39 <.::9 : ;/ 9;3 0 9. 9/03 ; 0;
0 1
&) #"* !"&#()% !" !#$% &"&' ((#
NIGERIA
9 /3;9.9 =. 0; :03.<0 :: 09 .9;.;= <2 .0 :9< 0 <9 /::<< :2 =; g
Pressure kg/cm²  GI%M  Rev.

Normal Operation Case
%9 ::/.= 9. =9 902/<0 99 0/ /.9;93 /= ;0 9=; 0 92 <<.; 9/ 9< Duty Gcal/h  
 L6%I! Process Flow Diagram SCALE: ""," +%
%2 2::2: 2 3= /<=9=; /3 :0 //3<;; 3; 3= /0<< . 0.
Flow kg/h &'GI! 
Ammonia Synthesis Loop
9) /9/ /9/ %-"
0L!1
!#8
DRY 9:=<;: /00 00 3920;2 /00 00 ;09../ /00 00 /90;2. /00 00 9:/// /00 00 NH3NH3 Flow kg/h &'JI! Rev. IN REPLACEMENT OF:&/(4!0<16
%&'
Flow Nm³/h %223&'GI! Issuer Specific number / !)&+-"%!
TOTAL
)6 9:==0: 3920;2 ;09../ /903<. 9:/// 1
Temperature °C  F 102/33 /
-)6"$"7 ; :3 3 3< // .< 1REPLACED
(.//0< BY:
MOLE WEIGHT /: 33 /0 2: 
  



This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
 +/.)
O+ +*( 1 860
+/) &*
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,
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ammonia expand to 2.7 kg/cm2g
51d&(e


 E 511
* and -4 oC
5 // -** %2
ammonia expand to 4.7 kg/cm2g V 505 5
 
+/(( &* E 508 E 514 E 506 5
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from the accumulator, 11-V-504,1 through the product heater, 11-E-512, to the first synthesis loop E 512
+- 5 /+
chiller, 11-E-506, where it is expanded to 4.7 kg/cm2g corresponding to a temperature of 7.2oC. 
 2 

*)3+ %2
*)3+ %2

Liquid ammonia from 11-E-506 is transferred to the second synthesis loop chiller, 11-E-508, and /+ /*
+.-(
the purge gas chiller, 11-E-514, where it is further expanded to 2.7 kg/cm2g corresponding to a +
(
-+,,* %2
 -+,,* % 2
5

temperature of -4oC. /(- 1
/() 4/(-4


Evaporated ammonia from the chillers and from the flash vessel, 11-V-503,
is compressed by the
ammonia compressor, 11-K-441. The suction pressures correspond to the (
O33  % 2
5

/, 1
pressures in the flash 4/,4
0 
6
/+
vessel and the chillers. After compression, the ammonia from 11-K-441
P 501 A/B
is condensed in the 5

 
ammonia condenser, 11-E-510A/B, and collected in the accumulator, 11-V-504. 1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello

Ammonia Liquid 0 04/09/2011 First Issue HTAS Cedrati Agnello

Inert gases accumulating in the refrigeration system are vented from the ammonia accumulator, REV. DATE DESCRIPTION PREPARED CHECKED APPROVED
11-V-504. Ammonia is condensed in the inert vent gas chiller, 11-E-511, and separated in the This PFD is valid for Unit 11(Train 1).
inert vent gas separator, 11-V-505. The gas, which still contains some ammonia, is sent to the Ammonia Gas Identical PFDDWG.
is validNo.:
for11-GD-4E-06900
Unit 21 (Train 2)
ammonia
PEAK FLOW OF AMMONIA FROM AMMONIA STORAGE TO UNIT 11 ONLY. 
 
  


 

       

 
 
Sh. 6 of. 8
   
   


 
 
recovery unit.* DISCONTINUOUS
Evaporated ammonia from 11-E-511 is sent to the ammonia compressor,
DANGOTE FERTILIZER LIMITED
11-K-441. #"- 1 17/10/13 Final Issue Acerbi Covelli Covelli
>9:00> >.<30> >.:00> >/.<<0> >/.;90> Job: 032124
&)-( %?  @ %?  @ %?  @ %?  @ %?  @ DANGOTE FERTILIZER PROJECT
 <2 0 0. /< 0 0/ 33 23 2 0= Pressure kg/cm² g 0 1
&. 9;3 0 9. /20 0 // 9 / 0 0< /:/ /9 :< NIGERIA
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Alt Rev.
9 :9< 0 <9 :2 0 0< / 0 0: <=. .. 32 
Pressure kg/cm² g 
%9 9=; 0 92 .2 0 0. 0 09 92; /; :3 Normal Operation Case
 GI%M
Process Flow Diagram 
SCALE: ""," +%
%2 //3<;; 3; 3= /90:.9 33 =3 /00 00 /9;: 33 ;: 9:2 90 :: Duty Gcal/h
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Ammonia Refrigeration
9) /9/ /22 /9 NH3 Flow kg/h %-"
NH3 &'JI! 
$
DRY
!#8 /90;2. /00 00 /90;32 /00 00 0 /00 00 /9;; /00 00 /9=< /00 00 Rev. IN REPLACEMENT OF:&/(4!0:1# 
5
%&'
TOTAL Flow Nm³/h Issuer Specific
%2
number
23&'GI! / !)&+-"%!
)6 /903<. /9/09: 0 /200 /9=< 1
MOLE WEIGHT Temperature °C  F 102/33 (.//0:
BY:
/
-)6"$"7 /: 33 /= 02 /= 02 /= 0. /9 39 
1 REPLACED
  



This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
1 8h
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This PFD is valid for Unit 26

common unit for for unit 11 (train 1) and Unit 21 (Train 2)
1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello
0 04/09/2011 First Issue HTAS Cedrati Agnello
REV. DATE DESCRIPTION PREPARED CHECKED APPROVED

1 17/10/13 Final Issue

DWG.
Acerbi No.: 11-GD-4E-06900
Covelli Covelli


 
  


 

       

 
 
8
Sh. 7
   
   


 
 
of.

#"- >.=<0> >.;20> >.;2<> >/9<0<> >/.<<0> >/.;90> DANGOTE FERTILIZER LIMITED
&)-( %?  @ %?  @ %?  @ %?  @ %?  @ %?  @ Job: 032124
 /.;: 9 3= =; 2 ;= /<:. 2 00 =.. 9 ;< 33 23 2 0= DANGOTE FERTILIZER PROJECT
&. .9/. ; .9 292 /< 3< .<2= ; =/ 9/03 ; 0; / 0 0< /:/ /9 :<
0 1
&) #"* !"&#()% !" !#$% &"&' ((#
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9 229;3 :: .: //.: <: :9 2..2. :: 03 /::<< :2 =; / 0 0: <=. .. 32 Pressure kg/cm² g  Rev.
 GI%M
Normal Operation Case
%9 //03/ 99 /< .=: 92 <: //<:; 99 90 <<.; 9/ 9< 0 09 92; /; :3 Duty Gcal/h  
 L6%I!
Process Flow Diagram SCALE: ""," +%
%2 9 .< 2 /0<< . 0. /9;: 33 ;: 9:2 90 ::
Flow kg/h &'GI!
Ammonia Recovery 
9) 2; /2 </ /9 %-"
NH3 Flow kg/h &'JI! 
%NL
DRY
!#8 <00;0 /00 00 9092 /00 00 <9/09 /00 00 9:/// /00 00 /9;; /00 00 /9=< /00 00 NH3 %&'
&/(4!0=1#  
Rev. IN REPLACEMENT OF:
TOTAL 23&'GI!
Issuer Specific number / !)&+-"%!
)6 <0//; 902: <9/<. 9:/// /200 /9=< Flow Nm³/h %2 1
MOLE WEIGHT Temperature °C  F 102/331 (.//0= /
-)6"$"7 /0 03 // ;3 /0 /: /0 2: /= 0. /9 39 
REPLACED BY:
  



This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.
 /+.(
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1 05/01/2012 General Revision after Client's Comments HTAS Cedrati Agnello

0 04/09/2011 First Issue HTAS Cedrati Agnello
REV. DATE DESCRIPTION PREPARED CHECKED APPROVED

DWG. No.: 11-GD-4E-06900

This PFD is valid for Unit 11(Train 1).
Identical PFD is valid for Unit 21 (Train 2)

 
  


 

       

 
 
Sh. 8 of. 8
   
   


 
 

DANGOTE FERTILIZER LIMITED

17/10/13 Final Issue Acerbi
Job: Covelli
032124 Covelli
DANGOTE FERTILIZER PROJECT
0 1
NIGERIA #"* !"&#()% !" !#$% &"&' ((#


Rev.

Normal Operation Case
Pressure kg/cm² g Process Flow Diagram 
SCALE: ""," +%
 GI%M
Process Condensate Stripping

Duty Gcal/h %-"
 L6%I! %#0
OF:
Rev. IN REPLACEMENT &/(4!0;1(& 
 
%&'
Flow kg/h &'GI!
Issuer Specific number / !)&+-"%!
1
Temperature °C  F 102/33 (.//0; /

1 REPLACED BY:
  



This document is prepared by Saipem SpA for Dangote Fertilizer Ltd. It contains proprietary and confidential information of Saipem and/or of the Technologies Licensors who will safeguard their rights according to the civil and criminal provisions of the law. It shall neither be disclosed to
third parties nor used for purposes other than those for which it has been disclosed.