Día 1 Área

[=] ppm Área [=] ppm Día 1

100 874.9406128 895.8702393 882.4846191 100 884.4318237
80 732.9207764 735.145874 700.4370728 80 722.8345744
60 535.6414795 525.0944214 533.0957642 60 531.2772217
40 378.0674438 374.8947449 379.7554321 40 377.5725403
20 861.7380371 878.9758301 932.1515503 20 890.9551392
10
Día 2 5
[=] ppm Área 2.5
100 1078.913696 1008.884888 1002.887024 1.125
80 729.2191162 815.9140625 809.378418 0.5625
60 505.5874329 505.8378906 510.2314148
40 347.2498474 462.5531921 325.8057861
20 135.3032379 184.5650024 131.1678314 Área vs [
1200
Día 3
[=] ppm Área 1000
100 1097.965942 1134.953735 1146.243652 f(x) = 8.22800959172353 x +
80 903.9641724 897.4055176 920.8157349 800 R² = 0.916585802877064
60 604.3389282 646.081604 624.9100342

Área
40 430.3971558 382.1664429 404.6607971 600
20 149.9148712 151.6467133 172.2976532
400
10 89.58270264 92.80486298 96.50827026
5 56.695961 62.06573868 49.37532425 200
2.5 33.77085114 29.83438301 25.99719429
1.125 11.85295773 12.34904385 13.03051186 0
10 20 30 40 50
0.5625 5.182677746 10.04333687 8.860201836
 Área
Día 2 Día 3 Prom. Área Desv. Estándar %CV S/N LoD
1030.228536 1126.3877763 1013.682712 108.4662749179 10.700219 9.345602703
784.8371989 907.39514163 805.02230497 85.61207265324 10.634745 9.403140001
507.2189128 625.1101888 554.53544109 55.03100429798 9.9238029 10.07678214
378.5362752 405.74146527 387.28342692 41.12444527011 10.618695 9.417353216
150.3453572 157.95307923 399.75119188 369.2259149886 92.363931 1.082673712
4.7636116
92.965278627 92.965278627 3.465569448095 3.7278105 26.82539768
56.045674643 56.045674643 6.370149830305 11.365997 8.798172121
29.867476147 29.867476147 3.886934083845 13.013936 7.684070659
12.410837813 12.410837813 0.591204112552 4.7636116 20.99247544
8.0287388173 8.0287388173 2.534758340254 31.571065 3.167457303

Área vs [=] ppm

f(x) = 8.22800959172353 x + 138.374439872283

R² = 0.916585802877064

20 30 40 50 60 70 80 90 100 110
[=] ppm
LoØ
[=] ppm tiempo (min)
iny 1 iny 2 iny 3
100 24.748541 24.011587 24.813236 24.478058 24.320175 24.265879 23.944735 23.887201
80 25.224937 24.53804 24.704212 24.202492 24.106409 24.074099 23.85372 23.771004
60 24.647785 24.894129 24.569822 24.004763 23.964064 24.075666 23.753061 23.777952
40 24.651693 24.697453 --- 24.011372 24.045643 24.022142 23.613167 23.682425
20 24.489809 24.489023 24.435305 23.977457 23.945944 23.894121 23.598032 23.671488

[=] ppm tiempo (min) iny 2 iny 3

100 22.114349 22.573015 22.166527 21.972591 21.785694 22.021526 21.494505 21.484285
80 22.578056 22.00251 22.286951 21.698885 21.870926 21.774965 21.494097 21.469193
60 22.232738 22.350121 22.549753 21.866501 21.771797 21.851288 21.486288 21.51326
40 22.354555 22.18918 22.298182 21.780462 21.760214 21.790194 21.441032 21.510569
20 22.547621 22.365427 22.329748 21.724501 21.871416 21.864157 21.546778 21.638351

Chart Title
120

100 f(x) = 11.2106816317777 x − 65.6502

R² = 0.998338449867221

800

600

400

200

0
10 20 30 40 50 60 7
 Alfa amirin data
Media Desvest %RSD Área
iny 3 iny 1
23.859283 24.258744 0.363419 1.4980949 1080.6331 1032.3408 1099.7656 917.73828 891.42664 898.63208
23.79579 24.2523 0.4855835 2.0022161 875.78717 908.01776 --- 845.02094 730.81702 767.04156
23.731676 24.157658 0.4343684 1.7980568 594.45142 588.14349 597.86371 514.78632 581.87659 553.08594
23.625195 24.043636 0.4292165 1.7851563 379.68417 385.11075 --- 352.51712 337.36304 325.60648
23.574434 24.008401 0.376357 1.5676054 186.57666 191.28467 204.23944 162.95195 143.01863 142.63907

Beta amirina data

iny 3 Media Desvest %RSD Área iny 2
21.465284 21.897531 0.3756999 1.7157182 874.94061 895.87024 882.48462 1078.9137 1008.8849 1002.887
21.531298 21.85632 0.3784918 1.7317272 732.92078 735.14587 700.43707 729.21912 815.91406 809.37842
21.504271 21.902891 0.3925375 1.7921723 535.64148 525.09442 533.09576 505.58743 505.83789 510.23141
21.506495 21.847876 0.351316 1.6080097 378.06744 374.89474 379.75543 347.24985 462.55319 325.80579
21.580912 21.94099 0.376421 1.7156061 861.73804 878.97583 932.15155 135.30324 184.565 131.16783

Chart Title Chart Title

120

2106816317777 x − 65.650296460105 100

8338449867221 f(x) = 10.684029328168 x − 58.1071390432739
R² = 0.997344417581894
800

600

400

200

0
40 50 60 70 80 90 100 110 10 20 30 40 50 60 70 80 90 100 110
 Media Desvest %RSD

1256.6165 1174.34 1177.9836 1058.8307 133.74721 12.631595

844.64166 856.6499 878.37738 838.29417 59.671138 7.1181621
657.45465 663.07489 647.8465 599.84261 49.415622 8.238098
361.64633 396.96558 358.31998 362.15168 24.214238 6.6862145
199.4422 175.24188 177.10982 175.83381 22.541688 12.819882

iny 3 Media Desvest %RSD

1097.9659 1134.9537 1146.2437 1013.6827 108.46627 10.700219
903.96417 897.40552 920.81573 805.0223 85.612073 10.634745
604.33893 646.0816 624.91003 554.53544 55.031004 9.9238029
430.39716 382.16644 404.6608 387.28343 41.124445 10.618695
149.91487 151.64671 172.29765 154.14922 20.794196 13.489654

β-amirina
alfa ppm area
20 175.83381 20 154.15
40 362.15168 40 387.28
60 599.84261 60 554.54
2739
80 838.29417 80 805.02
100 1058.8307 100 1013.68

11.207742 60
396.84112 2.8242392
beta
20 154.14922
40 387.28343
60 554.53544
80 805.0223
100 1013.6827
80 90 100 110
385.63338 4062
 α-amirina
ppm area
20 175.83
40 362.15
60 599.84
80 838.29
100 1058.83