DETAILS of ACTIVITIES REQUIRING N2

A. MERCURY GUARD BED CHANGE OUT

1. Purging
1.1 3 (three) times purging @ 100 psi @ 100 F prior to N2 circulation
* Volume (MGB+ related piping) 56.6

1.2 3 (three) times purging @ 100 psi @ 100 F After leak test
* Volume (MGB+ related piping) 56.6

2. Produce positive pressure during spent catalyst unloading

duration 8 hours
Pressure inside the vessel during unloading maintained at 2 bar (29 psi)
Vessel volume 24.0
Vessel opening during injection, 30" diameter

3. N2 Circulation @350 psi, T= 160 F

System volume + 30% contingency 451.0
Top-Up (assumed 100 %) of system volume to keep P @ 350 psi 451.0

4. Leak Test @ 750 psi, T= 90 F

* Volume (MGB+ related piping) 56.6

Connection: Raised Face 2", ANSI 600# TOTAL VOL GAS 1095.7
38,695.91

Assumption P= 350 psi T= 160F

then V'/V=119 SCF/BBL

Total Liquid N2 Requirement (=Total requirement/(V'/V)) 325.17567771

13657.378464
For Top-up ( assumed 100% of the system volume) 13657.378464
 DIALOG CALCULATION BASED ON HALLIBURTON EQUATION
AMMONIA CONVERTER PUSRI IB

UNLOADING

m3 Volume NH3 Converter + Related piping m3 405.63

m3 Volume NH3 Converter + Related piping m3 405.63

Duration to keep positive pressure 177 hours

m3 Vessel volume NH3 Converter 172 m3 3,805.50

m3 System volume + 30% contingency m3 3,232.17

m3 m3 3,232.17

m3 Volume NH3 Converter + Related piping m3 405.63

m3 Total volume m3 11,486.73

ft3 ft3 405,653.99

P= 350 psi = 24 kg/cm2, T= 160 deg F= 57 deg C

BBL 3,408.86
Galloon 143,172.00
Galloon 143,172.00

1 gallon N2 3.06 kg 46,788.23

46.79

LOADING JOB m3 94.30

1 Purging
2 Maintain positive pressure 751.67
Volume basket 1 40 m3
Duration of loading 73 hours
N2 Circulation m3 751.67

Total volume m3 1,597.63

ft3 56,420.34
BBL 474.12
Gallon 19,913.06
 kg 6,507.54
ton 6.51
Total N2 requirement Unoading + Loading ton 53.30
BBL
Galllon
Galllon

kg
ton