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Low (10-800 MHZ) and High (40 GHZ) Frequency Probes Applied To Petroleum Multiphase Flow Characterization
Low (10-800 MHZ) and High (40 GHZ) Frequency Probes Applied To Petroleum Multiphase Flow Characterization
Low (10–800 MHz) and high (40 GHz) frequency probes applied to petroleum multiphase flow
characterization
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Abstract
The method presented here is suited to the real-time characterization of fluids pumped from an
oil layer. Two kinds of flow in the production line are studied: homogeneous flow of oil and
water and annular flow (oil and water plus a gas column). The method is based on dielectric
spectroscopy. Two probes are used: one at high frequency (around 40 GHz) to determine the
composition of the liquid phase, i.e. the oil–liquid ratio (OLR) and the water–liquid ratio
(WLR); a second one at low frequency (10–800 MHz) to calculate the gas ratio or gas hold-up
(GHU). The electromagnetic models of each probe are presented. Experimental results for
static and dynamic fluids (measurements on a two phase flow loop) validate the principle for
homogeneous and annular flows for GHU between 60% and 95%.
Keywords: sensor, petroleum, oil, OLR, WLR, GHU, gas hold-up, multiphase, emulsion,
annular flow, microwave, dielectric spectroscopy, permittivity, flow loop, pipeline
2. Principle
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Meas. Sci. Technol. 19 (2008) 055602 E Bondet de la Bernardie et al
remain valid if the gas column is not detected by the HF of a coaxial window, the problem is solved by using the trivial
probe. So the maximum GHU must be defined. Let us note formula to calculate the admittance in the plane z = −dW from
that quantitative reasoning based on penetration depth is not the admittance in the plane z = 0 (found with [19]) for a TEM
possible; indeed, the matching between the tight window and mode (3) if we assume that the TM modes generated in the
the fluid in the pipeline must be included in the calculus. plane z = 0 are negligible in the calibration plane z = −dW
Qualitatively, the interest in working at very high frequency is (this assumption is valid if dW > 0.7 mm in the case of a peek
having a low penetration depth, except with very low losses in window in APC-7 mm)
liquid: the worst case for the validity domain is then when φ o √
y(z = 0) + i tan(k0 εWin dW )
is very high. According to simulations carried out the minimal y(z = −dW ) = √ , (3)
1 + iy(z = 0) tan(k0 εWin dW )
thickness of liquid for which the gas column has no influence
is 0.15 mm at 40 GHz, i.e. a maximal GHU equal to 98%, if where y is normalized admittance, εWin is the permittivity of
φ o < 0.90. If φ o > 0.95, the maximal GHU is around 95%. the window and k0 = 2πf c
( f is the working frequency and c is
the speed of light in vacuum).
4. Low-frequency probe: analytical model Thus, by using this analogy, the admittance YLF measured
with the LF probe is linked analytically to the permittivity of
For LF probe, the model linking φ w, φ o and the GHU the liquid layer and its thickness e. This one is thus computed
to the measured admittance is analytical. A geometrical from measured YLF and from the permittivity of the liquid
analogy between the device of figures 1 and 2 and the cell of (obtained with the HF probe) by minimizing on the frequency
figure 4 [19] denoted as SC is considered. The height h of the band the difference between YLFmeasured and YLF(e), e being the
cell corresponds to the thickness e of the liquid layer in the adjustable parameter. Then the GHU is trivially deduced from
pipeline (figure 2); on the plane z = h (figure 4) a magnetic e (cf the appendix).
wall corresponding to the interface between the liquid and the
gas column of figures 1 and 2 is placed. This analogy, limited 4.2. Validation and limit of the analogy, sensitivity
in frequency, is based on the fact that the field is primarily
concentrated around the tight window in the frequency band To validate the analogy between the two structures, admittance
used (10–800 MHz). The radius R of the cell SC (figure 4) is YLF simulated using HFSS for the structure of figures 1
fixed at 14.4 mm (same value as that for the pipeline). This and 2 (LF probe) is compared with that found for the structure
value is not influential since, as a consequence of the preceding of figure 4 denoted SC. Results presented are for standard
remark, the field intensity is negligible on the electric wall at GR900, a full window in peek with a thickness of 1 mm and for
y = R (figure 4) in our band, i.e. under the first resonance two GHU: 0% (homogeneous flow) and 95%. For a GHU equal
frequency of the cell. to 95%, the thickness of the liquid layer is 0.36 mm (cf the
appendix) and the value of h for cell SC is thus also 0.36 mm.
The imaginary part B of the admittances relative to the two
4.1. Analytical model
structures SC and LF probe with extreme liquids (100%
The electromagnetic problem relating to the structure of water and 100% oil) are compared at the low frequencies
figure 4, i.e. the expression of the admittance versus (figure 5).
permittivities of the window and of the liquid and versus The results obtained show that admittances are equal (with
dimensions of the cells (coaxial guide standard, thickness of a margin better than 1.5%) for the two geometries, except for
the window, radius and thickness of the liquid layer) is solved pure water (WLR = 100%) and GHU = 0% around 1 GHz.
in [16] by a modal method in the case R = a and with a full This is the first resonance frequency of the cell SC (which is
window and is solved in [19] in the case without a window the first non-trivial solution of YSC(f) = 0). In the other cases
but with R > a. The electromagnetic problem relative to (WLR = 0% with GHU 0% and 95%, WLR = 100% with
figure 4 is then a simple mix of these two cases. In the case GHU 95%), this frequency is higher than 2 GHz. So the worst
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Meas. Sci. Technol. 19 (2008) 055602 E Bondet de la Bernardie et al
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Meas. Sci. Technol. 19 (2008) 055602 E Bondet de la Bernardie et al
(a) (b)
Figure 6. Homogeneous case: oil in liquid ratio for mixtures of oil in water measured (a) with the LF probe between 1 MHz and 1.8 GHz
and (b) with the HF probe at 40 GHz (symbol: experimental results).
(a) (b)
Figure 7. Imaginary part of the admittance for annular flow water–air: (a) measured with LF probe and (b) measured with HF probe.
Agilent E8364B (10 MHz–50 GHz) with an average of 8 and and BGHU = 100% but is not. For this very high GHU (98%),
a bandwidth of 700 Hz. For a given GHU, measurements are we assume that the flow is not perfect as in figure 2: this
made five times over 20 s and then averaged. The two probes assumption is consolidated by the calculation of the GHU with
used are in standards GR900 (LF probe) and APC-2.4 mm (HF the LF probe at this point (section 5.2.2). For the LF probe,
probe). The two probes have full 1 mm thick windows in peek YLF depends in a very significant way on the GHU as desired
(ε r = 3.2). The admittances measured with LF and HF probes (figure 7(a)). In addition, let us note that a temporal average
are presented in figures 7(a) and (b), respectively, for various (five measurements during 20 s in addition to the average
GHU. of eight) makes it possible to obtain low noise curves of
One can note that with the HF probe (figure 7(b)), YHF admittances in the frequency bands studied, i.e. (10–800 MHz)
is sensitive to the fluid running out in the pipeline beyond and around 40 GHz. Moreover, for very high GHU (>95%) the
approximately 20 GHz: the variation of the admittance reference measurement (with the densitometer) is suspicious.
between the presence of water on the circumference and the It could be interesting to use more sensitive equipment to make
presence of air (GHU = 100%) increases with the frequency. this comparison.
YHF is also independent of the GHU as wished except for
a GHU of 98% beyond 36 GHz. The consistency of this 5.2.1. Calculation of φ w or φ o with the HF probe. The
case is doubtful: there is indeed an anomaly for this GHU theoretical φ w is of course equal to 1 (no oil in the loop)
at HF: BGHU = 98% should logically be between BGHU = 93% and thus, from figure 3, theoretically B = 32 mS. For the
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Meas. Sci. Technol. 19 (2008) 055602 E Bondet de la Bernardie et al
6. Conclusion
The theoretical study and the tests of the sensor in static and
dynamic conditions showed the effectiveness of the association
of a LF probe (10–800 MHz) with a HF probe (around 40 GHz)
for the determination of the water, oil and gas contents in the
case of annular or homogeneous flow. The validity domain for
the determination of the WLR and OLR using the HF probe
is included between GHU = 0% and 95%. Above 95% the
gas column disturbs the wave emitted by the HF probe. The
HF model is then invalid. For the determination of the GHU
with the LF probe knowing the WLR thanks to the HF probe,
the minimum GHU is 60% (absolute precision better than 4
points between 60% and 80%, better than 2 points above 80%);
under 60%, the admittance measured with the LF probe is no
longer sensitive to the gas column. Thus, the general range of
Figure 8. GHU measured with LF probe versus GHU measured validity of the sensor is fixed for GHU ranging between 60%
with the densitometer gamma. and 95%. If the GHU is lower than 60% (in the homogeneous
case for example), only the WLR and OLR can be calculated
various GHU, B measured at 40 GHz is equal to 32.5 mS ± (either with the LF probe since then the thickness of the liquid
0.5 mS, except for GHU = 98% (34.4 mS). The case 98% layer does not have any influence, or with the HF probe), the
is discussed in section 5.2.2. So the measurements are quite GHU being then unspecified. In addition, it was shown that
good below 95% but must be improved during the next tests on the nature of the emulsion could be given with the HF probe.
the flow loop: indeed, using section 3.2, the total uncertainty Measurements in flow loop moreover showed that this type of
in B (due to VNA, flow, mechanical tolerance, model) must be flow does not appreciably deteriorate measurement, a temporal
better than 0.1 mS—and not 0.5 mS as in our measurements— average reducing the noise due to the flow. On the other hand,
to have an absolute uncertainty in φ w(%) around 3 points. A a lack of precision for GHU higher than 95% was highlighted
way to improve measurements could be to increase the number with flow loop measurements: the shape of the gas column
of sweeps and to implement, in addition to the classical following figure 2 could be better modeled in the case of high
calibration, one with known fluids: air, oil and water for GHU, even really modified by changing the geometry of the
example. probe–pipeline interface.
With the Debye law (2) and Bruggeman–Hanai (1) In addition, this study was conducted for a pipeline with
(useless here), the permittivity of the liquid versus frequency a radius of 14.4 mm. If the radius is changed, it must remain
is then deduced from φ w. large enough compared with U (figure 2) so that the flow
is not too disturbed and remains like the shape assumed in
figure 2. A radius of at least 14.4 mm is advisable if GR900
5.2.2. Calculation of the GHU with LF probe. φ w, and thus standard is used (U = 14.3 mm). If the radius is greater than
the permittivity of the liquid, being known thanks to the HF 14.4 mm, the range of validity [GHUMIN; GHUMAX] shifts up:
probe, the thickness e of the liquid layer (and thus the GHU) is the LF probe investigates the gas column up to 3.2 mm deep
calculated using the LF probe following the principle described which corresponds to a GHUMIN of 60% if R = 14.4 mm and
in section 4 on the frequency band (10–800 MHz) and then 70% if R = 20 mm for example; in the same way, the minimal
averaged (e being of course independent of the frequency). thickness from which the HF probe does not see the gas column
GHU is then calculated from e and compared with the GHU is around 0.36 mm which correspond to a GHUMAX of 95% if
measured with the densitometer gamma (figure 8). R = 14.4 mm and 96.5% if R = 20 mm.
The calculation of the GHU with the LF probe is To complete the validation, it will also be necessary
superimposed on the behavior found with the gamma to carry out measurements on a triphasic loop (annular
densitometer with an absolute margin of error better than 2 flow of oil and water), this type of loop being much more
points for a GHU lower than 94%. For a GHU of 98%, the complicated to implement. Moreover, we assumed here that
absolute error is approximately 5 points. This too great error salinity, influencing the permittivity under about 30 GHz at
in the case of very high GHU can have various reasons such as 100 kppm, was known thanks to another sensor. Our sensor
the bad modeling of the shape of the gas column (figure 2) or could be extended to the determination of this parameter
the influence of the imperfections on the liquid–gas interface, by measurements of conductivity at low frequencies and by
the thickness of the liquid layer being then very weak. One can the determination of relaxation frequencies, two parameters
for example assume that the liquid–gas interface is then badly depending on salinity. The extension to other kinds of flow
defined (presence of fog) and that this imperfection, not taken (stopper, bubble and churn) should also be considered. A
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Meas. Sci. Technol. 19 (2008) 055602 E Bondet de la Bernardie et al
treatment for example with neural networks and databases [7] Arnstein W (Multi Phase Meters AS) 2005 A method and flow
obtained by simulations, on flow loops, and in real sites could meter for determining the flow rates of a multiphase fluid
then supplement the analytical study. World Patent WO 2005057142 (A1)
[8] Bo O L and Nyfors E 2002 Application of microwave
spectroscopy for the detection of water fraction and water
Acknowledgments salinity in water/oil/gas pipe flow J. Non-Cryst.
Solids 305 345–53
The authors greatly appreciate the assistance of Antonio [9] Hilland J 1997 Evaluation of modelling routines for on-line
Martino (Geoservices) for measurements with densitometer implementation of the open-ended coaxial probe Dr Sci.
gamma. They would also like to thank Agilent France for the Dissertation, University of Bergen, Norway
loan of VNA E8364B. [10] Fourrier-Lamer A, Dubrunfaut O, Badot J C, Bondet de la
Bernardie E, Le Brière B and David P Y 2006 Procédé et
dispositif de mesure d’un fluide polyphasique circulant dans
Appendix un conduit French Patent submitted no 06.07887
[11] Arndt G D, Nguyen T X and Carl J R (NASA) 1997 Method
While referring to figure 2, the expression for the GHU is
and apparatus for measuring fluid flow US Patent
SG 5675259
GHU = , (A.1) [12] Isaksen O (Christian Michelsen Research) 1999 Device for
ST
measurement of characteristic reflection coefficient for
R2
where ST = π · R 2 − 2
( − sin ) and SG = π · RG2 − electromagnetic waves in multiphase flour Patent WO
RG2 9942794
(
− sin
) where
, , in radian, are expressed by =
2 U [13] Belhadj-Tahar N E and Fourrier-Lamer A 1986 Broad-band
2 · arcsin 2·R and
= 2 · arccos A−d L
with A = analysis of a coaxial discontinuity used for dielectric
U 2
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R 2 − 2 and RG = R − dL . 34 346–52
[14] Bruggeman D A G 1955 Berechnung Verschiedener
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