3.

a. Konsentrasi -tokoferol : 15 mg -tokoferol dilarutkan dalam 50 ml etanol

15 mg
x 1000 ml/L = 300 ppm
50 mg

Larutan Baku Kerja

10 ml
1. x 300 ppm = 3 ppm
1000 ml

20 ml
2. x 300 ppm = 6 ppm
1000 ml

30 ml
3. x 300 ppm = 9 ppm
1000 ml

40 ml
4. x 300 ppm = 12 ppm
1000 ml

50 mg
5. x 300 ppm = 15 ppm
1000 ml

b. Konsentrasi -tokoferol : 5 mg -tokoferol dilarutkan dalam 50 ml etanol

5 mg
x 1000 ml/L = 100 ppm
50 mg

Larutan baku kerja

10 ml
1. x 100 ppm = 1 ppm
1000 ml

20 ml
2. x 100 ppm = 2 ppm
1000 ml

30 ml
3. x 100 ppm = 3 ppm
1000 ml

40 ml
4. x 100 ppm = 4 ppm
1000 ml

50 mg
5. x 100 ppm = 5 ppm
1000 ml

c. Konsentrasi -tokoferol : 10 mg -tokoferol dilarutkan dalam 50 ml etanol

10 mg
x 1000 ml/L = 200 ppm
50 mg
 Larutan baku kerja
10 ml
1. 1000 ml x 200 ppm = 2 ppm
20 ml
2. 1000 ml x 200 ppm = 4 ppm

30 ml
3. 1000 ml x 200 ppm = 6 ppm

40 ml
4. 1000 ml x 200 ppm = 8 ppm

50 mg
5. 1000 ml x 200 ppm = 10 ppm

A. Persamaan Regresi Linier Y = bx + a

 -tokoferol a: 7360,2
b: 35753
r: 0,9999
r2: 0,9998
y = 7360,2 + 35753x

 -tokoferol a: 4531,6
b: 65641,4
r: 0,9999
r2: 0,9998
y = 4531,6 + 65 641,4x

 -tokoferol a: 3768
b: 27234,1
r: 0,9996
r2: 0,9993
y = 3768 + 27234,1x

Kadar:
 Sampel 1 (-tokoferol)
- Puncak 1: y = 7360,2 + 35753x
272,675 = 7360,2 + 35753x
x = 7,421 mg/ml
- Puncak 2: y = 7360,2 + 35753x
190,987 = 7360,2 + 35753x
x = 5,136 mg/ml
- Puncak 3: y = 7360,2 + 35753x
225,799 = 7360,2 + 35753x
x = 6,110 mg/ml
- Puncak 4: y = 7360,2 + 35753x
 890,555 = 7360,2 + 35753x
x = 24,703 mg/ml
- Puncak 5: y = 7360,2 + 35753x
367,578 = 7360,2 + 35753x
x = 6,386 mg/ml

 Sampel 2 (-tokoferol)
- Puncak 1: y = 7360,2 + 35753x
285,666 = 7360,2 + 35753x
x = 7,788 mg/ml
- Puncak 2: 205,666 = 7360,2 + 35753x
x = 5,549 mg/ml
- Puncak 3: 235,578 = 7360,2 + 35753x
x = 6,386 mg/ml
- Puncak 4: 975,777 = 7360,2 + 35753x
x = 27,099 mg/ml
- Puncak 5: 477,932 = 7360,2 + 35753x
x = 13,168 mg/ml

 Sampel 3 (-tokoferol)
- Puncak 1: y = 7360,2 + 35753x
317,268 = 7360,2 + 35753x
x = 8,672 mg/ml
- Puncak 2: 205,666 = 7360,2 + 35753x
x = 6,812 mg/ml
- Puncak 3: 235,578 = 7360,2 + 35753x
x = 8,323 mg/ml
- Puncak 4: 1075,322 = 7360,2 + 35753x
x = 29,914 mg/ml
- Puncak 5: 589,123 = 7360,2 + 35753x
x = 16,280 mg/ml

-tokofero

 Sampel 1 (-tokoferol)
- Puncak 1: y = 3768 + 27234,1x
272.675 = 3768 + 27234,1x
x = 9,874 mg/ml
- Puncak 2: y = 3768 + 27234,1x
190,987 = 3768 + 27234,1x
x = 6,874 mg/ml
- Puncak 3: y = 3768 + 27234,1x
225,799 = 3768 + 27234,1x
x = 8,153 mg/ml
- Puncak 4: y = 3768 + 27234,1x
890,55 = 3768 + 27234,1x
x = 32,562 mg/ml
- Puncak 5: y = 3768 + 27234,1x
 367,889 = 3768 + 27234,1x
x = 13,37 mg/ml
 Sampel 2
- Puncak 1: y = 3,768 + 27234,1x
285,666= 3,768 + 27234,1x
x = 10,351 mg/ml
- Puncak 2: y = 3,768 + 27234,1x
205,666 = 3,768 + 27234,1x
x = 7,413 mg/ml
- Puncak 3: y = 3,768 + 27234,1x
235,578 = 3,768 + 27234,1x
x = 8,512 mg/ml
- Puncak 4: y = 3,768 + 27234,1x
975,777 = 3,768 + 27234,1x
x = 35,691 mg/ml
- Puncak 5: y = 3,768 + 27234,1x
477,932 = 3,768 + 27234,1x
x = 17,411 mg/ml
 Sampel 3
- Puncak 1: y = 3,768 + 27234,1x
317,268 = 3,768 + 27234,1x
x = 11,511 mg/ml
- Puncak 2: y = 3,768 + 27234,1x
250,796 = 3,768 + 27234,1x
x = 9,071 mg/ml
- Puncak 3: y = 3,768 + 27234,1x
304,778 = 3,768 + 27234,1x
x = 11,053 mg/ml
- Puncak 4: y = 3,768 + 27234,1x
1076,322 = 3,768 + 27234,1x
x = 39,383 mg/ml
- Puncak 5: y = 3,768 + 27234,1x
589,134 = 3,768 + 27234,1x
x = 21,494 mg/ml

-tokoferol

 Sampel 1 (-tokoferol)
- Pusat 1: y = 4531,6 + 656641,4x
272,675 = 4531,6 + 65641,4x
x = 4,085 mg/ml
- Pusat 2: y = 4531,6 + 656641,4x
190,987 = 4531,6 + 65641,4x
x = 2,841 mg/ml
- Pusat 3: y = 4531,6 + 656641,4x
225,799 = 4531,6 + 65641,4x
x = 3,371 mg/ml
 - Pusat 4: y = 4531,6 + 656641,4x
896,555 = 4531,6 + 65641,4x
x = 13,498 mg/ml
- Pusat 5: y = 4531,6 + 656641,4x
367,889 = 4531,6 + 65641,4x
x = 5,535 mg/ml
 Sampel 2 (-Tokoferol)
- Pusat 1: y = 4531,6 + 656641,4x
285,666= 4531,6 + 65641,4x
x = 4,283 mg/ml
- Pusat 2: y = 4531,6 + 656641,4x
205,666 = 4531,6 + 65641,4x
x = 3,064 mg/ml
- Pusat 3: y = 4531,6 + 656641,4x
235,578 = 4531,6 + 65641,4x
x = 3,520 mg/ml
- Pusat 4: y = 4531,6 + 656641,4x
975,777 = 4531,6 + 65641,4x
x = 14,796 mg/ml
- Pusat 5: y = 4531,6 + 656641,4x
477,932 = 4531,6 + 65641,4x
x = 7,212 mg/ml
 Sampel 3 (-tokoferol)
- Pusat 1: y = 4531,6 + 656641,4x
317,268= 4531,6 + 65641,4x
x = mg/ml
- Pusat 2: y = 4531,6 + 656641,4x
250,796 = 4531,6 + 65641,4x
x = mg/ml
- Pusat 3: y = 4531,6 + 656641,4x
304,778 = 4531,6 + 65641,4x
x = mg/ml
- Pusat 4: y = 4531,6 + 656641,4x
1076,322 = 4531,6 + 65641,4x
x = mg/ml
- Pusat 5: y = 4531,6 + 656641,4x
589,134 = 4531,6 + 65641,4x
x = mg/ml