Experiment 4

Name:fredo Josetrago larios

_____________________________ All April 1612021
Section: ______________ Date: ________________

SOLUBILITIES vs. REACTIONS

AND SYNTHESIS OF CALCIUM ACETATE

Laboratory Report

Part 1: Observations, Data and Calculations

1. In the table, describe your observations when the different solutes were dissolved in tap

water and when vinegar was added into the solution.

(2 marks) Table 1: Solubility and reactivity

Solute Solubility in water Reactivity with vinegar

Was highly solublein theWater Gas formation effervesce andpresence

Baking soda

doesntpresenta
change
of
colour 9 bubbles doesnt changecolour

Sugar was highly solublein theWater

doesntpresenta colour
No reaction

change
of

Salt was highly solublein theWater

doesntpresenta
change colour No reaction

of

2. (1.5 marks) Write a chemical equation to represent what you observed when you added

each solute to water.

Baking Soda NAHCOscssttkON.Natkocaq.itHM

Sugar
Cathal THON CHAqq.ittdk

saH

3. (0.5 mark) Write a chemical equation for the solute(s) that reacted with the vinegar. What

NaClssttk0asNaCkaa.sttk0 BakingS0da
type of chemical reaction does it represent?

OHq
Natk0caqjtCH.CO
sNaCHsC00

qstC0cgstHa0c
it Cag .Itis because
agasformation reaction formed

Itisanacidbasereaction sincethe reactants transferred protons CHEM 205 LAB 4: Synthesis 6

Htthatended formingwater

Experiment 4

Part 2: Observations, Data and Calculations

4. (2 marks) Table 2a: Raw data (Fill in the table. Report masses in grams.)

mass of empty beaker

18.769g

mass of beaker and calcium carbonate

21.343g

mass of graduated cylinder 16.937g

mass of graduated cylinder and 5% or 10% acetic acid 41.743g

mass of beaker and product mixture, as soon as reaction is

45.591g

completed

mass of beaker and air-dried calcium acetate after several days

30982g

Importantnote severaldaysthe
After intimesothat'sthereason I havemoremassthanexpected
mixturedidntdry

5. (2 marks) Table 2b: Calculated results (Fill in the table. Report masses in grams.)

net mass of calcium carbonate

a 2.574g

b moles of calcium carbonate 0.0257mA

c net mass of acetic acid 24806g

d moles of acetic acid 043m01

e net mass of product mixture, as soon as reaction is completed 26.822g

net mass of air-dried calcium acetate after several days 12.213g

f Importantnote mixturedidntdry timesothat'sthereason I havemoremass thanexpected

severaldaysthe
After in

6. (0.5 mark) Classify the type of reaction that occurs between calcium carbonate and acetic

acid.

itformedCag
It is agasformation reaction
because

Itisanacidbasereaction sincethe reactants transferred Htthatended formingwater

protons

7. (1 mark) Based on the quantities of the two reagents mixed, which one is the limiting

reagent? Show clear calculations that lead you to this conclusion.

Calcium carbonate

limitingreagent

CHEM 205 LAB 4: Synthesis 7

Experiment 4

8. (1 mark) Is there a mass loss as soon as the reaction is completed? Based on what you

know about the law of conservation of mass, justify your answer.

Yesitwas because weweightthemass thereactantswewill

noticethis greaterthantheone
is fromtheproducts
is g

duetothelaw conservation massweknowthismassdoesnt si disapeared what happeneddependson

of of µ

factors like example thisis a gas formation

reaction
sosome the Cor just scatteredintotheatmosphere
for q aceticacid sticker tothegranulated cylinder

factor dependson
Another human errors so exampleverysmall drops
for of

whenaddedintothecalciumcarbonate

9. (1 mark) Suppose the starting materials given to you were calcium sulfate and acetic acid
in excess. What would be different when you observe this reaction? Write the balanced

chemical equation to help justify your answer.

CaS0yt2lHsC00HcaqssCakHsC00Jz qstHaS0kaq.s

Thethingthese reactions have inCommon is one theproducts inthiscase isthecarbonateacetate

However

of
thereactionwillalsoproduce sulfuricacid whichdependingontheplastictypeq.mybeakerwillbecorroded or

notMesecondmaindifference isthatcapwillbenotjoined so thiswillnotbe a gasformationreaction

anymore andwillnotpresenteffervesce

10. (0.5 mark) If after several days you observe that the product in the beaker is completely

dry, what do you think is the composition of the substance(s) left in the beaker (Hint:

take a waft of the product in the beaker)?

We know that the beakerwilltheoreticaly contain Call HIMC4andHO becausethese

are the products andalso Up COOHbecause it isinexcessBut weknow Cor is a gas so

004areliquidsthat
itwillspreadinto theatmosphere andnolonger beonthe beakerAlsoHOand CHI

willevaporate duetoairdryingThis uswith onlyoneproductCaleb

leaves COOK calcium carbonate

CHEM 205 LAB 4: Synthesis 8

Experiment 4

11. (2 marks) How many millilitres of 6 M hydrochloric acid are required to react exactly

with (a) 1 g of calcium carbonate, and (b) 1 g of sodium carbonate? Show your

calculations, including the relevant balanced chemical equations.

a1.665mL

b1.573mL

12. (1 mark) Does the mass of the air-dried product agree with your answers to Prelab

Question 2 and Lab Report Question 6? If not, how can you account for the mass lost or

excess mass? (Hint: No calculations needed.)

several Butthe principal One is that since this a gas

It doesnt agree completely for the reasons CQ willspread intotheatmosphere and willchange
fomation reaction then a la

g gasformed
maynotbe100 pure so a lol y
randomsubstances
the mass noted inthe results Also my
reactants

will beinexcesswithmyproductmass

y airdryingNot
Mixture afterseveraldays
assoonasthereaction is completed
Mixture completed

CHEM 205 LAB 4: Synthesis 9

Calculations

Table 26

Calcium Carbonate AceticAcid Calciumacetate

a 21.343g 18,76952574g c 41.743g 16.937g 24806g e 45.591g 18.769g16.822g

bMolarmass100.08694mi dMolarmass60.0524mA f 30982g18.769g 12.213g

100,49
2.574

GO.fm fq24806g
and 6m01

a 0.0257mi
b 0.43mA

7
Formulas CaCOzcsjt2CHsC00Hcaqll.alEquationi2tkkaqstCal0s qs.ca 4 110 4,0
Molar
2
6 Aduaimdesfi

Moles I mass 36.4584mi 100.08694mi

iwo.dggqymdMojtkl
0.0257 0.43 Actualmass 9 9.9910

a0.7285 6M el 01

ateoretical 0.0257
0206
Moles 2 1

Actualm oles dudes 9 072859 e1,6651041.665mL

Limiting Imd dnd

reagent

d9.9910mol

IIb Equation.itlkaqstNaf0caqss2NaCkaqsttk0atl0cg

Mdarmass36.4584mo105.988µmol es la

105.98 0 Mq.tk 6M
72.9164mA
Actualmass vy
ftp9 hL
ttxkimol

Moles 2 1 i0.688g

9 0.6889

Actualm oles grades

Ima ama h1.5731041.574

g 10mol
9.44