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Effect of Milling Protocols on Trueness and Precision of Ceramic Crowns

Article  in  Journal of Prosthodontics · August 2020


DOI: 10.1111/jopr.13245

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Effect of Milling Protocols on Trueness and Precision of
Ceramic Crowns
Khaled Q. Al Hamad, BDS, MSc, MRD RCSEd, FDS RCSEd ,1 Rama B. Al-Rashdan, BDS ,2
Bashar A. Al-Rashdan, BDS, MS, FACP. ,2 & Nadim Z. Baba, DMD, MSD, FACP. 3
1
Department of Prosthodontics, Jordan University of Science & Technology, Irbid, Jordan
2
Private practice, Amman, Jordan
3
Advanced Specialty Education Program in Prosthodontics, Loma Linda University, School of Dentistry, Loma Linda, CA

Keywords Abstract
Trueness; milling protocol; ceramics;
precision; accuracy.
Purpose: To investigate the effect of different milling protocols for different ceramic
materials on the trueness and precision of milled ceramic crowns.
Correspondence
Materials and Methods: A definitive impression from a patient requiring a ceramic
Khaled Q. Al Hamad, Department of crown was used to fabricate forty glass ceramic crowns (VITABLOCS mark II, Vita
Prosthodontics, Faculty of Dentistry, Jordan. Zahnfabrik) milled with wet, hard milling protocol, and 40 zirconia crowns (inCoris
PO Box 3030, Irbid 22110. E-mail: TZI, Dentsply, Sirona) milled with dry, soft milling protocol, using a 5-axis milling
kqalhamad@just.edu.jo, machine (inLab MC X5; Dentsply Sirona). Trueness and precision for different crown
kqalhamad@gmail.com areas were evaluated with a 3D evaluation software (Geomagic Control X, 3D sys-
tems). Statistical analysis was performed between the 2 crown types with independent
This study was supported by a grant t-test, and analysis of variances followed by Bonferroni tests among crown areas for
(20190394) from the Jordan University of each crown.
Science and Technology, Irbid, Jordan. Results: All areas of the glass ceramic crowns had higher trueness than the zirconia
Authors declare no conflict of interest.
crown areas (p < 0.05). Crown areas of each crown type had significantly different
trueness values (p < 0.001, F = 175.17 for glass crowns, p < 0.001, F = 35.04 for
Accepted August 21, 2020 zirconia crowns). Glass crowns had 3.78 µm precision, while zirconia crowns had
4.12 µm precision, with a precision difference range between the 2 types of crowns
doi: 10.1111/jopr.13245 from 0.32 µm for the inner surface to 6.5 µm for the marginal surface.
Conclusions: Type of ceramic material and milling protocol affected trueness of
the milled crown, with higher trueness for the hardmilled glass crowns than the soft
milled zirconia crowns. Soft milled zirconia crowns were generally overmilled in
comparison with the reference design and glass crowns. However, glass crowns ex-
hibited more undermilling in thin and deep areas. The crown area affected trueness,
with external areas having better trueness than internal areas. The 5-axis milling ma-
chine had high precision, which was minimally affected by the ceramic type, milling
protocol, or crown area.

The fabrication of ceramic restorations with computer- Accuracy can be defined in terms of both trueness and
aided design and computer-aided manufacturing (CAD/CAM) precision.10 Trueness is the amount a measured object or data
technology comprises 3 steps; scanning, designing, and set deviates from the reference object or reference data set,
machining.1,2 All steps of fabrication must provide the nec- while precision represents the repeatability of measurements.11
essary accuracy to provide restorations of adequate quality.3,4 Superimposition analysis of measured data and reference data
Ceramic CAD/CAM restorations are machined out of material with a 3D inspection software is recommended for the eval-
blocks using form-grinding, which consists of removal of the uation of trueness.12 This method is nondestructive and pro-
ceramic surface with hard particles impregnated on the surface vides results both numerically and visually.11,13 The root mean
of the grinding tool at 1:1 ratio (hard grinding).5,6 However, square (RMS) value between the measured data and the ref-
yttrium-stabilized tetragonal zirconia polycrystals (Y-TZP) are erence data is often used to express trueness, with a low
commonly milled out of partially sintered blocks that are ap- RMS value representing a high trueness.14 One study reported
proximately 25% larger to compensate for sintering shrinkage a trueness of 61 ± 22 µm for inner surfaces and 55 ± 18
(soft milling).7–9 µm for occlusal surfaces of restorations for the 3- or 4-axis

Journal of Prosthodontics 00 (2020) 1–6 © 2020 by the American College of Prosthodontists 1


Milling Protocols Effect on Trueness and Precision of Crowns Hamad et al

machine, while higher trueness of 41 ± 15 µm for inner sur- temperature furnace, as recommended by the manufacturer’s
faces and 42 ± 10 µm for occlusal surfaces were reported for instructions.
the 5-axis machines.1 Other studies reported trueness of 37 to All crowns were scanned with the intraoral scanner, and were
43 µm for the internal surface of partially sintered 3Y-TZP and exported, along with the reference designs as high-resolution
37 to 38 µm for the internal surfaces of glass ceramics with Standard Tessellation Language files to a 3D evaluation soft-
5-axis milling machines.5,15 Differences in the constructions ware (Geomagic Control X, 3D systems). The software aligns
of milling machines, and differences in machining strategies the reference file and test file with iterative closest point al-
among different types of ceramic materials may influence the gorithm. The algorithm uses 3D correspondence between 2
trueness values.16–21 clouds of points and determines the minimum distance be-
The effects of the differences between soft and hard machin- tween objects. The reference design was divided by using the
ing strategies among different ceramic materials on the accu- split command function in the software into 7 areas of inter-
racy of milled restorations are not well documented. Therefore, est; occlusal area representing the occlusal surface, mesial area
the purpose of this study was to investigate the effect of differ- representing the mesial contact area, distal area representing
ent milling protocols on the trueness and precision of differ- the distal contact area, external area representing the rest of the
ent milled ceramic crowns. The null hypothesis was that there external surface, marginal area representing the marginal sur-
would be no effect of the type of ceramic material, the milling face with around 1mm of the internal surface, internal area rep-
protocol, or the area of the crown on the trueness and precision resenting the rest of the intaglio surface of the crown, and inner
of milled ceramic crowns. area representing both the internal and marginal areas. Each
area was evaluated for trueness by superimposing the mea-
Materials and methods sured data on the reference CAD design data. Best fit alignment
between the reference and the measured data was performed
Two ceramic materials were used in this study to represent with 20 maximum iteration count and 0.5 mm maximum av-
2 milling protocols; Feldspathic glass ceramics (G) with a hard erage deviation. A 3D comparison was performed with 100%
grinding protocol (VITABLOCS mark II; Vita Zahnfabrik, Bad specimen ratio, shortest projection direction, +0.5 mm and
Säckingen, Germany), and partially sintered Y-TZP (Z) with −0.5 mm for maximum and minimum deviations, and 0 spe-
a soft milling protocol (inCoris TZI; Dentsply Sirona, York, cific tolerance.
PA). A patient requiring a ceramic crown for the maxillary The results of the trueness evaluation were presented as a
left first premolar was selected for this study. The patient pro- color-difference map and numerical values of minimum, max-
vided informed consent, and the study protocol was approved imum, average, positive average, negative average, variation,
by the regional research committees (IRB 82-124-2019). The and RMS for each crown area. The RMS represents the aver-
patient received a tooth preparation for a ceramic crown with age of the positive and negative value coexistence according to
approximately 1-mm shoulder finish, 1-mm axial reduction, the following formula:
and 2-mm occlusal reduction. Proper soft tissue management 
n
i=1 (X 1, i − X 2, i)
2
was performed, and intraoral quadrant maxillary, mandibular,
and buccal scans were made with an intraoral scanner (Con- RMS = √
n
nect SW 4.6; CEREC Omnicam; Dentsply Sirona). A design
was created for a monolithic crown by using a dental design where n is the total number of measuring points, X1,i is the
software(inLab CAD SW 18.0; Dentsply Sirona) with the fol- measuring point of the reference scan data, and X2,i is the mea-
lowing design parameters; radial and occlusal spacer: 80 µm, suring point of the milled crown prosthesis scan data.11 The
proximal, occlusal and dynamic contacts: 25 µm, minimal ra- standard deviation of the RMS mean represented precision.
dial thickness: 500 µm, minimal occlusal thickness: 700 µm, Descriptive statistics are presented as means for RMS, posi-
marginal thickness: 50 µm, width of ramp: 150 µm, angle tive average, and negative average for each crown area. Homo-
of ramp: 60 µm, undercuts removal and instrument geome- geneity of variance was checked with the Levene test. Statisti-
try were considered. A total of 40 G crowns were fabricated cal differences were calculated with independent t-test between
with a set of 4 diamond grinding burs (Diamond bur, Dentsply the 2 crown types for each crown area, and analysis of vari-
Sirona), and wet, hard grinding, extra fine, and normal speed ances (ANOVA) and Bonferroni post hoc tests among crown
milling protocol. The same reference design was also used for areas for each crown. All statistical analyses were performed
the sequential fabrication of 40 Z crowns with a set of 3 tung- with a statistical software program (IBM Statistics for Win-
sten carbide milling burs (Bur ZrO2, Dentsply Sirona), and dry, dows, v22.0; IBM Corp) with α = 0.05.
soft milling, extra fine, and normal speed milling protocol. All
crowns were fabricated by using a 5-axis milling machine (in- Results
Lab MC X5, Dentsply Sirona) and were retrieved from the G
blocks and Z discs. The remains of the sprues were not ad- Means for RMS, positive averages, and negative averages are
justed and no finishing or glazing procedures were performed. shown in Table 1. All areas of the G crowns had signifi-
All crowns were freed from dust with a ceramic brush and cantly higher trueness (lower RMS) than the Z crown areas
compressed air and then dried in a drying cabinet at 80°C (p < 0.05). There were also significant differences among the
for 25 min. The Z crowns were sintered in a sintering fur- crown areas for each type of crown (p < 0.001, F = 175.17
nace (inFire HTC speed, Dentsply Sirona) by using the inCoris for the G crowns, p < 0.001, F = 35.04 for the Z crowns).
TZI program in a sintering tray with beads intended for high- There were significant differences among the G crown areas

2 Journal of Prosthodontics 00 (2020) 1–6 © 2020 by the American College of Prosthodontists


Hamad et al Milling Protocols Effect on Trueness and Precision of Crowns

Table 1 Means for root mean square (RMS), positive average (+AVG), negative average (–AVG), and P value and confidence intervals (CI) for glass
crowns (G) and zirconia crowns (Z) for each crown area

Crown area RMS (G) ± SD∗ +AVG (G) -AVG (G) RMS (Z) ±SD∗ +AVG (Z) -AVG (Z) p∗∗ 95% CI

External 37.5 ± 2.93 26.4 −29.7 44.23 ± 7.28 80.57 −58.05 p = 0.003 −6.93 to -1.54
Occlusal 35.9 ± 4.89 14.7 −33.5 61.45 ± 7.51 16.10 −64.45 p < 0.001 −25.21 to −18.53
Mesial 25.3 ± 3.26 17.4 −24 50.75 ± 6.80 6.59 −75.39 p < 0.001 −25.77 to −19.95
Distal 17.1 ± 2.44 15.0 −10.64 64.28 ± 1.88 6.47 −61.24 p < 0.001 −52.81 to −40.64
Marginal 48.9 ± 6.6 4.50 −45.78 71.14 ± 1.1 13.87 −58.13 p < 0.001 −22.27 to −13.48
Inner 43.9 ± 2.88 36.0 −35.3 78.95 ± 2.56 23.77 −47.62 p < 0.001 −40.27 to −23.56
Internal 41.4 ± 3.49 36.8 −24.31 83.89 ± 1.74 24.56 −41.43 p < 0.001 −46.32 to −35.01
*
SD: standard deviation representing the precision value.
**
Independent t-test.

except between the occlusal and external areas (p = 0.99), in- the sintering tray. In order to prevent the sintering beads from
ternal and inner areas (p = 0.077), occlusal and internal areas sticking, the crowns were not pressed or embedded into the
(p = 0.103), and external and internal areas (p = 0.262). There sintering beads layer, according to the manufacturer’s recom-
were also statistically significant differences among the crown mendations.
areas of the Z crowns (p < 0.001) except between the ex- All crowns were milled with a 5-axis milling machine, which
ternal and mesial areas (p = 0.99), distal and occlusal areas uses instruments with different geometry with one motor spin-
(p = 0.614), distal and marginal areas (p = 0.99), occlusal and dle sweeping the restoration in the z direction. Two spindles
marginal areas (p = 0.092), mesial and occlusal areas (p = that grind the restoration from both sides in a U-shaped move-
0.670), and inner and internal areas (p = 0.99). ment are used in the 3- or 4-axis milling machines.5 Higher
Precision analysis (based on the standard deviation of RMS) trueness and a more effective milling of surfaces close to the
showed a total precision of 3.78 µm for the G crowns and 4.12 insertion axis were reported for the 5-axis milling machines.1,12
µm for the Z crowns, with a precision difference range between However, the milling time is slower in comparison with 3- or
the 2 types of crowns from 0.32 µm for the inner surface to 4-axis milling machines.12
6.5 µm for the marginal surface (Table 1). The hard grinding of glass ceramics showed significantly
The color-difference maps between the reference design data higher trueness than the soft milling of partially sintered
and the measured data for a G and a Z crowns are presented Y-TZP in all crown areas. This could be attributed to the dif-
in Figures 1 and 2. Light to dark blue areas represent a nega- ferences in the machinability between the 2 ceramic materials.
tive deviation, which means that the measured data are lower The milling protocols are controlled by the numeric control
than the reference data. Yellow to red areas represent a posi- program that contains a set of instructions for the machine
tive deviation, which is the opposite of the negative deviation. tool to execute specific axis motions (tool path) at a given feed
Z crowns were generally over-milled (negative deviations) in rate, and to rotate the milling tool at a specific spindle speed.18
comparison with the reference design and also in comparison The G and Z crowns had different material hardness, types of
with the G crowns. burs, and milling protocols. The soft milling of the Z crowns
is widely used because it is cost-effective and easy to perform,
Discussion but it takes longer and requires milling to approximately
25% larger size to compensate for the sintering shrinkage.
This study investigated the effect of hard machining of glass The sintering process was reported to induce self-healing of
ceramics and soft machining of partially sintered Y-TZP on surface flaws caused during the milling process.8,9 The G
the trueness and precision of different areas of the milled crowns were milled out of ceramic blocks in their final size
crowns. Trueness was significantly different between the 2 and required no sintering process.
crown types for each crown area. It also was significantly The Z crowns were generally over-milled in comparison with
different among the crown areas for each crown type, so the reference design and also in comparison with the G crowns,
the null hypothesis was rejected for the trueness analysis. as shown by the negative average in Table 1 and the color-
The precision analysis showed minimal differences between difference map in Figures 1 and 2. This could be attributed to
the 2 crown types for each area, and also minimal differ- insufficient shrinkage compensation. One study reported less
ences among the areas for each type of crowns, and therefore, variation in the internal fit of hard machined restorations in
the null hypothesis was partially accepted for the precision comparison with soft machined restorations.19 This was a re-
analysis. flection of the complex production where sintering shrinkage
All Z crowns were sintered by using a sintering tray with must be counter weighed during the process of soft machining.
beads, which are intended for high-temperature furnace. Beads Zirconia could be milled from fully sintered blocks, and this
are used as rollers to allow the crowns to shrink and move dur- is advantageous due to the lack of post sintering process, how-
ing the sintering process. Crowns were positioned occlusally in ever, it requires a robust milling system with high accuracy,
the sintering layer without touching each other or the edge of especially in thin areas, and could be disadvantageous in terms

Journal of Prosthodontics 00 (2020) 1–6 © 2020 by the American College of Prosthodontists 3


Milling Protocols Effect on Trueness and Precision of Crowns Hamad et al

Figure 1 Color difference map trueness analysis for glass ceramic crown areas. A, Reference design. B, Glass ceramic crown specimen. C, Best-fitting
alignment between reference design and ceramic crown specimen. D, External area, positive deviation in 1st yellow color level. E and F, Mesial and
distal areas, mixed negative and positive deviations in 1st levels of yellow and blue colors. G, Occlusal area, deviation is mostly negative in 1st and
2nd blue color levels, with positive deviation in central fissure and marginal ridge area. H, Marginal area, negative deviation mostly in 1st blue color
level. I, Internal area, mixed deviations. Positive deviation in areas related to buccal and palatal cusps and also distal marginal ridge. Mild orange and
higher orange color levels are related to deeper cavities provided by software design. Rest of internal area showed negative deviation mostly in 1st
blue color level.

of surface flaws, surface roughness, and phase transformation.7 hardness, and the methodology of the 3D comparison analysis
The G and Z crowns had also different milling angles to the z between this study and the previous studies. To the authors’
axis of the milling spindle because the G glass was milled by knowledge, there were no available studies with similar crown
using ceramic blocks in a constant position in the milling ring, areas for comparison with the results of this study.
while the Z crowns were nested sequentially in variable posi- The color-difference map analysis of both types of crowns
tions in the disc. The effect of this on trueness is not clear and exhibited more positive deviations in thin areas, in the areas
requires further investigation. around the sprue, and occlusally in the central fissure area and
In agreement with another study, trueness analysis re- the distal marginal ridge area. However, G crowns exhibited
vealed significant differences among the different areas of the more positive deviations in these areas, and in the external sur-
crown.12 External, occlusal, and proximal areas had generally face. This is in agreement with other studies that reported the
higher trueness than the marginal, inner, and internal areas. In- presence of undermilling of deep areas due to the limitations
ternal area were reported to be more difficult to mill in com- of the tools for milling harder materials.5,12,13,20 Analysis of
parison with external areas.12 the tooth preparation showed sharp distal-occlusal and palatal-
Previous studies reported trueness values between 37 and occlusal line angles. The internal areas that corresponded to
43 µm for the internal, occlusal, or external areas.1,5,15 These the sharp line angles of the preparation showed increased pos-
were similar to the trueness values of the G crowns areas, how- itive deviation. Instrument geometry was considered in the de-
ever, the inner-internal areas of the Z crowns had higher RMS sign of the crown, and this meant that when the instrument di-
of around 79 to 84 µm. These differences could be attributed to ameter exceeded the dimension of curves in the preparation,
the differences in the type of milling machine, ceramic material unwanted cavities were produced.5 It can be recommended to

4 Journal of Prosthodontics 00 (2020) 1–6 © 2020 by the American College of Prosthodontists


Hamad et al Milling Protocols Effect on Trueness and Precision of Crowns

Figure 2 Color difference map of trueness analysis for zirconia ceramic crown areas. A, Reference design. B, Zirconia ceramic crown specimen. C,
Best fit alignment between reference design and Zirconia ceramic crown specimen. D, External area, negative deviation in 1st and 2nd blue color levels
and positive deviation in area related to sprue and beneath marginal ridge. E and F. Mesial and distal areas, Mostly negative deviations in 1st and 2nd
blue color levels with minor areas of 1st yellow color level. G, Occlusal area, negative deviations in 1st three blue color levels with positive deviations
in disto-buccal and central fissure areas. H, Marginal area, negative deviations in 1st and 2nd blue color levels. I, Internal area, mixed deviations with
negative deviations in 1st and 2nd blue color levels in most area and positive deviation of 1st yellow color level in areas related to distal marginal ridge
and palatal cusp.

remove sharp line angles in the prepared tooth, and to avoid material of the restoration could be recommended for better
deep grooves and acute bends in crown designs. Furthermore, milling quality.
extra attention is recommended to avoid sprue placement in The clinical relevance of the results in this study should
critical crown areas, such as the occlusal and proximal areas, be interpreted with caution. Two-dimensional techniques were
and also in adjustments of not only the remains of sprues but used in most previous studies that investigated the fit of milled
also to the area in close proximity around the sprue. restorations.22–24 Trueness, however, is a 3D measuring tech-
Despite using the default crown milling parameters, the nique with a large number of randomly distributed measur-
milling machine performed differently between the soft milling ing points, and it is not a measure of fit, nor is it a measure
of the Z crowns and the hard grinding of the G crowns. The G of clinical quality. It is a measure of the difference between
crowns were closer to the reference design in comparison with the crown and its reference design. Unfortunately, a reference
over-milled Z crowns. However, G crowns were less forgiving RMS value that indicates a clinically acceptable trueness is
than the Z crowns in the thin and sharp line angles, and in the lacking. One study recommended an RMS value of less than
areas around the sprue. Similar results of 30% to 200% devi- 10 µm for an excellent trueness.14 Others used 50 µm as a ref-
ation from the default parameter setting were reported by one erence tolerance.11,13 These recommendations, however, were
study.21 The complex manufacturing process, inherent material not based on objective criteria.
properties, and abutment geometry were reported as possible The 5-axis milling machine had an overall slightly higher
reasons. The design parameters recommended by the manufac- precision for the G crowns in comparison with the Z crowns,
turer should be considered a requirement for optimal results. which could be due to the lack of the sintering process.
However, changes to the default setting to suit the type and The precision analysis showed small differences in precision

Journal of Prosthodontics 00 (2020) 1–6 © 2020 by the American College of Prosthodontists 5


Milling Protocols Effect on Trueness and Precision of Crowns Hamad et al

values between the 2 crowns and also among crowns areas. The 8. Edwards Rezende CE, Sanches Borges AF, Macedo RM, et al:
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61-68
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with other studies,12,13 however, these differences are likely of (trueness and precision) of measurement methods and results
no clinical relevance. part 1: general principles and definitions. ISO 5725-1:1994(en).
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