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    Standmdizaton Otybroekrie: Expriment

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    Nilotpaul Kundu Dhrubo
    This experiment determined the concentration of hydrochloric acid using a standard sodium carbonate solution through titration. The titration reaction of HCl with Na2CO3 produces NaCl, CO2, and H2O. Two end points were observed - the first at pH 8.3-10 using phenolphthalein indicator, and the second at pH 4.3-4.7 using methyl orange. The concentration of the HCl solution was calculated to be 0.1077 N, with a percentage error of 1.25% compared to the known value of 0.105 N. Care must be taken to accurately measure volumes and avoid contamination when performing acid-base titrations.

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    Standmdizaton Otybroekrie: Expriment

    Uploaded by

    Nilotpaul Kundu Dhrubo
    23 views8 pages
    This experiment determined the concentration of hydrochloric acid using a standard sodium carbonate solution through titration. The titration reaction of HCl with Na2CO3 produces NaCl, CO2, and H2O. Two end points were observed - the first at pH 8.3-10 using phenolphthalein indicator, and the second at pH 4.3-4.7 using methyl orange. The concentration of the HCl solution was calculated to be 0.1077 N, with a percentage error of 1.25% compared to the known value of 0.105 N. Care must be taken to accurately measure volumes and avoid contamination when performing acid-base titrations.

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    chem 3

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    This experiment determined the concentration of hydrochloric acid using a standard sodium carbonate solution through titration. The titration reaction of HCl with Na2CO3 produces NaCl, CO2, and H2O. Two end points were observed - the first at pH 8.3-10 using phenolphthalein indicator, and the second at pH 4.3-4.7 using methyl orange. The concentration of the HCl solution was calculated to be 0.1077 N, with a percentage error of 1.25% compared to the known value of 0.105 N. Care must be taken to accurately measure volumes and avoid contamination when performing acid-base titrations.

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    © All Rights Reserved
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    23 views8 pages

    Standmdizaton Otybroekrie: Expriment

    Uploaded by

    Nilotpaul Kundu Dhrubo
    This experiment determined the concentration of hydrochloric acid using a standard sodium carbonate solution through titration. The titration reaction of HCl with Na2CO3 produces NaCl, CO2, and H2O. Two end points were observed - the first at pH 8.3-10 using phenolphthalein indicator, and the second at pH 4.3-4.7 using methyl orange. The concentration of the HCl solution was calculated to be 0.1077 N, with a percentage error of 1.25% compared to the known value of 0.105 N. Care must be taken to accurately measure volumes and avoid contamination when performing acid-base titrations.

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    of 8

    Eperiment Number: 03

    Name ok te expriment
    Standmdizaton otybroekrie
    acid win Atanduzd Sodim
    Cobonate xouon
    Cowwae : CHEM-114

    Name
    Souny Dip Bame
    RoL 1908 016
    Gvoup A1

    Depovdment: IPE

    Dede expøument : 9 Monch, 2020


    Dade e Aubmiaplen 6December, 2020
    Obieehie.
    The theme e thi expoumet ioto dotuumne
    he asmenth o siva ydoelarie aid. wtk a
    sdandord oodium carbonate audion .

    Indoducrion'
    he impodont matteva That ane swlatea to

    Re axpeúment me disoued one dy


    Oneone Main
    we madto eonduct a itration We will continue oun
    éXpUüment as Voluemebrve quoxhive analysid. he
    ditzaion baved reucion wbed to eonelude TRe

    expeumerd oiven bela


    PHCL Ca) +
    NogCe)- N a e l + Cop + Hz0

    This e0dion ds bpicall too tep eacion. At

    ind He eacta with Na,CO andL prioduc


    NaH and Nac Ad NaH a asie alt

    urtkor adeling Hel in e oludion Tepullb n

    Nc, HLO and Co2


    D2
    ebaBe 7R0ehon i actuall splittad a, allw:
    aHelCa) + Na,Cs (aa) NoHco (a)+ Nael()
    2
    HeD

    )NaHco (+Hel (ea) NatH 0(a)


    Heo + * +1420

    Ovwrall eaction

    Hel + NaCo Nacl +Co2 t H20


    2 CO2tHzO
    CD
    o pertimentJass ap
    The pH change ph
    iven beloa:

    Preopehalon
    HC 2CO dwrg

    e
    given.
    Coa
    Lodo
    ot
    -

    Metyp Oore
    H0 Co,',0

    Vol oh aod ded c )

    FFia pH chorge cmoph. ote Comducded experur


    Fro The gouph ue em Aee Rot uge qet tuo dikrent end coints.
    when Hel reach wtk Na,cos and produees

    NoHC (enction.awe get a


    6sem 0972 oldion whioh
    ptoducus , tnd
    Kas a erdpoirt Fudkesu addrhon k add,

    HO. d aho gived onoctrer erd point

    We
    We we tus mdicadoou auch a metryl omanp c

    o indicode thope tuo point and bosR. ok


    phenophthalain
    HRam wor n tuo dhoert pH nge. Methy onanp
    4Uonk TRe pH unp o 9.5-4.3 wnioh io Jha endpoirt
    the eachion ) . Fo he end point, ua
    o t we

    phenopthalein hat wwnks in 8.3-Jo.0.

    Meaniom p chang agen Jbelow.

    OH

    +H
    6
    o

    o (Pin)
    F oak mechamiom sk phenogtRalsin in bue)

    O
    o
    aeid
    t4*
    0

    OH
    O

    colbre

    g' wbnk mechonipn o phenphtholein aeid)


    omEnsaenesne

    App awratus
    1) Conicol. lask
    3) Burete
    ) Ppete
    4) Vokumebie flask
    5 Stund
    6 Fumel

    Expesümedal doda:
    Jnital weiht ok NagC 37.655
    Fino wuight o Ncog 37.031
    weiht taken ok N,C 0,571
    taken
    Shergtt eNa cda=Weht XO.1
    Weitht to be tuken

    Dat oheet
    No e Volame Bmete eading (mb) Di}haena. Dtmende Ac
    between beween TBR
    Obaswation Fint Second LBR& 1et 4 2nd end
    No09 18A
    end poined
    (m pointend"pamt(ml)
    CmL)
    10.0 O.0 4-0 8.6 4.0 B6
    S65
    02 lo.0 8.6 12.611.3 40
    Calculation
    e knoe hot
    VacidX Sacid VLaheX X ue
    Vare o m
    oare 0571
    X01
    053

    0.1077 N

    Vaud 865 m
    Sacid
    Vaare X Sbane
    Said =

    Vacid
    o 0.1017
    5
    125 N

    Repul
    The stnengk tRe ppled HCL i 0.135 N

    Peicendage ou
    Porucertaeenor =
    knoun value - Obrerredvaud
    Xla
    Knoun. Vajue

    UR5-0125 x
    O12
    Dipepion
    oorO aUze exma
    The Pobaible aulep

    ader asded in A vonetniec lask dhures Na,COg


    e exta uede
    abudion, tmay ehonge tRe reault
    whula
    Dnot counted. We hove to be vey caseful

    UBITg Cone Hel. We shoull ony add acid in wdern


    above cauts
    natker addng wadr in aud. Jf he

    eould have a pakeer


    ov ane dlealt icel we

    TOBul

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