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International Journal of Machine Tools & Manufacture 43 (2003) 121–128

Workpiece surface modification using electrical discharge


machining
J. Simao ∗, H.G. Lee, D.K. Aspinwall, R.C. Dewes, E.M. Aspinwall
School of Engineering, Interdisciplinary Research Centre (IRC) in Materials Processing, University of Birmingham, Edgbaston, Birmingham,
B15 2TT, UK

Received 23 August 2002; received in revised form 10 September 2002; accepted 19 September 2002

Abstract

Electrical discharge machining (EDM) is a widely used process in the mould / die and aerospace industries. Following a brief
summary of the process, the paper reviews published work on the deliberate surface alloying of various workpiece materials using
EDM. Details are given of operations involving powder metallurgy (PM) tool electrodes and the use of powders suspended in the
dielectric fluid, typically aluminium, nickel, titanium, etc. Following this, experimental results are presented on the surface alloying
of AISI H13 hot work tool steel during a die sink operation using partially sintered WC / Co electrodes operating in a hydrocarbon
oil dielectric. An L8 fractional factorial Taguchi experiment was used to identify the effect of key operating factors on output
measures (electrode wear, workpiece surface hardness, etc.). With respect to microhardness, the percentage contribution ratios (PCR)
for peak current, electrode polarity and pulse on time were ~24, 20 and 19%, respectively. Typically, changes in surface metallurgy
were measured up to a depth of ~30 µm (with a higher than normal voltage of ~270 V) and an increase in the surface hardness
of the recast layer from ~620 HK0.025 up to ~1350 HK0.025.
 2002 Elsevier Science Ltd. All rights reserved.

Keywords: EDM; EDT; Texturing; Surface alloying; Powder metallurgy

1. Introduction piece rather than the tool suffers the majority of erosion
(~50–95%), however, some material is inevitably lost by
Since its development in the mid 1940s, EDM has the tool electrode. The last decade has seen significant
become widely used for the manufacture of components development of EDM technology in terms of generator
such as moulds / dies and aeroengine parts. The process design, with the use of fuzzy logic, high frequency
is thermal in nature with material removal occurring via ‘nano-pulse’ operation, EDM ‘milling’ using simple
the discharge of energy between a tool and workpiece electrodes, etc. [2]. There is also growing interest in the
electrode, which are separated by a small gap (~5–100 use of ‘greener’ more eco-friendly water-based dielec-
µm depending on electrical parameters) filled with a trics [3]. Similarly, the range of applications has
dielectric fluid, typically a hydrocarbon oil or deionised expanded to encompass the growing requirement for
water. A DC pulse generator is used to initiate discrete micro-scale features including holes down to 5 µm in
sparks which have a duration in the region of 0.2–100 diameter [4,5].
µs, followed by a similar period during which deionis- A number of EDM process configurations are cur-
ation of the dielectric occurs and the gap is flushed of rently employed in industry, involving die sinking and
debris [1]. Preferred polarity arrangements for different wire cutting, together with more specialised formats such
electrode and workpiece materials ensure that the work- as electrical discharge texturing (EDT) [6] and electrical
discharge grinding (EDG). The latter process is increas-
ingly being used for the manufacture of polycrystalline

Corresponding author. Tel.: +44-121-414-3541; fax: +44-121- diamond (PCD) cutting tools [7,8], however, while there
414-3541. are hybrid machines which utilise both abrasive grinding
E-mail address: j.m.t.simao@bham.ac.uk (J. Simao). and spark erosion, the vast majority of commercial sys-

0890-6955/03/$ - see front matter  2002 Elsevier Science Ltd. All rights reserved.
PII: S 0 8 9 0 - 6 9 5 5 ( 0 2 ) 0 0 1 8 7 - 6
122 J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128

tems employ no abrasives and here the term is a mis- Typically, the properties / characteristics of materials
nomer, stemming primarily from the use of a rotating chosen for tool electrodes when EDM particularly die
wheel electrode and similarity with a tool and cutter sinking, relate primarily to electrical conductivity, melt-
grinder configuration. With such machines, material ing / sublimation temperature and wear resistance. The
removal is entirely due to the spark discharge, either rapid degradation of tool electrodes is in general not a
when using the face or periphery of the graphite / cop- desirable feature. Under such circumstances mould / die
per wheel. accuracy and possibly integrity may be significantly
At present, the available techniques for enhancing the compromised, in the latter case due to debris accumu-
surface mechanical / physical / topographical properties lation in the spark gap and subsequent arcing. There are
of components subject to wear, corrosion / oxidation, also obvious adverse effects in terms of the higher costs
etc. include: carburising, nitriding, chromium plating and associated with electrode supply, workpiece productivity
in some instances, chemical / physical vapour deposition and dielectric filtration. Nevertheless, research has been
(CVD / PVD), ion beam techniques and plasma arc carried out in recent years to determine the possibility
spraying [9]. Such processes can offer significant pro- of using electrodes as feed stock material, in an effort
perty enhancements, however, they are secondary oper- to produce significant workpiece surface alloying and in
ations which either require expensive in-house equip- so doing, enhance the wear (abrasion) and corrosion /
ment or the use of sub-contract companies. They oxidation resistance of the machined surface [17–28].
therefore add to costs and lead times, in some instances, The electrodes employed are generally produced using
significantly so. In addition, components that have been
a PM route, in order to achieve the necessary combi-
manufactured using standard EDM techniques may
nation of operating characteristics. Fig. 1 details deliber-
require prior removal of the white / recast layer before
ate surface alloying using an appropriate PM tool elec-
applying or depositing a hardmetal or ceramic coating
trode and a hydrocarbon dielectric fluid for the texturing
because of adverse residual stress conditions or
and surface alloying of a workpiece, in this instance a
unfavourable mechanical properties. An alternative
approach is deliberate surface alloying / modification cold mill work roll, however, it could also be a mould
during EDM which dispenses with the need for sup- / die cavity or alternatively an aeroengine component
plementary processing / coating following machining, such as a snubber contact area on a low pressure com-
thereby providing lower costs and more flexibility. pressor blade.
A wide range of powders with alternative compo-
sitions can be used for the manufacture of tool elec-
2. EDM surface alloying / modification method trodes. These tend to be materials which can form /
Spark discharge temperatures of up to 20,000 °C have transfer hard particles such as carbides and may incor-
been reported [1]. Consequently, surface alloying is larg- porate a secondary binder phase, e.g. WC/Co,
ely unavoidable albeit at a low level, even when using TiC/WC/Co, W/CrC/Cu, etc. By using electrodes made
standard electrodes with preferred polarity. Deliberate from different materials, the possibility exists to ‘engin-
alloying requires the use of appropriate electrodes, eer’ one or more alloyed layers (which may be func-
and/or the addition of powders suspended in the dielec- tionally graded) with different mechanical properties.
tric fluid which itself plays a key role. The former The compacting and sintering conditions under which
approach is the most widely published. Use of powders the PM electrodes are produced greatly affect their per-
has grown in recent years as a means of increasing pro- formance. Fig. 2 details measurements of density and
ductivity and reducing workpiece surface roughness / electrical resistivity for various green compact, partially
associated microcracks, due to greater electrical conduc- sintered and fully sintered PM electrodes produced from
tivity in the spark gap / reduction in the breakdown volt- WC / 6 wt.% Co binder. While electrodes sintered to
age and higher discharge frequency. Lower electrode full density may offer high conductivity and consistent
wear with water dielectrics containing a powder suspen- sparking, the release of material is generally low and
sion is also possible [10–13]. The powders (typically consequently, surface alloying limited.
⬍ 100 µm) include graphite, silicon, silicon carbide, The aim of the present work was to identify the effect
aluminium, aluminium oxide, nickel, titanium, chro- of relevant EDM operating parameters (voltage, current,
mium and copper. While academic and industrial work pulse on-time, polarity and capacitance) on material
indicates significant benefits, little is detailed on possible removal rate (MRR), electrode wear, workpiece surface
problems associated with the cost / life of powders, fluid roughness and surface microhardness, in order to achieve
concentration / circulation / filtration, agglomeration and enhanced surface alloying.
arcing. Surface alloying work using this technique for
the accretion of titanium carbide layers is detailed by
[14,15], while [16] used nickel powders to double the
surface hardness of an aluminium bronze.
J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128 123

Fig. 1. Schematic diagram of the EDM surface alloying process.

Fig. 2. Variation of electrical resistivity (⍀m) and density (g/cm3)


for a range of WC/Co PM tool electrodes.

3. Experimental work

3.1. Equipment, workpiece and tool electrode


materials
Fig. 3. EDG unit with retrofit servo head assembly.
Die-sink surface alloying tests were performed using a
miniature servo head unit mounted on an EDG machine length of 4 mm). Samples for metallographic examin-
connected to two Spark Tec International generators. ation were electrical discharge wire machined from the
The first of these employed an open circuit voltage of larger block using a Charmilles Technologies Robofil
~125 V, the second ~270 V, see Fig. 3. A hydrocarbon 200. Workpiece subsurface microstructure was analysed
oil dielectric BP 180 was used with a 1 µm filtration using a Leitz Wetzlar optical microscope fitted with a
system. Fluid was supplied to the electrode / workpiece JVC CCD camera, connected to a Mitsubishi DAT
via two flexible hoses at a flow rate of ~2 l/min. Figs. image recorder and laser printers. Microhardness depth
3 and 4 show the machining arrangement with details of profile measurements were made on a Mitutoyo MVK-
the servo head assembly, tool electrode and workpiece G3 hardness tester using a Knoop indenter, a load of 25
material. The workpiece material was AISI H13 hot g and an indentation time of 15 s. Statistical analysis
work tool steel hardened to 600–640 HK(0.025) which was undertaken using Minitab 13.1 software.
was a square sectioned block approximately
120 × 120 × 50 mm. The cylindrical PM tool electrodes 3.2. Experimental parameters and procedures
were made from WC / 6 wt.% Co binder in a partially
sintered state and were turned to a size of 6 mm In order to quantify the effect of EDM generator
diameter × 55 mm long prior to use. operating parameters, an L8 Taguchi type layout /
Workpiece surface roughness parameters (2–D), were experiment was used. Fractional factorials on which this
measured using a Rank Taylor Hobson (RTH) Form is based, involve substantially fewer experiments than
Talysurf-120L (cut-off length of 0.8 mm, evaluation their full factorial counterparts and it was possible in the
124 J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128

Table 2
L8 orthogonal array

Test Factors and interactions

A B AB C AC E (BC) D (ABC)

1 1 1 1 1 1 1 1
2 1 1 1 2 2 2 2
3 1 2 2 1 1 2 2
4 1 2 2 2 2 1 1
5 2 1 2 1 2 1 2
6 2 1 2 2 1 2 1
7 2 2 1 1 2 2 1
8 2 2 1 2 1 1 2

3.3. Results and discussion

Table 3 shows results of the Taguchi experiment,


where values of the various output measures are given
for the eight tests. The main effects plots of the means
for the output measures are given in Figs. 5–8.
Fig. 4. Detail of machining arrangement.
Essentially, within a figure, plots with a steeper slope
and longer line indicate a factor that has a greater impact
present work to assess 5 factors each at two levels with on the output measure. Where lines are similar in slope
two interactions by performing eight tests and a confir- and length the factors would generally have a similar
mation test. The tool electrode cross sectional area was effect on the output measure, ie. no one factor has a
kept small (6 mm diameter) in order to provide a realistic more significant effect than another. The main effects
energy density, despite the low levels of current plot for VTW showed the significant (at the 5% level)
employed and give meaningful electrode wear data. The influence of capacitance (factor E) on the output. The
die sink test arrangement, as opposed to use of a scan- calculated PCR was 苲73%. This gives the percentage
ning mode, was also useful in identifying any problems that each factor contributes to the total variation in the
associated with arcing due to electrode debris accumu- results and is a measure of how much the performance
lation in the spark gap. Table 1 details the variable and could be improved if the factor was controlled exactly.
fixed factor levels, while Table 2 gives the L8 orthogonal The main effects plot for MRR also showed the signifi-
array. A confirmation test was subsequently performed cant influence of capacitance, here the PCR was 苲49%,
with appropriate operating levels set to give a maximum while the electrode polarity (factor D) produced a value
workpiece surface hardness. of 苲18%. The main effects plot for Ra highlighted the

Table 1
Rationalised factors and levels for L8 orthogonal array

Fixed factors Level


Workpiece material & hardness (HK(0.025)) AISI H13 (~600–640)
Tool electrode material WC/Co (partially sintered at 1000 °C)
Tool electrode diameter (mm) ~6
Pulse off-time (µs) 20
Peck interval (s) and lift (mm) 15 and 5
Machining time (min) 60
Dielectric type BP 180 hydrocarbon oil
Variable factors Levels
Low (1) High (2)
A Open circuit voltage (V) ~125 ~270
B Peak current (A) 1 3∗
C Pulse on-time (µs) 20 40
D Electrode polarity + ⫺
E Capacitance (µF) 0 0.1


Only 2.9 A available with the ~270 V generator.
J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128 125

Table 3
Taguchi experiment—results

Volumetric tool wear VTW Workpiece MRR Workpiece surface roughness Workpiece surface microhardness (HK
(mm3) (mm3/min) Ra (µm) 0.025)

1 2.035 0.002 1.765 579


2 32.556 0.051 1.390 903
3 63.133 0.123 1.420 1095
4 2.826 0.009 3.206 789
5 3.109 0.011 2.340 729
6 22.778 0.033 2.950 1029
7 35.099 0.041 3.330 884
8 4.239 0.022 3.004 1351

Fig. 8. Main effects plot means for workpiece surface hardness


Fig. 5. Main effects plot means for volumetric tool wear (VTW). (HK0.025).

significant influence of open circuit voltage (factor A),


electrode polarity (factor D) and peak current (factor B).
The corresponding PCR values were 苲40, 苲26 and
苲17%, respectively. The main effects plot for microhard-
ness shows comparatively little difference in the slopes
of the lines, suggesting that each factor had a similar
influence on the output measure. The PCRs confirmed
this with voltage (factor A), peak current (factor B),
pulse on-time (factor C) and electrode polarity (factor
D) calculated at 苲12, 24, 19 and 20%, respectively. The
effect of capacitance was sufficiently small to be pooled
Fig. 6. Main effects plot means for metal removal rate (MRR).
as part of the error. Based on the analysis of variance
none of the factors were found to be significant at the 5%
level. Use of a Daniel’s Half Normal plot and subsequent
interaction diagrams, suggested that in nearly all cases,
the first order interactions AB and AC were not signifi-
cant and were therefore pooled into the experimental
error. The PCR with respect to error was ⬍ 14% for all
output measures, indicating that no other important fac-
tors had been omitted.
The results for the confirmation test are detailed in
Table 5. Here, the operating parameter levels were selec-
ted in order to maximise workpiece surface microhard-
ness (~270V, 3A, 40 µs, 0.1 µF and negative polarity).
Fig. 7. Main effects plot means for workpiece surface roughness A cross-sectional photomicrograph of the die-sink
(Ra).
machined surface and the corresponding microhardness
depth profile are shown in Figs. 9 and 10, respectively.
The alloyed/modified layer had relatively few
microcracks, an average thickness of ~30 µm and a sur-
126 J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128

Table 5
Confirmation test—results

Output measures
Volumetric tool wear VTW Workpiece MRR (mm3/min) Workpiece surface roughness Workpiece surface
(mm3) Ra (µm) microhardness HK 0.025)

96.48 0.216 1.59 1319

cular responses. Unfortunately, for factors with no more


than two levels, there is no compromise situation, other
than where an interaction may occur.
The surface hardness value of the recast surface
alloyed layer was substantially higher than either that of
the hardened AISI H13 steel (~600–640 HK(0.025)) or
the typical recast layer hardness (~600 HK(0.025)) when
using ‘conventional’ graphite or copper tool electrodes
[29] (this low value of hardness is due to retained austen-
ite, which will transform during initial use, eg. rolling,
Fig. 9. Cross-section of die sink surface machined using a partially
to give a higher hardness—~800 HK(0.025) and greater
sintered WC/Co tool electrode (Taguchi confirmation test).
toughness than with layers composed of martensite [30]).
Research on moulds / dies and also cutting tools
machined by EDM using PM electrodes made from pure
titanium, has shown that the modified / alloyed surface
is three times as wear resistant as one without such a
layer and that is also more wear resistant than a TiN
PVD coated surface [18].
Fig. 11 shows sample glow discharge optical emission
spectroscopy (GDOES) results from EDM surface
alloying work undertaken by the authors, which has a
bearing on the present work. The machining operation
involved EDM scanning / milling of AISI H13 rather
than die sinking and a voltage of ~270 V but with a
Fig. 10. Microhardness depth profile of die sink surface machined
current of 1 A and a partially sintered / dewaxed WC /
using a partially sintered WC/Co tool electrode (Taguchi confir- 6 wt.% Co binder PM electrode. The gradient transfer
mation test). of elements from the electrode, in particular tungsten,
together with pyrolytic carbon from the hydrocarbon
dielectric up to a depth of ~5 µm can clearly be seen.
face hardness of 1319 HK(0.025). This reflected the The thickness of the recast layer in this case was 10–
particular levels of electrical parameters chosen. Pre- 15 µm. While giving elements, the GDOES data do not
vious work has shown the integrity, uniformity and hard- indicate the presence of compounds such as WC. Simi-
ness of the white layer to be highly dependent on elec- larly, whether any compounds were directly transferred
trode material and electrical parameters, the higher the from the electrode or produced via the discharge process
discharge energy, in particular the current component, following elemental transfer. Plateau effects in relation
the greater the level of surface alloying [28]. This can to elements such as carbon, suggest the presence of com-
present problems, however, with respect to the required pounds, eg. WC, rather than atoms in solution, which
workpiece surface roughness, in that low values of Ra give a gradual decay. Research is at present underway
can only be obtained with low levels of discharge to resolve these aspects.
energy. The use of Taguchi type experimental design
techniques enables the relative importance of factors and
their levels to be assessed in order to maximise / mini- 4. Conclusions
mise the desired response. In some cases however, a
compromise solution is required, for example, in the The Taguchi approach employed enabled the identifi-
present research a high workpiece surface hardness with cation of significant factors and their associated levels
an acceptable (low) workpiece surface roughness. Here, on specific output measures. Selection of appropriate
the only option is to assess the relative merits of parti- operating values from these data enabled preferred work-
J. Simao et al. / International Journal of Machine Tools & Manufacture 43 (2003) 121–128 127

Fig. 11. Presence of elements in the electrical discharge machined workpiece.

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