SErsosacnour X-ray fluorescence energy a RESEARCH AND PRODUCTION ENTERPRISE BOUREVESTNIK dispersive general purpose RESEARCH “* DESIGN + PRODUCTION spectrometer BRA-135F Range of chemical elements to be analysed — °F -9U Analysis of liquid, powder and solid samples Quantitative and semiquantitative analysis by the ‘method of fundamental parameters Built-in control PC The special prepared room is not required for the instrument, It is registered in the State Registry of Measuring Equipment of Russia under 1N56937-14 of Kazakhstan under 'NKZ.02.03.06074-2014/56937-14 Received CE declaration of conformity. X-ray fluorescence energy dispersive general purpose spectrometer BRA-135F allows simultaneous determination of up to two dozens of chemical elements for a period not exceeding 300 s over a wide range of concentrations of hundred ppb. BRA-135F analyzes solid, powder and liquid samples, and ones coated on the surface or deposited on filters. Sampl ‘Sample chamber analyeed / Vacuumized chamber Diving window rime raciaton ers Xeray tube Operating principle ‘The spectrometer operating principle is based on excitation of fluorescence radiation of atoms in the substance being analyzed by radiation coming from the low-power X-ray tube. The fluorescence radiation from the sample gets into the SDD semiconductor detector where quanta of any energy are converted into electrical pulses, which amplitudes are proportional to the energy of absorbed quanta, Pulse-repetition rate with the certain amplitude is proportional Detector scheme to the chemical element concentration in the sample.High efficiency SDD detector The silicon drift detector (SDD) with ultrathin entrance window allows registering x-ray radiation in wide energy range on retention of energy resolution and response. Odd-size samples analysis Itis possible measurement of large-size or odd-shaped samples: + Large-size minerals and massive golds; A . Sample feeding disk with solid, liquid and Metals incoming control; evey samples + Analysis of liquids in the special cells or on the special filters. + Industrial articles for analysis for ROHS requirements; Compaction and functionality + Industry-standard strong casing is reliable protection against mechanical damages. + Removal handles for carrying. + ndustrial integrated Windows computer * Possibility for connection to LAN for remote control and archiving of ‘measurement results. + Protection against unauthorized access to data and possibility for separation of access rights. Odd-size sample Technical data Range of determined elements oF 92 Limits of detection without preliminary enrichment, % - for elements from Na to Mg 102 for elements from Alto Cl 2103 - for elements from K to U 5104 Limit of determination at sample preconcentration, depending on chemical element, % 15105 Limit of determination in mid group element liquids, mg/d? 0.1 ‘Average time of one sample analysis, s 100 Energy resolution on MnKa line at pulses counting rate up to 10 st, not more than, eV 145 Utmost voltage of X-ray tube, kW 50 X-ray power, W 10 Xray tube cooling aie Primary X-ray radiation filters Ca, Sr, Ni, Nb, Ti Number of samples installed into sample supply disk, up to, 15 Maximum odd-size sample, mm 20x60 Ethernet connection Yes Possibility for remote control Yes Overall dimensions (LxWsH), mm 700x410x400 Instrument weight, kg 65 Power 220 V, 50 Hz Consumed power, VA 500‘Scope of application Up-to-date software BRA-135F software is the optimal combination of high performance and functionality with an intuitive interface and tooltips. Owing to this, performance of routine measurements requires no special staff, For measurements it is enough to make a few simple steps: select the sample position, enter its code, choose the research method and run the analysis. BRA-135F a @ nae ra = 3 @ vin rr 7 fa Sree oo Pa —— a ee cunnenrnstnunen connmion Era DutaQualitative and quantitative analysis BRA-135F software unveils wide ‘opportunities for on-line receiving of information on the chemical composition of the material to be analyzed. The user chooses the method of substance analysis: qualitative oor quantitative, ‘The registered spectra can be: A, + saved in suably structured archive; \ | \||-ae ae got out for repeat analysis based on a i i} Hh ih ue fy ))| a Be hnew calibration characteristics; extn. He LAA IN sg ‘+ processed as per user's request: added, ~s ~ deducted, KLM-marked: Spectram meosuring and its procesing conditions * scaled +k SS Ae Se NOES For operator convenience in operation, the auxiliary utilities were implemented to minimize errors during the analysis. For example, semi-automatic marker of lines allows correct identification of spectral lines of different elements. Fundamental parameters method The software implementing fundamental parameters method allows. semi-quantitative and quantitative determination of elements within the range from Mg (12) to Pb (82) in solid samples of steels and alloys with composition of 0.1% to 100%, If there are no standard composition samples, to calibrate the spectrometer and with large list of materials under analysis, the standardless semi-quantitative analysis is implemented, which represents the following dependences: + integrated spectrometer sensitivity on Z element; + relative (to the integral sensitivity) intensity of analytical line corrected for background and drift, on sample composition (this dependence was implemented through absorption parameter P), COM ae DTC RC Cae Wee nu Tena a Dees SC Eye eee yma) ieery ea nace) w boure\ MU hcl eee