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Squeeze-Off of Polyethylene Pressure Pipes: Experimental Analysis
Squeeze-Off of Polyethylene Pressure Pipes: Experimental Analysis
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POLYMER
TESTING
Polymer Testing 26 (2007) 132–141
www.elsevier.com/locate/polytest
Product Performance
Abstract
Squeeze-off is used in routine or emergency situations to stop, or nearly stop, flow in polyethylene (PE) pipe by flattening
the pipe between parallel bars. Gas and water industries utilizing PE pipe in their systems have designed squeeze-off
procedures to suit their pipe material, environmental conditions and constructional needs, where it may be inconvenient
and/or expensive to isolate and empty pipelines.
The method provides a quick shut-off the lines, saving many hours, and eliminates the need for dangerous, costly and
lengthy excavations. Despite its widespread use, it is not known whether squeeze-off of the pipe damages the pipe and, if
so, what is the degree of the damage and how it should be minimized.
This paper is about the investigation of squeeze-off of pipes of various dimensions made from PE 80 and PE 100 grade
high-density PE and crosslinked PE. Experimental investigation on the damage related with the squeeze-off of the pipes
was carried out to study the influence of squeeze-off phenomenon on the short and long term performance of the pipes.
Hydrostatic pressure tests were performed on the squeezed pipe to examine the degree of damage. The influence of
squeezing ratio, pipe diameter and squeeze-off tool geometry on the overall pipe performance was also investigated.
r 2006 Elsevier Ltd. All rights reserved.
0142-9418/$ - see front matter r 2006 Elsevier Ltd. All rights reserved.
doi:10.1016/j.polymertesting.2006.09.006
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P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141 133
industry has not defined a level of gas flow when number of failures in older PE pipelines resulting at
shut-off is said to have been achieved, but generally the squeeze-off locations.
a gas flow of less than 0.1 ft3/h (one-tenth cubic foot A successful squeeze-off depends on a combina-
per hour) is considered acceptable [1]. Würst [2] tion of the pipe material being squeezed, the tool
ascertained that, up to a pipe wall thickness of being used and the procedure. The following factors
approximately 10 mm, the pipe materials examined should be considered when developing a field
could be squeezed-off sufficiently, but for thicker procedure for squeeze-off. The geometry of the
pipe walls the squeezed-off point is no longer gas or squeeze-off tool should meet ASTM F 1563 and the
water tight due to the formation of large internal squeeze-off procedures should meet ASTM F 1041
wrinkles which caused lasting damage of the pipe. standard. Further, the operator should qualify his
The more the pipe wall is squeezed, the greater chosen combination of pipe, tool and procedure in
the amount of wall compression. However, this accordance with ASTM F 1734 [5,6,8].
technique is recommended according to DVGW The amount of squeeze bar displacement can be
leaflet GW 332 [3] only up to diameter of 160 mm defined in terms of the amount of pipe wall
with a maximum wall thickness of 10 mm. In order compression. Zero percent wall compression implies
to avoid damage to the PE pipe, the maximum the inner walls of the pipe are not compressed but
squeezing ratio of 80% must not be exceeded. The are just touching each other. One hundred percent
undefined squeezing of the pipe until it is tight is wall compression implies the bars have completely
therefore not permitted. The distance from the compressed, thus no plastic is left between the
squeezed region to the nearest connection or squeeze-off bars. Negative wall compression indi-
another squeezed region must exceed about five cates that the inside walls are not in contact.
times the external pipe diameter [4]. With the squeeze-off, drop-shaped areas of the
Damage mechanism research has shown that wall pipe create as the walls of the pipe are compressed
compression greater than 30% is typically necessary toward each other. A wrinkle in the wall of PE pipe
to induce damage in slow crack growth (SCG) at the squeezed region occurs and the pipe material
resistant materials of recent vintage. For less SCG- flows out from between the squeeze bars. Thus, the
resistant PE pipe materials, damage may occur with wall is locally thinner compared to adjacent areas.
less than 30% wall compression. Furthermore, if an Although most of the standards and application
incorrect squeeze-off tool or procedure is applied instructions require the users of the squeeze-of
the flow in the pipe may continue since insufficient methods to inspect the squeeze-off area for any
compression has been applied. If the pipe is over visible damage, assessing the damage is not an easy
squeezed there is a possibility to induce damage to task.
the pipe. It is, therefore, rather important to Battelle Memorial Institute [1,9–12] has reported
understand the whole squeeze-off phenomenon [1]. that the damage could begin below the surface at
Sometimes it is recommended to re-round the the squeeze-off ears; hence the assessment included
pipe if it does not regain its former shape once the a sub-surface examination, Fig. 1. In some cases,
squeeze-off procedure is completed. Re-rounding sub-surface voids were found to confirm the
provides no practical benefits from the point of view hypothesis. The growth rate of the damage depends
of damage formation or prevention in SCG- on the slow-crack-growth resistance of the materi-
resistant materials, but it may be performed for als.
other reasons such as increasing the flow area to In order to assess the squeeze-off induced damage
maintain a high flow rate. Rerounding may be a combination of squeeze-off experiments, damage
detrimental in cases where immediate damage assessment, and phenomenological modelling was
develops [5,6].
Research indicates that the duration of time the
F
pipe is compressed is of secondary importance to
the likelihood of inducing damage. Stresses decay Squeeze-off Squeeze-off
rapidly after wall compression is completed, and ear cylinders
then change relatively less with the length of time
held in the compressed position. Consequently, no F
limitations are necessary on the length of time the
pipe is compressed [1]. Palermo [7] has reported a Fig. 1. Schematics of squeeze-off test [2].
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134 P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141
performed in this study. In many squeeze-off tests, were used. These PE materials were pressure pipe
the parameters such as pipe material, tool size and graded PE 80, PE 100 and silane crosslinked PE-Xb
geometry, wall thickness and pipe diameter were materials. These materials are being extensively used
repeatedly varied. After the pipe was released, it was in pressure pipe systems, mainly in water and gas
examined for signs of damage in the proximity of transportations. The minimum required strength
the squeeze ears. Hydrostatic pressure and tensile (MRS) for PE 80, and PE 100 pipes on the bases of
tests were performed on the squeezed pipe to assess 50 yr minimum service life is 8 and 10 MPa,
the degree of damage on the pipes. The influence of respectively. Pipes of different diameters and
squeezing ratio, pipe diameter and squeeze-off tool standard dimensional ratio (SDR) were extruded
geometry on the overall pipe performance was also according to the raw material producers’ instruc-
investigated. tions. The pipes were conditioned at least 1 month
before the testing.
2. Experimental analysis
2.2. Squeeze-off tests
In this study, PE pipes of different diameters
made from PE80, PE100 and crosslinked polyethy- The pipe samples were at least six pipe diameters
lene (PE-Xb) materials were examined to under- in length. The wall thickness of the pipe around the
stand the squeeze-off phenomenon in general; and circumference at 451 increments was measured and
to assess their squeeze-off performance in particu- the location of maximum wall thickness was
lar. The effect of the geometry of the squeeze-off identified.
tool on the pipe performance was also investigated. The pipes and the squeeze-off tool were condi-
After the pipe was squeezed-off, hydrostatic and tioned for 24 h before squeeze-off. The test specimen
tensile tests were performed on the pipes to examine was placed in the squeeze-off apparatus with the
for signs of damage in the proximity of the squeeze plane of maximum wall thickness parallel with the
ears. squeeze bars (i.e., the thickest portion of the pipe in
the squeeze-off ear). The specimen was located in
2.1. PE materials such a way that the midpoint of its length was
between the squeeze-off cylinders (Fig. 2).
In this study, based on current practice, pipes The squeeze tests were performed on a computer
made from three different types of PE materials controlled servo hydraulic DARTEC tensile testing
Fig. 2. DARTEC servo-hydraulic tensile testing machine used in the squeeze-off tests and the configuration of the squeeze-off tests.
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P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141 135
machine with a M9500 controlling unit. The Stress whitening occurs when many plastic products
machine was operated at a constant crosshead are subjected to excessive bending or impact. In the
speed of 50 mm/min until the predefined squeezing squeeze-off tests, this stress whitening was more
ratio was attained, and then held at this compres- pronounced at the inner and outer surfaces at the
sion position for a duration of 60 min. Then the squeeze-off ears. These remarkable stress whitening
specimen was released at the designated rate. features have not been correlated with the overall
A typical force–time curve is shown in Fig. 3. As
seen, it has three unique sections. Between points A
and B, the pipe is squeezed-off until the inner 7
30%
surfaces of the pipe wall touch each other,
corresponding to 0% squeezing ratio. The variation
of squeeze force with time is not linear during this
20%
period of the test. After point B, the pipe walls are 6
compressed until the pre-defined squeezing ratio is
attained. The increase in force is rather sharp during
Forc e (kN)
this period of the test. At point C, the pre-defined
squeezing ratio is attained and the displacement is 4
held constant. Between points C and D, the 10%
squeezed pipe was kept at a fixed displacement for
1 h. As seen from the CD section of the curve the
0%
force decreased to almost half of the peak force
2
during this period. This decay in the force is due to
the visco-elastic nature of PE.
In these tests, the squeezing ratios were also
changed to determine its effects on the PE pipe
performance. It was observed that the maximum
squeeze-off force increased linearly with squeezing 0 5 10 15
ratio, as shown in Fig. 4. Displacement (mm)
After squeeze-off, damage in the form of stress Fig. 4. Variation of the squeezing force with compression rate for
whitening at the squeeze-off ears was observed. PE 80 f20 3 HDPE pipe.
120 120
C
100 100
Displacement
Displacement (mm)
80 80
Force
Force (kN)
60 60
D
40 40
B
20 20
A
0 0
0 1 2 3 4 5 40 50 60
Time (min)
Fig. 3. A typical displacement–time curve used in the squeeze-off tests and correspondent squeezing force–time response for PE 80
f110 11 HDPE pipe.
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136 P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141
3rdcycle
Force (kN)
4
nd
2 cycle
3 st
1 cycle Fig. 6. Squeeze tool geometries used in this study. fD1 ¼ 35 mm,
fD2 ¼ 70 mm, fD3 ¼ 120 mm, and for D4 straight bar with
2 50 mm width and 5 mm side radius.
240
%40
220
200 Cylindrical %30
180
160 %0 %20
140
%10
%20
%30
Squeeze-off Force (N)
100
%40
80
%10
60
40
20
%0
0
20 40 60 80 100 120
Squeeze Cylinder Diameter (mm) Flat Squeeze Bar
Fig. 7. Variation of squeeze-off force as a function of squeeze tool diameter for different squeeze-off ratios for 63 4.3 mm PE 100 pipe.
160 Flat 50 mm
140
21.7 MPa, about 4% less than that of normal pipe
(22.6 MPa). As the squeezing ratio increases the
120
yield stress diminishes significantly and for 40%
100
squeezing ratio the yield stress is 20.1 MPa. Thus,
80 compared with the normal pipe, 0% squeezed pipe
60 gives 7% lower yield stress, 40% squeezed pipe gives
40 11% less yield stress. A similar trend is also
20 observed from tensile samples extracted along the
0 circumferential direction. Yield strain results are
0 10 20 30 40 given in Fig. 12.
Squeezing Ratio [%] From these tensile tests results it could be
concluded that the by squeezing PE 80, PE100 and
Fig. 8. Variation of squeeze-off force as a function of squeezing
ratio for different squeeze tool geometry for 63 4.3 mm PE 100 PEX pipes, the yield stresses decreases by around
pipe. 11% for all three PE grades. For the yield strains,
however, there are some variations from one grade
to another: a decrease for PE100 pipe, and increases
for PE 80 and PEX pipes (Figs. 13–17).
All the tensile properties for the squeezed-off
pipes have deteriorated. Particularly, the reduction 2.4. Pressure tests
of both yield stress as well as the yield strain for
40% squeezed circumferential sample is rather It is rather important to determine whether and to
striking (curve 4 in Fig. 11). The importance of this what degree the squeezing induces any reduction in
observation comes from the fact that the circumfer- the hydrostatic performance of PE pipe. To this
ential strength of the pipe determines the overall end, the hydrostatic pressure tests are vital to assess
performance of the pipe structure. the level of the damage.
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138 P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141
Fig. 9. Position of the tensile tests samples extracted from the squeezed-off PE pipes.
25 15
14
12
Fig. 10. Dimensions of the tensile tests samples. 15
Yield Stress 11
Yield Strain
1 10 10
20 0 10 20 30 40
2 Squeeze-off Rate (%)
Stress [N/mm2]
25 15
5
14
Yield Stress (MPa)
10 10
0 10 20 30 40
Squeeze-off Rate (%)
Squeezed PE 80, PE 100 and PEX pipes were
Fig. 13. Variation in yield stress and yield strain in PE 100,
hydrostatically tested according to the ISO 9080 f32 3 pipe, samples were extracted in circumferential direc-
standard. For the pressure tests, IPT 1443 (Ger- tions. (The normal pipe has a yield stress of 21.9 MPa, and yield
many) hydrostatic pressure testing equipment was strain of 14.5%).
used. Squeezing ratios at 0%, 10%, 20%, 30% and
40% were applied to a number of PE 80, PE 100
and PE-Xb pipes having different diameters and for PE 80 and 5.5 MPa for PE 100 at 80 1C
thicknesses. Then, the squeezed PE 80 and PE100 according to the EN 12201-2. PE-Xb pipes were
pipes were hydrostatically tested with internal tested at 95 1C according to EN 12318 standard for
pressure equivalent to a hoop stress of 4.6 MPa a duration of 165 h.
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P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141 139
25 20 20 24
22
18 19
Yield Stress (MPa)
14 17 16
15
14
Yield Stress 12 16
Yield Strain Yield Stress 12
Yield Strain
10 10 15 10
0 10 20 30 40 0 10 20 30 40
Squeeze-off Rate (%) Squeeze-off Rate (%)
Fig. 14. Variation in yield stress and yield strain in PE 80, Fig. 17. Variation in yield stress and strain in PEX f63 5.65
f32 2.8 pipe. The samples were extracted in axial directions pipe. The samples were extracted in circumferential directions.
(The normal pipe has a yield stress of 21.0 MPa, and yield strain (The normal pipe has a yield stress of 19.3 MPa and yield strain
of 12.7%). of 11.7%).
20
Yield Strain (%)
Fig. 18. f63 pipe made from PE 100 material, squeezed with fs ¼ 70 mm tool. The failure took place at 0% squeezing ratio region. Failed
at 7 h 38 min at the squeeze ear (ductile failure).
Fig. 19. f63 6.4 pipe made from PE 80 material, squeezed with fs ¼ 70 mm tool. The failure took place at 40% squeezing ratio region.
Passed 165 h successfully, withstand 40% extra pressure for about 4 min at the squeeze ear (ductile failure).
Fig. 20. f32 3.1 pipe made from PE 100 material, squeezed with fs ¼ 70 mm tool. The failure took place at 40% squeezing ratio region.
Failed at 55 h at the squeeze ear (ductile failure).
Fig. 21. f32 3.0 pipe made from PE 80 material, squeezed with fs ¼ 70 mm tool. The failure took place at 40% squeezed region. Passed
165 h successfully, withstand 40% extra pressure for about 20 min at the squeeze ear (ductile failure).
Fig. 22. f32 pipe made from PE 80 material, squeezed with fs ¼ 70 mm tool. The failure took place at 30% squeezed region. Passed 165 h
successfully, withstand 40% extra pressure for about 28 min.
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P. Yayla, Y. Bilgin / Polymer Testing 26 (2007) 132–141 141
Fig. 23. f63 pipe made from PE 100 material, squeezed with fs ¼ 70 mm tool. The failure took place at 40% squeezed region. Failed at
26 h at the squeeze ear (ductile failure).
on the hydrostatic pressure performance. The their positive interest, and especially to Arili Pipelife
ductile failure mode implies that the PE pipes’ Plastik Sanayi A.S. of Turkey. Dr. PS Leevers of
squeeze-off performance is not determined by Imperial College of Science, Technology and
the environmental stress-cracking resistance Medicine (UK) and Prof. E Cavusoglu of Arili
(ESCR) of the PE material. The pipes at the Pipelife Plastik Sanayi A.S. (Turkey) are also
squeeze-off ears undergo a visible thinning process appreciated for their valuable discussion and com-
and, as the squeezed pipe is pressurized, it expands ments on the manuscript.
at these regions and a nucleation zone at the most
thinned region triggers the ductile failure.
(3) Although the tensile properties of PE 80, PE 100 References
and PE-Xb pipes deteriorate with increasing
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(4) Squeezing ratios, varied between 0% and 40%, made of PE80, PE100 and PE-Xa, in: Plastic Pipes XI
had no detectable effects on the hydrostatic Conference, Munich, Germany, 2001.
pressure performance. In some squeezed pipes, [3] DVGW GW 332, Abquetschen von Rohrleitungen aus
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Data Sheet, 2000.
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However, the tensile tests on squeezed pipes PE pipe systems, in: Plastics Pipes XII Conference, Milan,
indicated that the tensile properties deteriorate Italy, 2004.
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tests the yield stress diminished with squeezing
Term Damage in Polyethylene Gas Pipe.
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varies from one grade to another. Thus, it is Polyethylene (PE) Gas Pipe or Tubing.
recommended that the squeeze-off tools should [7] G. Polermo, Correlating aldyl ‘‘A’’ and century PE pipe rate
have a stop mechanism to prevent excessive process method projections with actual field performance,
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[8] ASTM F 1041, Standard Guide for Squeeze-off of Polyolefin
(5) In order to eliminate any risk resulting from the Gas Pressure Pipe and Tubing.
squeeze-off, it is advised that the pipe should be [9] D.R. Stephens, B.N. Leis, Guidelines and Technical
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encirclement or support clamp. This will sup- Using Squeeze Tools, GRI-94/0205, 1994.
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Users’ Guide on Squeeze-off of Polyethylene Gas Pipes, vol.
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Pipes, vol. 2, GRI-92/0147.2, 1992.
[12] D.R. Stephens, M.J. Cassady, B.N. Leis, Progress Report on
Acknowledgements
Preliminary Screening Tests on Squeeze–Off of Polyethylene
Gas Pipes, GRI-91/0403, 1991.
The authors are greatly indebted to colleagues at [13] A.P. Boresi, O.M. Sidebottom, Advanced Mechanics of
both industrial as well as university laboratories for Materials, fourth ed., Wiley, New York, 1985.