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Article history: The effects of strain rate on the mechanical properties and failure mechanism of AA5754 and AA5182 sheets
Received 21 August 2007 were investigated. Tensile tests were conducted at quasi-static (less than 10−1 s−1 ) and dynamic (600, 1100
Received in revised form 18 March 2008 and 1500 s−1 ) strain rates at room and elevated temperature using an INSTRON machine and Tensile Split
Accepted 19 March 2008
Hopkinson Bar (TSHB) apparatus, respectively. Shear band decoration, interrupted tensile tests, electron
microscopy, and image analysis techniques were also utilized. The results obtained show that the studied
Keywords:
alloys exhibit negative strain rate sensitivity at quasi-static rates, but mild positive sensitivity at dynamic
Strain rate
rates. Different failure mechanisms were also observed. Strain localization and shear band formation was
Aluminum alloys
Failure mechanism
found to be a necessary pre-requisite for the development of damage and final failure under quasi-static
Shear band conditions. In the dynamic strain rate regime however, less shear banding was observed. Void nucleation,
Hopkinson bar growth and coalescence that is characteristic of dynamic tensile fracture appears to be the dominant mode
for failure under dynamic conditions.
© 2008 Elsevier B.V. All rights reserved.
1. Introduction in flow stress was reported for all strain rates (10−4 to 1 s−1 ) at 400
or 500 ◦ C. In several 5xxx aluminum alloys, Daoming and Ghosh
In the last decade, because of their enhanced formability and [9] found that the elongation to failure increased with increasing
high specific strength, aluminum alloys have been increasingly temperature but decreased with increasing strain rates.
utilized as structural components in automobiles and high-speed Ductile failure occurs as a result of nucleation, growth and coa-
ships. During service, these components can be subjected to lescence of micro-voids [10,11]. However, an important step in the
dynamic loading, such as during impact or collision with foreign failure process is strain localization. During failure, strain localiza-
objects. Therefore, the material properties and failure behavior of tion may be a consequence of the fracture process that occurs just
these alloys at low and high rates of deformation need to be well prior to, or long before, final fracture [12]. Strain rate hardening or
understood. softening during deformation may contribute to strain localization
Alloy composition, strain rate, service temperature and and the failure mechanisms involved. While strain rate hardening
microstructure may have an effect on mechanical properties and can improve ductility [13], strain rate softening may lead to plastic
failure mechanism of aluminum alloys [1–6]. Naka and Yoshida strain localization and reduce ductility [13,14]. Discontinuous yield-
[7] measured the strain rate sensitivity of a 5xxx aluminum alloy ing [15] and negative strain rate sensitivity in 5xxx series aluminum
at a 20–250 ◦ C, at strain rates of 5 × 10−5 to 50 s−1 . A negative alloys [16] may also result in a reduction of the strain required
strain rate sensitivity was observed at room temperature while a for void growth [17,18]. In general, the constitutive responses and
positive strain rate sensitivity was observed at temperatures over deformation behavior of aluminum alloys are not yet well under-
200 ◦ C. Wagenhofer et al. [3] reported a negative and positive strain stood. Thus, it is the objective of this work to investigate the effects
rate sensitivity for AA5083 when deformed below and above 1 s−1 , of strain rate on the mechanical properties and failure mechanism
respectively. Similarly, Clausen et al. [8] found that AA5083 exhibits of automotive AA5754 and AA5182 sheets.
serrated stress–strain curves and negative strain rate sensitivity
when deformed at 10−4 to 1 s−1 . When the strain rate exceeds 1 s−1 , 2. Experimental procedure
a large increase in fracture strain was measured. A severe reduction
2.1. Materials
∗ Corresponding author. Fax: +0098 7116287294. The materials studied are 1.6-mm thick AA5754 and AA5182
E-mail address: hadianfa@shirazu.ac.ir (M.J. Hadianfard). sheets in the “O” condition, provided by Novelis Global Tech-
0921-5093/$ – see front matter © 2008 Elsevier B.V. All rights reserved.
doi:10.1016/j.msea.2008.03.037
284 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292
Table 1
Nominal composition of the AA5182 and AA5754 (weight percent)
Mg Mn Si Fe Ti Zn Cu Cr
Table 2
Result of the detail measurement on polished and etched surfaces of the specimens
ond of Al, Fe (about 10%), Mg and Mn; and the third of aluminum
oxide. The population of the two first groups is much higher than
the third. Four distinct groups of particles were found in AA5754.
The first group, which makes up about 55% of population, consisted
of aluminum oxide; the second of Al, Fe (2–3%) and Mn; the third of
Al, Fe (about 10%), Mn and Mg; and the fourth of Al, Mg and Si. The
population of the two last groups is much lower than the first two.
Porosity measurements conducted found that the porosity of
the as-received AA5182 and AA5754 sheets are 0.085% and 0.017%,
respectively. The microstructure of AA5754 appears to be cleaner
than AA5182 with less and smaller second phase particles.
Fig. 3a and b shows the shear bands revealed by the decora-
tion treatment in a quasi-static and a dynamic strain rate specimen,
respectively. Fig. 3c shows typical thickness of a shear band area on
a quasi-static strain rate specimen.
Fig. 7. Change in the elongation to failure of AA5182 and AA5754 with strain rate at
dynamic rates.
Fig. 4. Engineering stress–strain curves obtained from quasi-static tensile tests of
AA5182 specimens.
Fig. 8. Effect of temperature on the flow stress of AA5182 and AA5754 at 15% strain
at strain rate of 1500 s−1 .
Fig. 5. Effect of strain rate on ultimate tensile strength of AA5182 and AA5754 at
quasi-static rates. intense shear bands on the surface of all specimens. A large number
of damage including voids, microcracks and damaged second phase
3.3. Failure analysis particles were observed in these shear bands (Fig. 10). Although
some damaged particles were also observed out of these bands,
3.3.1. Quasi-static regime most of the damaged particles were found on, or near, these bands.
Examination of the surfaces of the specimens after quasi-static These shear bands with a high density of damaged particles are
tensile testing, heat treatment and etching showed several large
Fig. 6. Change in the yield strength of AA5754 and AA5754 with strain rate at quasi- Fig. 9. Change in elongation to failure of AA5182 and AA5754 with temperature at
static rates. 1500 s−1 .
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 287
Fig. 10. Shear bands and damaged area on the surface of a AA5182 specimen failed Fig. 12. A part of the crack path in a AA5182 specimen which was fractured at
at 1.3 × 10−3 s−1 . 1.3 × 10−2 s−1 .
present in close proximity to the main crack or fracture path. in AA5754. Shear band thicknesses are also dependent on strain
Damage was observed to initiate at the second phase particles rate. Fig. 15a shows that the thickness of shear bands increases
by means of particle cracking and/or particle-matrix decohesion. with increasing strain rate for both alloys in the quasi-static
Fig. 11 shows typical optical micrographs of AA5754 specimens regime.
after shear band decoration that was tested 1.3 × 10−3 s−1 . These Statistical analysis of the size of the damaged particles was per-
images indicate that shear band formation or localization occurs formed. The average size of damaged particles as a function of strain
prior to fracture. Detailed analysis of the crack path by optical and rate is presented in Fig. 15b. A comparison of these results with
electron microscopy show that most of the crack trail in the quasi- particles measured from specimens in the as-received condition
static specimens lies either along or parallel the shear bands. This (average of 4.4 and 2.3 m for AA5182 and AA5754, respectively)
phenomena is illustrated in Fig. 12, and is observed in both ASTM indicates that the larger particles are more prone to damage than
and dog-bone type specimens. the smaller particles. Furthermore, the average size of damaged
Analysis of the interrupted AA5182 specimens showed that at particles was found to increase with increasing strain rate. Fig. 15b
small plastic strains, damage was only visible at larger second phase shows that while the average damaged particle size for AA5182
particles located at grain boundaries (Fig. 13). However, at interme- specimens that failed at 1.3 × 10−4 s−1 is 5.3 m, it is 7.36 m for
diate plastic strain levels some are present at second phase particles those that failed at 1.3 × 10−1 s−1 .
inside the grains (Fig. 14). At high plastic strain levels and shear The fracture surfaces of all specimens contain dimples, a
localization, intense damage located inside the shear bands are typical feature of ductile fracture. Some differences between
present (Fig. 11). A similar observation is made with AA5754. How- the fracture surfaces of high and low strain rate specimens
ever, AA5754 tends to show slightly less grain boundary effects. were observed. The fracture morphology of specimens that
Some large damaged particles are observed away from the grain failed at lower strain rates (Fig. 16a) is characterized by well-
boundaries at low and intermediate plastic strain levels, but the vast formed voids centered mostly around the damaged second
majority of them are located at the grain boundaries. Under iden- phase particles, with thin matrix ligaments between the pri-
tical test conditions, the area of localized plastic deformation and
thickness of the shear bands were found to be higher in AA5182 than
Fig. 11. An intense deformation area and shear bands in the AA5754 specimens Fig. 13. Damaged large second phase particles on the grain boundaries of an inter-
failed at 1.3 × 10−3 s−1 . rupted AA5182 specimen at low levels of plastic strain.
288 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292
Fig. 14. Damaged large second phase particles inside the grain of an interrupted
AA5182 specimen at intermediate strain levels after shear band decoration treat-
ment.
Fig. 16. (a) Fracture surface of a AA5182 specimen failed at 1.3 × 10−4 s−1 and (b)
fractured surface of a AA5182 specimen failed at 1.3 × 10−1 s−1 .
Fig. 15. (a) The average thickness of shear bands as a function of strain rate for
specimens failed in the quasi-static regime. (b) Average size of damaged particles as Fig. 17. Measured dimple size vs. strain rate of AA5182 and AA5754 specimens failed
a function of strain rate for specimens failed in the quasi-static regime. in the quasi-static regime.
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 289
Fig. 20. Shear band thickness as a function of strain rate at dynamic rates.
areas were found outside of these bands. An area with a high den-
sity of damage was observed a short distance from the main fracture
path in all specimens, most of which are associated with second
phase particles.
Micrographs of a AA5182 specimen tested at 1100 s−1 follow-
ing shear band decoration is shown in Fig. 18. Examinations of the
specimen show that at larger distances (more than 0.3 mm) from
the crack path, damage was only present on the larger second phase
particles. However, damage is observed at smaller particles near the
crack path. A similar behavior was observed from AA5754 material.
Fig. 19 shows the change in damage particle size with strain rate. It
is observed that under dynamic conditions, the average damaged
particle size decreases with increasing strain rate for both alloys.
The presence and thickness of shear bands were found to be Fig. 21. Measured dimple size vs. strain rate of AA5182 and AA5754 specimens failed
influenced by strain rate and alloy composition. Less shear localiza- in the dynamic regime.
tion was observed in AA5754 compared to AA5182. Fig. 20 shows
that shear band thickness tend to decrease with increasing strain 3.5. Elevated temperature tests
rate for both alloys. The crack profiles of failed TSHB specimens
show less evidence of crack path dependence with strain rate than Although the general characteristics of TSHB specimens tested
those failed under quasi-static rates. at 150 and 300 ◦ C are similar to those tested at room temperature,
The fracture surfaces of all specimens that failed at room tem- some evidence of shear band localization was found on the surface
perature exhibit ductile fracture morphology. The primary dimples of these specimens. A significant difference was observed for spec-
around the damaged particles are deep with some small secondary imens failed at 300 ◦ C. Specimens from both alloys show evidence
dimples surrounding them. The change in average primary dimple of particle fracture at grain boundaries. Fig. 22 shows a crack profile
size with strain rate is shown in Fig. 21. These results show that the
primary dimple size tend to decrease with increasing strain rates.
Fig. 19. Average size of damaged particles of specimens failed at dynamic rates. Fig. 22. Crack profile in the AA5182 specimen tested at 300 ◦ C.
290 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292
this alloy at strain rates below 1 s−1 . Negative strain rate sensitiv-
ity in Al–Mg alloys has also been reported by other investigators
[1,15,24–26]. DSA is described by the interaction of fast diffusing
solute atoms such as magnesium with moving dislocations [3,22].
Since DSA is diffusion controlled, it is a function of temperature
and strain rate. At very low strain rates, solute atoms interact
with obstacles preventing dislocation movements, resulting in
higher flow stresses. As the strain rate increases, the dampening
effect of the solutes on dislocation movement decreases and lower
flow stresses are obtained. When sufficiently high strain rates are
reached, DSA disappears as the deformation time is too short for
diffusion to occur [1,3,22,24].
Interrupted test specimens show that little damage is present
prior to the onset of flow instability. Shear banding and damage
are observed in all failed quasi-static specimens, with the majority
of the voids located within the shear bands regions. The thickness
of the shear bands present was found to increase with increasing
strain rates. Reviews by Wright [28] and Bassim and co-workers
Fig. 23. Crack profile characterization of a AA5754 specimen tested at 300 ◦ C. [29] show that shear bands can act as a preferential crack nucle-
ation sites and fragmentation in Al alloys, Ti alloys and steels at
higher strain rates. The larger densities of damage observed on and
near the shear bands of the failed specimens suggest that plastic
localization and shear banding enhance the local damage process
prior to failure in the quasi-static regime.
Softening due to the PLC effect is a source of plastic flow insta-
bility or localization in Al–Mg alloys [17,27]. Localization occurs
due to the interaction between different factors such as material
hardening or softening, geometry and loading conditions [12,27].
It commences when the softer regions in a material deform more
rapidly than other regions and represents a drastic change in mate-
rial deformation from a relatively uniform to a non-uniform one
involving high strain gradients. The larger strains present in the
shear bands lead to degradation of the material’s strength and stiff-
ness [30]; nucleation, growth, and coalescence of microcracks or
voids [31,32]; and a reduction in the load-bearing area. The nega-
tive strain rate sensitivity of a material not only provides the right
conditions for localization, but can also reduce the magnitude of
the strain required for void growth within a shear band [17]. The
Fig. 24. Fractured surface of a AA5182 specimen failed at 300 ◦ C at a strain rate of
decrease in elongation to failure observed with increasing strain
1500 s−1 . rate can hence be attributed to the lower strains required for void
growth within the shear band regions.
Void nucleation usually occurs at inclusions and/or second
of a AA5182 specimen which failed at 300 ◦ C. The crack profile char-
phase particles in a metallic matrix. Different criteria are available
acterization for a AA5754 specimen is presented in Fig. 23. Fig. 24
to describe void nucleation; some based on critical stress while
shows the fracture surface of a AA5182 specimen failed at 1500 s−1
others on critical strain [11,33,34]. The strain-controlled nucleation
at 300 ◦ C. In contrast to the specimens tested at room tempera-
criterion is often used to describe the formation of damage from
ture, regions containing small shallow dimples and, large flat areas
particles [11,33–36]. The strain for void nucleation has been esti-
(evidence of local melting) on the fractured surfaces were observed.
mated through different models [37]. In the presence of plastic
strain, larger particles are more prone to damage and are favor-
4. Discussion able sites for void nucleation as less strain is required [35]. Thus,
the average size of damaged particles can be used to estimate
From the tensile test results and microstructural observations the amount of plastic strain required to produce localization and
obtained over a range of strain rates, the mechanical response and damage in a specimen. Quantitative measurements of the size of
failure mechanism of the aluminum alloys studied are found to be damaged particles found that the average damaged particle size
influenced by the strain rate at which they are deformed. tend to increase with increasing strain rate (Fig. 15b). This suggests
that the critical strain required for strain localization decreases with
4.1. Quasi-static regime increasing strain rate in the QS regime. This is also in agreement
with the decrease in elongation to failure with increasing strain
A slight negative strain rate effect was observed at quasi- rate observed.
static rates at room temperature. Serrations or Portevien-Le
Chateler (PLC) instability is also present. These observations may 4.2. Dynamic regime
be attributed to the dynamic strain ageing (DSA) phenomena
[1,3,22,23], which are in agreement with the findings of other In contrast to the tensile test results obtained in quasi-static
researchers. During testing of AA5083, Clausen et al. [8] found ser- regime, a mild positive strain rate sensitivity was observed in the
rated stress–strain curves and negative strain rate sensitivity for alloys studied with increasing strain rates in the dynamic regime.
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 291
Small shear bands were observed in only some of the tested speci- perature of AA5383 alloy as 563 ◦ C. This liquid phase produces an
mens and damage was mostly present in regions outside the shear inhomogeneity, which makes deformation unstable and produces
bands. As the strain rate increases, the thickness of the shear bands strain localization [42]. These localization areas act as nucleation
(when present) was found to decrease. These observations sug- sites for cracks. The local liquid phase limits the maximum tolera-
gest that, unlike the quasi-static regime, shear localization plays ble plastic strain during deformation, and decreases the elongation
a lesser role in the damage processes and final failure of the mate- to failure and flow stress of the tested materials.
rials studied at dynamic rates. In this regime, shear localization
appears to be a consequence of the void nucleation, growth and
4.4. Concluding remarks
coalescence at second phase particles that are primarily generated
by homogeneous plastic deformation.
The AA5182 and AA5754 alloys studied were found to exhibit
The two main failure modes observed in aluminum alloys when
a negative strain rate sensitivity when tested in the quasi-static
deformed under dynamic rates are dimple fracture (dynamic ten-
strain rate regime, but mild positive strain rate sensitivity in the
sile fracture) and shear fracture (adiabatic shear banding) [32,38].
dynamic strain rate regime. Under quasi-static conditions, increas-
Dynamic tensile fracture involves void nucleation, growth and coa-
ing strain rates resulted in increased material softening and more
lescence processes. The growth and coalescence of the nucleated
pronounced shear band formation. Strain localization appears to
micro-voids and the formation of shear bands occurs with increas-
be a necessary pre-requisite for damage and final failure to occur.
ing plastic strain [32]. Dynamic shear localization or adiabatic shear
Under dynamic conditions, however; significantly less shear local-
banding (ABS) on the other hand is governed by the competition
ization is observed. The void nucleation, growth and coalescence
between strain hardening and thermal softening of the material.
process at the second phase particles is the dominant failure
Damage is often present in ABS bands due to the higher strains
mechanism which develops prior to localization. Analysis of TSHB
present within them. It is the growth and coalescence of these voids
specimens failed at elevated temperatures show the presence of
or ABS themselves that ultimately results in final failure at high
local melting zones at grain boundaries, which may contribute to
strain rates [28,32,38].
the lower ductility and flow stresses measured.
In this study, shear bands were not observed in all TSHB spec-
imens, and where present, they were small in size. Furthermore,
the majority of damage present was found in regions outside the Acknowledgements
shear bands. This suggests that the dynamic tensile fracture mode
is the dominant failure mechanism for AA5182 and AA5754 when Authors thank the Novelist Global Technologies, Canada, for pro-
deformed under the range of dynamic strain rates investigated. viding the Al alloys. M.J. Hadianfard would like to thank Shiraz
The deformation mechanisms of a material can vary with the University, Shiraz, Iran for the financial support of sabbatical leave
rate of strain [39]. The different failure mechanisms and mechanical of the author.
behaviors of AA5754 and AA5182 at quasi-static and dynamic strain
rates can be accredited to the different dislocation mechanisms
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