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Materials Science and Engineering A 492 (2008) 283–292

Contents lists available at ScienceDirect

Materials Science and Engineering A


journal homepage: www.elsevier.com/locate/msea

Effects of strain rate on mechanical properties and failure mechanism


of structural Al–Mg alloys
M.J. Hadianfard a,∗ , R. Smerd b , S. Winkler b , M. Worswick b
a
Department of Materials Science and Engineering, School of Engineering, Shiraz University, Shiraz, Iran
b
Department of Mechanical Engineering, University of Waterloo, 200 University Avenue W., Waterloo, Ontario N2L 3G1, Canada

a r t i c l e i n f o a b s t r a c t

Article history: The effects of strain rate on the mechanical properties and failure mechanism of AA5754 and AA5182 sheets
Received 21 August 2007 were investigated. Tensile tests were conducted at quasi-static (less than 10−1 s−1 ) and dynamic (600, 1100
Received in revised form 18 March 2008 and 1500 s−1 ) strain rates at room and elevated temperature using an INSTRON machine and Tensile Split
Accepted 19 March 2008
Hopkinson Bar (TSHB) apparatus, respectively. Shear band decoration, interrupted tensile tests, electron
microscopy, and image analysis techniques were also utilized. The results obtained show that the studied
Keywords:
alloys exhibit negative strain rate sensitivity at quasi-static rates, but mild positive sensitivity at dynamic
Strain rate
rates. Different failure mechanisms were also observed. Strain localization and shear band formation was
Aluminum alloys
Failure mechanism
found to be a necessary pre-requisite for the development of damage and final failure under quasi-static
Shear band conditions. In the dynamic strain rate regime however, less shear banding was observed. Void nucleation,
Hopkinson bar growth and coalescence that is characteristic of dynamic tensile fracture appears to be the dominant mode
for failure under dynamic conditions.
© 2008 Elsevier B.V. All rights reserved.

1. Introduction in flow stress was reported for all strain rates (10−4 to 1 s−1 ) at 400
or 500 ◦ C. In several 5xxx aluminum alloys, Daoming and Ghosh
In the last decade, because of their enhanced formability and [9] found that the elongation to failure increased with increasing
high specific strength, aluminum alloys have been increasingly temperature but decreased with increasing strain rates.
utilized as structural components in automobiles and high-speed Ductile failure occurs as a result of nucleation, growth and coa-
ships. During service, these components can be subjected to lescence of micro-voids [10,11]. However, an important step in the
dynamic loading, such as during impact or collision with foreign failure process is strain localization. During failure, strain localiza-
objects. Therefore, the material properties and failure behavior of tion may be a consequence of the fracture process that occurs just
these alloys at low and high rates of deformation need to be well prior to, or long before, final fracture [12]. Strain rate hardening or
understood. softening during deformation may contribute to strain localization
Alloy composition, strain rate, service temperature and and the failure mechanisms involved. While strain rate hardening
microstructure may have an effect on mechanical properties and can improve ductility [13], strain rate softening may lead to plastic
failure mechanism of aluminum alloys [1–6]. Naka and Yoshida strain localization and reduce ductility [13,14]. Discontinuous yield-
[7] measured the strain rate sensitivity of a 5xxx aluminum alloy ing [15] and negative strain rate sensitivity in 5xxx series aluminum
at a 20–250 ◦ C, at strain rates of 5 × 10−5 to 50 s−1 . A negative alloys [16] may also result in a reduction of the strain required
strain rate sensitivity was observed at room temperature while a for void growth [17,18]. In general, the constitutive responses and
positive strain rate sensitivity was observed at temperatures over deformation behavior of aluminum alloys are not yet well under-
200 ◦ C. Wagenhofer et al. [3] reported a negative and positive strain stood. Thus, it is the objective of this work to investigate the effects
rate sensitivity for AA5083 when deformed below and above 1 s−1 , of strain rate on the mechanical properties and failure mechanism
respectively. Similarly, Clausen et al. [8] found that AA5083 exhibits of automotive AA5754 and AA5182 sheets.
serrated stress–strain curves and negative strain rate sensitivity
when deformed at 10−4 to 1 s−1 . When the strain rate exceeds 1 s−1 , 2. Experimental procedure
a large increase in fracture strain was measured. A severe reduction
2.1. Materials

∗ Corresponding author. Fax: +0098 7116287294. The materials studied are 1.6-mm thick AA5754 and AA5182
E-mail address: hadianfa@shirazu.ac.ir (M.J. Hadianfard). sheets in the “O” condition, provided by Novelis Global Tech-

0921-5093/$ – see front matter © 2008 Elsevier B.V. All rights reserved.
doi:10.1016/j.msea.2008.03.037
284 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292

Table 1
Nominal composition of the AA5182 and AA5754 (weight percent)

Mg Mn Si Fe Ti Zn Cu Cr

AA5182 4.5 0.35 0.08 0.27 0.1 0.05 0.05 0.03


AA5754 3.2 0.2 0.06 0.3 0.01 – – –

nology Center. Table 1 shows the typical composition of these


alloys.

2.2. Quasi-static (qs) tensile tests

Dog-bone type tensile specimens with a gage length and width


of 12.5 and 1.75 mm, respectively; were utilized. Tensile tests were
conducted using an INSTRON machine at strain rates of 1.3 × 10−4 ,
1.3 × 10−3 , 1.3 × 10−2 , 6.6 × 10−2 and 1.3 × 10−1 s−1 at room tem-
perature with the applied load parallel to the rolling direction. A
minimum of three tensile tests was conducted for each test con-
dition. Tensile tests at 1.3 × 10−3 s−1 using standard-sized tensile Fig. 1. Microstructure of AA5182.
specimens (ASTM E8M-04) [19] were used as reference.
localized plastic deformation and energy pile up is needed for pre-
2.3. Interrupted tensile tests cipitation. However, because magnesium is a key element in the
formation of Al–Mg precipitates, this method works better for the
Tensile specimens that were interrupted before final failure higher Mg containing alloy AA5182 (4.5% Mg) than for AA5754 (3%
occurred were used to study the damage evolution, crack path Mg).
and their interaction with second phase particles. The gage area Following heat treatment, the samples were etched in a solu-
of these specimens were polished and examined by light and scan- tion of 10% phosphoric acid at 50 ◦ C for duration of 1–2 min. The
ning electron microscopy with the aid of a computer-controlled actual etching time is dependent on the level of magnesium and
image analysis (Image Pro Plus) system. the magnitude of localized plastic strain present. The higher the Mg
or strain levels, the shorter the etching time. This etching solution
2.4. High strain rate tensile tests reacts with the Al–Mg precipitates and creates contrast between
shear bands that contain higher amounts of precipitation and other
A TSHB apparatus with an incident and transmitted bar of areas that are precipitate deficient. Following this shear band dec-
15.87 mm in diameter and 1.44 m in length was utilized for the oration and etching process the specimens were analyzed using
dynamic tensile tests. Tests were carried out using the dog-bone microscopy techniques.
specimens at strain rates of 600, 1100 and 1500 s−1 ; at 23 (room
temperature), 150 and 300 ◦ C. A detailed description of this appa- 3. Results
ratus and technique is presented in [20].
Figs. 1 and 2 show the typical microstructure of AA5182 and
2.5. Microstructural and damage characterization AA5754, respectively. The results of grain size and second phase
particles measurements are presented in Table 2.
Microstructural and damage characterization were carried out Chemical analysis of the second phase particles indicates that
using metallographic and microscopy techniques. Fractography and there are several different particle groups. In AA5182, three groups
quantitative chemical analysis of the second phase particles present were identified. The first group consisted of Al, Mg and Si; the sec-
was conducted using a Jeol JSM 6460 scanning electron microscope
(SEM) equipped with an Oxford Instrument energy dispersive spec-
troscopy (EDS) system. At least 30 different particles were analyzed
for each alloy. The failure mechanisms involved and damage evolu-
tion of the failed and interrupted specimens were analyzed using
SEM and an Olympus BX61 optical microscope equipped with an
Image-Pro Plus 5.0 image analysis software.

2.6. Shear band decoration

A shear band decoration method [21] was used to study bands


of intense shear on the surface of the specimens following tensile
testing. The samples were aged for duration of 10–20 days at 100 ◦ C.
The longer ageing period was used for AA5754. This heat treatment
builds up precipitation of Al–Mg phase on high-energy areas such
as highly deformed bands and grain boundaries. Development of
incoherent precipitates is essential for obtaining enough contrast
between different areas on the surface of the specimens. A sufficient
energy pile up at highly strained areas is source for distinguishing
them from their neighbouring areas. Thus, a minimum amount of Fig. 2. Microstructure of AA5754.
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 285

Table 2
Result of the detail measurement on polished and etched surfaces of the specimens

Material AA5182 AA5754

Grain size (␮m) 22.4 ± 7.63 25.3 ± 8.86


Grain aspect ratio 1.35 1.77
Volume of second phase particles (%) 1.1 ± 0.07 0.73 ± 0.05
Size range of the particles (␮m) 0.8–10.1 0.68–7.1
Average particle size (␮m) 4.4 ± 0.274 2.3 ± 0.0201
Average particle aspect ratio 2.1 1.6

ond of Al, Fe (about 10%), Mg and Mn; and the third of aluminum
oxide. The population of the two first groups is much higher than
the third. Four distinct groups of particles were found in AA5754.
The first group, which makes up about 55% of population, consisted
of aluminum oxide; the second of Al, Fe (2–3%) and Mn; the third of
Al, Fe (about 10%), Mn and Mg; and the fourth of Al, Mg and Si. The
population of the two last groups is much lower than the first two.
Porosity measurements conducted found that the porosity of
the as-received AA5182 and AA5754 sheets are 0.085% and 0.017%,
respectively. The microstructure of AA5754 appears to be cleaner
than AA5182 with less and smaller second phase particles.
Fig. 3a and b shows the shear bands revealed by the decora-
tion treatment in a quasi-static and a dynamic strain rate specimen,
respectively. Fig. 3c shows typical thickness of a shear band area on
a quasi-static strain rate specimen.

3.1. Quasi-static tensile tests

The engineering stress–strain curves obtained from quasi-static


tensile tests of AA5182 dog-bone specimens are presented in Fig. 4.
This figure shows that increasing quasi-static strain rates tend
to reduce the flow stress and strain to failure of the alloy. No
change in the shape of the stress–strain curves with strain rate
was observed. A similar trend is observed for AA5754. The serrated
yielding phenomena or discontinuous flow associated with Luders
band (Portevin-Le Chatelier instability) propagation is observed in
all specimens and is more pronounced in specimens tested at lower
strain rates. Each of these serrations is known to correspond to the
nucleation and propagation of deformation band along the ten-
sile specimen [1,22]. Similar results (at strain rate of 1.3 × 10−3 s−1 )
were obtained from ASTM standard sized specimens.
Fig. 5 shows the effect of strain rate on the ultimate tensile
strength of AA5182 and AA5754. The change in yield strength with
stain rate is shown in Fig. 6. A reduction in both ultimate and yield
strength for both alloys is observed with increasing strain rate, indi-
cating a negative rate sensitivity. This reduction in strength is less
for AA5754 (9.3% for AA5754, 10.6% for AA5182). Only a slight reduc-
tion in elongation to failure (14% for AA5182 and 10% for AA5754)
is observed with increasing strain rates for both alloys.

3.2. High strain rate tensile tests

The change in elongation to failure of AA5182 and AA5754 with


strain rate at dynamic rates [20] is shown in Fig. 7. The elongation to
failure was found to increase with strain rate. A mild increase in the
flow stress was observed for AA5754 while no significant change is
seen for AA5182. These results suggest that these alloys have a small
positive rate sensitivity when deformed under dynamic conditions Fig. 3. (a) Shear band in a quasi-static specimen, (b) shear bands in a dynamic strain
[20]. rate specimen and (c) thickness of a shear band area on a quasi-static strain rate
At elevated temperature tests of 150 and 300 ◦ C, a drop in flow specimen.
stress was observed for both AA5182 and AA5754 when deformed
at dynamic rates [20]. Fig. 8 illustrates this change in strength with
temperature at 15% strain for both alloys at a strain rate of 1500 s−1 .
In addition to a reduction in strength, increasing temperatures was
found to be detrimental to the ductility of these alloys (Fig. 9).
286 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292

Fig. 7. Change in the elongation to failure of AA5182 and AA5754 with strain rate at
dynamic rates.
Fig. 4. Engineering stress–strain curves obtained from quasi-static tensile tests of
AA5182 specimens.

Fig. 8. Effect of temperature on the flow stress of AA5182 and AA5754 at 15% strain
at strain rate of 1500 s−1 .

Fig. 5. Effect of strain rate on ultimate tensile strength of AA5182 and AA5754 at
quasi-static rates. intense shear bands on the surface of all specimens. A large number
of damage including voids, microcracks and damaged second phase
3.3. Failure analysis particles were observed in these shear bands (Fig. 10). Although
some damaged particles were also observed out of these bands,
3.3.1. Quasi-static regime most of the damaged particles were found on, or near, these bands.
Examination of the surfaces of the specimens after quasi-static These shear bands with a high density of damaged particles are
tensile testing, heat treatment and etching showed several large

Fig. 6. Change in the yield strength of AA5754 and AA5754 with strain rate at quasi- Fig. 9. Change in elongation to failure of AA5182 and AA5754 with temperature at
static rates. 1500 s−1 .
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 287

Fig. 10. Shear bands and damaged area on the surface of a AA5182 specimen failed Fig. 12. A part of the crack path in a AA5182 specimen which was fractured at
at 1.3 × 10−3 s−1 . 1.3 × 10−2 s−1 .

present in close proximity to the main crack or fracture path. in AA5754. Shear band thicknesses are also dependent on strain
Damage was observed to initiate at the second phase particles rate. Fig. 15a shows that the thickness of shear bands increases
by means of particle cracking and/or particle-matrix decohesion. with increasing strain rate for both alloys in the quasi-static
Fig. 11 shows typical optical micrographs of AA5754 specimens regime.
after shear band decoration that was tested 1.3 × 10−3 s−1 . These Statistical analysis of the size of the damaged particles was per-
images indicate that shear band formation or localization occurs formed. The average size of damaged particles as a function of strain
prior to fracture. Detailed analysis of the crack path by optical and rate is presented in Fig. 15b. A comparison of these results with
electron microscopy show that most of the crack trail in the quasi- particles measured from specimens in the as-received condition
static specimens lies either along or parallel the shear bands. This (average of 4.4 and 2.3 ␮m for AA5182 and AA5754, respectively)
phenomena is illustrated in Fig. 12, and is observed in both ASTM indicates that the larger particles are more prone to damage than
and dog-bone type specimens. the smaller particles. Furthermore, the average size of damaged
Analysis of the interrupted AA5182 specimens showed that at particles was found to increase with increasing strain rate. Fig. 15b
small plastic strains, damage was only visible at larger second phase shows that while the average damaged particle size for AA5182
particles located at grain boundaries (Fig. 13). However, at interme- specimens that failed at 1.3 × 10−4 s−1 is 5.3 ␮m, it is 7.36 ␮m for
diate plastic strain levels some are present at second phase particles those that failed at 1.3 × 10−1 s−1 .
inside the grains (Fig. 14). At high plastic strain levels and shear The fracture surfaces of all specimens contain dimples, a
localization, intense damage located inside the shear bands are typical feature of ductile fracture. Some differences between
present (Fig. 11). A similar observation is made with AA5754. How- the fracture surfaces of high and low strain rate specimens
ever, AA5754 tends to show slightly less grain boundary effects. were observed. The fracture morphology of specimens that
Some large damaged particles are observed away from the grain failed at lower strain rates (Fig. 16a) is characterized by well-
boundaries at low and intermediate plastic strain levels, but the vast formed voids centered mostly around the damaged second
majority of them are located at the grain boundaries. Under iden- phase particles, with thin matrix ligaments between the pri-
tical test conditions, the area of localized plastic deformation and
thickness of the shear bands were found to be higher in AA5182 than

Fig. 11. An intense deformation area and shear bands in the AA5754 specimens Fig. 13. Damaged large second phase particles on the grain boundaries of an inter-
failed at 1.3 × 10−3 s−1 . rupted AA5182 specimen at low levels of plastic strain.
288 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292

Fig. 14. Damaged large second phase particles inside the grain of an interrupted
AA5182 specimen at intermediate strain levels after shear band decoration treat-
ment.

mary voids. In contrast, the fracture surfaces of specimens that


failed at higher quasi-static rates (Fig. 16b) were covered with
large and small shallow voids. The matrix between neighbour-
ing voids was almost ruptured by the formation of smaller
dimples. As illustrated in Fig. 17, image analysis of the frac-
ture surfaces shows that the diameter of the central deep
voids on the fractured surfaces decreases with increasing strain
rate.

Fig. 16. (a) Fracture surface of a AA5182 specimen failed at 1.3 × 10−4 s−1 and (b)
fractured surface of a AA5182 specimen failed at 1.3 × 10−1 s−1 .

3.4. High strain rate regime

3.4.1. Room temperature tests


Several small shear bands were observed on some TSHB spec-
imens that failed at room temperature. No shear bands or shear
localization are observed in the other specimens. Although some
damage was observed in the shear bands, most of the damaged

Fig. 15. (a) The average thickness of shear bands as a function of strain rate for
specimens failed in the quasi-static regime. (b) Average size of damaged particles as Fig. 17. Measured dimple size vs. strain rate of AA5182 and AA5754 specimens failed
a function of strain rate for specimens failed in the quasi-static regime. in the quasi-static regime.
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 289

Fig. 20. Shear band thickness as a function of strain rate at dynamic rates.

Fig. 18. A AA5182 specimen failed at 1100 s−1 .

areas were found outside of these bands. An area with a high den-
sity of damage was observed a short distance from the main fracture
path in all specimens, most of which are associated with second
phase particles.
Micrographs of a AA5182 specimen tested at 1100 s−1 follow-
ing shear band decoration is shown in Fig. 18. Examinations of the
specimen show that at larger distances (more than 0.3 mm) from
the crack path, damage was only present on the larger second phase
particles. However, damage is observed at smaller particles near the
crack path. A similar behavior was observed from AA5754 material.
Fig. 19 shows the change in damage particle size with strain rate. It
is observed that under dynamic conditions, the average damaged
particle size decreases with increasing strain rate for both alloys.
The presence and thickness of shear bands were found to be Fig. 21. Measured dimple size vs. strain rate of AA5182 and AA5754 specimens failed
influenced by strain rate and alloy composition. Less shear localiza- in the dynamic regime.
tion was observed in AA5754 compared to AA5182. Fig. 20 shows
that shear band thickness tend to decrease with increasing strain 3.5. Elevated temperature tests
rate for both alloys. The crack profiles of failed TSHB specimens
show less evidence of crack path dependence with strain rate than Although the general characteristics of TSHB specimens tested
those failed under quasi-static rates. at 150 and 300 ◦ C are similar to those tested at room temperature,
The fracture surfaces of all specimens that failed at room tem- some evidence of shear band localization was found on the surface
perature exhibit ductile fracture morphology. The primary dimples of these specimens. A significant difference was observed for spec-
around the damaged particles are deep with some small secondary imens failed at 300 ◦ C. Specimens from both alloys show evidence
dimples surrounding them. The change in average primary dimple of particle fracture at grain boundaries. Fig. 22 shows a crack profile
size with strain rate is shown in Fig. 21. These results show that the
primary dimple size tend to decrease with increasing strain rates.

Fig. 19. Average size of damaged particles of specimens failed at dynamic rates. Fig. 22. Crack profile in the AA5182 specimen tested at 300 ◦ C.
290 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292

this alloy at strain rates below 1 s−1 . Negative strain rate sensitiv-
ity in Al–Mg alloys has also been reported by other investigators
[1,15,24–26]. DSA is described by the interaction of fast diffusing
solute atoms such as magnesium with moving dislocations [3,22].
Since DSA is diffusion controlled, it is a function of temperature
and strain rate. At very low strain rates, solute atoms interact
with obstacles preventing dislocation movements, resulting in
higher flow stresses. As the strain rate increases, the dampening
effect of the solutes on dislocation movement decreases and lower
flow stresses are obtained. When sufficiently high strain rates are
reached, DSA disappears as the deformation time is too short for
diffusion to occur [1,3,22,24].
Interrupted test specimens show that little damage is present
prior to the onset of flow instability. Shear banding and damage
are observed in all failed quasi-static specimens, with the majority
of the voids located within the shear bands regions. The thickness
of the shear bands present was found to increase with increasing
strain rates. Reviews by Wright [28] and Bassim and co-workers
Fig. 23. Crack profile characterization of a AA5754 specimen tested at 300 ◦ C. [29] show that shear bands can act as a preferential crack nucle-
ation sites and fragmentation in Al alloys, Ti alloys and steels at
higher strain rates. The larger densities of damage observed on and
near the shear bands of the failed specimens suggest that plastic
localization and shear banding enhance the local damage process
prior to failure in the quasi-static regime.
Softening due to the PLC effect is a source of plastic flow insta-
bility or localization in Al–Mg alloys [17,27]. Localization occurs
due to the interaction between different factors such as material
hardening or softening, geometry and loading conditions [12,27].
It commences when the softer regions in a material deform more
rapidly than other regions and represents a drastic change in mate-
rial deformation from a relatively uniform to a non-uniform one
involving high strain gradients. The larger strains present in the
shear bands lead to degradation of the material’s strength and stiff-
ness [30]; nucleation, growth, and coalescence of microcracks or
voids [31,32]; and a reduction in the load-bearing area. The nega-
tive strain rate sensitivity of a material not only provides the right
conditions for localization, but can also reduce the magnitude of
the strain required for void growth within a shear band [17]. The
Fig. 24. Fractured surface of a AA5182 specimen failed at 300 ◦ C at a strain rate of
decrease in elongation to failure observed with increasing strain
1500 s−1 . rate can hence be attributed to the lower strains required for void
growth within the shear band regions.
Void nucleation usually occurs at inclusions and/or second
of a AA5182 specimen which failed at 300 ◦ C. The crack profile char-
phase particles in a metallic matrix. Different criteria are available
acterization for a AA5754 specimen is presented in Fig. 23. Fig. 24
to describe void nucleation; some based on critical stress while
shows the fracture surface of a AA5182 specimen failed at 1500 s−1
others on critical strain [11,33,34]. The strain-controlled nucleation
at 300 ◦ C. In contrast to the specimens tested at room tempera-
criterion is often used to describe the formation of damage from
ture, regions containing small shallow dimples and, large flat areas
particles [11,33–36]. The strain for void nucleation has been esti-
(evidence of local melting) on the fractured surfaces were observed.
mated through different models [37]. In the presence of plastic
strain, larger particles are more prone to damage and are favor-
4. Discussion able sites for void nucleation as less strain is required [35]. Thus,
the average size of damaged particles can be used to estimate
From the tensile test results and microstructural observations the amount of plastic strain required to produce localization and
obtained over a range of strain rates, the mechanical response and damage in a specimen. Quantitative measurements of the size of
failure mechanism of the aluminum alloys studied are found to be damaged particles found that the average damaged particle size
influenced by the strain rate at which they are deformed. tend to increase with increasing strain rate (Fig. 15b). This suggests
that the critical strain required for strain localization decreases with
4.1. Quasi-static regime increasing strain rate in the QS regime. This is also in agreement
with the decrease in elongation to failure with increasing strain
A slight negative strain rate effect was observed at quasi- rate observed.
static rates at room temperature. Serrations or Portevien-Le
Chateler (PLC) instability is also present. These observations may 4.2. Dynamic regime
be attributed to the dynamic strain ageing (DSA) phenomena
[1,3,22,23], which are in agreement with the findings of other In contrast to the tensile test results obtained in quasi-static
researchers. During testing of AA5083, Clausen et al. [8] found ser- regime, a mild positive strain rate sensitivity was observed in the
rated stress–strain curves and negative strain rate sensitivity for alloys studied with increasing strain rates in the dynamic regime.
M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292 291

Small shear bands were observed in only some of the tested speci- perature of AA5383 alloy as 563 ◦ C. This liquid phase produces an
mens and damage was mostly present in regions outside the shear inhomogeneity, which makes deformation unstable and produces
bands. As the strain rate increases, the thickness of the shear bands strain localization [42]. These localization areas act as nucleation
(when present) was found to decrease. These observations sug- sites for cracks. The local liquid phase limits the maximum tolera-
gest that, unlike the quasi-static regime, shear localization plays ble plastic strain during deformation, and decreases the elongation
a lesser role in the damage processes and final failure of the mate- to failure and flow stress of the tested materials.
rials studied at dynamic rates. In this regime, shear localization
appears to be a consequence of the void nucleation, growth and
4.4. Concluding remarks
coalescence at second phase particles that are primarily generated
by homogeneous plastic deformation.
The AA5182 and AA5754 alloys studied were found to exhibit
The two main failure modes observed in aluminum alloys when
a negative strain rate sensitivity when tested in the quasi-static
deformed under dynamic rates are dimple fracture (dynamic ten-
strain rate regime, but mild positive strain rate sensitivity in the
sile fracture) and shear fracture (adiabatic shear banding) [32,38].
dynamic strain rate regime. Under quasi-static conditions, increas-
Dynamic tensile fracture involves void nucleation, growth and coa-
ing strain rates resulted in increased material softening and more
lescence processes. The growth and coalescence of the nucleated
pronounced shear band formation. Strain localization appears to
micro-voids and the formation of shear bands occurs with increas-
be a necessary pre-requisite for damage and final failure to occur.
ing plastic strain [32]. Dynamic shear localization or adiabatic shear
Under dynamic conditions, however; significantly less shear local-
banding (ABS) on the other hand is governed by the competition
ization is observed. The void nucleation, growth and coalescence
between strain hardening and thermal softening of the material.
process at the second phase particles is the dominant failure
Damage is often present in ABS bands due to the higher strains
mechanism which develops prior to localization. Analysis of TSHB
present within them. It is the growth and coalescence of these voids
specimens failed at elevated temperatures show the presence of
or ABS themselves that ultimately results in final failure at high
local melting zones at grain boundaries, which may contribute to
strain rates [28,32,38].
the lower ductility and flow stresses measured.
In this study, shear bands were not observed in all TSHB spec-
imens, and where present, they were small in size. Furthermore,
the majority of damage present was found in regions outside the Acknowledgements
shear bands. This suggests that the dynamic tensile fracture mode
is the dominant failure mechanism for AA5182 and AA5754 when Authors thank the Novelist Global Technologies, Canada, for pro-
deformed under the range of dynamic strain rates investigated. viding the Al alloys. M.J. Hadianfard would like to thank Shiraz
The deformation mechanisms of a material can vary with the University, Shiraz, Iran for the financial support of sabbatical leave
rate of strain [39]. The different failure mechanisms and mechanical of the author.
behaviors of AA5754 and AA5182 at quasi-static and dynamic strain
rates can be accredited to the different dislocation mechanisms
References
involved. At lower quasi-static strain rates local stress concen-
trations are suppressed by local dislocation motion (thermally [1] T. Mukai, K. Ishikawa, K. Higashi, Mater. Sci. Eng. A 204 (1995) 12–18.
activated obstacles). With increasing strain rates, more dislocations [2] L.D. Oosterkamp, A. Ivankovic, G. Venizelos, Mater. Sci. Eng. A278 (2000)
are immobilized and the local stresses may rise above a nucleation 225–235.
[3] M. Wagenhofer, M. Erickson-Natishan, R.W. Armstrong, Scripta Mater. 41 (11)
threshold so that damage can be nucleated from weak spots such (1999) 1177–1184.
as grain boundaries and/or second-phase particles. The growth and [4] J.P. Fowler, M.J. Worswick, A.K. Pilkey, H. Nahme, Metall. Mater. Trans. A 31A
coalescence of these nucleated voids finally leads to the failure of (2000) 831–844.
[5] Y. Li, K.T. Ramesh, E.S.C. Chin, Mater. Sci. Eng. A 382 (2004) 162–170.
materials [32].
[6] E. El-Magd, M. Brodmann, Mater. Sci. Eng. A 307 (2001) 143–150.
In the quasi-static regime, plastic strain localization leads to [7] T. Naka, F. Yoshida, J. Mater. Process. Technol. 89/90 (1999) 19.
higher strain rate and enhanced softening in the localized area. This [8] A.H. Clausen, T. Borvik, O.S. Hopperstad, A. Benallal, Mater. Sci. Eng. A 364
(2004) 260–272.
local softening effect creates larger localized zones with thicker
[9] D. Li, A. Ghosh, Mater. Sci. Eng. A 352 (2003) 279–286.
shear bands and higher damage density. Due to the positive rate [10] J. Gurland, J. Plateau, Trans. ASM 56 (1963) 442–456.
sensitivity of the alloys studied under dynamic conditions, increas- [11] C.C. Chu, A. Needleman, J. Eng. Mater. Technol. 102 (1980) 249–256.
ing strain rates resulted in higher flow stresses within the localized [12] T. Pardone, Y. Brechet, Philos. Mag. 84 (3–5) (2004) 269–297.
[13] J. Pan, M. Saje, A. Needleman, Int. J. Fract. 21 (1983) 261–278.
area, stabilizing the deformation. Thus, the onset of strain local- [14] M.J. Worswick, N. Qiang, P. Niessen, R.J. Pick, in: M.A. Meyers, L.E. Murr, K.P.
ization is delayed at dynamic rates, as indicated by the thinner Standhammer (Eds.), Shock Wave and High-Strain Rate Phenomena in Metals,
shear bands present in the TSHB specimens. An increase in elonga- Dekker, New York, NY, 1990, pp. 87–95.
[15] D.J. Lloyd, Metall. Mater. Trans. A 11 (1980) 1287–1294.
tion to failure with increasing strain rate measured under dynamic [16] M. Lebyodkin, L. Dunin-Barkowskii, Y. Brechet, Acta Mater. 48 (2000) 2529.
conditions further supports this hypothesis [40]. [17] N. Chung, J.D. Embury, J.D. Evensen, R.G. Hoagland, C.M. Sargent, Acta Metall.
25 (1977) 377.
[18] K. Spencer, S.F. Corbin, D.J. Lloyd, Mater. Sci. Eng. A 332 (2002) 81–90.
4.3. High strain rate, elevated temperature [19] E8M-04 Standard Test Methods for Tension Testing of Metallic Materials [Met-
ric].
Results of TSHB tests at 300 ◦ C and strain rate of 1500 s−1 show [20] R. Smerd, S. Winkler, C. Salisbury, M. Worswick, D. Lloyd, M. Finn, Int. J. Impact
Eng. 32 (2005) 541–560.
a considerable change in the flow stress, elongation to failure and
[21] D.J. Lloyd, E.F. Butryn, M. Ryvola, Microstruct. Sci. 10 (1982) 373–384.
shape of the stress–strain [20]. Compared to the specimens tested [22] M. Abbadi, P. Hahner, A. Zeghloul, Mater. Sci. Eng. A 337 (2002) 194–201.
at room temperature, the 300 ◦ C specimens appear to have weak- [23] K. Peng, W. Chen, K. Qian, Mater. Sci. Eng. A 415 (2006) 53–58.
[24] H. Zhang, K.T. Ramesh, E.S.C. Chin, Mater. Sci. Eng. A 384 (2004) 26–34.
ened grain boundaries, with evidence of local melting (Figs. 22–24).
[25] B.A. Wilcox, A.R. Rosenfield, Mater. Sci. Eng. 1 (1966) 201–205.
Adiabatic deformation of the material at high strain rate provides a [26] A. Korbel, H. Dybiec, Acta Metall. 29 (1981) 89–93.
situation where the heat generated in a localized area does not have [27] X. Duan, M. Jain, D. Metzger, J. Kang, Mater. Sci. Eng. A 394 (2005) 192–203.
adequate time to dissipate. Coupled this with the heat from the test [28] T.W. Wright, The Physics and Mathematics of Adiabatic Shear Bands, Cambridge
University Press, 2002.
temperature (300 ◦ C) incipient melting may be present at the grain [29] A.G. Odeshi, S. Al-Ameeri, S. Mirfakhraei, F. Yazdani, M.N. Bassim, Theor. Appl.
boundaries. Deschamps et al. [41] have measured the solidus tem- Fract. Mech. 45 (2006) 18–24.
292 M.J. Hadianfard et al. / Materials Science and Engineering A 492 (2008) 283–292

[30] G.M. Owolabi, A.G. Odeshi, M.N.K. Singh, M.N. Bassim, Mater. Sci. Eng. A 457 [37] H. Wilsdorf, Mater. Sci. Eng. A 59 (1983) 1–39.
(2007) 114–119. [38] H. Zhu, L. Zhu, J.-H. Chen, Key Eng. Mater. 353–358 (2007) 1157–1160.
[31] D. Curran, L. Seaman, D. Shockey, Phys. Rep. 147 (1987) 253–388. [39] T. Nicholas, in: J.A. Zukas, et al. (Eds.), Impact Dynamics, John Wiley & Sons,
[32] G.Z. Voyiadjis, A.N. Palazotto, X.-L. Gao, Appl. Mech. Rev. 55 (no. 5) (2002) New York, 1982, pp. 227–332.
481–493. [40] M.J. Worswick, R. Smerd, C.P. Salisbury, Mater. Sci. Forum 519–521 (2006)
[33] A.S. Argon, J. Im, Metall. Trans. A 6A (1973) 839–851. 139–146.
[34] S.H. Goods, L.M. Brown, Acta Metall. 27 (1979) 1–15. [41] A. Deschamps, S. Peron, Y. Brechet, Mater. Sci. Eng. A 319–321 (2001) 583–586.
[35] M.J. Hadianfard, J. Healy, Y.-W. Mai, J. Mater. Sci. 29 (1994) 2321–2327. [42] R. Dormeval, in: T.Z. Blazynski (Ed.), Materials at High Strain Rates, Elsevier
[36] M. Zhou, R.J. Strain, Int. J. Impact Eng. 19 (3) (1997) 189–206. Applied Science, London, 1987, pp. 47–70.

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