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    Z245.20-98 Z245.21-98

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    G 1 F Instruction No. 2 LE COPY, Z245.20-98/Z245.21-98 April 2000 Title: External Fusion Bond Epoxy Coating for Steel Pipe/External Polyethylene Coating for Pipe, originally published April 1998 The following revisions have been formally approved and are marked by the symbol delta (A) in the margin on the attached replacement pages: Revised | Table 3 of 2245.21-98 New None Deleted | None CSA Standard Z245,20-98/Z245.21-98 originally consisted of 85 pages (xviii preliminary and 67 text), each dated April 1998. It now consists of the following pages: xviii, 3-58, and 61-85 dated April 1998; and 59 and 60 dated April 2000. © Update your copy by inserting these revised pages. Keep the pages you remove for reference. Table 3 Virgin Polyethylene Resin Requirements (See Clauses 5.3 and 5.6.) External Polyethylene Coating for Pipe “Acceptance criteri ‘Low density a) Linearlow ‘Medium density ‘High density Test Unit density (LLD) (MD) (HD) ‘Test method Density giem? 0.925 0925-0940 30.940 ASTM D 792 or [ASTM D 1505 Elongation at break 9% 600 minimum 600 minimum ASTM D 638 ‘Type V sample CCrosshead speed 50 mm/min Flow rate gMOmin LD: 0.15-06 01-10 0.15-0.80 ASTM D 1238 LD: 05-20 190°C/2.16 kg Hardness ShoreD 45 minimum SO-minimum 60 minimum ASTM D 2240 Tensile strength at MPa 9.7 minimum 12.4 minimum 18.5 minimum ASTM D 638 yield Type IV sample Crosshead speed 50 mm/min Oxidative-induction minute 10 minimum 10 minimum = 10-minimum ASTM D 3895 time in oxygen at 220°C, aluminum pan, no screen’ Brittleness *c 7Oorlower —-70orlower 70 orlower_ «ASTM 746 ‘temperature * (or Fx) (or Fa) (or Fad) Environmental stres-—h 300 minimum 300 minimum 300 minimum ASTM D 1693 cracking resistance or Fs) (for Fa) or Fu) 100% Igepal condition® Condition “C* Condition “C” Condition “8” Vicat softening point’ °C. 90 minimum 110 minimum 120 minimum _ ASTM D 1525 “Testing of these properties is required at least once per 12 months. ‘April 2000 (Replaces p. 59, April 1998) 59 2245.21.98 Table 4 GQ Coating Qualification Test Requirements a (Gee Clauses 5.2, 5.3, and 6.1.2.) Test “Acceptance criteria ‘Test method. 28 d cathodic disbondment at 20°C 15 mm maximum radius ‘Clause 12.3 28 d cathodic disbondment at Purchaser's specification Clause 12.3 maximum design temperature Impact resistance A minimum of 3.0 J/mm of CSA Standard 2245.20, actual total coating thickness ‘Clause 12.12, except that for ‘each im of thickness the voltage setting shall be 10 V, up toa ‘maximum of 15 000 V for Clause 12.12.3.3 Flexibility No cracking of polyethylene CSA Standard 7245.20, Clause 12.11; bend of 2.5° Peel adhesion Clause 12.4 0r 12.5, system AT 3.0N minimum System AZ 19.6 N minimum System 8 150.0 N minimum Table 5 € Polyethylene Qualification Test Requirements (Gee Clause 6.1.3.) Test. Acceptance criteria “Test method. Tensile stress at yield ASTM D 638 Dor LD 8.5 MPa minimum, Type IV sample; MD 11.0 MPa minimum, crosshead speed HD. 17.0 MPa minimum, 50 mm/min Elongation at break 300% minimum ASTM D 638 Type IV sample; crosshead speed 50 mm/min Heat ageing ‘At least 65% of original tensile stress at_ Clause 12.6 yield; minimum elongation of 150% ( 60 April 2000 (Replaces p. 60, April 1998) 2Z245.20-98 External Fusion Bond Epoxy Coating for Steel Pipe 2245.21-98 External Polyethylene Coating for Pipe Q General Instruction No. 1 Z245.20-98/Z245.21-98 April 1998 Title: External Fusion Bond Epoxy Coating for Steel Pipe/External Polyethylene Coating for Pipe Pagination: 85 pages (xviii preliminary and 67 text), each dated April 1998 For information about updates to this CSA publication, please complete and return the attached card. Name Organization Address City Province/State Country, Postal/Zip Code Z245.20-98/Z245.21-98 Z245.20-98 External Fusion Bond Epoxy Coating for Steel Pipe Z245.21-98 External Polyethylene Coating for Pipe ISSN 0317-5669 Published in April 1998 by Canadian Standards Association 178 Rexdale Boulevard Etobicoke, Ontario, Canada MOW 1R3 Technical Editor: Solomon Ko Managing Editor: Gary Burford Senior Project Editor: Ann Martin Editor: Maria Adragna Publishing System Coordinators: Ursula Das/Grace Da Silva/Tarsem Suri © Canadian Standards Association — 1998 All rights reserved. No part of this publication may be reproduced in any form whatsoever without the prior permission of the publisher. ‘Externa Fusion Bond Epoxy Coating for Steel Pipe/ External Polyethylene Coating for ie Contents Technical Committee on Oil and Gas Industry Pipeline Systems viii Subcommittee on Materials xi ‘Task Force on Coated Pipe xiv Preface xvi 245.20 External Fusion Bond Epoxy Coating For Stee! Pipe 1. Scope 3 2. Reference Publications 3 3. Definitions 4 4. General Requirements 4 4.1 Product Ordering Requirements 4 4.1.1 Standard Requirements 4 4.1.2 Optional Requirements 5 4.2 Rounding Procedure 5 4.3 Quality Program 5 44 Compliance $ 5. Materials 5 5.1 Pipe 5 5.2 Epoxy Powder 5 5.2.1 General 5 5.2.2 Properties 6 5.2.3 Packaging 6 6. Coating Application 6 6.1 Coating Qualification 6 6.1.1 General 6 6.1.2 Preparation of Laboratory-Coated Test Specimens 6 6.1.3 Coating Qualification Test Requirements 7 6.2 Production Application Practices and Equipment 7 6.2.1 General 7 6.2.2 Surface Preparation 7 6.2.3 Application and Curing Temperatures 7 6.2.4 Coating Thickness 7 625 End Finish 8 April 1998 fii Z245.20-98/2245.21-98 7. Production, Inspection, and Testing & 7.1 Inspection Notice 8 7.2 Plant Access & 7.3 Production Tests 8 7.3.1. Epoxy Powder and Coating 8 7.3.2 In-Line Inspection and Measurement 9 7.3.3 Production Test Rings 10 8. Repair of Coated Pipe 17 8.1 General 17 8.2 Patching 7 8.3 Stripping and Recoating 12 9. Markings 12 9.1 General 12 9.2 Required Markings 12 10. Handling and Storage 12 10.1 Handling 12 10.2 Storage 13 11. Test Reports and Certificates of Compliance 73 12. Test Procedures 13 12.1 Cure Time of the Epoxy Powder 13 12.1.1 Equipment 73 12.1.2 Procedure 14 12.1.3 Report 14 12.2 Gel Time of the Epoxy Powder 15 12.2.1 Equipment 15 12.2.2 Procedure 15 12.2.3 Report 15 12.3. Moisture Content of the Epoxy Powder — Titration 16 12.3.1 Equipment 16 12.3.2 Reagents 16 12.3.3 Procedure 16 12.3.4 Report 16 12.4 Moisture Content of the Epoxy Powder — Mass Loss 76 12.4.1 Procedure A 16 12.4.2 Procedure B 17 12.43 Report 17 12.5 Particle Size of the Epoxy Powder 17 12.5.1 Equipment. 17 125.2 Procedure 17 12.5.3 Report 18 12.6 Density of the Epoxy Powder 18 12.6.1 Equipment 78 12.6.2 Procedure 18 12.6.3 Report 19 12.7 Thermal Characteristics of the Epoxy Powder and Coating 20 12.7.1 General 20 iv April 1998 12.7.2 Equipment 20 12.73 Procedure 20 12.7.4 Report 21 128 Cathodic Disbondment of the Coating 27 12.8.1 Equipment 27 12.8.2 Test Specimen 27 12.8.3 Procedure 22 12.8.4 Report 22 12.9 Chemical Resistance of the Coating 23 12.9.1 Equipment 23 12.9.2 Test Specimen 23 12.9.3 Test Reagents 23 12.9.4 Procedure 23 12.9.5 Report 23 12.10 Porosity of the Coating 23 12.10.1 Equipment 23 12.10.2 Test Specimen 23 12.10.3 Procedure 24 12.104 Report 24 12.11 Flexibility of the Coating 24 12.11.1 Equipment 24 12.1.2 Test Specimen 24 12.1.3 Procedure 24 12.11.4 Report 25 12.12 Resistance to Impact of the Coating 25 12.12.1 Equipment 25 12.12.2 Test Specimen 25 12.123 Procedure 26 12.124 Report 26 12.13 Cathodic Disbondment of Strained Coating 26 12.13.1 Equipment 26 12.13.2 Test Specimen 26 12.133 Procedure 26 12.134 Report 27 12.14 Adhesion of the Coating 27 12.14.1 Equipment 27 12.14.2 Test Specimen 27 12.143 Procedure 27 12.14.4 Report 27 12.15 Interface Contamination of the Coating 28 12.15.1 Equipment 28 12.15.2 Test Specimen 28 12.15.3 Procedure 28 12.15.4 Report 28 Tables 28 Figures 31 April 1998 {External Fusion Bond Epoxy Coating for Stee! Ppe/ External Polyethylene Coating for Pipe Z245.20-98/Z245.21-98 2245.21 External Polyethylene Coating for Pipe 1, Scope 39 2. Reference Publications 39 3. Definitions 47 4. General Requirements 42 4.1 Product Ordering Requirements 42 4.1.1 Standard Requirements 42 4.1.2 Optional Requirements 42 4.2 Rounding Procedure 42 4.3 Quality Program 42 4.4 Compliance 42 5. Materials 42 5.1 Pipe 42 5.2 Coating Systems 43 5.3 Manufacturer's Documentation 43 5.4 Primer 43 5.4.1 Liquid Primer 43 5.4.2 Powdered Primer 43 5.5 Adhesive 43 5.6 Polyethylene 43 5.7 Packaging 43 6. Coating Application 44 6.1 Coating Qualification 44 6.1.1 General 44 6.1.2 Testing Requirements 44 6.1.3 Polyethylene Evaluation 44 6.2 Production Application Practices and Equipment 44 6.2.1 General 44 6.2.2 Surface Preparation 44 6.2.3 Application 45 6.24 End Finish 45 7. Production, Inspection, and Testing 45 7.1 Inspection Notice 45 7.2 Plant Access 45 7.3 Incoming Raw Materials Testing 46 7.4 Production Tests 46 7.4.1 In-Line Inspection and Measurement 46 7.4.2 Holiday Inspection 46 7.4.3 Production Test Rings 47 8. Repair of Coated Pipe 48 8.1 General 48 vi April 1998 8.2 Patching 48 8.3 Stripping and Recoating 48 9. Markings 48 9.1 General 48 9.2 Required Markings 49 10. Handling and Storage 49 10.1 Handling 49 10.2 Storage 49 11. Test Reports and Certificates of Compliance 49 12, Test Procedures 50 12.1 Viscosity 50 12.1.1 Equipment 50 12.1.2 Procedure 50 12.13 Report 50 12.2 Flow Test 57 12.2.1 Equipment 51 12.2.2 Procedure 57 12.2.3 Report 51 12.3 Cathodic Disbondment of the Coating 52 12.3.1 Equipment 52 12.3.2 Test Specimens 52 12.3.3 Procedure 52 12.3.4 Report 53 12.4 Peel Adhesion (Constant Rate of Peel) 53 12.4.1 Equipment 53 12.4.2 Test Specimen 53 12.4.3 Test Parameters 54 12.4.4 Procedure 54 12.4.5 Calculations 55 12.4.6 Report 55 12.5 Peel Adhesion (Hanging Mass) 55 12.5.1 Equipment 55 12.5.2 Test Specimen 55 12.5.3 Test Parameters 55 12.5.4 Procedure 55 12.5.5 Report 56 12.6 Heat Ageing 57 12.6.1 Equipment 57 12.6.2 Test Specimen 57 12.6.3 Procedure 57 12.6.4 Report 57 Tables 58 Figures 63 Aprit 1998 External Fusion Bond Epoxy Coating for Steel Pie/ External Polyethylene Coating for Pipe 2245.20-98/2245.21-98 Technical Committee on Oil and Gas Industry Pipeline Systems A.B. Rothwell NOVA Gas Transmission Ltd., Calgary, Alberta R.R. Bryant Union Gas Limited, Chatham, Ontario M.F. Hallihan Shell Canada Limited, Calgary, Alberta AR. Pick Interprovincial Pipe Line Inc., Edmonton, Alberta K.G. Sharp Alberta Energy and Utilities Board, Calgary, Alberta J. Abes National Energy Board, Calgary, Alberta HE. Allen Northwestern Utilties Limited, Edmonton, Alberta AO. Alonso Technical Standards and Safety Authority, Toronto, Ontario Canadian Gas Association, Don Mills, Ontario R. Basaraba TransCanada Pipelines Ltd., Calgary, Alberta B.A. Broderick Canadian Westem Natural Gas Company Limited, Calgary, Alberta B. Brown Pipeline Contractors Association, Mississauga, Ontario D.R. Christensen ‘Amoco Canada Petroleum Company Limited, Calgary, Alberta F.M. Christensen Stelpipe/Camrose Pipe Company, Qualicum Beach, British Columbia vili Chair Vice-Chair Vice-Chair Vice-Chair Vice-Chair Associate Associate Associate April 198 ‘External Fusion Bond Epoxy Coating for Steel Pipe! External Polyethylene Coating fr Pipe DW. Clarke Trans-Northern Pipelines Inc., Richmond Kill, Ontario L.A. Colgan Ministry of Employment and Investment, Victoria, British Columbia Ru. Coote NOVA Gas Transmission Ltd., Associate Calgary, Alberta RJ. Cowel Sun-Canadian Pipe Line Company Limited, Waterdown, Ontario J. Cripps Westcoast Energy Inc., Vancouver, British Columbia G.L. de Caux Prudential Steel Ltd., Calgary, Alberta J. DeJong Canadian Hibernia Holding Corporation, Associate Calgary, Alberta J.R. Ellwood Foothills Pipe Lines Ltd., Calgary, Alberta M.C. Enwright Husky Oil Operations Limited, Calgary, Alberta B.E, Fowlie Imperial Oil Resources Limited, Calgary, Alberta LH. Gales ‘Transportation Safety Board of Canada, Associate Hull, Québec S¥J. Gillard PanCanadian Petroleum Limited, Calgary, Alberta A.M. Gilroy-Scott Integrity Management, Calgary, Alberta H. Harden B.C. Gas Utility Ltd, Surrey, British Columbia RJ. Henderson Centra Gas Ontario inc., Associate North Bay, Ontario MLR. Horner Trans Mountain Pipe Line Company Ltd., Vancouver, British Columbia D. Hudson olls-Radtke Ltd, Cambridge, Ontario ix April 1998 2245.20-98/2245.21-98. LW. Hunt Canspec Group Inc., © Oakville, Ontario E. Johnston ‘Aluminum Pipe Systems Inc, Associate Calgary, Alberta J.T. Justice J-T. Justice Consulting Limited, Mississauga, Ontario R.D. King Gulf Canada Resources Limited, Calgary, Alberta D. Kopperson PanCanadian Petroleum Limited, Associate Calgary, Alberta K.T. Lau Alberta Boilers Safety Association, Edmonton, Alberta T. Lawrence IPSCO Inc., Regina, Saskatchewan P.M. Marreck Mobil Oil Canada Ltd., Calgary, Alberta 5. E. McConkey Shaw Pipe Protection, Calgary, Alberta & P. Meanwel Union Gas Limited, Associate Chatham, Ontario D.B. Milmine DM Professional Services Ltd., Calgary, Alberta P. Noiseux Gaz Métropolitain Inc., Montréal, Québec W. Partington Marine Pipeline Construction of Canada Ltd., Nisku, Alberta Ty. Pesta Alberta Energy and Utilities Board, Associate Calgary, Alberta D. Piccinin-Craig Consumers Gas, Scarborough, Ontario |. Reynolds Canadian Welding Bureau, Associate Mississauga, Ontario P.A. Sandham SaskEnergy Corporation, Regina, Saskatchewan x April 1998 J. Sandison L Scott T.C. Stimmon NJ. Truster N. Van Wyngaarden EA. Yasinko April 1998. External Fusion Bond Epoxy Coating for Stee! Pipe/ External Polyethylene Coating for Pipe IDG Stanley in Winnipeg, Manitoba Canadian Association of Petroleum Producers, Associate Calgary, Alberta NOVA Gas Transmission Ltd, Associate Calgary, Alberta B.C. Gas Utility Ltd., Associate Surrey, British Columbia Taylor Forge Canada Corporation, ‘Niagara Falls, Ontario EA. Yasinko Engineering, Calgary, Alberta Canadian Standards Association, Project Manager Etobicoke, Ontario xi 2245.20-98/2245.21-98 Subcommittee on Materials 1.C. Slimmon NOVA Gas Transmission Ltd., Chair Calgary, Alberta F.M. Christensen Stelpipe/Camrose Pipe Company, Qualicum Beach, British Columbia KEW. Coulson NOVA Gas Transmission Ltd., Calgary, Alberta J. W. Cox Du Pont Canada Inc., Calgary, Alberta GL. de Caux Prudential Steel Ltd., Calgary, Alberta DH. Dunsmuir WFF Fittings and Flanges (Canada) Ltd., Calgary, Alberta M.C. Enwright Husky Oil Operations Limited, Calgary, Alberta AG. Glover NOVA Gas Transmission Ltd., Calgary, Alberta K.G. Goerz Shell Canada Limited, Calgary, Alberta M. Ishkanian Stream-Flo Industries Lta., Edmonton, Alberta FS. Jeglic National Energy Board, Calgary, Alberta H. Kraft Westcoast Energy Inc., Vancouver, British Columbia D.A, LaRose Moody International Limited, Edmonton, Alberta T. Lawrence IPSCO Inc., Regina, Saskatchewan RB. Lazor Interprovincial Pipe Line Inc., Edmonton, Alberta xii April 1998 Externa’ Fusion Bond Epoxy Coating for Stee Pipe/ External Polyethylene Coating for Pi D. Lebsack S.C. Lee R. Lessard D.B. Milmine LR. Mitchell GP. Pappas T.A. Pfaff B. Sjoberg M. Tomkins WAR. Tyson N. Van Wyngaarden D.H. Weaver B. Wilson R.LS. Wong 5. Ko Apri! 1998 ‘Amoco Worldwide Engineering and Construction, Houston, Texas, USA Alberta Energy and Utilties Board, Calgary, Alberta Welland Pipe Ltd., Welland, Ontario DM Professional Services Ltd., Calgary, Alberta Camrose Pipe Company, Calgary, Alberta Union Gas Limited, Chatham, Ontario Pfaff Intemational, Toronto, Ontario Shaw Pipe Protection, Calgary, Alberta Valgro Ltd., Edmonton, Alberta CANMET/MTL, Ottawa, Ontario Taylor Forge Canada Corporation, Niagara Falls, Ontario 3M Canada inc., London, Ontario Canspec Group Inc., Calgary, Alberta ‘TransCanada PipeLines Ltd, Calgary, Alberta Canadian Standards Association, Project Manager Etobicoke, Ontario xiii 2245.20.98/2245.21-98 Task Force on Coated Pipe K.E.W. Coulson NOVA Gas Transmission Ltd., Chair Calgary, Alberta M. Alexander Pipe Coating Systems, Nisku, Alberta JJ. Baron Shell Canada Ltd., Calgary, Alberta M. Cetiner TransCanada Pipelines Ltd., Calgary, Alberta G. Connelly Bitumes Spéciaux, Paris, France J.W. Cox DuPont Canada Inc., Mississauga, Ontario €. D’Agostino NOVACOR Chemicals, Mississauga, Ontario M.C. Enwright Husky Oil Operations Ltd., Calgary, Alberta H. Kraft Westcoast Energy Ltd., Vancouver, British Columbia WJ. Kresic Interprovincial Pipe Line Inc., Edmonton, Alberta D. LaRose Moody international Limited, Edmonton, Alberta TA. Pfaff Pfaff International, Toronto, Ontario AJ. Sansum ITI Anti-CORROSION Inc., Houston, Texas, USA B. Sjoberg Shaw Pipe Protection, Calgary, Alberta EJ. Sperling ‘Amoco Corporation, Calgary, Alberta xiv ‘Aor 1998 ‘Externl Fusion Bond Epoxy Coating for Stee Pipe/ External Polyethylene Coating for Pipe RE, Steele Shaw Industries Ltd., Etobicoke, Ontario D.G. Temple 3M Canada Inc., Calgary, Alberta D. Thomas BASF Lacke and Farben AG Protective Coatings, Minster, Germany D.H. Weaver 3M Canada Inc., London, Ontario D. Wong Shaw Industries Ltd., Etobicoke, Ontario xv April 1998 Z245,20-98/2245.21-98. Preface © ‘This is the third edition of CSA Standard 2245.20, External Fusion Bond Epoxy Coating for Stee Line Pipe. It supersedes the previous editions published in 1992 and 1986. CSA Standard 2245.20 deals with the requirements for external fusion bond epoxy coating for steel pipe. This edition differs from the previous edition mainly as follows: (a) definitions for “defect” and “imperfection” have been added; (b) the product ordering requirements have been revised; (©) the list of acceptable quality programs has been revised (d) the powder manufacturer is now required to certify the minimum flexibility test temperature; (©) a requirement for the monitoring of surface finish has been added (D) the requirements for the measuring of surface profile have been revised; (g) overcoating is no longer an acceptable method of repairing coated pipe; (h) the requirements for the frequency of obtaining production test rings have been revised; @_ the requirements for inspection by the purchaser have been revised; @)_ the requirements for production coating retests have been revised: (K) the requirernents for the repair of coated pipe have been revised; (D the requirements for marking coated pipe have been revised; (an) the requirements for test reports and certificates of compliance have been revised; (A) an alternative procedure for determining moisture content of the epoxy powder by mass loss has been added; and (0). an alternative pycnometer for determining the density of epoxy powder has been added. This is the second edition of CSA Standard 2245.1, External Polyethylene Coating for Pipe. It supersedes € the previous edition published in 1992. CSA Standard Z245.21 deals with the requirements for extemal polyethylene coating for pipe. This edition differs from the previous edition mainly as follows: (2) definitions for “defect” and “imperfection” have been added; (b) the product ordering requirements have been revised; (©) the list of acceptable quality programs has been revised; (@) the requirements for the powdered epoxy primer have been revised; (@) the requirements for the qualification of coating systems have been revised; (D) the requirements for blast cleaning have been revised; (Q) the requirements for inspéction by the purchaser have been revsed; (h) a requirement for the monitoring of surface finish has been added; (i) a requirement for the measuring of surface profile has been added; ()_ the requirements for the direct current potential of the detector used for holiday inspection have been revised; (W) the requirements for the frequency of obtaining production test rings have been revised; ()_ the requirements for the repair of coated pipe have been revised; (mm) the requirements for marking coated pipe have been revised; and (A) the requirements for test reports and certificates of compliance have been revised. ‘These Standards were prepared by the Task Force on Coated Pipe and the Subcommittee on Materials, and formally approved by the Technical Committee on Oil and Gas Industry Pipeline Systems under the jurisdiction of the Standards Steering Committee on Oil and Gas Industry Systems and Materials. April 1998 Notes: o @ ofthe singular does not exclude the plural (and vice versa) when the sense allows. xvi April 198: External Fusion Bond Epoxy Coating for Stee! Pipe/ External Polyethylene Coating for Pipe (2) Although the intended primary application ofthis Standard is stated in its Scope, iis important to note that it remains the responsibilty ofthe users ofthe Standard to judge is sutabilty for their particular purpose. (3) This publication was developed by consensus, which is defined by the CSA Regulations Governing Standardization as “substantial agreement reached by concemed interests. Consensus includes an attempt to remove ail objections and Jmplies much more than the concept ofa simple majority, ut not necessarily unanimity’. It consistent with this

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