Professional Documents
Culture Documents
Geosyntec: Consultants
Geosyntec: Consultants
Prepared for
Renesas Electronics America, Inc.
1001 Murphy Ranch Road
Milpitas, California 95035
Prepared by
Geosyntec Consultants, Inc.
1111 Broadway, 6th Floor
Oakland, California 94607
Prepared for
Renesas Electronics America, Inc.
1001 Murphy Ranch Road
Milpitas, California 95035
Prepared by
Geosyntec Consultants, Inc.
1111 Broadway, 6th Floor
Oakland, California 94607
Stamped 4/15/20
TABLE OF CONTENTS
1. INTRODUCTION ....................................................................................................................1
1.1 Site Background ..............................................................................................................1
1.2 Local Hydrogeology ........................................................................................................1
1.3 Summary of Remedial Actions .......................................................................................2
1.3.1 Soil.......................................................................................................................2
1.3.2 Groundwater ........................................................................................................2
1.3.3 Vapor Intrusion Pathway .....................................................................................3
1.4 Summary of 2019 Activities............................................................................................4
1.4.1 Field Activities ....................................................................................................4
1.4.2 Reporting Activities ............................................................................................4
4. PROBLEMS ENCOUNTERED.............................................................................................11
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LIST OF TABLES
Table 1: SCGWR System Performance Summary
Table 2: Summary of Extraction Well and Monitoring Well Construction Details
Table 3: Groundwater Levels – September 2019
Table 4: Analytical Results – 2018 Biennial Groundwater Monitoring Event
Table 5: Analytical Results – 2019 NEC-1AE Quarterly Sampling
LIST OF FIGURES
Figure 1: Site Location Map
Figure 2: Site Layout
Figure 3: Groundwater Extracted and Mass of VOCs Removed
Figure 4: Groundwater Elevations in Selected Monitoring Wells
Figure 5: Groundwater Elevation Contour Map and Capture Zone – Third Quarter 2019
Figure 6: Simulated A Aquifer Capture Zone – First Quarter 2019
Figure 7: Simulated A Aquifer Capture Zone – Second Quarter 2019
Figure 8: Simulated A Aquifer Capture Zone – Third Quarter 2019
Figure 9: Simulated A Aquifer Capture Zone – Fourth Quarter 2019
Figure 10: TCE Concentration Contour Map – 2018 Biennial Groundwater Monitoring Event
Figure 11: VOC Concentrations in Groundwater
Figure 12: VOC Concentrations in Well NEC-1AE
Figure 13: TCE Concentration Trend Analysis
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LIST OF APPENDICES
Appendix A: 2019 Annual Report Remedy Performance Checklist
Appendix B: Capture Zone Calculations
Appendix C: 2019 Laboratory Analytical Reports
Appendix D: Annual Quality Assurance Report
Appendix E: VOC Concentration Mann-Kendall Trend Analysis
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1. INTRODUCTION
This Annual Progress Report (Report) summarizes facility-specific environmental work and
related activities that were performed at 501 Ellis Street, Mountain View, California (the Site)
during the period of January 1 through December 31, 2019. The work described in this Report
was performed pursuant to Sections XV A&B of Comprehensive Environmental Response,
Compensation, and Liability Act (CERCLA) §106 Order, United States Environmental
Protection Agency (EPA) Docket No. 91-4, as amended on September 16, 2011 (106 Order)
(EPA, 1990a; 2011). Geosyntec Consultants, Inc. (Geosyntec) prepared this Report on behalf of
Renesas Electronics America, Inc. (Renesas) in accordance with the EPA May 6, 2005, email
correspondence prescribing 2004 and future Annual Progress Report contents (EPA, 2005). The
2019 Annual Report Remedy Performance Checklist is included as Appendix A. In addition,
this Report includes the annual progress reporting requirements prescribed in Section 2.6.2 of the
Statement of Work for Remedial Design and Remedial Action to Address the Vapor Intrusion
Pathway included in the amended 106 Order (EPA, 2011).
1.1 Site Background
The Site is located at 501 Ellis Street, Mountain View, California, and lies within the area
bounded by Middlefield Road, Ellis Street, Whisman Road, and United States Highway 101 in
Mountain View, California (Figure 1). This area includes historical locations of semiconductor
manufacturing and other industrial activities, including the Site. In 1985, the EPA identified this
area as the Middlefield-Ellis-Whisman (MEW) Superfund Study Area. Numerous investigations
at the properties within the MEW Study Area have been conducted, and extensive soil and
groundwater remedial activities have been implemented and are ongoing at many of the
properties.
The Site is approximately 2 acres in size. A single-story building, constructed in 1967, occupies
about 28,000 square feet of the western portion of the property, and a paved parking area
occupies the eastern portion of the property (Figure 2). From 1968 to 1978, Electronic Arrays
Corporation operated at the Site and manufactured semiconductor devices and related
components. Solvents and other chemicals were used in the manufacturing process. From 1978
until April 1984, NEC Electronics America, Inc. (NEC) operated at the Site. The 501 Ellis Street
building is currently used for office and meeting space.
In 1982, NEC initiated a groundwater monitoring and soil sampling program at the Site in
response to a California Regional Water Quality Control Board (RWQCB) investigation of all
companies that used underground chemical tanks in their production processes prior to January
1, 1975. Between 1982 and 1990, NEC completed several Site investigations that identified the
presence of volatile organic compounds (VOCs), in particular trichloroethene (TCE), in the soil
and groundwater beneath the Site. Soil and groundwater remedial actions were implemented in
the 1990s, and groundwater remedial actions are ongoing (Section 1.3).
1.2 Local Hydrogeology
The Site is located on a relatively flat tract of land that slopes gently to the north towards San
Francisco Bay, located approximately 2 miles away.
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Sediments beneath the Site are composed of varying proportions of unconsolidated to poorly
consolidated gravel, sand, silt, and clay typical of alluvial, estuarine, and bay deposits. The
interbedded materials are generally lenticular, laterally gradational, and heterogeneous (Bechtel
Environmental, Inc. [Bechtel], 1996).
Water-bearing materials beneath the Site and the larger MEW Study Area are divided into an
upper aquifer zone, comprised of the A and B aquifers and their associated aquitards, and a lower
aquifer zone, comprised of the C and deeper aquifers and their associated aquitards (Geosyntec,
2014). The A aquifer at the Site is approximately 15 to 20 feet thick, extending from a depth of
about 10 feet below ground surface (bgs) to a maximum depth of about 30 feet bgs. Based on
geologic logs prepared during the drilling of Site wells, the A aquifer is composed of silty sand,
sand, and gravel, with interbedded layers of silty clay, silt, and gravelly silt.
1.3 Summary of Remedial Actions
Remedial actions at the Site have reduced soil concentrations of TCE to below cleanup levels
specified in the MEW Study Area Record of Decision (ROD) and two associated Explanations of
Significant Differences (ESDs) (EPA, 1989; 1990b; 1996) and continue to control and reduce the
concentrations of VOCs in groundwater. Investigation and remediation efforts at the Site have
been documented in several reports (e.g., Bechtel, 1992; 1996) and are periodically updated in
progress reports to EPA, as required by the 106 Order (EPA, 2011).
1.3.1 Soil
On September 6, 1991, NEC submitted a proposed final remedial design for treating VOCs in
unsaturated soils located east of the Site building. Applicable treatment technologies for shallow
unsaturated soils at the MEW Study Area are specified in the ROD and consist of soil removal
and aeration or soil vapor extraction. NEC elected to excavate and send unsaturated soils with
TCE concentrations greater than the cleanup level of 0.5 milligrams per kilogram (mg/kg) offsite
for treatment and disposal. Soil excavations are complete, and NEC received EPA approval of
the soil investigations and remediation at the Site in 1995 (EPA, 2004).
1.3.2 Groundwater
In October 1997, NEC began operating the Source Control Groundwater Remediation (SCGWR)
system at the Site. The SCGWR system is a groundwater extraction and treatment system
designed to control, contain, and extract VOCs at the Site and to complement the regional
groundwater remediation program (RGRP) for the MEW Study Area. The SCGWR system has
been operated continuously (i.e., shut down only for routine and non-routine maintenance) since
startup in October 1997.
As originally designed, the SCGWR system extracted groundwater from the A aquifer at the Site
for treatment with granular activated carbon prior to discharge to the storm drain. On September
3, 2008, Geosyntec submitted an Optimization Evaluation for the SCGWR system on behalf of
NEC (Geosyntec, 2008). The Optimization Evaluation recommended the following
modifications to the SCGRW system:
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During a November 3, 2008, meeting between EPA and Geosyntec, EPA concurred with these
recommendations, provided that:
1. Contingencies were given for restart of NEC-1AE if groundwater capture became
inadequate; and
2. A monitoring program for evaluating groundwater capture was implemented.
A plan for implementing the Optimization Evaluation recommendations and addressing EPA
comments was provided in the 2008 Annual Progress Report for the Site (Geosyntec, 2009). The
Optimization Evaluation recommendations were implemented in 2009 and the SCGWR system
has operated in the optimized configuration since that time. Operation of the optimized SCGWR
system includes direct discharge of extracted groundwater to the Palo Alto RWQCP in
accordance with City of Mountain View Wastewater Discharge Permit ID Number 925.
1.3.3 Vapor Intrusion Pathway
In 2012, the potential for vapor intrusion at the 501 Ellis Street building was evaluated, including
collection of indoor air, outdoor air, and sub-slab vapor samples (Geosyntec, 2012). The
sampling results indicated that concentrations of VOCs in indoor air were below cleanup levels
specified in the MEW Study Area ROD Amendment for the Vapor Intrusion Pathway (EPA,
2010) but were greater than outdoor air concentrations. Based on these findings, a preliminary
recommendation was made that the building at 501 Ellis Street be categorized as Tier 3A, which
would require long-term indoor air monitoring and institutional controls.
Tenant improvement construction work was subsequently completed inside the 501 Ellis Street
building in 2014. The construction work included temporarily opening the building slab,
trenching for the installation of sub slab utilities, slab repair, and sealing of potential conduits
that could act as preferential pathways for vapor intrusion. Indoor and outdoor air sampling was
conducted by Iris Environmental (Iris) prior to and following the tenant improvement
construction activities. MEW Study Area chemicals of potential concern (COPCs) were not
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detected in indoor air samples collected following construction, except for Freon 113, which was
detected at comparable concentrations in outdoor air (Iris, 2015).
The results from the samples collected by Iris indicate that a Tier 3B categorization, which is
limited to implementation of institutional controls, is appropriate for the 501 Ellis Street building
with completion of the 2014 tenant improvement activities. A final determination of the vapor
intrusion response action tier for the Site will be made following EPA approval of the Revised
Site-Wide Vapor Intrusion Sampling and Analysis Work Plan for Response Action Tiering
(Haley & Aldrich, Inc. [Haley & Aldrich], 2013).
1.4 Summary of 2019 Activities
The following section summarizes field and reporting activities that were completed for the Site
in 2019.
1.4.1 Field Activities
• February 12. Locus Technologies (Locus) replaced the submersible pump at NEC-
27AE.
• March 4, June 20, September 11, and December 10. Locus performed quarterly
operation and maintenance (O&M) for the SCGWR system. As part of each O&M
event, a sample was collected from the SCGWR system effluent as required by the
City of Mountain View Wastewater Discharge Permit and from well NEC-1AE as
specified in the revised SCGWR extraction and monitoring program (Geosyntec,
2009). The system effluent samples were analyzed for VOCs by EPA Method 624
and total dissolved solids (TDS) by Method SM 2540C. The NEC-1AE samples were
analyzed for VOCs by EPA Method 8260B.
• September 19. Annual groundwater levels were measured in Site monitoring wells.
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2. GROUNDWATER REMEDY
The following sections present a summary of 2019 O&M activities, results of a hydraulic control
and capture zone analysis for the SCGWR system, and results from the most recent groundwater
sampling at the Site.
2.1 SCGWR System Description
The SCGWR system is a groundwater extraction and treatment system designed to control,
contain, and extract VOCs from the A aquifer at the Site and to complement the MEW Study
Area RGRP extraction program. The SCGWR system has operated since October 1997. On May
13, 2009, the modifications to the SCGRW system recommended in the 2008 Optimization
Evaluation (Section 1.3) were completed. These modifications included adjustments to
groundwater extraction rates and converting the system to directly discharge untreated
groundwater to the sanitary sewer for treatment at the Palo Alto RWQCP under a City of
Mountain View wastewater discharge permit.
2.2 SCGWR System Flow Rates and Mass Removal
Performance of the SCGWR system, including average flow rates, extraction totals, and
calculated VOC mass removal is summarized in Table 1. The data was collected monthly
through 2009 and quarterly since. As of December 30, 2019, approximately 49,950,000 gallons
of groundwater had been extracted since startup of the SCGWR system. The average daily
processing rate since startup is 6,435 gallons per day (gpd), or 4.47 gpm. Since system
optimization in 2009, the average daily processing rate has been 3.94 gpm, with an average 2019
daily processing rate of 4.05 gpm.
Approximately 1.6 pounds of VOCs were removed by the SCGWR system in 2019. The total
mass of VOCs removed by the treatment system since startup is approximately 57 pounds.
Figure 3 shows the cumulative volume of groundwater extracted and mass of VOCs removed
since system startup.
2.3 Hydraulic Control and Capture Zone Analysis
Site monitoring and extraction wells are completed within the A aquifer (Table 2). Depth to
groundwater ranged from 6.62 to 21.45 feet below top of casing (btoc) during the September
2019 gauging event (Table 3). A hydrograph of groundwater elevations in selected monitoring
wells across the Site is shown in Figure 4.
2.3.1 Capture Zone Analysis Methods
Capture of groundwater beneath the Site was estimated using two methods.
Javandel and Tsang Method. The first method is the analytical solution of Javandel and Tsang
(1987), which consists of calculating a stagnation point and capture zone width, followed by
projection of streamlines perpendicular to groundwater elevation contours. The 2019 capture
zone calculations using this approach are provided in Appendix B.
Numerical Modeling Method. The second method for estimating groundwater capture uses a
steady-state numerical simulation of groundwater flow incorporating particle tracking.
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In addition to the decreasing TCE concentration trends, seven wells at the Site show increasing
cis-1,2-DCE concentration trends (Appendix E), which indicates that natural attenuation
processes at the Site are resulting in the reductive dechlorination of TCE.
2.4.2 Data Quality Assurance Summary
Quality control results for samples collected in 2019 are summarized in Appendix D.
• Percent recoveries and relative percent differences (RPDs) for laboratory control
spikes were within project goals (Table D-1).
• VOCs were not detected in trip or laboratory blanks (Table D-2).
• During the first quarter 2019 O&M event, a duplicate sample was collected at
monitoring well NEC-1AE. The average of the RPD values for analytes detected in
the primary and duplicate samples was 10.2%, which is well below the project RPD
goal of less than 35% (Table D-3).
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4. PROBLEMS ENCOUNTERED
The extraction rate at NEC-27AE was below the target pumping rate of 2 gpm in January and
February 2019. In response, the submersible pump in the well was replaced on February 12,
2019, and the extraction rate increased to approximately 2 gpm. During the fourth quarter 2019,
the pumping rate at NEC-27AE decreased to a rate of 1.74 gpm in December of 2019. In
response, NEC-27AE and its associated conveyance pipeline will be chemically treated in early
2020.
No additional problems related to operation of the SCGWR system were encountered in 2019.
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6. OPTIMIZATION PROGRESS
As described in Section 1.3, Renesas has implemented the groundwater remedy optimizations
recommended in the Optimization Evaluation for 501 Ellis Street (Geosyntec, 2008).
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8. FOLLOW-UP ACTIONS
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10. REFERENCES
Bechtel Environmental, Inc. (Bechtel). 1989. Phase III Hydrogeologic Investigation, Field
Documentation Report. September.
Bechtel. 1992. Soil Remediation Report for 501 Ellis Street, Mountain View. March.
Bechtel. 1996. Source Control Groundwater Remediation Final Design, 501 Ellis Street,
Mountain View. 26 August.
Driscoll. 1986. Groundwater and Wells, Second Ed. published by Johnson Division, St. Paul,
Minnesota.
Geosyntec Consultants, Inc. (Geosyntec). 2001. Evaluation of Extraction Well NEC-22AE. 31
August.
Geosyntec. 2008. Optimization Evaluation, 501 Ellis Street, Source Control Groundwater
Remediation System, Mountain View, California. 3 September.
Geosyntec. 2009. 2008 Annual Progress Report, NEC Electronics America, Inc. 501 Ellis Street,
Mountain View, California. 15 April.
Geosyntec. 2012. Results of Summer 2012 Investigation of Potential Vapor Intrusion Pathway
and Response Action Work Plan. 21 December.
Geosyntec. 2014. 2013 Annual Progress Report, Middlefield-Ellis-Whisman Regional
Groundwater Remediation Program, Mountain View, California. 15 April.
Geosyntec, 2015. “Request for Reduction in Groundwater Monitoring Frequency, Middlefield-
Ellis-Whisman Study Area, Mountain View, California.” February 13.
Haley & Aldrich, Inc. 2013. Revised Site-Wide Vapor Intrusion Sampling and Analysis Work
Plan for Response Action Tiering, Middlefield-Ellis-Whisman Superfund Area, Mountain
View, California and Moffett Field. 22 March.
Iris Environmental (Iris). 2015. Summary Report of Soil Management Plan Implementation for
Subsurface Improvement Activities Conducted at 501 and 515 Ellis Street, Mountain View.
12 March.
Javandel, I., and C.F. Tsang. 1987. “Capture-Zone Type Curves: A Tool for Aquifer Cleanup.”
Ground Water, 24(5), 616-625.
United States Environmental Protection Agency (EPA). 1989. Record of Decision, Fairchild,
Intel, and Raytheon Sites, Middlefield-Ellis-Whisman Study Area, Mountain View,
California, Superfund Records Center Document No. 2807-02332. 9 June.
EPA. 1990a. Administrative Order for Remedial Design and Remedial Action, U.S. EPA Docket
No. 91-4. 29 November.
EPA. 1990b. EPA Superfund Explanation of Significant Differences: Middlefield-Ellis-Whisman
Study Area, Mountain View, California. 1 September.
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TABLES
Discharge Discharge Total Discharge Average Rate Influent VOCs Effluent VOCs VOCs Removed
Period (days) (gallons) (gpd) (µg/L) (µg/L) (lbs)
Startup Oct 16, 1997 0 0 NA NA NA 0.00
Oct 16- Nov 13, 1997 27 109,340 4,050 152 0 0.14
Nov 14- Dec 17, 1997 34 153,010 4,500 202 0 0.26
Dec 18, 1997-Jan 15, 1998 29 152,110 5,245 134 0 0.17
Jan 16-Feb 19, 1998 35 194,870 5,568 138.1 0 0.22
Feb 20-Mar 19, 1998 28 149,510 5,340 144 1.4 0.18
Mar 20-Apr 22, 1998 34 157,430 4,630 137.4 0 0.18
Apr 23-May 28, 1998 36 104,370 2,899 69.9 0 0.06
May 29-June 23, 1998 25 95,110 3,804 110 15.28 0.08
June 24-July 22, 1998 29 145,370 5,013 83 0 0.10
July 23-Aug 20, 1998 29 118,290 4,107 60.8 0 0.06
Aug 21-Sep 23, 1998 34 129,190 3,791 196.6 1.1 0.21
Sep 24-Oct 28, 1998 35 277,800 7,919 125.3 0 0.29
Oct 29-Nov 30, 1998 32 283,740 8,890 110 0 0.26
Dec 1-Dec 15, 1998 15 120,120 7,959 146.2 0 0.15
Dec 16, 1998 - Jan 27, 1999 42 326,540 7,777 168.7 0 0.46
Jan 28 - Feb 24, 1999 27 233,490 8,721 167.9 0 0.33
Feb 25 - Mar 24, 1999 27 242,060 8,956 195 0 0.39
Mar 25 - Apr 28, 1999 35 289,730 8,253 159.4 0 0.39
Apr 21 - May 26, 1999 30 237,970 7,953 202.1 0 0.40
May 27 - June 23, 1999 26 235,210 9,040 182.4 0 0.36
June 23 - July 28, 1999 35 292,100 8,325 178.4 2.8 0.43
July 29 - Aug 25, 1999 28 228,510 8,209 184 3.3 0.34
Aug 26 - Sep 22, 1999 28 160,730 5,730 57.9 0 0.08
Sep 23 - Oct 27, 1999 36 224,710 6,242 184 3.7 0.34
Oct 28 - Nov 23, 1999 26 210,000 8,024 180.4 0 0.32
Nov 24 - Dec 22, 1999 29 222,120 7,696 231.9 2.2 0.43
Dec 23, 1999 - Jan 26, 2000 35 275,070 7,872 201.3 1.2 0.46
Jan 27 - Feb 23, 2000 28 212,950 7,608 208.6 8.8 0.35
Feb 24 - Mar 22, 2000 27 202,020 7,493 210 0 0.35
Mar 23 - Apr 26, 2000 35 260,110 7,432 186.5 0 0.40
Apr 27 - May 31, 2000 35 252,920 7,226 201.5 0 0.43
June 1 - June 28, 2000 28 190,590 6,807 170.1 0 0.27
June 29 - July 26, 2000 28 187,760 6,706 212.8 0 0.33
July 27 - Aug 23, 2000 28 183,790 6,564 204.7 0 0.31
Aug 24 - Sep 27, 2000 35 229,820 6,566 194.9 0 0.37
Sep 28 - Oct 26, 2000 29 175,300 6,325 138.5 0 0.20
Oct 27 - Nov 22, 2000 27 169,590 6,014 213.0 202.7 0.01
Nov 23 - Dec 20, 2000 28 141,930 5,046 159.7 0 0.19
Dec 21, 2000 - Jan 24, 2001 35 207,970 6,498 213.4 0 0.37
Jan 25 - Feb 28, 2001 35 215,600 6,151 178.3 0 0.32
Mar 1 - Mar 28, 2001 28 176,650 6,314 159.4 0 0.23
Mar 29 - Apr 25, 2001 28 155,570 5,504 181.5 0 0.24
Apr 26 - May 30, 2001 35 192,810 5,382 164.4 0 0.26
May 31 - June 27, 2001 28 136,610 5,013 202 0 0.23
June 28 - July 25, 2001 28 173,810 6,439 226.9 0 0.33
July 26 - Aug 22, 2001 28 187,720 6,697 237.4 0 0.37
Aug 23 - Sep 26, 2001 35 232,980 6,668 217.4 0 0.42
Sep 27, 2001 - Oct 24, 2001 28 186,960 6,672 225.4 0 0.35
Oct 25, 2001 - Nov 28, 2001 35 214,470 6,125 223.8 0 0.40
Nov 29, 2001 - Dec 19, 2001 21 117,130 5,580 176.6 0 0.17
Dec 20, 2001 - Jan 16, 2002 28 163,130 5,549 210.7 0 0.29
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Table 1 Geosyntec Consultants
Discharge Discharge Total Discharge Average Rate Influent VOCs Effluent VOCs VOCs Removed
Period (days) (gallons) (gpd) (µg/L) (µg/L) (lbs)
Jan 17, 2002 - Feb 25, 2002 40 215,500 5,210 159.1 0 0.29
Feb 26, 2002 - Mar 20, 2002 23 136,160 4,643 238.4 0 0.27
Mar 21, 2002 - Apr 15, 2002 26 94,470 4,544 140.5 0 0.11
Apr 16, 2002 - May 22, 2002 37 175,070 5,315 202.7 0 0.30
May 23, 2002 - June 19, 2002 28 201,600 7,156 207.4 0 0.35
June 20, 2002 - July 10, 2002 21 255,090 9,769 202 0 0.43
July 11, 2002 - Aug 21, 2002 42 193,600 6,518 141.8 0 0.23
Aug 22, 2002 - Sep 18, 2002 27 143,530 4,870 201.2 0 0.24
Sep 19, 2002 - Oct 17, 2002 28 175,390 5,770 203.8 0 0.30
Oct 18, 2002 - Nov 20, 2002 33 250,780 6,920 201 0 0.42
Nov 21, 2002 - Dec 18, 2002 27 184,290 7,009 137.2 0 0.21
Dec 19, 2002 - Jan 22, 2003 35 220,900 6,330 189.3 0 0.35
Jan 23, 2003 - Feb 19, 2003 28 166,230 6,183 226.7 0 0.31
Feb 20, 2003 - Mar 19, 2003 28 179,360 6,090 166.3 0 0.25
Mar 20, 2003 - Apr 28, 2003 39 207,300 5,504 146.7 0 0.25
Apr 29, 2003 - May 19, 2003 21 131,770 6,315 172.7 0 0.19
May 20, 2003 - June 30, 2003 41 227,380 5,732 160 0 0.30
July 1, 2003 - Aug 5, 2003 36 230,950 6,186 186 0 0.36
Aug 6, 2003 - Sep 3, 2003 28 160,410 5,960 143.4 0 0.19
Sep 4, 2003 - Sep 30, 2003 26 166,270 6,162 195.7 0 0.27
Oct 1, 2003 - Nov 5, 2003 35 238,150 6,608 186 0 0.37
Nov 6, 2003 - Dec 5, 2003 29 186,150 6,225 200.4 0 0.31
Dec 6, 2003 - Dec 31, 2003 25 164,280 6,315 201.4 0 0.28
Jan 1, 2004 - Jan 28, 2004 27 168,040 6,235 199.1 0 0.28
Jan 29, 2004 - Feb 27, 2004 29 183,810 6,169 167.1 0 0.26
Feb 28, 2004 - Mar 29, 2004 30 191,270 6,587 168.7 0 0.27
Mar. 30, 2004 - Apr. 22, 2004 23 149,410 6,546 173.8 0 0.22
Apr. 23, 2004 - May 19, 2004 26 174,000 6,500 168.6 0 0.24
May 20, 2004 - June 21, 2004 32 201,810 6,361 156.3 0 0.26
June 22, 2004 - July 21, 2004 30 171,870 5,729 144.8 0 0.21
July 22, 2004 - Aug 17, 2004 27 145,690 5,396 167.5 0 0.20
Aug 18, 2004 - Sep 22, 2004 36 162,960 4,527 173.3 0 0.24
Sep 23, 2004 - Oct 20, 2004 28 145,290 5,189 131.9 0 0.16
Oct 21, 2004 - Nov 15, 2004 26 182,140 7,005 152.9 0 0.23
Nov 16, 2004 - Dec 22, 2004 37 257,700 6,965 150.5 0 0.32
Dec 23, 2004 - Jan 19, 2005 28 205,800 7,350 144.9 0 0.25
Jan 20, 2005 - Feb 15, 2005 27 185,870 6,884 147.9 0 0.23
Feb 16, 2005 - Mar 28, 2005 41 283,820 6,922 149.1 0 0.35
Mar 29, 2005 - Apr 20, 2005 23 153,380 6,669 150.6 0 0.19
Apr 21, 2005 - May 25, 2005 35 255,110 7,289 144.2 0 0.31
May 26, 2005 - June 27, 2005 33 239,120 7,246 149.1 0 0.30
June 28, 2005 - July 25 2005 28 184,260 6,581 153.7 0 0.24
July 26, 2005 - Aug 15, 2005 21 152,620 7,268 139.2 0 0.18
Aug 16, 2005 - Oct 3, 2005 49 378,200 7,718 163.5 0 0.52
Oct 4, 2005 - Oct 24, 2005 21 160,050 7,621 149.8 0 0.20
Oct 25, 2005 - Nov 21, 2005 28 208,170 7,435 162.7 0 0.28
Nov 22, 2005 - Dec 30, 2005 39 302,470 7,756 158.5 0 0.40
Dec 31, 2005 - Jan 30, 2006 31 237,010 7,645 143.1 0 0.28
Jan 31, 2006 - Feb 27, 2006 28 205,260 7,331 134.3 0 0.23
Feb 28, 2006 - Apr 3, 2006 35 246,150 7,033 153.9 0 0.32
Apr 4, 2006 - Apr 24, 2006 21 150,040 7,145 145.6 0 0.18
Apr 25, 2006 - May 30, 2006 36 252,130 7,004 142.8 0 0.30
May 31, 2006 - June 30, 2006 31 205,290 6,622 156 0 0.27
July 1, 2006 - Aug 7, 2006 37 247,740 6,696 129.4 0 0.27
Aug 8, 2006 - Sep 5, 2006 28 183,410 6,550 128.6 0 0.20
Page 2 of 4
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 1 - SCGWR Info
Table 1 Geosyntec Consultants
Discharge Discharge Total Discharge Average Rate Influent VOCs Effluent VOCs VOCs Removed
Period (days) (gallons) (gpd) (µg/L) (µg/L) (lbs)
Sep 6, 2006 - Oct 2, 2006 26 182,180 7,007 158.6 0 0.24
Oct 3, 2006 - Nov 6, 2006 34 232,190 6,829 145.7 0 0.28
Nov 7, 2006 - Dec 4, 2006 27 179,870 6,662 170.9 0 0.26
Dec 5, 2006 - Jan 2, 2007 28 181,650 6,488 174.5 0 0.26
Jan 3, 2007 - Feb 1, 2007 29 193,140 6,660 146 0 0.24
Feb 2, 2007 - Mar 5, 2007 31 200,650 6,473 135.2 0 0.23
Mar 6, 2007 - Apr 2, 2007 27 176,910 6,552 134.9 0 0.20
Apr 2, 2007 - May 7, 2007 35 235,030 6,715 148 0 0.29
May 7, 2007 - June 4, 2007 28 200,670 7,167 145.8 0 0.24
June 4, 2007 - June 29, 2007 25 180,590 7,224 134.5 0 0.20
June 29, 2007 - July 30, 2007 32 230,300 7,197 127.6 0 0.25
July 30, 2007 - Sept 4, 2007 36 281,730 7,826 138 0 0.32
Sept 4,2007 - Oct 1, 2007 27 184,930 6,849 164.8 0 0.25
Oct 2, 2007 - Oct 29, 2007 28 220,880 7,889 127.4 0 0.23
Oct 30, 2007 - Nov 26, 2007 28 221,870 7,924 115.5 0 0.21
Nov 27, 2007 - Dec 31, 2007 35 282,300 8,066 145.8 0 0.34
Jan 1, 2008 - Jan 28, 2008 28 204,940 7,319 156.9 0 0.27
Jan 29, 2008 - Feb 25, 2008 28 214,970 7,678 141.8 0 0.25
Feb 26, 2008 - Mar 31, 2008 35 270,880 7,739 137.3 0 0.31
Apr 1, 2008 - Apr 28, 2008 27 215,770 7,991 144.9 0 0.26
Apr 29, 2008 - May 27, 2008 28 233,230 8,330 148.9 0 0.29
May 28, 2008 - June 30, 2008 33 215,260 6,523 135.8 0 0.24
July 1, 2008 - July 28, 2008 27 213,290 7,900 145.5 0 0.26
July 29, 2008 - Sep 2, 2008 35 271,770 7,765 157.2 0 0.36
Sep 3, 2008 - Sep 29, 2008 26 206,440 7,940 147.5 0 0.25
Sep 30, 2008 - Nov 3, 2008 34 255,440 7,513 145.6 0 0.31
Nov 4, 2008 - Dec 1, 2008 27 201,980 7,481 160.9 0 0.27
Dec 2, 2008 - Dec 29, 2008 27 199,220 7,379 146.5 0 0.24
Dec 30, 2008 - Feb 2, 2009 35 262,400 7,497 144.5 0 0.32
Feb 3, 2009 - March 2, 2009 28 208,760 7,456 132 0 0.23
March 3, 2009 - April 6, 2009 35 261,780 7,479 123.5 0 0.27
Apr 7, 2009 - May 4, 2009 28 202,690 7,239 133.5 0 0.23
May 5, 2009 - Jun 1, 2009 28 172,870 6,174 133.4 0 0.19
Jun 2, 2009 - Jun 29,2009 28 150,880 5,389 --* 98.6* 0.12
Jun 30, 2009 - Oct 5,2009 98 538,960 5,500 -- 114.2 0.51
Oct 6, 2009 - Dec 31,2009 87 483,970 5,563 -- 119.6 0.48
Jan 1, 2010 - March 17, 2010 76 412,870 5,433 -- 119.0 0.41
March 18, 2010 - June 30, 2010 105 577,330 5,498 -- 110.6 0.53
July 1, 2010 - Sep 14, 2010 76 412,240 5,424 -- 129.3 0.44
Sep 14, 2010 - Dec 30, 2010 108 537,210 4,974 -- 126.3 0.57
Dec 31, 2010 - Mar 14, 2011 73 367,480 5,034 -- 124.3 0.38
Mar 15, 2011 - Jun 13, 2011 91 493,950 5,428 -- 119.7 0.49
Jun 14, 2011 - Sep 12, 2011 91 531,530 5,841 -- 106.7 0.47
Sep 13, 2011 - Dec 12, 2011 91 521,590 5,732 -- 117.5 0.51
Dec 13, 2011 - Mar 14, 2012 92 515,530 5,604 -- 104.7 0.45
Mar 15, 2012 - Jun 18, 2012 95 515,360 5,425 -- 111.1 0.48
Jun 19, 2012 - Sep 10, 2012 83 466,110 5,616 -- 123.2 0.48
Sep 11, 2012 - Dec 17, 2012 97 564,160 5,816 -- 128.8 0.61
Dec 17, 2012 - Mar 13, 2013 86 493,330 5,736 -- 130.8 0.54
Mar 13, 2013 - Jun 17, 2013 96 570,110 5,939 -- 106.5 0.51
Jun 17, 2013 - Sep 27, 2013 102 639,190 6,267 -- 108.4 0.58
Sep 27, 2013 - Dec 31, 2013 95 626,700 6,597 -- 114.0 0.60
Jan 1, 2014 - Mar 26, 2014 85 555,620 6,537 -- 111.5 0.52
Mar 27, 2014 - Jun 23, 2014 89 566,410 6,364 -- 103.9 0.49
Jun 24, 2014 - Sep 30, 2014 99 616,450 6,227 -- 104.0 0.53
Oct 1, 2014 - Dec 31, 2014 92 530,290 5,764 -- 96.5 0.43
Page 3 of 4
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 1 - SCGWR Info
Table 1 Geosyntec Consultants
Discharge Discharge Total Discharge Average Rate Influent VOCs Effluent VOCs VOCs Removed
Period (days) (gallons) (gpd) (µg/L) (µg/L) (lbs)
Jan 1, 2015 - Mar 30, 2015 89 453,480 5,095 -- 103.2 0.39
Mar 31, 2015 - Jun 29, 2015 91 468,620 5,150 -- 98.0 0.38
Jun 30, 2015 - Sep 30, 2015 93 457,910 4,924 -- 131.0 0.50
Oct 1, 2015 - Dec 22, 2015 83 431,260 5,196 -- 111.4 0.40
Dec 23, 2015 - Mar 29, 2016 98 590,480 6,025 -- 98.9 0.49
Mar 30, 2016 - Jun 29, 2016 92 382,680 4,160 -- 106.6 0.34
Jun 30, 2016 - Sep 30, 2016 93 382,050 4,108 -- 82.8 0.26
Oct 1, 2016 - Dec 28, 2016 89 465,360 5,229 -- 95.2 0.37
Dec 29. 2016 - Mar 31, 2017 93 441,090 4,743 -- 89.5 0.33
Apr 1, 2017 - Jun 30, 2017 91 607,390 6,675 -- 87.0 0.44
Jul 1, 2017 - Sept 29, 2017 91 553,210 6,079 -- 98.0 0.45
Sept 30, 2017 - Dec 29, 2017 91 597,730 6,568 -- 101.0 0.50
Dec 30. 2017 - Mar 30, 2018 91 627,540 6,896 -- 99.4 0.52
Mar 31, 2018 - Jun 29, 2018 91 561,650 6,172 -- 82.2 0.39
Jun 30, 2018 - Sept 28, 2018 91 544,940 5,988 -- 86.7 0.39
Sept 29, 2018 - Dec 28, 2018 91 548,840 6,031 -- 100.6 0.46
Dec 29, 2018 - Mar 29, 2019 91 548,900 6,032 -- 80.7 0.37
Mar 30, 2019 - Jun 28, 2019 91 527,980 5,802 -- 85.5 0.38
Jun 29, 2019 - Sept 30, 2019 94 533,280 5,673 -- 90.9 0.40
Oct 1, 2019 - Dec 30, 2019 91 530,970 5,835 -- 101.5 0.45
TOTALS 8,065 49,950,420 6,435 -- -- 57.21
Notes:
*Beginning 13 May 2009, extracted groundwater is discharged without pre-treatment to the sanitary sewer under City of Mountain View Wastewater Discharge
Permit Number 925. At this time, collection of influent samples was discontinued. Quarterly effluent samples are collected as required by the City of Mountain
View Wastewater Discharge Permit. VOC recovery is estimated quarterly based on effluent concentration and total discharge.
µg/L - micrograms per liter
gpd - gallons per day
lbs - pounds
NA - Not Available
SCGWR - Source Control Groundwater Remediation
VOCs - volatile organic compounds
Page 4 of 4
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 1 - SCGWR Info
Geosyntec Consultants
Table 2
Summary of Extraction Well and Monitoring Well
Construction Details
501 Ellis Street, Mountain View, California
Reference Depth of
Well Screen
Elevation Screened
Well ID Date Installed Diameter Slot Size Aquifer Zone
(top of PVC) Interval
(inches) (inches)
(feet) (feet)
Extraction Wells
NEC-1AE May 1997 43.90 6 0.02 12.8-27.8 A
NEC-27AE May 1997 43.73 6 0.02 12.7-27.7 A
NEC-28AE April 2002 42.27 6 0.02 9-29 A
Monitoring Wells
NEC-1A September 1982 44.47 2 0.01 5-25 A
NEC-3A October 1985 43.76 4 0.02 24.95-28.72 A
NEC-7A October 1983 43.80 2 0.02 6-26.5 A
NEC-8A October 1983 42.29 2 0.02 5-25 A
NEC-9A October 1983 43.14 2 0.02 5-30 A
NEC-10A August 1984 39.43 2 0.02 10-30 A
NEC-11A August 1984 45.97 2 0.02 10-30 A
NEC-12A October 1985 44.24 4 0.02 18.90-28.32 A
NEC-20A January 1989 46.62 4 0.02 26-28 A
NEC-21A December 1988 44.06 4 0.02 26-28 A
NEC-22A May 1989 43.17 4 0.02 25-27 A
NEC-23A May 1989 43.77 4 0.02 26-28 A
NEC-24A December 1991 44.50 4 0.02 15.8-25.8 A
NEC-25A March 1996 42.30 4 0.02 17.19-27.19 A
NEC-26A March 1996 43.65 4 0.02 28.24-33.24 A
NEC-PZ-1A April 1999 42.47 2 0.02 11-16 A
NEC-PZ-2A April 1999 43.02 2 0.02 9-14 A
NEC-PZ-3A April 1999 43.16 2 0.02 8-13 A
Notes:
PVC - polyvinyl chloride
Page 1 of 1
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 2 - Well Info
Geosyntec Consultants
Table 3
Groundwater Levels - September 2019
501 Ellis Street, Mountain View, California
Notes:
Water levels were collected on September 19, 2019
1
Regional Groundwater Remediation Program (RGRP) monitoring wells.
PVC - polyvinyl chloride
Page 1 of 1
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 3 - Sept20 GWE
Geosyntec Consultants
Table 4
Analytical Results - 2018 Biennial Groundwater Monitoring Event
501 Ellis Street, Mountain View, California
WELL ID NEC-1A NEC-7A NEC-8A NEC-9A NEC-10A NEC-11A NEC-12A NEC-20A NEC-21A NEC-22A NEC-23A NEC-23A(dup) NEC-24A NEC-25A NEC-26A NEC-27AE NEC-28AE NEC-PZ-1A NEC-PZ-2A NEC-PZ-3A
DATE OF SAMPLE 10/11/18 10/11/18 10/11/18 10/11/18 10/11/18 10/11/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/06/18 10/11/18 10/11/18 10/11/18
UNITS µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Bromodichloromethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Bromoform < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Bromomethane < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Carbon Tetrachloride < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Chlorobenzene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Chloroethane < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Chloroform < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Chloromethane < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 10 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.0
Dibromochloromethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,2-Dichlorobenzene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 0.7 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,3-Dichlorobenzene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,4-Dichlorobenzene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,1-Dichloroethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 0.6 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,2-Dichloroethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,1-Dichloroethene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 1.7 1.4 < 0.5 < 0.5 1.3 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
cis-1,2-Dichloroethene 14 10 11 32 6.0 3.4 5.5 < 0.5 < 0.5 19 98 98 39 6.8 100* 10 31 5.2 8.7 28
trans-1,2-Dichloroethene 1.5 < 0.5 1.7 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 1.2 1.1 2.4 2.1 3.0 1.1 11 < 0.5 0.7 1.4
1,2-Dichloropropane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
cis-1,3-Dichloropropene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
trans-1,3-Dichloropropene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Freon 113 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 4.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0 < 2.0
Methylene Chloride < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 40 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20
1,1,2,2-Tetrachloroethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Tetrachloroethene < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,1,1-Trichloroethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
1,1,2-Trichloroethane < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Trichloroethene 23 53 83 2.7 15 15 2.2 < 0.5 0.6 22 17 15 23 26 21 59 45 51 70 5.1
Trichlorofluoromethane < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Vinyl Chloride < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 1.0 < 0.5 < 0.5 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5
Dilution Factor (DF) 1 1 1 1 1 1 1 1 1 1 1 2 1 1 1* 1 1 1 1 1
Notes:
"<" indicates not detected above the reported detection limit
Samples analyzed by EPA Method 8260 (8010 Analyte list) by Enthalpy Analytical (formerly Curtis & Tompkins, Ltd.) of Berkeley, California.
* - DF of 2.5 for cis-1,2-Dichloroethene analysis
µg/L - micrograms per liter
Page 1 of 1
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 4 - VOC
Geosyntec Consultants
Table 5
Analytical Results - 2019 NEC-1AE Quarterly Sampling
501 Ellis Street, Mountain View, California
Notes:
µg/L - micrograms per liter
NA - not analyzed
"<" indicates not detected above the reported detection limit
March 2019 samples were analyzed by EPA Method 8260 by Ethalpy Analytical (formerly Curtis & Tompkins, Ltd.) of Berkeley, California.
June, September, and December 2019 samples were analyzed by EPA Method 8260 by Eurofins TestAmerica of Pleasanton, California
Page 1 of 1
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Tables\2019 Annual Report TablesTable 5 - 01AEVOC
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Notes:
- Water levels were collected on September 19, 2019. Geosyntec <> Figure
- Extraction from well NEC-1AE discontinued on May 13, 2009.
5
ft MSL - feet mean sea level
consultants
gpm - gallons per minute 0 80
- Imagery provided by USGS, April 2011 Feet WR2814 April 2020
D:\GIS\NEC\Project\2019_AnnualReport\Fig05_GWcontours_3Q.mxd 3/13/2020 6:22:37 PM
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consultants
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Geosyntec <>
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consultants
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9
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April 2020
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consultants
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/ \ \ \ \ \ /
555A ELLIS STREET
\ / / / / / / /
/
/ \ / \ /
\ \ /\ \ \ /
Feet
\
\ \ \
/
/ / \ \
\
/ \ / / /\ / /
³
/ \ / \
80
\ \ \ \ \ /
\ \ / / / / / / /
/ / \ / \ \ / \ / \
\ \ \ \ / \ \
" NEC-9A
/ \ \ \
/ /\ / /
\ / \
" NEC-21A
\ \
\
\ \ / / \
/
/ \ / / / / / /
\
NEC-27AE - 1.78
NEC-28AE - 2.03
\ / / / \ \ / \ \ \
\ / \ \ / \ \
NEC-1AE - 0.00
/ \ \ / \ \ /
\ /
/
/\ / / \
\
/ / / \ \ / \
\ \ \ / / / /
" NEC-3A
\ / / / \ / \ / \
/ / \ / \ \
" NEC-1AE
\ \
/\ \ \ /
/
/ \ \ /
515 ELLIS STREET
/ \
\
/ \ /\ / / \ /
/ \
/
\
/ \ /
/
/ \ / / \
\
\ / / /
\
/ \ /\ / \ / \ \ / /
NEC-22A
/ \ \ / \ \ \ /
0
\
/
\ / / \ \ \ \
NEC-PZ-3A\
\ / / / / \
\ / / \ / /
\ /\ \ \ / / / \ \
/ \ / \ / / / \
/ / \ \ /
/\ \ / \ /
(
!
/ \ / \ \ \ / \ /
\
NEC-25A
\ /
\
\ /
/
/\ \
/
/ / /
/
/
\
\
NEC-1A
/ / / \
" NEC-10A
\
\/ \ /\ \ \ / / / / \ \ \
\/ / \ / \ / \ / \ / /
/ \ /
" "
\ / \
"
\ \ / / \
/\
/
/ \ \
\
/ \ / \ \ / \
\ /
NEC-26A
\ /\ / \
Ñ
/ / / / / \ / /
/ \ / \
·
\ \ \ \ \ /
NEC-PZ-2A
\ / \ / \ \ / / \
I C T
/ / \
\\/ NEC-28AE
/
/
/ \ \ / \
\
/ \
\
/\ \
/
\
/
/
\
\
\/
\ / / / / / / \ / / /
/
\
\
/
/
/ \/ \ / \ / \ \ / \ \ \
\
\
\ \ \
Hydraulic Gradient
/ /\ / \ / \ \ / / / \
/
Model Parameters:
\ \ \ / \ \
T R
\ / \
NEC-24A
\
\
/ /
/
/ / / / / / \ / / \ /
/\ /\ / / \ / /
NEC-8A
\/ \ \ \ \ \ \ / \ \ \
/\ \ /\ \ \ / /
// / \
Ñ
/\ / / \
D I S
\ / \ \
/
/
/
\/ \ / \ / \
/\
\
/ / \
\
//
\ / / / / \
\
/ / \ /
\
\ \ / / /
/
\
/
\
\ \ \
/\ /\ \
Recharge
\
/ \ \ / \ \ \
/
1 in/yr
\ /\ /
(
!
/ \ / / \
///\\ / \
/
/ / / \ \ /
E T / \
\\
"
"
/ \
\ \\ / \ / / /
// \
\ \ \ \ / \ \ / / /
R
\
/
R E \
/ / \ \ \ / \ \ \
/ /
\NEC-27AE
/
\
\ \ / / / / / \ \ / \
T E
S T / \
/
\ \ \ \ / / \ \ / / \
/ \
Ñ
\ \ / / /
/ / / \ \
S / / / / \ \ \
L I
·
\ \ /
W A
\ / / / \ \ \ / \
E L / \ \ \ / / \
\ /
NEC-PZ-1A
/
" NEC-23A
/ \ \ /
" NEC-7A
/
\/\ / \ / /
\
/ /
/
/
\\
/ / \ \
/
//\
\ \ / \ \ / \
\/ \ \ \
.
\/ / \ / \
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/
/ / / / / / \ \ / / /
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\\ \
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//
\
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\ / / / \
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/
/
/\
/\
/
/ \ / / / \ \
\
\ /
/
\ / /
\
/\ \
/
\ / \ \ / \ \ \
Piezometer
/\ \ / \
\ \ / \ \ \
/
\
/ \ / / \ \ / / / /
/ / /\ \ / / / / \ \ \
/
\ / \
\
\ \\ / \ \
/ \ \
/
/ / \
\
\
/
/ /
//\ / \ /
\
/ \ / / / \ /
/ \\ / \ \ \ \ \
/ \ \ \
/
/
\
\ / / / \ / \ / / /
\
\ / / /
\ \ \ / \ / \ \ \ \ \
/ \
Ñ
/ \ \ / /
--------=
____J
/ / / / / \ \ /
\ /
·
\ \ \ \ / \
\ \ / \ / \
L
/ \ / \ /
/ \ / \ /
/ \ / \ \
yr - year
Monitoring Well
U E
Extraction Well
E N
E T
R E
S T
Legend
in - inches
AV
S
L I
ft - feet
(
!
E L
Notes:
"
L
N A
NEC10A
" 15
5.0
E T
R E
NECPZ2A
L I
NECPZ1A 70 ·
51 Ñ· Ñ NECPZ3A
5.1
E L
NEC8A " Ñ·
" NEC22A
83 (
!
NEC28AE 22
"
NEC25A " NEC9A
( 45
! NEC27AE 26 2.7
59
NEC12A
" NEC23A 2.2
"
17
501 ELLIS STREET
NEC7A NEC21A
53
" 0.6
!.. . . . . . . . . . . . .
"
NEC24A "
NEC1A
23 " NEC3A
23
( NS
NEC26A "
!
"
S . F
. W A 21 NEC1AE
T E 21 5.0
R D I S
T R
I C T
NEC11A "
15
³
21
Monitoring Well
TCE Concentration
" 2.2
LHHj 501 Ellis Street Boundary 501 Ellis Street
l'"H"""';
10
TCE - Trichloroethene
consultants
µg/L - micrograms per liter 0 100
- Imagery provided by USGS, April 2011 Feet WR2814 April 2020
D:\GIS\NEC\Project\2019_AnnualReport\Fig10_TCE.mxd 3/13/2020 6:42:09 PM
NEC-11A NEC-1A NEC-26A
100000 100000 100000
Concentration (μg/L)
Concentration (μg/L)
1000 1000 1000
10 10 10
1 1 1
Concentration (μg/L)
Concentration (μg/L)
1000 1000 1000
10 10 10
1 1 1
Concentration (μg/L)
Concentration (μg/L)
1000 1000 1000
10 10 10
1 1 1
NEC-7A NEC-23A
100000 100000
10000 10000
Concentration (μg/L)
Concentration (μg/L)
1000 1000
100 100
10 10
1 1
0.1 0.1
1990 1994 1998 2002 2006 2010 2014 2018 2022 1990 1994 1998 2002 2006 2010 2014 2018 2022 VOC Concentrations in Groundwater
Date Date
501 Ellis Street
Notes: Monitoring Well 501 Ellis Street Boundary Mountain View, California
Trichloroethene - Open symbols are non-detects, presented at limit of quantification.
VOC - Volatile Organic Compounds Figure
cis-1,2-Dichloroethene μg/L - micrograms per liter
- Imagery provided by USGS
Vinyl Chloride 11
WR2814 April 2020
D:\GIS\NEC\Project\2019_AnnualReport\[Fig11_VOCsinGW_Timeseries.xlsx]
1000
100
Concentration (μg/L)
10
0.1
1997 1998 1999 2000 2001 2002 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2015 2016 2017 2018 2019 2020 2021 2022
Date
Trichloroethene Vinyl Chloride
Notes: VOC Concentrations in Well NEC-1AE
cis-1,2-Dichloroethene trans-1,2-Dichloroethene Open symbols are non-detects,
presented at limit of quantification. 501 Ellis Street
VOC - volatile organic compound Mountain View, California
1,2-Dichlorobenzene Tetrachloroethene μg/L - micrograms per liter
Figure
Extraction at NEC-1AE Discontinued
WR2814 April 2020
12
D:\GIS\NEC\Project\2019_AnnualReport\[Fig12_NEC1AE_Timeseries.xlsx]
E T
R E
"
NEC-10A
S T
15
S
555A ELLIS STREET
L I
5.0
E L
NEC-PZ-2A
NEC-PZ-1A 70
NECPZ3A
51
Ñ Ñ Ñ
·
NEC-8A "
·
·
5.1
NEC-22A
83(
! " " 22
NEC-27AE NEC-28AE
59 NEC-25A
45
"
(
! 26 NEC-9A
2.7
NEC-23A
" 17 "
NEC-12A
501 ELLIS STREET 2.2
NEC-21A
NEC-7A
53 " 0.6
" NEC-24A
23 NEC-3A
" NEC-1A " NS
S . F 23
. W A " (
!
"
5.
T E NEC-26A NEC-1AE 0
R D I S 21 21
T R
I C T
"
NEC-11A
15
Notes:
- TCE concentrations measured in µg/L.
NS - Not Sampled "
TCE - Trichloroethene NEC-20A
µg/L - micrograms per liter <0.5
-Imagery provided by USGS, April 2011
E T
Legend
(
! Extraction Well NEC-11A Decreasing TCE Concentration Trend Analysis
TCE Concentration
³
TCE Concentration Trend
R E
21 15
Monitoring Well
501 Ellis Street
"
2.2
TCE Concentration NEC-7A No Observed
Piezometer Mountain View, California
TCE Concentration Trend
S T
53
Ñ ·
70 TCE Concentration
TCE Concentration NEC-PZ-2A Increasing Geosyntec e> Figure
Contour (µg/L) 70 TCE Contentration Trend
S
13
consultants
r···-·1
, ______ .,, 501 Ellis Street Boundary
L I
0 100
Feet WR2814 April 2020
E L
Site Remedy Components (Include Other Reference Documents for More Information, as appropriate): (See Section
4.2.5 “Final, Second Five-Year Report for MEW Superfund Study Area, Mountain View, California.” U.S. EPA
Region 9. September 2009.) Soil Remedy. Excavation and aeration. About 210 cubic yards of soil were
excavated and aerated. 55 cubic yards were reused as backfill on site; the remaining 155 cubic yards were disposed
offsite. Groundwater Remedy. Source control groundwater extraction system consisting of two A zone
groundwater extraction wells, and discharge to City of Mountain View sanitary sewer under City of Mountain View
Wastewater Discharge Permit ID Number 925.
II. CONTACTS
List important personnel associated with the Site: Name, title, phone number, e-mail address:
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
Checklist\AppA_2019_AnnualReportChecklist_MB.docx Page 1
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What is your annual O&M cost total for the reporting year?
Breakout your annual O&M cost total into the following categories (use either dollars or %):
Analytical (e.g., lab costs):
Labor (e.g., site maintenance, sampling):
Materials (e.g., treatment chemicals):
Oversight (e.g., project management):
Utilities (e.g., electric, gas, phone, water):
Reporting (e.g., NPDES, progress):
Other (e.g., capital improvements):
Describe unanticipated/unusually high or low O&M costs (go to section [fill in] to recommend optimization
methods):
O&M Manual O&M Maintenance Logs O&M As-built drawings O&M reports
Daily access/Security logs
Site-Specific Health & Safety Plan Contingency/Emergency Response Plan
O&M/OSHA Training Records Settlement Monument Records
Gas Generation Records Groundwater monitoring records Leachate extraction records
Discharge Compliance Records
Air discharge permit Effluent discharge permit Waste disposal, POTW permit
Are these documents currently readily available? Yes No If no, where are records kept?
ICs are being properly implemented and enforced? Yes No, elaborate below
ICs are adequate for site protection? Yes No, elaborate below
Additional remarks regarding ICs:
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
Checklist\AppA_2019_AnnualReportChecklist_MB.docx Page 2
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VII. REDEVELOPMENT
Is redevelopment on property planned? Yes No
If yes, what is planned? Please describe below.
Is redevelopment plan complete Yes, date: _______________________; No ? Not Applicable
Redevelopment proposal in progress? Yes, elaborate below
No; If no, is a proposal anticipated? Yes No
Is the redevelopment proposal compatible with remedy performance? Yes No
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
Checklist\AppA_2019_AnnualReportChecklist_MB.docx Page 3
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VIII. GROUNDWATER REMEDY (reference concentration, capture zone maps, trend analysis, and
other documentation to support analysis)
Groundwater Quality Data
List the types of data that are available: What is the source report?
2019 Annual Progress Report submitted April 2020. Data includes groundwater levels, groundwater elevation
contours and estimated capture zone analyses, groundwater sampling results (lab reports and summary tables) and
trichloroethene (TCE) concentration contour maps, concentration versus time graphs for all monitoring wells, and
Mann-Kendall concentration trend analyses for TCE and cis-1,2-dichloroethene (cis-1,2-DCE) in all sampled
wells.
Contaminant trend(s) tracked during O&M (i.e., temporal analysis of groundwater contaminant trends).
Groundwater data tracked with software for temporal analyses.
Reviewed MNA parameters to ensure health of substrate (e.g., DO, pH, temperature), if appropriate?
Groundwater Pump & Treat Extraction Well and Treatment System Data
List the types of data that are available: What is the source report?
2019 Annual Progress Report submitted April 2020. Data includes extraction system operating parameters (e.g.,
flow rates and volumes), operations and maintenance records, and effluent monitoring results per City of
Mountain View reporting requirements. In addition, the progress report documents reports submitted,
investigations performed, and historical and current groundwater elevation and sampling results.
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
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Recommendations/Next Steps:
Additional vapor sampling will be completed following EPA approval of the Revised Site-Wide Vapor Intrusion
Sampling and Analysis Work Plan for Response Action Tiering for the purpose of placing the building into a
final response action tier.
Schedule:
Have you done a trend analysis? Yes No; If Yes, what does it show?
(Is it inconclusive due to inadequate data? Are the concentrations increasing or decreasing?) Explain and provide
source document reference.
Figure 13 of the 2019 Annual Report indicates decreasing TCE concentrations in most monitoring wells. In five
of the wells with decreasing TCE concentrations, cis-1,2-DCE concentrations are increasing, which is indicative
of TCE natural attenuation.
B. Vertical Migration
Have you done an assessment of vertical gradients? Yes No; If Yes, what does it show? (Is it inconclusive
due to inadequate data? Are the concentrations increasing or decreasing? Explain and provide source document
reference)
Vertical gradients were assessed in 1995. The vertical gradients were assessed between the A and B1 units, B1
and B2 units, and B2 and B3 units. Gradients in 16 of 17 well pairs were upward. Gradient in the deeper B2-B3
well pair was downward.
C. Source Control Remedies
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
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Elaborate on basis for determining progress or lack of progress toward these goals:
On-site capture is achieved through two extraction wells, NEC27AE and NEC28AE, and TCE concentration
trends are generally decreasing.
XI. PROJECTIONS
Administrative Issues
Dates of next monitoring and sampling events for next annual reporting period:
A. Groundwater Remedies - Projections for the upcoming year and long-term (Check all that apply)
Remedy Projections for the upcoming year (2020)
No significant changes projected.
Groundwater remedy will be converted to monitored natural attenuation. Target date:
Groundwater Pump & Treat will be shut down. Target date:
Groundwater cleanup standards to be modified. Target date:
PRP will request remedy modification. Target date of request:
Change in the number of monitoring wells. Increasing or decreasing? Target date:
Change in the number and/or types of analytes being analyzed. Increasing or decreasing?
Target date:
Change in groundwater extraction system. Expansion or minimization (i.e., number of extraction wells and/or
pumping rate)? Target date:
Modification on groundwater treatment? Elaborate below. Target date:
Change in discharge location. Target date:
Other modification(s) anticipated:____________________ Elaborate below. Target date:
Elaborate on Remedy Projections:
XII. RECOMMENDATIONS
Based on performance of the current remedy, continued implementation of the optimized remedy is
recommended.
In March 2016, EPA conditionally approved the Request for Reduction in Groundwater Monitoring Frequency,
allowing a trial reduction in sampling frequency from an annual to biennial basis. The frequency of monitoring at
NEC-1AE will be reduced to a biennial schedule matching the rest of the Site monitoring wells.
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix A - 2019 Annual Report
Checklist\AppA_2019_AnnualReportChecklist_MB.docx Page 7
APPENDIX B
Capture Zone Calculations
The 2019 capture zone analysis was conducted using two methodologies: the Javandel and Tsang (1987)1
methodology and a site-specific numerical model. Both methodologies require the same input parameters to
estimate the capture zones of the groundwater extraction wells. The input parameters used in the numerical
model were evaluated during the fourth quarter 2004 and are consistent with the current understanding of the
Site conditions. Other than average quarterly pumping rates by extraction wells, input parameters were
unchanged in 2019.
Pumping Rate
The average quarterly pumping rates during 2019 for the two operating extraction wells at 501 Ellis Street are
summarized below:
Average Average
Quarterly Flow Quarterly Flow
Quarter Well Average Monthly Flow (gpm) Q (gpm) Q (ft3/day)
27AE 1.24 1.63 2.13 1.67 321
1
28AE 2.06 2.03 2.06 2.05 395
Hydraulic Gradient
The hydraulic gradient, i, was calculated using the November 2004 regional potentiometric surface in the
vicinity of the Site from Weiss Associates (2004)2.
-□
5 ft ft
i 0.008
625 ft ft
Aquifer Thickness
The aquifer thickness, B, was assumed to be uniform and 20 feet. The interlayered heterogeneities of the A
aquifer are treated as a single unit extending from 10 to 30 feet below ground surface.
Transmissivity
1
Javandel and Tsang (1987). Groundwater, Vol. 25, No. 5. pp. 616-625.
2
Weiss Associates, 2004. Draft A/A1 Aquifer (South) Groundwater Elevations and Estimated Capture Zones. 18
November.
Page 1
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix B - Capture Zone
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Geosyntec Consultants
Transmissivity (T) was measured by Bechtel (1996) in monitoring wells NEC-12A, NEC-22A, and NEC-25A.
3
Hydraulic Conductivity
The hydraulic conductivity, K, is calculated from the transmissivity, T, and aquifer thickness as follows:
T 91.3 ft 2 / day
K = = 4.6 ft/day
B 20 ft
The input parameters for the Javandel and Tsang methodology, as well as the numerical model are summarized
as follows:
From Javandel and Tsang, the stagnation point for each extraction well was calculated using the expression:
Q
Xs
2BKi
3
Bechtel, 1996. Source Control Groundwater Remediation Final Design, 501 Ellis Street, Mountain View. 26
August.
Page 2
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix B - Capture Zone
Calculations\Draft_AppB_CaptureZoneCalcs_2019.docx
Geosyntec Consultants
where: Xs = distance to stagnation point (ft)
Q = pumping rate (ft3/day)
B = saturated aquifer thickness (ft)
K = hydraulic conductivity (ft/day)
i = hydraulic gradient (ft/ft)
Using this equation and the above input parameters, the distance to stagnation points for the two wells, in feet,
are:
1 69.4 85.4
2 78.6 82.1
3 77.6 80.5
4 74.1 84.7
Third quarter capture zones calculated using the Javandel and Tsang methodology are shown in Figure 5.
Page 3
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Report\Drafts\Client Review\Appendices\Appendix B - Capture Zone
Calculations\Draft_AppB_CaptureZoneCalcs_2019.docx
APPENDIX C
2019 Laboratory Analytical Reports
ENTHALPY
ANALYTICAL
Enthalpy Analytical
2323 Fifth Street, Berkeley, CA 94710, Phone (510) 486-0900
Laboratory Job Number 307905
ANALYTICAL REPORT
Sample ID Lab ID
271NEC-EFT 307905-001
TRIP BLANK 307905-002
This data package has been reviewed for technical correctness and completeness.
Release of this data has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature which applies to
this PDF file as well as any associated electronic data deliverable files. The
results contained in this report meet all requirements of NELAP and pertain
only to those samples which were submitted for analysis. This report may be
reproduced only in its entirety.
1 of 13
r--~ENTHALPY
~..J ANALYTICAL
CASE NARRATIVE
This data package contains sample and QC results for two water samples,
requested for the above referenced project on 03/05/19. The samples were
received cold and intact.
Page 1 of 1
11.0
2 of 13
it.ocus CHAIN-OF-CUSTODY.- RECORD
• TECHNOLOGIES
5)7 qa:s-- .
(See Reverse for Instructions)
SERIAL NO.
1513'-f
PROJECT NAME -----'---"""-...-C'----- SAMPLERS .J/ell tY C,,.3 -1-~ 7 v;
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□ MOUNTAIN VIEW• 299 FAIRCHILobRIVE • MTN VIEW, CA 94043 • TEL ( f969) 0 • FA~0)~-07~ 5,~ r-r.:rJcJ
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Paddna In caoler: (If odNlr., describe) / ·.
a Bubble Wrap., a foam blades, a Bags, ~one, □ Oath material, □ Cardboard, □ 9.yrofoam, □ Paper~
□ Samples ntmlvad on Ice dJNCl:IV from the 11.ad. CooDna procm had besun , · .
e of Ice used : B1Nat, □ Blue/Gel, □ None Temperature blanlc(s) ~ ~□ No
amperatln mauurad uslna □ Thennometer ID:_ _ _ _ _ __, or IR Gun# a A B"f'"
C.OOW Ti . · · #2: #3: . #4: #$: #6: 17:
cated tests?
late?
res?
Results for any subcontracted analyses are not included in this summary.
No Detections
Page 1 of 1 14.0
5 of 13
,..,~ENTHALPY
~_J ANALYTICAL
6 of 13
,..,~ENTHALPY
~_J ANALYTICAL
7 of 13
,..,~ENTHALPY
~_J ANALYTICAL
Batch QC Report
Enthalpy Analytical - Berkeley Analytical Report
Lab #: 307905 Location: NEC
Client: Locus Technologies Prep: EPA 624
Project#: 98007-99-2200 Analysis: EPA 624
Type: BLANK Diln Fac: 1.000
Lab ID: QC967563 Batch#: 268441
Matrix: Water Analyzed: 03/08/19
Units: ug/L
Analyte Result RL
Chloromethane ND 1.0
Vinyl Chloride ND 0.5
Bromomethane ND 1.0
Chloroethane ND 1.0
Trichlorofluoromethane ND 1.0
1,1-Dichloroethene ND 0.5
Methylene Chloride ND 10
MTBE ND 0.5
trans-1,2-Dichloroethene ND 0.5
1,1-Dichloroethane ND 0.5
cis-1,2-Dichloroethene ND 0.5
Chloroform ND 0.5
1,1,1-Trichloroethane ND 0.5
Carbon Tetrachloride ND 0.5
1,2-Dichloroethane ND 0.5
Benzene ND 0.5
Trichloroethene ND 0.5
1,2-Dichloropropane ND 0.5
Bromodichloromethane ND 0.5
cis-1,3-Dichloropropene ND 0.5
Toluene ND 0.5
trans-1,3-Dichloropropene ND 0.5
1,1,2-Trichloroethane ND 0.5
Tetrachloroethene ND 0.5
Dibromochloromethane ND 0.5
Chlorobenzene ND 0.5
Ethylbenzene ND 0.5
Bromoform ND 1.0
1,1,2,2-Tetrachloroethane ND 0.5
1,3-Dichlorobenzene ND 0.5
1,4-Dichlorobenzene ND 0.5
1,2-Dichlorobenzene ND 0.5
Surrogate %REC Limits
Dibromofluoromethane 106 80-121
1,2-Dichloroethane-d4 99 80-134
Toluene-d8 93 80-120
Bromofluorobenzene 99 80-120
8 of 13
,..,~ENTHALPY
~_J ANALYTICAL
Batch QC Report
9 of 13
,..,~ENTHALPY
~_J ANALYTICAL
Batch QC Report
Enthalpy Analytical - Berkeley Analytical Report
Lab #: 307905 Location: NEC
Client: Locus Technologies Prep: EPA 624
Project#: 98007-99-2200 Analysis: EPA 624
Type: BLANK Diln Fac: 1.000
Lab ID: QC967800 Batch#: 268494
Matrix: Water Analyzed: 03/11/19
Units: ug/L
Analyte Result RL
Chloromethane ND 1.0
Vinyl Chloride ND 0.5
Bromomethane ND 1.0
Chloroethane ND 1.0
Trichlorofluoromethane ND 1.0
1,1-Dichloroethene ND 0.5
Methylene Chloride ND 10
MTBE ND 0.5
trans-1,2-Dichloroethene ND 0.5
1,1-Dichloroethane ND 0.5
cis-1,2-Dichloroethene ND 0.5
Chloroform ND 0.5
1,1,1-Trichloroethane ND 0.5
Carbon Tetrachloride ND 0.5
1,2-Dichloroethane ND 0.5
Benzene ND 0.5
Trichloroethene ND 0.5
1,2-Dichloropropane ND 0.5
Bromodichloromethane ND 0.5
cis-1,3-Dichloropropene ND 0.5
Toluene ND 0.5
trans-1,3-Dichloropropene ND 0.5
1,1,2-Trichloroethane ND 0.5
Tetrachloroethene ND 0.5
Dibromochloromethane ND 0.5
Chlorobenzene ND 0.5
Ethylbenzene ND 0.5
Bromoform ND 1.0
1,1,2,2-Tetrachloroethane ND 0.5
1,3-Dichlorobenzene ND 0.5
1,4-Dichlorobenzene ND 0.5
1,2-Dichlorobenzene ND 0.5
Surrogate %REC Limits
Dibromofluoromethane 111 80-121
1,2-Dichloroethane-d4 99 80-134
Toluene-d8 87 80-120
Bromofluorobenzene 101 80-120
10 of 13
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Batch QC Report
11 of 13
,..,~ENTHALPY
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12 of 13
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Batch QC Report
Type Lab ID MSS Result Spiked Result RL %REC Limits RPD Lim
BS QC967328 90.20 86.00 95 80-121
BSD QC967329 90.20 88.00 98 80-121 2 5
SDUP QC967330 1,054 1,052 10.00 0 5
13 of 13
♦
ENTHALPY
ANALYTICAL
Enthalpy Analytical
2323 Fifth Street, Berkeley, CA 94710, Phone (510) 486-0900
Laboratory Job Number 307897
ANALYTICAL REPORT
Sample ID Lab ID
271 NEC-01AE 307897-001
DUPLICATE 307897-002
This data package has been reviewed for technical correctness and completeness.
Release of this data has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature which applies to
this PDF file as well as any associated electronic data deliverable files. The
results contained in this report meet all requirements of NELAP and pertain
only to those samples which were submitted for analysis. This report may be
reproduced only in its entirety.
1 of 9
r--~ENTHALPY
~..J ANALYTICAL
CASE NARRATIVE
This data package contains sample and QC results for two water samples,
requested for the above referenced project on 03/05/19. The samples were
received cold and intact.
Page 1 of 1
6.0
2 of 9
♦I. DCUS 23)1 ~l SERIAL NO.
~ TECHNOLOGIES CHAIN-OF-CUSTODY RECORD (See Reverse for Instructions) 1513~
. . ·---- ........ _ A/E _, ..... --· ..... Jle/lrY
/"t ~,f1:~(Jj-, SAMPLE CONTAINER ~MPLE DESCRIPTION CODES TAT CODES
II NUMBER OF
CONTAINERS
ANALYSIS REQUESTED
".,, i~ll LABORATORY USE ONLY
F4
0 GI
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ANALYTICAL LAB
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li PRESERVATION
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7
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NOTES/ MISCELLANEOUS Field/ Container Temp. Relinch~gnature) Received By: (Signature) Date Time
- I~ ,,,,
Relinquished Efy: (Signature) Received By: (Signature) Date Time
o/l~ >--119
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----
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REV.6/02
WHrTE: LabcratoryCopy YELLOW: Project Copy PINK: Database Copy
Cllant: _ _ _ _ __
LO(_....M
Project:
kr_
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.
CjND (llllps.llall ,....,
usq IR Gun #I □ A, er Cl B
dlrectly from the field~ 'r..0011111 pracess had~
(NJ',_)
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_ _ ___'
...,.f=--<
=--_·_·-
Ant a.mad¥_. prm■nt? EtNi('ar Cl Yes. If yes, where? C Ql1 cooler, Cl on samples, Don paclcaae
a Dia: _ _ _ _ How ffllllY _ _ □ Sllnatu~ lnltllls, □ Nam □
w.. ... Intact u arrival? □ Vas C No
!I: IMpo,ftlfft:,_ .,,PMltm....... __.rc_. .... frmln.
Packlnlla caalar:(lf DIM"1desc:rlbe) ~ ·
a Mlbla w... a roam blades, a 1ap, □
13fbttt,
0oth matllrlal, □ ciardbaard, a St-,aom-n. a PapartaM!ls
□ ~ ntatlvadon lcedlra:tlVframtheflf!ld. Coatna pracass had beflUII , · ..
• af Jca usm : B"\¥111;, a Bka/GIII, □ No,- Temperature blanlc(s) lnc:ludlJll- ~ □ No
._...... mwurad mini □ 'ffwmomlW ID· orlR Gun I □ A ~
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Dlltr.
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Did you dDcummt ¥D11r praservarJve check? ~
pH strip lotlt _ _ _ _ _ pH strip lat#. _ _ _ _ _ _ 1 _H strip lolt _ _ _ _ __
..,...,,._lldda ll:
a H2504 lotl
a HO.led
----- - added to •mples
•mples
----- ----- --'an/at
----- -~
an/at ....-·-·------- 1
an/at ----- --t
added to
□ HNCII kd added.to samples
□ NIIOH led added to am at ·
Sacllanl:
~
----- ----- ---+ ----- ----- ----.. .
8Y(lll'lntt_ _ _ _ _ _ _ _ _ ,.....,_ __,__ _ ___
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EnlhalpynlWlk:al-......, llav.25, m/02flDJa
4 of 9
,..,~ENTHALPY
~_J ANALYTICAL
Results for any subcontracted analyses are not included in this summary.
Page 1 of 1 9.0
5 of 9
,..,~ENTHALPY
~_J ANALYTICAL
Volatile Organics
Lab #: 307897 Location: NEC
Client: Locus Technologies Prep: EPA 5030B
Project#: 98007-99-2200 Analysis: EPA 8260B
Field ID: 271 NEC-01AE Batch#: 268441
Lab ID: 307897-001 Sampled: 03/04/19
Matrix: Water Received: 03/05/19
Units: ug/L Analyzed: 03/08/19
Diln Fac: 1.000
Analyte Result RL
Chloromethane ND 5.0
Vinyl Chloride ND 0.5
Bromomethane ND 1.0
Chloroethane ND 1.0
Trichlorofluoromethane ND 1.0
Freon 113 ND 2.0
1,1-Dichloroethene ND 0.5
Methylene Chloride ND 20
MTBE ND 0.5
trans-1,2-Dichloroethene 2.5 0.5
1,1-Dichloroethane ND 0.5
cis-1,2-Dichloroethene 26 0.5
Chloroform ND 0.5
1,1,1-Trichloroethane ND 0.5
Carbon Tetrachloride ND 0.5
1,2-Dichloroethane ND 0.5
Benzene ND 0.5
Trichloroethene 20 0.5
1,2-Dichloropropane ND 0.5
Bromodichloromethane ND 0.5
cis-1,3-Dichloropropene ND 0.5
Toluene ND 0.5
trans-1,3-Dichloropropene ND 0.5
1,1,2-Trichloroethane ND 0.5
Tetrachloroethene ND 0.5
Dibromochloromethane ND 0.5
Chlorobenzene ND 0.5
Ethylbenzene ND 0.5
m,p-Xylenes ND 0.5
o-Xylene ND 0.5
Bromoform ND 0.5
1,1,2,2-Tetrachloroethane ND 0.5
1,3-Dichlorobenzene ND 0.5
1,4-Dichlorobenzene ND 0.5
1,2-Dichlorobenzene ND 0.5
Surrogate %REC Limits
Dibromofluoromethane 105 80-121
1,2-Dichloroethane-d4 99 80-134
Toluene-d8 93 80-120
Bromofluorobenzene 99 80-120
6 of 9
,..,~ENTHALPY
~_J ANALYTICAL
Volatile Organics
Lab #: 307897 Location: NEC
Client: Locus Technologies Prep: EPA 5030B
Project#: 98007-99-2200 Analysis: EPA 8260B
Field ID: DUPLICATE Batch#: 268441
Lab ID: 307897-002 Sampled: 03/04/19
Matrix: Water Received: 03/05/19
Units: ug/L Analyzed: 03/08/19
Diln Fac: 1.000
Analyte Result RL
Chloromethane ND 5.0
Vinyl Chloride ND 0.5
Bromomethane ND 1.0
Chloroethane ND 1.0
Trichlorofluoromethane ND 1.0
Freon 113 ND 2.0
1,1-Dichloroethene ND 0.5
Methylene Chloride ND 20
MTBE ND 0.5
trans-1,2-Dichloroethene 2.9 0.5
1,1-Dichloroethane ND 0.5
cis-1,2-Dichloroethene 29 0.5
Chloroform ND 0.5
1,1,1-Trichloroethane ND 0.5
Carbon Tetrachloride ND 0.5
1,2-Dichloroethane ND 0.5
Benzene ND 0.5
Trichloroethene 21 0.5
1,2-Dichloropropane ND 0.5
Bromodichloromethane ND 0.5
cis-1,3-Dichloropropene ND 0.5
Toluene ND 0.5
trans-1,3-Dichloropropene ND 0.5
1,1,2-Trichloroethane ND 0.5
Tetrachloroethene ND 0.5
Dibromochloromethane ND 0.5
Chlorobenzene ND 0.5
Ethylbenzene ND 0.5
m,p-Xylenes ND 0.5
o-Xylene ND 0.5
Bromoform ND 0.5
1,1,2,2-Tetrachloroethane ND 0.5
1,3-Dichlorobenzene ND 0.5
1,4-Dichlorobenzene ND 0.5
1,2-Dichlorobenzene 0.5 0.5
Surrogate %REC Limits
Dibromofluoromethane 105 80-121
1,2-Dichloroethane-d4 98 80-134
Toluene-d8 93 80-120
Bromofluorobenzene 104 80-120
7 of 9
,..,~ENTHALPY
~_J ANALYTICAL
Batch QC Report
Volatile Organics
Lab #: 307897 Location: NEC
Client: Locus Technologies Prep: EPA 5030B
Project#: 98007-99-2200 Analysis: EPA 8260B
Type: BLANK Diln Fac: 1.000
Lab ID: QC967563 Batch#: 268441
Matrix: Water Analyzed: 03/08/19
Units: ug/L
Analyte Result RL
Chloromethane ND 5.0
Vinyl Chloride ND 0.5
Bromomethane ND 1.0
Chloroethane ND 1.0
Trichlorofluoromethane ND 1.0
Freon 113 ND 2.0
1,1-Dichloroethene ND 0.5
Methylene Chloride ND 20
MTBE ND 0.5
trans-1,2-Dichloroethene ND 0.5
1,1-Dichloroethane ND 0.5
cis-1,2-Dichloroethene ND 0.5
Chloroform ND 0.5
1,1,1-Trichloroethane ND 0.5
Carbon Tetrachloride ND 0.5
1,2-Dichloroethane ND 0.5
Benzene ND 0.5
Trichloroethene ND 0.5
1,2-Dichloropropane ND 0.5
Bromodichloromethane ND 0.5
cis-1,3-Dichloropropene ND 0.5
Toluene ND 0.5
trans-1,3-Dichloropropene ND 0.5
1,1,2-Trichloroethane ND 0.5
Tetrachloroethene ND 0.5
Dibromochloromethane ND 0.5
Chlorobenzene ND 0.5
Ethylbenzene ND 0.5
m,p-Xylenes ND 0.5
o-Xylene ND 0.5
Bromoform ND 0.5
1,1,2,2-Tetrachloroethane ND 0.5
1,3-Dichlorobenzene ND 0.5
1,4-Dichlorobenzene ND 0.5
1,2-Dichlorobenzene ND 0.5
Surrogate %REC Limits
Dibromofluoromethane 106 80-121
1,2-Dichloroethane-d4 99 80-134
Toluene-d8 93 80-120
Bromofluorobenzene 99 80-120
8 of 9
,..,~ENTHALPY
~_J ANALYTICAL
Batch QC Report
Volatile Organics
Lab #: 307897 Location: NEC
Client: Locus Technologies Prep: EPA 5030B
Project#: 98007-99-2200 Analysis: EPA 8260B
Matrix: Water Batch#: 268441
Units: ug/L Analyzed: 03/08/19
Diln Fac: 1.000
9 of 9
.;; eurofins ■12
Environment Testing
3
TestAmerica
4
5
ANALYTICAL REPORT
6
Eurofins TestAmerica, Pleasanton
1220 Quarry Lane 7
Pleasanton, CA 94566
Tel: (925)484-1919 8
Laboratory Job ID: 720-93627-1 9
Client Project/Site: NEC
Revision: 1 10
For: 11
Locus Technologies
299 Fairchild Drive 12
Mountain View, California 94043
13
Attn: Nancy-Jeanne LeFevre
14
15
Authorized for release by:
7/18/2019 11:23:31 AM
Nathaniel Horner, Project Management Assistant I
nathaniel.horner@testamericainc.com
Designee for
Micah Smith, Project Manager II
(925)484-1919
micah.smith@testamericainc.com
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-93627-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
8
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
17
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
trans-1,2-Dichloroethene
- - -
6.5
- - - -
0.50
- - -
ug/L
- -
1
- -
624
- - -
Total/NA 4
Trichloroethene 57 0.50 ug/L 1 624 Total/NA
cis-1,2-Dichloroethene 22 0.50 ug/L 1 624 Total/NA 5
LTotal Dissolved Solids 840 10 mg/L 1 SM 2540C Total/NA
6
7
8
9
10
11
12
13
14
15
iGeneral Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Surrogate Legend 7
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr) 8
L TOL = Toluene-d8 (Surr)
9
10
11
12
13
14
15
■9
1,1-Dichloroethene ND 0.50 ug/L 07/02/19 08:24 1
1,2-Dichlorobenzene ND 0.50 ug/L 07/02/19 08:24 1
8
1,2-Dichloroethane ND 0.50 ug/L 07/02/19 08:24 1
1,2-Dichloropropane ND 0.50 ug/L 07/02/19 08:24 1
1,3-Dichlorobenzene ND 0.50 ug/L 07/02/19 08:24 1
1,4-Dichlorobenzene ND 0.50 ug/L 07/02/19 08:24 1 10
Benzene ND 0.50 ug/L 07/02/19 08:24 1
Bromoform ND 1.0 ug/L 07/02/19 08:24 1 11
Bromomethane ND 0.50 ug/L 07/02/19 08:24 1
Carbon tetrachloride ND 0.50 ug/L 07/02/19 08:24 1 12
Chlorobenzene ND 0.50 ug/L 07/02/19 08:24 1
Dibromochloromethane ND 0.50 ug/L 07/02/19 08:24 1 13
Chloroethane ND 1.0 ug/L 07/02/19 08:24 1
Chloroform ND 0.50 ug/L 07/02/19 08:24 1 14
Chloromethane ND 0.50 ug/L 07/02/19 08:24 1
cis-1,3-Dichloropropene ND 0.50 ug/L 07/02/19 08:24 1
Bromodichloromethane ND 0.50 ug/L 07/02/19 08:24 1
15
Ethylbenzene ND 0.50 ug/L 07/02/19 08:24 1
Methylene Chloride ND 2.0 ug/L 07/02/19 08:24 1
Tetrachloroethene ND 0.50 ug/L 07/02/19 08:24 1
Toluene ND 0.50 ug/L 07/02/19 08:24 1
trans-1,2-Dichloroethene ND 0.50 ug/L 07/02/19 08:24 1
trans-1,3-Dichloropropene ND 0.50 ug/L 07/02/19 08:24 1
Trichlorofluoromethane ND 0.50 ug/L 07/02/19 08:24 1
Vinyl chloride ND 0.50 ug/L 07/02/19 08:24 1
Trichloroethene ND 0.50 ug/L 07/02/19 08:24 1
cis-1,2-Dichloroethene ND 0.50 ug/L 07/02/19 08:24 1
Methyl tert-butyl ether ND 0.50 ug/L 07/02/19 08:24 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
4-Bromofluorobenzene (Surr) 120 80 - 120 07/02/19 08:24 1
Dibromofluoromethane (Surr) 91 76 - 132 07/02/19 08:24 1
Lab Sample ID: LCS 440-555711/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 555711
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
- - - - - - - - - - - - - - -
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 116 80 - 120
Dibromofluoromethane (Surr) 91 76 - 132
Lab Sample ID: LCS 440-554202/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 554202
Spike LCS LCS %Rec.
L- - - - - - - - - - -
Analyte
Total Dissolved Solids
Added
1000
Result Qualifier
986
Unit
mg/L
D %Rec
99
Limits
90 - 110 --
Eurofins TestAmerica, Pleasanton
,
Analysis Batch: 555711
Lab
_ Sample
_
720-93627-1
ID
MB 440-555711/4
_ Client
_ Sample
_
272NEC-EFT
ID _ _ _ Prep
Method Blank
_ Type_ _
Matrix _ _
Method _ _
Total/NA
Total/NA
Prep Batch
Water
Water
_
624
624
3
4
5
LLCS 440-555711/5 Lab Control Sample Total/NA Water 624
6
General Chemistry
Analysis Batch: 554202 7
1- - - - - - - - - - - - - - - -
Lab Sample ID
720-93627-1
Client Sample ID
272NEC-EFT
Prep Type
Total/NA
Matrix
Water
Method
SM 2540C
Prep Batch
8
■
MB 440-554202/1 Method Blank Total/NA Water SM 2540C
9
LLCS 440-554202/2 Lab Control Sample Total/NA Water SM 2540C
10
11
12
13
14
15
-
Prepared
Number or Analyzed Analyst
- - -
Lab
-
5
Total/NA Analysis 624 1 555711 07/02/19 12:57 RM TAL IRV
■
10
11
12
13
14
15
■56
USDA Federal P330-17-00380 12-11-20
■
Nevada State Program 9 CA015312019-5 07-31-19 *
New Mexico State Program 6 N/A 01-29-20
11
Oregon NELAP 10 4028 01-29-20
US Fish & Wildlife Federal 058448 07-31-19 *
12
USDA Federal P330-18-00214 07-09-21
Washington State Program 10 C900 09-03-19
13
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~ NUMBEROF
CONTAINERS
.,.,, ~:x- LABORATORY USE ONLY
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NO. I DATE I TIME I SAMPLE ID T~~p I nt~cm I c\1l z NUMBERS
RECEIPT
1 1£ ~o79l~S-5 I::2.. 7.2. #JEc.-~ F7 k'l-lA+ I I3. I I lXI><
2 16-.iot<fl '?-!?s- 1 K 1,,,_ V\. Cl/t i/ I I I I ~ I lX
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Page 15 of 18
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lllll/11111/llllllll111~111
720-93627 Chain of Custody
13
14 I
15
16
NOTES/ MISCELLANEOUS Field/ Container Temp. jR~shed By: (Signature)
('//_..,_ _ a eceived By: (Signature)
• '{;l,.,..,; ... cl
Date
4/4~.h
Time
I/.!2-: ,
0,)c, ature)
~ ~ !.~J
/ Dafo • Time
(
0 MOUNTAIN VIEW• 299 FAIRCHILD DRIVE• MTN VIEW, CA 94043 • TEL (650) 960-1640 • FAX (650) 960-0739
□ WALNUT CREEK• 1701 N. CALIFORNIA BLVD• WALNUT CREEK, CA 94596 • TEL (925) 906-8100 • FAX (925) 906-8101
0 SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
□ OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ FAX _ _ _ __
REV.6/02
WHITE: L.aboratO!)' Copy YELLOW: Project Copy PINK: Database Copy
15
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6
5
4
3
2
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1,
Eurofins TestAmerica, Pleasanton
~:: eurofins Ii
1220 Quarry Lane
Chain of Custody Record 111111111111111111111111111 Environment Testrn ; j !
Pleasanton. CA 94566 TestAm en ca : I
Sampler· Lab PM Carner Tracktng No(s)· COC No:
Client Information (Sub Contract Lab) Smith, Micah 720-42587.1
Ghent Contact Phone. E-Mail. State of Dngm Page·
Shipping/Receiving micah.smllh@testamericarnc com Callfornra Page 1 of 1 '
Company: Accred•tatrons Required (See note) Job#·
TestAmerica Laboratories, Inc 720-93627-1
Address Due D•te Requested : Preservation Codes:
17461 Derian Ave, Suite 100, 7/2/2019 Analysis Requested
A- HCL M- Hexane
City TAT Requested (days):
Irvine
,,
',, ' it:~ ;' '
6-NaOH
C - Zn Acetate
N-None
O- AsNa02
State, Zip: D - N1tnc Acid P- Na204S
l
'' !
CA, 9261 4-5817 E- NaHS04 O-Na2S03
' F- MeOH R-Na2520 3
PO #
Phone
949-261-1022(Tel) 949-260-3297(Fax)
-~ G-Amchlor
H - Ascom,c Acid
S-H2S04 i
Email: WO #. ig i
1
I~ Ic e
T • TSP Dodecahydrate
U - Acetone
! J • DI Water V- MCAA
Proiect Name ProJect # 'I . :I!
uj J'· K -EDTA
L -EDA
W-pH4-5
Z • other (specify)
NEC
Site
72014506
SSOW#·
u
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:').°
. . . . II
,--.
+
Sample Matrix '0
Type
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i,
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Samele Identification • Client ID (Lab ID) Samele Date
Sample
Time
(C=comp,
G=arabl
0-WHlt/ofi,
BT•TIMu., A-Air) ' .~ ~I
i..i
:,.;;,
.j'
Soeclal Instructions/Note:
I
Page 16 of 18
Nate· Since laboratory acered1tat1ons are subJect to change, TestAmenca Laboratones, Inc places the ownershtp of method, analyte & accreditation compliance upon out subcontract laboratortes This sample shipment is forwarded under cha1n--of-custody. If the laboratory does not
currently maintain aecreditat1on 1n the State of Ong1n listed above for analysls/tests/matnx being analyZeO. the samples must be shipped back to the TestAmenca laboratory or other Instructions w1U be provided Any changes to accreditation status should be bto vght to TestAmenca
Lat>oratones, Inc attention 1mmed1ately. If all requested accred1tabons are current to date, return the signed Chain of Custody attesting to said comphcance to TestAmenca Laboratones. Inc.
Possible Hazard Identification Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)
Unconfirmed D Return To Client CJ Disposal By Lab CJ Archive For Months
Deliverable Requested: I, II, Ill, IV, Other (specify) Primary Deliverable Rank: 2 Special lnstructrons/QC Requirements: II
Method of Shipment
~•Yn '"'°"l.qu,shed bL Dale: Time. I/ ,,
'II a1
7/18/2019 (Rev. 1)
Reh"')"1Shedr
'\..../ ~ X D(.';,'7?11 IC/ I 60I /7tPL6 c
Received by:
/?fr''' Datemm..-_
C/41..2 //0 0 Cor'}f-?~y
i
i
Rel!1~u,s,by u Dale!Tt/"e I Company Received by
-;. Oafl'/1,me , Company ''
Relmqu,shed by. Daterr1me: Company Received by Date/Time: Company II
-
Yes I!. No
<...:.._./ Ver 01116/2019
,-----, ,---
,--- J
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1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-93627-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-93628-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
8
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
17
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
Page 3 of 17 7/5/2019
Case Narrative 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Job ID: 720-93628-1 3
Laboratory: Eurofins TestAmerica, Pleasanton
4
Narrative
Job Narrative 5
720-93628-1
6
Comments
No additional comments. 7
Receipt
The sample was received on 6/20/2019 12:50 PM; the sample arrived in good condition, properly preserved and, where required, on ice. 8
The temperature of the cooler at receipt was 4.3º C.
9
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. 10
11
12
13
14
15
trans-1,2-Dichloroethene
- - -
2.4
- - - -
0.50
- - -
ug/L
- -
1
- -
8260B
- - -
Total/NA 4
cis-1,2-Dichloroethene 26 0.50 ug/L 1 8260B Total/NA
Trichloroethene 20 0.50 ug/L 1 8260B Total/NA 5
L1,2-Dichlorobenzene 0.54 0.50 ug/L 1 8260B Total/NA
6
7
8
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Page 5 of 17 7/5/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Client Sample ID: 272NEC-01AE Lab Sample ID: 720-93628-1
Date Collected: 06/20/19 10:00 Matrix: Water
3
Date Received: 06/20/19 12:50
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1-Dichloroethene ND 0.50 ug/L 07/03/19 12:31 1
1,1-Dichloroethane ND 0.50 ug/L 07/03/19 12:31 1 6
Dichlorodifluoromethane ND 0.50 ug/L 07/03/19 12:31 1
Vinyl chloride ND 0.50 ug/L 07/03/19 12:31 1
Chloroethane ND 1.0 ug/L 07/03/19 12:31 1
7
Trichlorofluoromethane ND 1.0 ug/L 07/03/19 12:31 1
Methylene Chloride ND 5.0 ug/L 07/03/19 12:31 1
8
trans-1,2-Dichloroethene 2.4 0.50 ug/L 07/03/19 12:31 1
cis-1,2-Dichloroethene 26 0.50 ug/L 07/03/19 12:31 1
9
Chloroform ND 1.0 ug/L 07/03/19 12:31 1
1,1,1-Trichloroethane ND 0.50 ug/L 07/03/19 12:31 1 10
Carbon tetrachloride ND 0.50 ug/L 07/03/19 12:31 1
1,2-Dichloroethane ND 0.50 ug/L 07/03/19 12:31 1 11
Trichloroethene 20 0.50 ug/L 07/03/19 12:31 1
1,2-Dichloropropane ND 0.50 ug/L 07/03/19 12:31 1 12
Dichlorobromomethane ND 0.50 ug/L 07/03/19 12:31 1
trans-1,3-Dichloropropene ND 0.50 ug/L 07/03/19 12:31 1 13
cis-1,3-Dichloropropene ND 0.50 ug/L 07/03/19 12:31 1
1,1,2-Trichloroethane ND 0.50 ug/L 07/03/19 12:31 1 14
Tetrachloroethene ND 0.50 ug/L 07/03/19 12:31 1
Chlorodibromomethane ND 0.50 ug/L 07/03/19 12:31 1
Chlorobenzene ND 0.50 ug/L 07/03/19 12:31 1
15
Bromoform ND 1.0 ug/L 07/03/19 12:31 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 07/03/19 12:31 1
1,3-Dichlorobenzene ND 0.50 ug/L 07/03/19 12:31 1
1,4-Dichlorobenzene ND 0.50 ug/L 07/03/19 12:31 1
1,2-Dichlorobenzene 0.54 0.50 ug/L 07/03/19 12:31 1
Chloromethane ND 1.0 ug/L 07/03/19 12:31 1
Bromomethane ND 1.0 ug/L 07/03/19 12:31 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 07/03/19 12:31 1
Ethylene Dibromide ND 0.50 ug/L 07/03/19 12:31 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 07/03/19 12:31 1
Benzene ND 0.50 ug/L 07/03/19 12:31 1
Toluene ND 0.50 ug/L 07/03/19 12:31 1
Ethylbenzene ND 0.50 ug/L 07/03/19 12:31 1
m-Xylene & p-Xylene ND 1.0 ug/L 07/03/19 12:31 1
o-Xylene ND 0.50 ug/L 07/03/19 12:31 1
Xylenes, Total ND 0.50 ug/L 07/03/19 12:31 1
Page 6 of 17 7/5/2019
Surrogate Summary 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
3
Percent Surrogate Recovery (Acceptance Limits) 4
TOL DCA
Lab Sample ID Client Sample ID (70-130) (72-130) 5
720-93628-1 272NEC-01AE 92 95
LCS 720-268680/6 Lab Control Sample 92 96 6
LCSD 720-268680/7 Lab Control Sample Dup 92 95
MB 720-268680/5 Method Blank 90 99
7
Surrogate Legend
TOL = Toluene-d8 (Surr) 8
L DCA = 1,2-Dichloroethane-d4 (Surr)
9
10
11
12
13
14
15
Page 7 of 17 7/5/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 720-268680/5 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 268680
MB MB 5
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1-Dichloroethene ND 0.50 ug/L 07/03/19 09:39 1 6
1,1-Dichloroethane ND 0.50 ug/L 07/03/19 09:39 1
Dichlorodifluoromethane ND 0.50 ug/L 07/03/19 09:39 1
Vinyl chloride ND 0.50 ug/L 07/03/19 09:39 1
7
■9
Chloroethane ND 1.0 ug/L 07/03/19 09:39 1
Trichlorofluoromethane ND 1.0 ug/L 07/03/19 09:39 1
8
Methylene Chloride ND 5.0 ug/L 07/03/19 09:39 1
trans-1,2-Dichloroethene ND 0.50 ug/L 07/03/19 09:39 1
cis-1,2-Dichloroethene ND 0.50 ug/L 07/03/19 09:39 1
Chloroform ND 1.0 ug/L 07/03/19 09:39 1 10
1,1,1-Trichloroethane ND 0.50 ug/L 07/03/19 09:39 1
Carbon tetrachloride ND 0.50 ug/L 07/03/19 09:39 1 11
1,2-Dichloroethane ND 0.50 ug/L 07/03/19 09:39 1
Trichloroethene ND 0.50 ug/L 07/03/19 09:39 1 12
1,2-Dichloropropane ND 0.50 ug/L 07/03/19 09:39 1
Dichlorobromomethane ND 0.50 ug/L 07/03/19 09:39 1 13
trans-1,3-Dichloropropene ND 0.50 ug/L 07/03/19 09:39 1
cis-1,3-Dichloropropene ND 0.50 ug/L 07/03/19 09:39 1 14
1,1,2-Trichloroethane ND 0.50 ug/L 07/03/19 09:39 1
Tetrachloroethene ND 0.50 ug/L 07/03/19 09:39 1
Chlorodibromomethane ND 0.50 ug/L 07/03/19 09:39 1
15
Chlorobenzene ND 0.50 ug/L 07/03/19 09:39 1
Bromoform ND 1.0 ug/L 07/03/19 09:39 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 07/03/19 09:39 1
1,3-Dichlorobenzene ND 0.50 ug/L 07/03/19 09:39 1
1,4-Dichlorobenzene ND 0.50 ug/L 07/03/19 09:39 1
1,2-Dichlorobenzene ND 0.50 ug/L 07/03/19 09:39 1
Chloromethane ND 1.0 ug/L 07/03/19 09:39 1
Bromomethane ND 1.0 ug/L 07/03/19 09:39 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 07/03/19 09:39 1
Ethylene Dibromide ND 0.50 ug/L 07/03/19 09:39 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 07/03/19 09:39 1
Benzene ND 0.50 ug/L 07/03/19 09:39 1
Toluene ND 0.50 ug/L 07/03/19 09:39 1
Ethylbenzene ND 0.50 ug/L 07/03/19 09:39 1
m-Xylene & p-Xylene ND 1.0 ug/L 07/03/19 09:39 1
o-Xylene ND 0.50 ug/L 07/03/19 09:39 1
Xylenes, Total ND 0.50 ug/L 07/03/19 09:39 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
Toluene-d8 (Surr) 90 70 - 130 07/03/19 09:39 1
Page 8 of 17 7/5/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCS 720-268680/6 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 268680
Spike LCS LCS %Rec. 5
Analyte Added Result Qualifier Unit D %Rec Limits
- - - - - - - - - - - - - - -
■9
Chloroethane 25.0 24.2 ug/L 97 70 - 131
Trichlorofluoromethane 25.0 24.0 ug/L 96 75 - 141
8
Methylene Chloride 25.0 22.2 ug/L 89 75 - 117
trans-1,2-Dichloroethene 25.0 22.6 ug/L 90 79 - 117
cis-1,2-Dichloroethene 25.0 25.5 ug/L 102 77 - 117
Chloroform 25.0 24.1 ug/L 96 82 - 119 10
1,1,1-Trichloroethane 25.0 24.0 ug/L 96 74 - 130
Carbon tetrachloride 25.0 24.0 ug/L 96 72 - 142 11
1,2-Dichloroethane 25.0 24.8 ug/L 99 73 - 122
Trichloroethene 25.0 23.2 ug/L 93 80 - 123 12
1,2-Dichloropropane 25.0 25.4 ug/L 102 79 - 119
Dichlorobromomethane 25.0 25.3 ug/L 101 81 - 130 13
trans-1,3-Dichloropropene 25.0 23.2 ug/L 93 76 - 122
cis-1,3-Dichloropropene 25.0 24.4 ug/L 98 82 - 119 14
1,1,2-Trichloroethane 25.0 24.0 ug/L 96 80 - 117
Tetrachloroethene 25.0 23.3 ug/L 93 81 - 130
Chlorodibromomethane 25.0 24.6 ug/L 99 77 - 133
15
Chlorobenzene 25.0 24.1 ug/L 96 76 - 116
Bromoform 25.0 23.2 ug/L 93 75 - 127
1,1,2,2-Tetrachloroethane 25.0 23.5 ug/L 94 70 - 115
1,3-Dichlorobenzene 25.0 24.0 ug/L 96 76 - 116
1,4-Dichlorobenzene 25.0 24.2 ug/L 97 76 - 116
1,2-Dichlorobenzene 25.0 23.0 ug/L 92 77 - 117
Chloromethane 25.0 27.0 ug/L 108 49 - 134
Bromomethane 25.0 22.9 ug/L 92 70 - 132
1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 20.5 ug/L 82 70 - 133
ne
Ethylene Dibromide 25.0 23.5 ug/L 94 80 - 121
1,2,4-Trichlorobenzene 25.0 23.2 ug/L 93 78 - 120
Benzene 25.0 23.3 ug/L 93 79 - 119
Toluene 25.0 23.6 ug/L 95 75 - 120
Ethylbenzene 25.0 24.7 ug/L 99 77 - 117
m-Xylene & p-Xylene 25.0 24.0 ug/L 96 74 - 119
o-Xylene 25.0 24.5 ug/L 98 77 - 118
LCS LCS
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 92 70 - 130
Page 9 of 17 7/5/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCSD 720-268680/7 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 268680
Spike LCSD LCSD %Rec. RPD 5
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
- - - - - - - - - - - - - - -
■9
Chloroethane 25.0 23.9 ug/L 96 70 - 131 1 20
Trichlorofluoromethane 25.0 23.7 ug/L 95 75 - 141 1 20
8
Methylene Chloride 25.0 22.0 ug/L 88 75 - 117 1 20
trans-1,2-Dichloroethene 25.0 22.2 ug/L 89 79 - 117 2 20
cis-1,2-Dichloroethene 25.0 25.0 ug/L 100 77 - 117 2 20
Chloroform 25.0 23.7 ug/L 95 82 - 119 1 20 10
1,1,1-Trichloroethane 25.0 23.8 ug/L 95 74 - 130 1 20
Carbon tetrachloride 25.0 23.9 ug/L 95 72 - 142 1 20 11
1,2-Dichloroethane 25.0 24.1 ug/L 96 73 - 122 3 20
Trichloroethene 25.0 23.1 ug/L 92 80 - 123 1 20 12
1,2-Dichloropropane 25.0 25.0 ug/L 100 79 - 119 1 20
Dichlorobromomethane 25.0 24.9 ug/L 100 81 - 130 1 20 13
trans-1,3-Dichloropropene 25.0 22.5 ug/L 90 76 - 122 3 20
cis-1,3-Dichloropropene 25.0 23.9 ug/L 96 82 - 119 2 20 14
1,1,2-Trichloroethane 25.0 23.1 ug/L 92 80 - 117 4 20
Tetrachloroethene 25.0 23.1 ug/L 92 81 - 130 1 20
Chlorodibromomethane 25.0 23.8 ug/L 95 77 - 133 4 20
15
Chlorobenzene 25.0 23.1 ug/L 92 76 - 116 4 20
Bromoform 25.0 21.9 ug/L 88 75 - 127 6 20
1,1,2,2-Tetrachloroethane 25.0 22.9 ug/L 91 70 - 115 3 20
1,3-Dichlorobenzene 25.0 23.8 ug/L 95 76 - 116 1 20
1,4-Dichlorobenzene 25.0 24.1 ug/L 96 76 - 116 1 20
1,2-Dichlorobenzene 25.0 23.0 ug/L 92 77 - 117 0 20
Chloromethane 25.0 26.8 ug/L 107 49 - 134 1 20
Bromomethane 25.0 22.7 ug/L 91 70 - 132 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 20.6 ug/L 82 70 - 133 0 20
ne
Ethylene Dibromide 25.0 22.3 ug/L 89 80 - 121 5 20
1,2,4-Trichlorobenzene 25.0 23.4 ug/L 94 78 - 120 1 20
Benzene 25.0 23.1 ug/L 92 79 - 119 1 20
Toluene 25.0 22.9 ug/L 91 75 - 120 3 20
Ethylbenzene 25.0 24.0 ug/L 96 77 - 117 3 20
m-Xylene & p-Xylene 25.0 23.2 ug/L 93 74 - 119 3 20
o-Xylene 25.0 23.5 ug/L 94 77 - 118 4 20
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 92 70 - 130
Page 10 of 17 7/5/2019
QC Association Summary 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
GC/MS VOA
3
Analysis Batch: 268680
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 4
720-93628-1 272NEC-01AE Total/NA Water 8260B
MB 720-268680/5 Method Blank Total/NA Water 8260B 5
LCS 720-268680/6 Lab Control Sample Total/NA Water 8260B
■9
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Page 11 of 17 7/5/2019
Lab Chronicle 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Client Sample ID: 272NEC-01AE Lab Sample ID: 720-93628-1
Date Collected: 06/20/19 10:00 Matrix: Water
3
Date Received: 06/20/19 12:50
4
i Batch Batch Dilution Batch Prepared
5
L- - - - - - - - - - - - - - -
Prep Type
Total/NA
Type
Analysis
Method
8260B
Run Factor
1
Number or Analyzed Analyst
268680 07/03/19 12:31 AJS
Lab
TAL PLS
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919
7
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Page 12 of 17 7/5/2019
Accreditation/Certification Summary 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
Laboratory: Eurofins TestAmerica, Pleasanton
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. 3
Authority Program EPA Region Identification Number Expiration Date 4
California State Program 9 2496 01-31-20
■56
USDA Federal P330-17-00380 12-11-20
7
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Page 13 of 17 7/5/2019
Method Summary 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
3
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL PLS
5030B Purge and Trap SW846 TAL PLS
4
Protocol References:
5
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 7
8
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Page 14 of 17 7/5/2019
Sample Summary 1
Client: Locus Technologies Job ID: 720-93628-1
Project/Site: NEC 2
3
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
720-93628-1 272NEC-01AE Water 06/20/19 10:00 06/20/19 12:50
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Page 15 of 17 7/5/2019
~OCUS CHAIN-OF-CUSTODY RECORD (Se~everse tor'in"strbctions)
.Al/(/() 77,<;f I SERIAL NO.
TECHNOLOGIES 15 137
PROJECT NAME #G C SAMPLERS J/-enry, C ._3·-/1,, :, J r~
(PRIND
SAMPLE CONTAINER SAMPLE DESCRIPTION CODES TAT CODES
PROJECT NUMBER 9 :t,-v O 7 - 'f Cj ~ .?--r) D DESCRIPTION CODES
K'>.o-ml VOA Vial
~ round Water
urface Water
F.
G.
Oil
Waste & standard
~ ~ ~~ Glass Liter
(SIGN) C. Leachate H. Blank/Spike 2. 48 Hour
E. Brass Tube
RECORDER
GN) 7JD- 11&zv C. Plastic 500-ml
D. Plastic Liter
F. Other--~ D. Rinseate
E. Soil/Sediment
I. Other _ _ _ 3. 24 Hour
4. Other _ _ _
IH
.!. -;; 1--.---~ - ~-1 L- (J "
~.e g- "'- .,a.
~
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ea:
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L i"CA, !5- ~i='8
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COOJO...J G> 0 "
~ SAMPLE
~
;;;
AVERAGE 8 gi f i "ij
::; ::;
~
:I:
~
ASSIGNED
.!!
NOTES BOTTLE CONDITION
1 II II I TEMP E~
NO. I DATE TIME SAMPLE ID •c I COND I
miciomhoslcm IJ) Jl u: Lll
Jl z NUMBERS
UPON
RECEIPT
1
2
lt :JOi'il/ ooo ~ Al'£C - oJA-5 IA- ILl •
,,., I)<'.
3
4
5
6
7
8
Page 16 of 17
9
10
11
12
11111 H lll ll lWI
720-93628 Chain of Custody
13
14
15
16 1
Ji m
I I
I I
J_J
-"-1--1--- t--t--t--t--tt--t-------+--t- t--- - -- -+- -- -+-- -- ---l
--·· - . -
NOTES/ MISCELLANEOUS Field/ Container Temp. Date Time
1Relinquished By: ~
y,_) 2-
- . y: ( S i g ~ .;;
~-<= _· --r .·-nu,10~11 d1Lc 10:;{i,
I Re,~nqui5l1ed By/fSJ,9.ignnaa,O,e) I Rec;;~d By: (Signa.tu~- - / - __ Time
~ o/ 6 ~>t>f'1_
Send Lab Results to (Name): Al'a l'L '-. Iy JeA".,1 ;,.,e le.- ~ v re.,__ (Check Office Below) Verbals Requested: Yes D No 0
0 MOUNTAIN VIEW• 299 FAIRCHILD DRIVE • MTN VIEW, CA 94043 • TEL (650) 960-1640 • FAX (650) 960-0739
0 WALNUT CREEK• 1701 N. CALIFORNIA BLVD• WALNUT CREEK, CA 94596 • TEL (925) 906-8100 • FAX (925) 906-8101
0
7/5/2019
SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
0 OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ FAX _ _ _ __
REV.6/02
WHITE: Laboratcxy Copy YELLOW: Project Copy PINK: DatabaseCopy
15
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4
3
2
1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-93628-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-95003-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
8
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
17
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
Page 3 of 18 9/25/2019
Case Narrative 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Job ID: 720-95003-1 3
Laboratory: Eurofins TestAmerica, Pleasanton
4
Narrative
Job Narrative 5
720-95003-1
6
Comments
No additional comments. 7
Receipt
The sample was received on 9/11/2019 2:45 PM; the sample arrived in good condition, properly preserved and, where required, on ice. 8
The temperature of the cooler at receipt was 2.0º C.
9
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. 10
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
11
12
13
14
15
trans-1,2-Dichloroethene
- - - -
6.9
- - - -
0.50
- - -
ug/L
- -
1
- -
624
- - -
Total/NA 4
Trichloroethene 62 0.50 ug/L 1 624 Total/NA
cis-1,2-Dichloroethene 22 0.50 ug/L 1 624 Total/NA 5
LTotal Dissolved Solids 800 10 mg/L 1 SM 2540C Total/NA
6
7
8
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12
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Page 5 of 18 9/25/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Client Sample ID: 273NEC-EFT Lab Sample ID: 720-95003-1
Date Collected: 09/11/19 08:30 Matrix: Water
3
Date Received: 09/11/19 14:45
4
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1,1-Trichloroethane ND 0.50 ug/L 09/20/19 15:17 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 09/20/19 15:17 1 6
1,1,2-Trichloroethane ND 0.50 ug/L 09/20/19 15:17 1
1,1-Dichloroethane ND 0.50 ug/L 09/20/19 15:17 1
1,1-Dichloroethene ND 0.50 ug/L 09/20/19 15:17 1
7
1,2-Dichlorobenzene ND 0.50 ug/L 09/20/19 15:17 1
1,2-Dichloroethane ND 0.50 ug/L 09/20/19 15:17 1
8
1,2-Dichloropropane ND 0.50 ug/L 09/20/19 15:17 1
1,3-Dichlorobenzene ND 0.50 ug/L 09/20/19 15:17 1
9
1,4-Dichlorobenzene ND 0.50 ug/L 09/20/19 15:17 1
Benzene ND 0.50 ug/L 09/20/19 15:17 1 10
Bromoform ND 1.0 ug/L 09/20/19 15:17 1
Bromomethane ND 0.50 ug/L 09/20/19 15:17 1 11
Carbon tetrachloride ND 0.50 ug/L 09/20/19 15:17 1
Chlorobenzene ND 0.50 ug/L 09/20/19 15:17 1 12
Dibromochloromethane ND 0.50 ug/L 09/20/19 15:17 1
Chloroethane ND 1.0 ug/L 09/20/19 15:17 1 13
Chloroform ND 0.50 ug/L 09/20/19 15:17 1
Chloromethane ND 0.50 ug/L 09/20/19 15:17 1 14
cis-1,3-Dichloropropene ND 0.50 ug/L 09/20/19 15:17 1
Bromodichloromethane ND 0.50 ug/L 09/20/19 15:17 1
Ethylbenzene ND 0.50 ug/L 09/20/19 15:17 1
15
Methylene Chloride ND 2.0 ug/L 09/20/19 15:17 1
Tetrachloroethene ND 0.50 ug/L 09/20/19 15:17 1
Toluene ND 0.50 ug/L 09/20/19 15:17 1
trans-1,2-Dichloroethene 6.9 0.50 ug/L 09/20/19 15:17 1
trans-1,3-Dichloropropene ND 0.50 ug/L 09/20/19 15:17 1
Trichlorofluoromethane ND 0.50 ug/L 09/20/19 15:17 1
Vinyl chloride ND 0.50 ug/L 09/20/19 15:17 1
Trichloroethene 62 0.50 ug/L 09/20/19 15:17 1
cis-1,2-Dichloroethene 22 0.50 ug/L 09/20/19 15:17 1
Methyl tert-butyl ether ND 0.50 ug/L 09/20/19 15:17 1
i General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Page 6 of 18 9/25/2019
Surrogate Summary 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Method: 624 - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
3
Percent Surrogate Recovery (Acceptance Limits) 4
BFB DBFM TOL
Lab Sample ID Client Sample ID (80-120) (76-132) (80-128) 5
720-95003-1 273NEC-EFT 99 99 103
LCS 440-569819/5 Lab Control Sample 99 103 99 6
MB 440-569819/7 Method Blank 97 98 100
Surrogate Legend 7
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr) 8
L TOL = Toluene-d8 (Surr)
9
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12
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Page 7 of 18 9/25/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Method: 624 - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 440-569819/7 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 569819
MB MB 5
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1,1-Trichloroethane ND 0.50 ug/L 09/20/19 10:17 1 6
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 09/20/19 10:17 1
1,1,2-Trichloroethane ND 0.50 ug/L 09/20/19 10:17 1
1,1-Dichloroethane ND 0.50 ug/L 09/20/19 10:17 1
7
■9
1,1-Dichloroethene ND 0.50 ug/L 09/20/19 10:17 1
1,2-Dichlorobenzene ND 0.50 ug/L 09/20/19 10:17 1
8
1,2-Dichloroethane ND 0.50 ug/L 09/20/19 10:17 1
1,2-Dichloropropane ND 0.50 ug/L 09/20/19 10:17 1
1,3-Dichlorobenzene ND 0.50 ug/L 09/20/19 10:17 1
1,4-Dichlorobenzene ND 0.50 ug/L 09/20/19 10:17 1 10
Benzene ND 0.50 ug/L 09/20/19 10:17 1
Bromoform ND 1.0 ug/L 09/20/19 10:17 1 11
Bromomethane ND 0.50 ug/L 09/20/19 10:17 1
Carbon tetrachloride ND 0.50 ug/L 09/20/19 10:17 1 12
Chlorobenzene ND 0.50 ug/L 09/20/19 10:17 1
Dibromochloromethane ND 0.50 ug/L 09/20/19 10:17 1 13
Chloroethane ND 1.0 ug/L 09/20/19 10:17 1
Chloroform ND 0.50 ug/L 09/20/19 10:17 1 14
Chloromethane ND 0.50 ug/L 09/20/19 10:17 1
cis-1,3-Dichloropropene ND 0.50 ug/L 09/20/19 10:17 1
Bromodichloromethane ND 0.50 ug/L 09/20/19 10:17 1
15
Ethylbenzene ND 0.50 ug/L 09/20/19 10:17 1
Methylene Chloride ND 2.0 ug/L 09/20/19 10:17 1
Tetrachloroethene ND 0.50 ug/L 09/20/19 10:17 1
Toluene ND 0.50 ug/L 09/20/19 10:17 1
trans-1,2-Dichloroethene ND 0.50 ug/L 09/20/19 10:17 1
trans-1,3-Dichloropropene ND 0.50 ug/L 09/20/19 10:17 1
Trichlorofluoromethane ND 0.50 ug/L 09/20/19 10:17 1
Vinyl chloride ND 0.50 ug/L 09/20/19 10:17 1
Trichloroethene ND 0.50 ug/L 09/20/19 10:17 1
cis-1,2-Dichloroethene ND 0.50 ug/L 09/20/19 10:17 1
Methyl tert-butyl ether ND 0.50 ug/L 09/20/19 10:17 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
4-Bromofluorobenzene (Surr) 97 80 - 120 09/20/19 10:17 1
Dibromofluoromethane (Surr) 98 76 - 132 09/20/19 10:17 1
Lab Sample ID: LCS 440-569819/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 569819
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
- - - - - - - - - - - - - - -
Page 8 of 18 9/25/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Method: 624 - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCS 440-569819/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 569819
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
5
- - - - - - - - - - - - -
■9
1,4-Dichlorobenzene 10.0 10.1 ug/L 101 70 - 130
Benzene 10.0 10.2 ug/L 102 68 - 130 8
Bromoform 10.0 9.13 ug/L 91 60 - 148
Bromomethane 10.0 9.23 ug/L 92 64 - 139
Carbon tetrachloride 10.0 9.99 ug/L 100 60 - 150
Chlorobenzene 10.0 10.7 ug/L 107 70 - 130 10
Dibromochloromethane 10.0 10.6 ug/L 106 69 - 145
Chloroethane 10.0 9.19 ug/L 92 64 - 135 11
Chloroform 10.0 10.3 ug/L 103 70 - 130
Chloromethane 10.0 9.13 ug/L 91 47 - 140 12
cis-1,3-Dichloropropene 10.0 10.9 ug/L 109 70 - 133
Bromodichloromethane 10.0 10.3 ug/L 103 70 - 132
Ethylbenzene 10.0 9.86 ug/L 99 70 - 130
13
Methylene Chloride 10.0 9.64 ug/L 96 52 - 130
Tetrachloroethene 10.0 9.40 ug/L 94 70 - 130
14
Toluene 10.0 10.2 ug/L 102 70 - 130
trans-1,2-Dichloroethene 10.0 10.6 ug/L 106 70 - 130
15
trans-1,3-Dichloropropene 10.0 10.9 ug/L 109 70 - 132
Trichlorofluoromethane 10.0 9.94 ug/L 99 60 - 150
Vinyl chloride 10.0 8.53 ug/L 85 59 - 133
Trichloroethene 10.0 10.4 ug/L 104 70 - 130
cis-1,2-Dichloroethene 10.0 10.1 ug/L 101 70 - 133
Methyl tert-butyl ether 10.0 10.8 ug/L 108 63 - 131
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 99 80 - 120
Dibromofluoromethane (Surr) 103 76 - 132
Lab Sample ID: LCS 440-569350/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 569350
Spike LCS LCS %Rec.
L- - - - - - - - - - -
Analyte
Total Dissolved Solids
Added
1000
Result Qualifier
976
Unit
mg/L
D %Rec
98
Limits
90 - 110 --
Eurofins TestAmerica, Pleasanton
Page 9 of 18 9/25/2019
QC Association Summary 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
GC/MS VOA
,
Analysis Batch: 569819
Lab
_ Sample_
720-95003-1
ID
MB 440-569819/7
_ Client
_ Sample
273NEC-EFT
_ ID _ _ _ Prep
Method Blank
_ Type _ _
Total/NA
Matrix
Water
Method _ _
_ _
624
Total/NA
Prep Batch
_
Water 624
3
4
5
LLCS 440-569819/5 Lab Control Sample Total/NA Water 624
6
General Chemistry
Analysis Batch: 569350 7
1- - - - - - - - - - - - - - - -
Lab Sample ID
720-95003-1
Client Sample ID
273NEC-EFT
Prep Type
Total/NA
Matrix
Water
Method
SM 2540C
Prep Batch
8
■
MB 440-569350/1 Method Blank Total/NA Water SM 2540C
9
LLCS 440-569350/2 Lab Control Sample Total/NA Water SM 2540C
10
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13
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Page 10 of 18 9/25/2019
Lab Chronicle 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Client Sample ID: 273NEC-EFT Lab Sample ID: 720-95003-1
Date Collected: 09/11/19 08:30 Matrix: Water
3
Date Received: 09/11/19 14:45
4
iPrep Type
- - -
Batch
Type
-
Batch
Method
- -
Run
-
Dil
Factor
-
Initial
Amount
-
Final
Amount
-
Batch
Number
- -
Prepared
or Analyzed
-
Analyst
-
Lab
-
5
Total/NA Analysis 624 1 10 mL 10 mL 569819 09/20/19 15:17 DCI TAL IRV
LTotal/NA Analysis SM 2540C 1 100 mL 100 mL 569350 09/18/19 09:36 XL TAL IRV 6
Laboratory References: 7
TAL IRV = Eurofins TestAmerica, Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022
8
9
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14
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Page 11 of 18 9/25/2019
Accreditation/Certification Summary 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
Laboratory: Eurofins TestAmerica, Pleasanton
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
3
Authority Program Identification Number Expiration Date 4
California State 2496 01-31-20
■56
California State Program 2496 01-31-20
USDA Federal P330-17-00380 12-11-20
USDA US Federal Programs P330-18-00328 11-06-21
■
California State Program CA ELAP 2706 06-30-20
Guam State 19-005R 01-23-20
11
Guam State Program Cert. No. 19-005R 01-23-20
Hawaii State Program N/A 01-29-20
12
Kansas NELAP E-10420 07-31-20
Kansas NELAP E-10420 07-31-20
13
Nevada State Program CA015312019-5 07-31-20
New Mexico State Program N/A 01-29-20 14
Oregon NELAP 4028 01-29-20
Oregon NELAP 4028 - 006 01-29-20 15
US Fish & Wildlife Federal 058448 07-31-20
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA Federal P330-18-00214 07-09-21
USDA US Federal Programs P330-18-00214 07-09-21
Washington State Program C900 09-03-19 *
Page 12 of 18 9/25/2019
Method Summary 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
3
Method Method Description Protocol Laboratory
624 Volatile Organic Compounds (GC/MS) 40CFR136A TAL IRV
SM 2540C Solids, Total Dissolved (TDS) SM TAL IRV
4
Protocol References:
5
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions. 6
SM = "Standard Methods For The Examination Of Water And Wastewater"
7
Laboratory References:
TAL IRV = Eurofins TestAmerica, Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022
8
9
10
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Page 13 of 18 9/25/2019
Sample Summary 1
Client: Locus Technologies Job ID: 720-95003-1
Project/Site: NEC 2
3
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
720-95003-1 273NEC-EFT Water 09/11/19 08:30 09/11/19 14:45
4
5
6
7
8
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Page 14 of 18 9/25/2019
SERIAL NO.
it,.ocus CHAIN-OF-CUSTODY RECORD 151'-l~
/V/;::. k: .
PROJECT NAME
z SAMPLERS-- - - - ~ ~ - - - - - SAMPLE CONTAINER ctf~P~E;ESCRl~TiSNCODES TAT CODES
PROJECT NUMBER
Q ~ A ")
~ ,:) Cl'«:, -
~r~--oo
~ - - ? "7
£)
~
•
RECORDER - ----'--1~1=-"""~C"e:.~-"'-.rc--------~~
(SIG
--------------
, .,.,,,
I<,
(PRINl)
~SIGN
r7
'I
~0-ml VOA Vial
DESCRIPTION CODES
B. Glass Liter;::t.5"OE. Brass Tube
/O)Plastic-,...IF. Other _ _ _
'If" Plastic Liter ____
round Water
Surtace Water
C. Leachate
D. Rinseate
E. So11/Sed1ment
F. Oil
G. Waste
H. Blank/Spike
I. Other___
____
~
andard
B Hour
3. 24Hour
4. Other _ _
f:
12
1n1 IU11111\lll l
720-95003 Chain of Custody
13
14 , , 1 II I I
15 ---.----+-+
11-+--+1-+--+1-tt---i11--+---+--t--1f--t---+--+-tt--+--+-+-+-------+,7-- ,--/,.""'J_al'--t-------l
16 I I I I II 4 ' v- L- _
NOTES/ MISCELLANEOUS Field/ Container Temp. R:!n~uishedJJ (?ignature) I✓ : eceive~ign~ture) Date Time_...
1---?LL- ~..,.., -,. ? - ,,~ ~-1/-IJ I y:J y,
Relinquished !:V"(Signature) ~ d l h - : (Signatur - Date ' Time
__, ~ ~ I:::?'" ~~
1
0,
,-/./.Pp - ~ · ,-,:;,., rll-/1 JLj,'t,,,:r
Relinquishecl By: (Signature) Received By: (Signature) Date Time
Container Sealed with Custody Seal: Yes O
No 0
Method of Shipment Description of Other Chains-of-Custody Dispatched By: (Signature) Date Time Received for lab By: (Signature) Date Time --
Transport Container Transported with this
Chain (by Serial No.) .4] / ,,,c:;::> ./ , } J _} _
7 , " ~ ~ ~ '1-1&~9 >
/1/'011-cv 'J"'elf"/fn-e. Le. ~"rP
0 MOUNTAIN VIEW• 299 FAIRCHILD DRIVE • MTN VIEW, CA 94043 • TEL (650) 960-1640 • FAX (650) 960-0739
0 WALNUT CREEK• 1701 N . CALIFORNIA BLVD• WALNUT CREEK, CA 94596 • TEL (925) 906-8100 • FAX (925) 906-8101
9/25/2019
0 SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
0 OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ _ FAX _ _ _ __
REV.6/02
WHITE: L.aboratcxyCopy YELLOW: Project Copy PINK: Database Copy
15
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10
9
8
7
6
5
4
3
2
1
Eurofins TestAmerica, Pfeasanton
1220 Quarry Lane
Pleasanton, CA 94566
Chain of Custody Record I1111m1n1111~1 -;~ eurofins Env1ronmen1 Testing
Test/lmenca
I:
J-OIWater V-M(:AA
·• ·1112!,' ! K-EOTA W-pH4-5
Proiect Name· Pro)eCI #· - w L - EDA z - other (specify)
~
NEC 72014506
Site
1------------------+------,,----,----,.----t
,.,: ISSOW#: I
~
u
·
li
Other:
1:·t --------------1
+
Sample i ~ ·J
Sam_J)le Identification - Client ID (Lab ID}
Sample
Type
(C=comp,
..,
'-',
Sam~
-·· :15'<,
08:30
273NEC-EFT (720-95003-1) 9/11/19 Water XIX ·4
Pacific
Note Since laboratory accreditallons are subiect to change, TestAmerica Laboratories, Inc. places the O'M1ersh1p of method, analyte & accr&ditatmn campl1ance upon out subcontract laboratones. This sample shipment rs forwarded under cha1n-0f-custody If the taboralary does not
,currenUy maintain accred,tabon m the State of Ong,n listed above for ana1ys1s/lests1matrix being analyzed. the samples must be shipped back to the TestAmerica laboratory or other instructions will be provided Any changes to accreditabon status should be brought to TestAmenca
Laboratones. Inc attenbon ,mmedIately ~ al! requested accred1tabons are current to date, return the signed Chain of Custody attesbng to said compUcance to TestAmerica Labaratones, Inc
Possible Hazard Identification Sample Disposal ( A fee may be assessed If samples are retained longer than 1 month)
Unconnrmed □Return To Client □Disposal Br Lab □Archrve For _ _ _ _ Months
Deliverable Requested· I, II, Ill. IV. Other (specify) Primary Deliverable Rank: 2 Special Instructions/QC Requirements:
■
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2
1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-95003-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-95002-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
8
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
17
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
Page 3 of 17 9/25/2019
Case Narrative 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Job ID: 720-95002-1 3
Laboratory: Eurofins TestAmerica, Pleasanton
4
Narrative
Job Narrative 5
720-95002-1
6
Comments
No additional comments. 7
Receipt
The sample was received on 9/11/2019 2:45 PM; the sample arrived in good condition, properly preserved and, where required, on ice. 8
The temperature of the cooler at receipt was 2.0º C.
9
Receipt Exceptions
One or more containers for the following sample(s) was received broken or leaking: 2 out of 3 containers received broken. Sample was 10
analyzed from the remaining vial.
GC/MS VOA
11
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
12
13
14
15
trans-1,2-Dichloroethene
- - -
2.7
- - - -
0.50
- - -
ug/L
- -
1
- -
8260B
- - -
Total/NA 4
cis-1,2-Dichloroethene 29 0.50 ug/L 1 8260B Total/NA
Trichloroethene 22 0.50 ug/L 1 8260B Total/NA 5
L1,2-Dichlorobenzene 0.54 0.50 ug/L 1 8260B Total/NA
6
7
8
9
10
11
12
13
14
15
Page 5 of 17 9/25/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Client Sample ID: 273NEC-01AE Lab Sample ID: 720-95002-1
Date Collected: 09/11/19 09:30 Matrix: Water
3
Date Received: 09/11/19 14:45
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1-Dichloroethene ND 0.50 ug/L 09/13/19 11:54 1
1,1-Dichloroethane ND 0.50 ug/L 09/13/19 11:54 1 6
Dichlorodifluoromethane ND 0.50 ug/L 09/13/19 11:54 1
Vinyl chloride ND 0.50 ug/L 09/13/19 11:54 1
Chloroethane ND 1.0 ug/L 09/13/19 11:54 1
7
Trichlorofluoromethane ND 1.0 ug/L 09/13/19 11:54 1
Methylene Chloride ND 5.0 ug/L 09/13/19 11:54 1
8
trans-1,2-Dichloroethene 2.7 0.50 ug/L 09/13/19 11:54 1
cis-1,2-Dichloroethene 29 0.50 ug/L 09/13/19 11:54 1
9
Chloroform ND 1.0 ug/L 09/13/19 11:54 1
1,1,1-Trichloroethane ND 0.50 ug/L 09/13/19 11:54 1 10
Carbon tetrachloride ND 0.50 ug/L 09/13/19 11:54 1
1,2-Dichloroethane ND 0.50 ug/L 09/13/19 11:54 1 11
Trichloroethene 22 0.50 ug/L 09/13/19 11:54 1
1,2-Dichloropropane ND 0.50 ug/L 09/13/19 11:54 1 12
Dichlorobromomethane ND 0.50 ug/L 09/13/19 11:54 1
trans-1,3-Dichloropropene ND 0.50 ug/L 09/13/19 11:54 1 13
cis-1,3-Dichloropropene ND 0.50 ug/L 09/13/19 11:54 1
1,1,2-Trichloroethane ND 0.50 ug/L 09/13/19 11:54 1 14
Tetrachloroethene ND 0.50 ug/L 09/13/19 11:54 1
Chlorodibromomethane ND 0.50 ug/L 09/13/19 11:54 1
Chlorobenzene ND 0.50 ug/L 09/13/19 11:54 1
15
Bromoform ND 1.0 ug/L 09/13/19 11:54 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 09/13/19 11:54 1
1,3-Dichlorobenzene ND 0.50 ug/L 09/13/19 11:54 1
1,4-Dichlorobenzene ND 0.50 ug/L 09/13/19 11:54 1
1,2-Dichlorobenzene 0.54 0.50 ug/L 09/13/19 11:54 1
Chloromethane ND 1.0 ug/L 09/13/19 11:54 1
Bromomethane ND 1.0 ug/L 09/13/19 11:54 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 09/13/19 11:54 1
Ethylene Dibromide ND 0.50 ug/L 09/13/19 11:54 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 09/13/19 11:54 1
Benzene ND 0.50 ug/L 09/13/19 11:54 1
Toluene ND 0.50 ug/L 09/13/19 11:54 1
Ethylbenzene ND 0.50 ug/L 09/13/19 11:54 1
m-Xylene & p-Xylene ND 1.0 ug/L 09/13/19 11:54 1
o-Xylene ND 0.50 ug/L 09/13/19 11:54 1
Xylenes, Total ND 0.50 ug/L 09/13/19 11:54 1
Page 6 of 17 9/25/2019
Surrogate Summary 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
3
Percent Surrogate Recovery (Acceptance Limits) 4
TOL DCA
Lab Sample ID Client Sample ID (70-130) (72-130) 5
720-95002-1 273NEC-01AE 99 109
LCS 720-272829/5 Lab Control Sample 99 101 6
LCSD 720-272829/6 Lab Control Sample Dup 98 101
MB 720-272829/4 Method Blank 97 106
7
Surrogate Legend
TOL = Toluene-d8 (Surr) 8
L DCA = 1,2-Dichloroethane-d4 (Surr)
9
10
11
12
13
14
15
Page 7 of 17 9/25/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 720-272829/4 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 272829
MB MB 5
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1-Dichloroethene ND 0.50 ug/L 09/13/19 10:53 1 6
1,1-Dichloroethane ND 0.50 ug/L 09/13/19 10:53 1
Dichlorodifluoromethane ND 0.50 ug/L 09/13/19 10:53 1
Vinyl chloride ND 0.50 ug/L 09/13/19 10:53 1
7
■9
Chloroethane ND 1.0 ug/L 09/13/19 10:53 1
Trichlorofluoromethane ND 1.0 ug/L 09/13/19 10:53 1
8
Methylene Chloride ND 5.0 ug/L 09/13/19 10:53 1
trans-1,2-Dichloroethene ND 0.50 ug/L 09/13/19 10:53 1
cis-1,2-Dichloroethene ND 0.50 ug/L 09/13/19 10:53 1
Chloroform ND 1.0 ug/L 09/13/19 10:53 1 10
1,1,1-Trichloroethane ND 0.50 ug/L 09/13/19 10:53 1
Carbon tetrachloride ND 0.50 ug/L 09/13/19 10:53 1 11
1,2-Dichloroethane ND 0.50 ug/L 09/13/19 10:53 1
Trichloroethene ND 0.50 ug/L 09/13/19 10:53 1 12
1,2-Dichloropropane ND 0.50 ug/L 09/13/19 10:53 1
Dichlorobromomethane ND 0.50 ug/L 09/13/19 10:53 1 13
trans-1,3-Dichloropropene ND 0.50 ug/L 09/13/19 10:53 1
cis-1,3-Dichloropropene ND 0.50 ug/L 09/13/19 10:53 1 14
1,1,2-Trichloroethane ND 0.50 ug/L 09/13/19 10:53 1
Tetrachloroethene ND 0.50 ug/L 09/13/19 10:53 1
Chlorodibromomethane ND 0.50 ug/L 09/13/19 10:53 1
15
Chlorobenzene ND 0.50 ug/L 09/13/19 10:53 1
Bromoform ND 1.0 ug/L 09/13/19 10:53 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 09/13/19 10:53 1
1,3-Dichlorobenzene ND 0.50 ug/L 09/13/19 10:53 1
1,4-Dichlorobenzene ND 0.50 ug/L 09/13/19 10:53 1
1,2-Dichlorobenzene ND 0.50 ug/L 09/13/19 10:53 1
Chloromethane ND 1.0 ug/L 09/13/19 10:53 1
Bromomethane ND 1.0 ug/L 09/13/19 10:53 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 09/13/19 10:53 1
Ethylene Dibromide ND 0.50 ug/L 09/13/19 10:53 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 09/13/19 10:53 1
Benzene ND 0.50 ug/L 09/13/19 10:53 1
Toluene ND 0.50 ug/L 09/13/19 10:53 1
Ethylbenzene ND 0.50 ug/L 09/13/19 10:53 1
m-Xylene & p-Xylene ND 1.0 ug/L 09/13/19 10:53 1
o-Xylene ND 0.50 ug/L 09/13/19 10:53 1
Xylenes, Total ND 0.50 ug/L 09/13/19 10:53 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
Toluene-d8 (Surr) 97 70 - 130 09/13/19 10:53 1
Page 8 of 17 9/25/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCS 720-272829/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 272829
Spike LCS LCS %Rec. 5
Analyte Added Result Qualifier Unit D %Rec Limits
- - - - - - - - - - - - - - -
■9
Chloroethane 25.0 24.8 ug/L 99 70 - 131
Trichlorofluoromethane 25.0 24.3 ug/L 97 75 - 141
8
Methylene Chloride 25.0 23.1 ug/L 92 75 - 117
trans-1,2-Dichloroethene 25.0 24.1 ug/L 96 79 - 117
cis-1,2-Dichloroethene 25.0 26.2 ug/L 105 77 - 117
Chloroform 25.0 24.3 ug/L 97 82 - 119 10
1,1,1-Trichloroethane 25.0 25.4 ug/L 101 74 - 130
Carbon tetrachloride 25.0 25.2 ug/L 101 72 - 142 11
1,2-Dichloroethane 25.0 26.2 ug/L 105 73 - 122
Trichloroethene 25.0 24.3 ug/L 97 80 - 123 12
1,2-Dichloropropane 25.0 25.3 ug/L 101 79 - 119
Dichlorobromomethane 25.0 25.1 ug/L 100 81 - 130 13
trans-1,3-Dichloropropene 25.0 25.1 ug/L 100 76 - 122
cis-1,3-Dichloropropene 25.0 24.5 ug/L 98 82 - 119 14
1,1,2-Trichloroethane 25.0 23.5 ug/L 94 80 - 117
Tetrachloroethene 25.0 24.1 ug/L 97 81 - 130
Chlorodibromomethane 25.0 26.5 ug/L 106 77 - 133
15
Chlorobenzene 25.0 23.5 ug/L 94 76 - 116
Bromoform 25.0 26.4 ug/L 106 75 - 127
1,1,2,2-Tetrachloroethane 25.0 21.7 ug/L 87 70 - 115
1,3-Dichlorobenzene 25.0 24.1 ug/L 97 76 - 116
1,4-Dichlorobenzene 25.0 24.1 ug/L 97 76 - 116
1,2-Dichlorobenzene 25.0 23.1 ug/L 93 77 - 117
Chloromethane 25.0 26.6 ug/L 107 49 - 134
Bromomethane 25.0 23.0 ug/L 92 70 - 132
1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 24.4 ug/L 97 70 - 133
ne
Ethylene Dibromide 25.0 23.9 ug/L 95 80 - 121
1,2,4-Trichlorobenzene 25.0 23.3 ug/L 93 78 - 120
Benzene 25.0 24.1 ug/L 96 79 - 119
Toluene 25.0 23.9 ug/L 96 75 - 120
Ethylbenzene 25.0 24.9 ug/L 100 77 - 117
m-Xylene & p-Xylene 25.0 24.5 ug/L 98 74 - 119
o-Xylene 25.0 24.7 ug/L 99 77 - 118
LCS LCS
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 99 70 - 130
Page 9 of 17 9/25/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCSD 720-272829/6 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 272829
Spike LCSD LCSD %Rec. RPD 5
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
- - - - - - - - - - - - - - -
■9
Chloroethane 25.0 24.2 ug/L 97 70 - 131 2 20
Trichlorofluoromethane 25.0 25.1 ug/L 100 75 - 141 3 20
8
Methylene Chloride 25.0 23.0 ug/L 92 75 - 117 1 20
trans-1,2-Dichloroethene 25.0 23.8 ug/L 95 79 - 117 1 20
cis-1,2-Dichloroethene 25.0 26.3 ug/L 105 77 - 117 0 20
Chloroform 25.0 24.4 ug/L 98 82 - 119 0 20 10
1,1,1-Trichloroethane 25.0 25.3 ug/L 101 74 - 130 0 20
Carbon tetrachloride 25.0 25.3 ug/L 101 72 - 142 0 20 11
1,2-Dichloroethane 25.0 26.0 ug/L 104 73 - 122 1 20
Trichloroethene 25.0 24.2 ug/L 97 80 - 123 0 20 12
1,2-Dichloropropane 25.0 25.5 ug/L 102 79 - 119 1 20
Dichlorobromomethane 25.0 25.3 ug/L 101 81 - 130 1 20 13
trans-1,3-Dichloropropene 25.0 25.0 ug/L 100 76 - 122 0 20
cis-1,3-Dichloropropene 25.0 24.5 ug/L 98 82 - 119 0 20 14
1,1,2-Trichloroethane 25.0 23.8 ug/L 95 80 - 117 1 20
Tetrachloroethene 25.0 23.8 ug/L 95 81 - 130 1 20
Chlorodibromomethane 25.0 26.5 ug/L 106 77 - 133 0 20
15
Chlorobenzene 25.0 23.2 ug/L 93 76 - 116 1 20
Bromoform 25.0 26.1 ug/L 104 75 - 127 1 20
1,1,2,2-Tetrachloroethane 25.0 21.8 ug/L 87 70 - 115 1 20
1,3-Dichlorobenzene 25.0 24.2 ug/L 97 76 - 116 0 20
1,4-Dichlorobenzene 25.0 24.2 ug/L 97 76 - 116 0 20
1,2-Dichlorobenzene 25.0 23.4 ug/L 93 77 - 117 1 20
Chloromethane 25.0 26.2 ug/L 105 49 - 134 2 20
Bromomethane 25.0 23.4 ug/L 93 70 - 132 1 20
1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 24.0 ug/L 96 70 - 133 1 20
ne
Ethylene Dibromide 25.0 23.8 ug/L 95 80 - 121 0 20
1,2,4-Trichlorobenzene 25.0 23.7 ug/L 95 78 - 120 2 20
Benzene 25.0 24.0 ug/L 96 79 - 119 0 20
Toluene 25.0 23.8 ug/L 95 75 - 120 0 20
Ethylbenzene 25.0 24.7 ug/L 99 77 - 117 1 20
m-Xylene & p-Xylene 25.0 24.4 ug/L 97 74 - 119 1 20
o-Xylene 25.0 24.6 ug/L 98 77 - 118 0 20
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 98 70 - 130
Page 10 of 17 9/25/2019
QC Association Summary 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
GC/MS VOA
3
Analysis Batch: 272829
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 4
720-95002-1 273NEC-01AE Total/NA Water 8260B
MB 720-272829/4 Method Blank Total/NA Water 8260B 5
LCS 720-272829/5 Lab Control Sample Total/NA Water 8260B
■9
10
11
12
13
14
15
Page 11 of 17 9/25/2019
Lab Chronicle 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Client Sample ID: 273NEC-01AE Lab Sample ID: 720-95002-1
Date Collected: 09/11/19 09:30 Matrix: Water
3
Date Received: 09/11/19 14:45
4
i Batch Batch Dil Initial Final Batch Prepared
5
L- - - - - - - - - - - - - - -
Prep Type
Total/NA
Type
Analysis
Method
8260B
Run Factor
1
Amount
10 mL
Amount
10 mL
Number
272829
or Analyzed Analyst
09/13/19 11:54 A1C
Lab
TAL PLS
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919
7
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Page 12 of 17 9/25/2019
Accreditation/Certification Summary 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
Laboratory: Eurofins TestAmerica, Pleasanton
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. 3
Authority Program Identification Number Expiration Date 4
California State 2496 01-31-20
■56
California State Program 2496 01-31-20
USDA Federal P330-17-00380 12-11-20
USDA US Federal Programs P330-18-00328 11-06-21
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Page 13 of 17 9/25/2019
Method Summary 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
3
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL PLS
5030B Purge and Trap SW846 TAL PLS
4
Protocol References:
5
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 7
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Page 14 of 17 9/25/2019
Sample Summary 1
Client: Locus Technologies Job ID: 720-95002-1
Project/Site: NEC 2
3
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
720-95002-1 273NEC-01AE Water 09/11/19 09:30 09/11/19 14:45
4
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Page 15 of 17 9/25/2019
SERIAL NO.
it,.acus
TECHNOLOGIES CHAIN-OF-CUSTODY RECORD (See Rove,~ fo, lostm,Uoo-!j,,o/ZZ fJ 151 '/f
NAME __
PROJECT -
---J-.''-£:---""'"'----------- SAMPLER S
(PRINT)
I SAMPLE CONTAINER I SAMPLE DESCRIPTION CODES TAT CODES
DESCRIPTION CODES
~ 0-ml VOA Vial
Ground Water F. Oil
PROJECTNUMBER_~-=-~:_:::::::.=:::~-C) (SIGN) . Surface Water G. Waste · 1. tandard
7Zo • -,
Glass Liter
C. Plastic 500-ml
E. Brass Tube
F. Other___
C. Leachate
D. Rinseate
H.
I.
Blank/Spike
Other _ __
_ _ _ _ _C'-~~~~~~~~lrJ_~D~.~P~l~as~ti~c~L~it~e r:__ __:-=-::,:-;=-=-=;-=~~1~E~.~S:o:il~/S:e~d~im:e~n~t--__::-:-:-:-:-:-:-:-:~J~4~·~0~1h:•~r~=-=-=-=-=-J
48 Hour
3. 24 Hour
-~lil
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I AVERAGE
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ASSIGNED SAMPLE
CONDITION
~
~
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a. NOTES BOTTLE
NO. I DATE I TIME I SAMPLE ID
TEMP
°C
I COND
mcromh06/cm
I pH li
1/1 c\1l
§
U: Ul
E o
ci1l z NUMBERS UPON
RECEIPT
1 'ff,Ji-!<tlCJZQ r:zJ3~c-e,1AEE.
- · . . - - .... - - - - -- - ----- IA-IA ~ I')(
2
3
9
10
11
12
\\l~\\\\1\1\\1\li l\l\i\l\\\\\\\\lil\\\
720-95002 Chain of Custody
13
14
15
16
II
]
I I
I
I J
i' f)~
NOTES/ MISCELLANEOUS Field/ Container Temp. Date Time
Rel?;::.hed ~: ~ignature) l~~ure)
-7:L \ee£,,- '7-111'7 I f,f\:
l~(Si~ Date
~J/-1J. /'/,'fr
Time
0 SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
0 OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ _ FAX _ _ _ __
REV.6/02
WHITE: LaboratoryGopy YELLOW: Project Copy PINK: Database Copy
15
14
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10
9
8
7
6
5
4
3
2
1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-95002-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. False Containers recd broken. Sufficient sample in
15
remaining containers for analysis.
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-96482-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
9
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
18
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
Page 3 of 20 12/19/2019
Case Narrative 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Job ID: 720-96482-1 3
Laboratory: Eurofins TestAmerica, Pleasanton
4
Narrative
Job Narrative 5
720-96482-1
6
Comments
No additional comments. 7
Receipt
The samples were received on 12/10/2019 2:19 PM; the samples arrived in good condition, properly preserved and, where required, on 8
ice. The temperature of the cooler at receipt was 1.6º C.
9
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. 10
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
11
VOA Prep 12
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
13
14
15
cis-1,2-Dichloroethene
- - -
25
- - - -
0.50
- - -
ug/L
- -
1
- -
624.1
- - -
Total/NA 4
trans-1,2-Dichloroethene 7.5 0.50 ug/L 1 624.1 Total/NA
Trichloroethene 69 0.50 ug/L 1 624.1 Total/NA 5
L Total Dissolved Solids 780 10 mg/L 1 SM 2540C Total/NA
6
Client Sample ID: TRIP BLANK Lab Sample ID: 720-96482-2
[ No Detections. 7
8
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12
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Page 5 of 20 12/19/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Client Sample ID: 275NEC-EFT Lab Sample ID: 720-96482-1
Date Collected: 12/10/19 09:50 Matrix: Water
3
Date Received: 12/10/19 14:19
4
Method: 624.1 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1,1-Trichloroethane ND 0.50 ug/L 12/15/19 16:40 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 12/15/19 16:40 1 6
1,1,2-Trichloroethane ND 0.50 ug/L 12/15/19 16:40 1
1,1-Dichloroethane ND 0.50 ug/L 12/15/19 16:40 1
1,1-Dichloroethene ND 0.50 ug/L 12/15/19 16:40 1
7
1,2-Dichlorobenzene ND 0.50 ug/L 12/15/19 16:40 1
1,2-Dichloroethane ND 0.50 ug/L 12/15/19 16:40 1
8
1,2-Dichloropropane ND 0.50 ug/L 12/15/19 16:40 1
1,3-Dichlorobenzene ND 0.50 ug/L 12/15/19 16:40 1
9
1,4-Dichlorobenzene ND 0.50 ug/L 12/15/19 16:40 1
Benzene ND 0.50 ug/L 12/15/19 16:40 1 10
Bromoform ND 1.0 ug/L 12/15/19 16:40 1
Bromomethane ND 0.50 ug/L 12/15/19 16:40 1 11
Carbon tetrachloride ND 0.50 ug/L 12/15/19 16:40 1
Chlorobenzene ND 0.50 ug/L 12/15/19 16:40 1 12
Dibromochloromethane ND 0.50 ug/L 12/15/19 16:40 1
Chloroethane ND 1.0 ug/L 12/15/19 16:40 1 13
Chloroform ND 0.50 ug/L 12/15/19 16:40 1
Chloromethane ND 0.50 ug/L 12/15/19 16:40 1 14
cis-1,2-Dichloroethene 25 0.50 ug/L 12/15/19 16:40 1
cis-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 16:40 1
Bromodichloromethane ND 0.50 ug/L 12/15/19 16:40 1
15
Ethylbenzene ND 0.50 ug/L 12/15/19 16:40 1
Methyl tert-butyl ether ND 0.50 ug/L 12/15/19 16:40 1
Methylene Chloride ND 2.0 ug/L 12/15/19 16:40 1
Tetrachloroethene ND 0.50 ug/L 12/15/19 16:40 1
Toluene ND 0.50 ug/L 12/15/19 16:40 1
trans-1,2-Dichloroethene 7.5 0.50 ug/L 12/15/19 16:40 1
trans-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 16:40 1
Trichloroethene 69 0.50 ug/L 12/15/19 16:40 1
Trichlorofluoromethane ND 0.50 ug/L 12/15/19 16:40 1
Vinyl chloride ND 0.50 ug/L 12/15/19 16:40 1
iGeneral Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Page 6 of 20 12/19/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Client Sample ID: TRIP BLANK Lab Sample ID: 720-96482-2
Date Collected: 12/10/19 00:00 Matrix: Water
3
Date Received: 12/10/19 14:19
4
Method: 624.1 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1,1-Trichloroethane ND 0.50 ug/L 12/15/19 17:08 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 12/15/19 17:08 1 6
1,1,2-Trichloroethane ND 0.50 ug/L 12/15/19 17:08 1
1,1-Dichloroethane ND 0.50 ug/L 12/15/19 17:08 1
1,1-Dichloroethene ND 0.50 ug/L 12/15/19 17:08 1
7
1,2-Dichlorobenzene ND 0.50 ug/L 12/15/19 17:08 1
1,2-Dichloroethane ND 0.50 ug/L 12/15/19 17:08 1
8
1,2-Dichloropropane ND 0.50 ug/L 12/15/19 17:08 1
1,3-Dichlorobenzene ND 0.50 ug/L 12/15/19 17:08 1
9
1,4-Dichlorobenzene ND 0.50 ug/L 12/15/19 17:08 1
Benzene ND 0.50 ug/L 12/15/19 17:08 1 10
Bromoform ND 1.0 ug/L 12/15/19 17:08 1
Bromomethane ND 0.50 ug/L 12/15/19 17:08 1 11
Carbon tetrachloride ND 0.50 ug/L 12/15/19 17:08 1
Chlorobenzene ND 0.50 ug/L 12/15/19 17:08 1 12
Dibromochloromethane ND 0.50 ug/L 12/15/19 17:08 1
Chloroethane ND 1.0 ug/L 12/15/19 17:08 1 13
Chloroform ND 0.50 ug/L 12/15/19 17:08 1
Chloromethane ND 0.50 ug/L 12/15/19 17:08 1 14
cis-1,2-Dichloroethene ND 0.50 ug/L 12/15/19 17:08 1
cis-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 17:08 1
Bromodichloromethane ND 0.50 ug/L 12/15/19 17:08 1
15
Ethylbenzene ND 0.50 ug/L 12/15/19 17:08 1
Methyl tert-butyl ether ND 0.50 ug/L 12/15/19 17:08 1
Methylene Chloride ND 2.0 ug/L 12/15/19 17:08 1
Tetrachloroethene ND 0.50 ug/L 12/15/19 17:08 1
Toluene ND 0.50 ug/L 12/15/19 17:08 1
trans-1,2-Dichloroethene ND 0.50 ug/L 12/15/19 17:08 1
trans-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 17:08 1
Trichloroethene ND 0.50 ug/L 12/15/19 17:08 1
Trichlorofluoromethane ND 0.50 ug/L 12/15/19 17:08 1
Vinyl chloride ND 0.50 ug/L 12/15/19 17:08 1
Page 7 of 20 12/19/2019
Surrogate Summary 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Method: 624.1 - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
3
Percent Surrogate Recovery (Acceptance Limits) 4
BFB DBFM TOL
Lab Sample ID Client Sample ID (60-140) (60-140) (60-140) 5
720-96482-1 275NEC-EFT 95 101 95
720-96482-2 TRIP BLANK 95 107 95 6
LCS 440-586032/1002 Lab Control Sample 96 101 93
MB 440-586032/4 Method Blank 93 105 96
7
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr) 8
DBFM = Dibromofluoromethane (Surr)
Page 8 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Method: 624.1 - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 440-586032/4 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 586032
MB MB 5
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1,1-Trichloroethane ND 0.50 ug/L 12/15/19 12:16 1 6
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 12/15/19 12:16 1
1,1,2-Trichloroethane ND 0.50 ug/L 12/15/19 12:16 1
1,1-Dichloroethane ND 0.50 ug/L 12/15/19 12:16 1
7
■9
1,1-Dichloroethene ND 0.50 ug/L 12/15/19 12:16 1
1,2-Dichlorobenzene ND 0.50 ug/L 12/15/19 12:16 1
8
1,2-Dichloroethane ND 0.50 ug/L 12/15/19 12:16 1
1,2-Dichloropropane ND 0.50 ug/L 12/15/19 12:16 1
1,3-Dichlorobenzene ND 0.50 ug/L 12/15/19 12:16 1
1,4-Dichlorobenzene ND 0.50 ug/L 12/15/19 12:16 1 10
Benzene ND 0.50 ug/L 12/15/19 12:16 1
Bromoform ND 1.0 ug/L 12/15/19 12:16 1 11
Bromomethane ND 0.50 ug/L 12/15/19 12:16 1
Carbon tetrachloride ND 0.50 ug/L 12/15/19 12:16 1 12
Chlorobenzene ND 0.50 ug/L 12/15/19 12:16 1
Dibromochloromethane ND 0.50 ug/L 12/15/19 12:16 1 13
Chloroethane ND 1.0 ug/L 12/15/19 12:16 1
Chloroform ND 0.50 ug/L 12/15/19 12:16 1 14
Chloromethane ND 0.50 ug/L 12/15/19 12:16 1
cis-1,2-Dichloroethene ND 0.50 ug/L 12/15/19 12:16 1
cis-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 12:16 1
15
Bromodichloromethane ND 0.50 ug/L 12/15/19 12:16 1
Ethylbenzene ND 0.50 ug/L 12/15/19 12:16 1
Methyl tert-butyl ether ND 0.50 ug/L 12/15/19 12:16 1
Methylene Chloride ND 2.0 ug/L 12/15/19 12:16 1
Tetrachloroethene ND 0.50 ug/L 12/15/19 12:16 1
Toluene ND 0.50 ug/L 12/15/19 12:16 1
trans-1,2-Dichloroethene ND 0.50 ug/L 12/15/19 12:16 1
trans-1,3-Dichloropropene ND 0.50 ug/L 12/15/19 12:16 1
Trichloroethene ND 0.50 ug/L 12/15/19 12:16 1
Trichlorofluoromethane ND 0.50 ug/L 12/15/19 12:16 1
Vinyl chloride ND 0.50 ug/L 12/15/19 12:16 1
MB MB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
4-Bromofluorobenzene (Surr) 93 60 - 140 12/15/19 12:16 1
Dibromofluoromethane (Surr) 105 60 - 140 12/15/19 12:16 1
Lab Sample ID: LCS 440-586032/1002 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 586032
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
- - - - - - - - - - - - - - -
Page 9 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCS 440-586032/1002 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 586032
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
5
- - - - - - - - - - - - -
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 96 60 - 140
Dibromofluoromethane (Surr) 101 60 - 140
Lab Sample ID: LCS 440-586378/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 586378
Spike LCS LCS %Rec.
L- - - - - - - - - - -
Analyte
Total Dissolved Solids
Added
1000
Result Qualifier
974
Unit
mg/L
D %Rec
97
Limits
90 - 110 --
Eurofins TestAmerica, Pleasanton
Page 10 of 20 12/19/2019
QC Association Summary 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
GC/MS VOA
3
Analysis Batch: 586032
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 4
720-96482-1 275NEC-EFT Total/NA Water 624.1
720-96482-2 TRIP BLANK Total/NA Water 624.1 5
MB 440-586032/4 Method Blank Total/NA Water 624.1
■
720-96482-1 275NEC-EFT Total/NA Water SM 2540C
MB 440-586378/1 Method Blank Total/NA Water SM 2540C
9
LLCS 440-586378/2 Lab Control Sample Total/NA Water SM 2540C
10
11
12
13
14
15
Page 11 of 20 12/19/2019
Lab Chronicle 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Client Sample ID: 275NEC-EFT Lab Sample ID: 720-96482-1
Date Collected: 12/10/19 09:50 Matrix: Water
3
Date Received: 12/10/19 14:19
4
i
-
Prep Type
-
Batch
Type
Batch
Method Run
Dil
Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed Analyst Lab 5
Total/NA Analysis 624.1 1 10 mL 10 mL 586032 12/15/19 16:40 JB TAL IRV
LTotal/NA Analysis SM 2540C 1 100 mL 100 mL 586378 12/17/19 09:10 XL TAL IRV 6
Client Sample ID: TRIP BLANK Lab Sample ID: 720-96482-2 7
Date Collected: 12/10/19 00:00 Matrix: Water
Date Received: 12/10/19 14:19 8
iPrep Type
Batch
Type
Batch
Method Run
Dil
Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed Analyst Lab 9
LTotal/NA Analysis 624.1 1 10 mL 10 mL 586032 12/15/19 17:08 JB TAL IRV
Laboratory References:
TAL IRV = Eurofins TestAmerica, Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022
■
10
11
12
13
14
15
Page 12 of 20 12/19/2019
Accreditation/Certification Summary 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
Laboratory: Eurofins TestAmerica, Pleasanton
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. 3
Authority Program Identification Number Expiration Date 4
California State 2496 01-31-20
■56
USDA US Federal Programs P330-18-00328 11-06-21
California
Districts
State 2706 06-30-20
9
Guam State 19-005R 01-23-20
Hawaii State CA01531 01-29-20
10
■
Kansas NELAP E-10420 07-31-20
Nevada State CA015312020-4 07-31-20
11
New Mexico State CA01531 01-29-20
Oregon NELAP 4028 - 006 01-29-20 12
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA US Federal Programs P330-18-00214 07-09-21 13
Washington State C900 09-03-20
14
15
Page 13 of 20 12/19/2019
Method Summary 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
3
Method Method Description Protocol Laboratory
624.1 Volatile Organic Compounds (GC/MS) 40CFR136A TAL IRV
SM 2540C Solids, Total Dissolved (TDS) SM TAL IRV
4
Protocol References:
5
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions. 6
SM = "Standard Methods For The Examination Of Water And Wastewater"
7
Laboratory References:
TAL IRV = Eurofins TestAmerica, Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022 8
9
10
11
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12
13
14
15
Page 14 of 20 12/19/2019
Sample Summary 1
Client: Locus Technologies Job ID: 720-96482-1
Project/Site: NEC 2
3
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
720-96482-1 275NEC-EFT Water 12/10/19 09:50 12/10/19 14:19
720-96482-2 TRIP BLANK Water 12/10/19 00:00 12/10/19 14:19
4
5
6
7
8
9
10
11
12
■
13
14
15
Page 15 of 20 12/19/2019
720 .. tl[fff:z,_ i,.ocus CHAIN-OF-CUSTODY RECORD ~/93f~1 SERIAL NO .
/V!.E C----~
.··· TECHNOLOGIES (See Reverse for Instructions) (7, 1514'1
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Container Sealed with Custody Seal: Yes D No D
Method of Shipment Description of Other Chains-of-Custody Dispatched By: (Signature) Date Time Received for lab By: (Signature) Date Time
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WALNUT CREEK• 1701 N. CALIFORNIA BLVD• WALNUT CREEK, CA 94596 • TEL (925) 906-8100 • FAX (925) 906-8101
0 SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
0 OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ FAX _ _ _ __
REV. 6/02
WHITE: Laboratcxy Copy YELLOW: Project Copy PINK: Database Copy
15
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Eurofins TestAmerica, Pleasanton
1220 Quarry Lane
Pleasanton, CA 94566
Chain of Custody Record lllffllllllllll -:::' eurofins Envnonmr. nt Test ing
TestAmcrrca
I
State, zip ·\~ .. D • Nitric Acid
CA, 92614-5817 ,'l!j Lil ' E-NaHS04 Q . Na2SO3
, ~~ f!! F-MeOH R- Na2S2O3
Phone PO# ~:~. :E ' G • Amchlor S -H2SO4
949-261-1022(Tel) 949-260-3297(Fax) 1-s ~ ~ , H-Ascom1cAc1d T - TSP Dodecahydrate
U-Acetone
Email: WO#:
~ ' !:!c '' I - Ice
J-OI Water V-MCAA
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Project Name Project # 1 ' { A
NEC
Site
72014506
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Page 17 of 20
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275NEC-EFT (720-96482- 1) 12/10/19
Pacific
Water XIX 4
TRIP BLANK (720-96482-2) 12/10/19 f:>acific Water X ·:3
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Note Since laboratory accred1tat1ons are subJect to change, Eurofins- TestAmenca places the ownership of method, analyte & accreditation compliance upoll out subcontract laboratories. This sampfe shipment 1s forwarded under chaln--of.-eustody If the laboratory does not currently
ma1nta1n accred1tallon m the State of Ongm listed above for analysis/tests/matnx being analyzed, the samples must be shipped back to the Eurofins TestAmer1ca laboratory or other instructions W1U be provided Any changes to accred1taUon status should be brovght to Eurofins
ITestAmenca attenton 1mmed1ately if all requested accredttat:lons are current to date, return the signed Chain of Custody attesting to said complteance to Euroflns TestAmerica
Possible Hazard Identification S8mple Disposal ( A fee may be assessed If samples are retained longer than 1 month)
Unconfrrmed □ Return To Client □ Disposal By Lab □ Archive For Months
Deliverable Requested. I, II, Ill, IV, Other (specify) Primary Deliverable Rank. 2 Special Instructions/QC Requirements:
■
15
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9
8
7
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1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-96482-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
TotalAccess
Have a Question.
. ,
k This report has been electronically signed and authorized by the signatory. Electronic signature is
The
~ intended to be the legally binding equivalent of a traditionally handwritten signature.
Ex ert Results relate only to the items tested and the sample(s) as received by the laboratory.
Visit us at:
www.testamericainc.com
Client: Locus Technologies Laboratory Job ID: 720-96481-1 1
Project/Site: NEC
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
9
8
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 9
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 12
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
20
13
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
15
Glossary 5
Abbreviation These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
6
%R Percent Recovery
CFL Contains Free Liquid 7
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference) 8
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE) 9
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry) 10
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE) 11
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry) 12
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
13
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
14
PQL Practical Quantitation Limit
QC Quality Control 15
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Page 3 of 20 12/19/2019
Case Narrative 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Job ID: 720-96481-1 3
Laboratory: Eurofins TestAmerica, Pleasanton
4
Narrative
Job Narrative 5
720-96481-1
6
Comments
No additional comments. 7
Receipt
The sample was received on 12/10/2019 2:19 PM; the sample arrived in good condition, properly preserved and, where required, on ice. 8
The temperature of the cooler at receipt was 1.6º C.
9
GC/MS VOA
Method 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 720-277577 10
recovered outside control limits for the following analytes: 1,2,4-Trimethylbenzene, 1,2-Dichloroethane and 1,1,1-Trichloroethane. These
analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.
11
Method 8260B: No MS/MSD were reported for the following samples due to an autosampler error: 275NEC-01AE (720-96481-1).
12
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
13
14
15
Page 5 of 20 12/19/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Client Sample ID: 275NEC-01AE Lab Sample ID: 720-96481-1
Date Collected: 12/10/19 10:45 Matrix: Water
3
Date Received: 12/10/19 14:19
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
Methyl tert-butyl ether ND 0.50 ug/L 12/17/19 17:18 1
Acetone ND 50 ug/L 12/17/19 17:18 1 6
Benzene ND 0.50 ug/L 12/17/19 17:18 1
Dichlorobromomethane ND 0.50 ug/L 12/17/19 17:18 1
Bromobenzene ND 1.0 ug/L 12/17/19 17:18 1
7
Chlorobromomethane ND 1.0 ug/L 12/17/19 17:18 1
Bromoform ND 1.0 ug/L 12/17/19 17:18 1
8
Bromomethane ND 1.0 ug/L 12/17/19 17:18 1
2-Butanone (MEK) ND 50 ug/L 12/17/19 17:18 1
9
n-Butylbenzene ND 1.0 ug/L 12/17/19 17:18 1
sec-Butylbenzene ND 1.0 ug/L 12/17/19 17:18 1 10
tert-Butylbenzene ND 1.0 ug/L 12/17/19 17:18 1
Carbon disulfide ND 5.0 ug/L 12/17/19 17:18 1 11
Carbon tetrachloride ND 0.50 ug/L 12/17/19 17:18 1
Chlorobenzene ND 0.50 ug/L 12/17/19 17:18 1 12
Chloroethane ND 1.0 ug/L 12/17/19 17:18 1
Chloroform ND 1.0 ug/L 12/17/19 17:18 1 13
Chloromethane ND 1.0 ug/L 12/17/19 17:18 1
2-Chlorotoluene ND 0.50 ug/L 12/17/19 17:18 1 14
4-Chlorotoluene ND 0.50 ug/L 12/17/19 17:18 1
Chlorodibromomethane ND 0.50 ug/L 12/17/19 17:18 1
1,2-Dichlorobenzene ND 0.50 ug/L 12/17/19 17:18 1
15
1,3-Dichlorobenzene ND 0.50 ug/L 12/17/19 17:18 1
1,4-Dichlorobenzene ND 0.50 ug/L 12/17/19 17:18 1
1,3-Dichloropropane ND 1.0 ug/L 12/17/19 17:18 1
1,1-Dichloropropene ND 0.50 ug/L 12/17/19 17:18 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 12/17/19 17:18 1
Ethylene Dibromide ND 0.50 ug/L 12/17/19 17:18 1
Dibromomethane ND 0.50 ug/L 12/17/19 17:18 1
Dichlorodifluoromethane ND 0.50 ug/L 12/17/19 17:18 1
1,1-Dichloroethane ND 0.50 ug/L 12/17/19 17:18 1
1,2-Dichloroethane ND * 0.50 ug/L 12/17/19 17:18 1
1,1-Dichloroethene ND 0.50 ug/L 12/17/19 17:18 1
cis-1,2-Dichloroethene 24 0.50 ug/L 12/17/19 17:18 1
trans-1,2-Dichloroethene 2.1 0.50 ug/L 12/17/19 17:18 1
1,2-Dichloropropane ND 0.50 ug/L 12/17/19 17:18 1
cis-1,3-Dichloropropene ND 0.50 ug/L 12/17/19 17:18 1
trans-1,3-Dichloropropene ND 0.50 ug/L 12/17/19 17:18 1
Ethylbenzene ND 0.50 ug/L 12/17/19 17:18 1
Hexachlorobutadiene ND 1.0 ug/L 12/17/19 17:18 1
2-Hexanone ND 50 ug/L 12/17/19 17:18 1
Isopropylbenzene ND 0.50 ug/L 12/17/19 17:18 1
4-Isopropyltoluene ND 1.0 ug/L 12/17/19 17:18 1
Methylene Chloride ND 5.0 ug/L 12/17/19 17:18 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 12/17/19 17:18 1
Naphthalene ND 1.0 ug/L 12/17/19 17:18 1
N-Propylbenzene ND 1.0 ug/L 12/17/19 17:18 1
Styrene ND 0.50 ug/L 12/17/19 17:18 1
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 12/17/19 17:18 1
Page 6 of 20 12/19/2019
Client Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Client Sample ID: 275NEC-01AE Lab Sample ID: 720-96481-1
Date Collected: 12/10/19 10:45 Matrix: Water
3
Date Received: 12/10/19 14:19
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 12/17/19 17:18 1
Tetrachloroethene ND 0.50 ug/L 12/17/19 17:18 1 6
Toluene ND 0.50 ug/L 12/17/19 17:18 1
1,2,3-Trichlorobenzene ND 1.0 ug/L 12/17/19 17:18 1
1,2,4-Trichlorobenzene ND 1.0 ug/L 12/17/19 17:18 1
7
1,1,1-Trichloroethane ND * 0.50 ug/L 12/17/19 17:18 1
1,1,2-Trichloroethane ND 0.50 ug/L 12/17/19 17:18 1
8
Trichloroethene 20 0.50 ug/L 12/17/19 17:18 1
Trichlorofluoromethane ND 1.0 ug/L 12/17/19 17:18 1
9
1,2,3-Trichloropropane ND 1.0 ug/L 12/17/19 17:18 1
1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.50 ug/L 12/17/19 17:18 1 10
1,2,4-Trimethylbenzene ND * 0.50 ug/L 12/17/19 17:18 1
1,3,5-Trimethylbenzene ND 0.50 ug/L 12/17/19 17:18 1 11
Vinyl acetate ND 10 ug/L 12/17/19 17:18 1
Vinyl chloride ND 0.50 ug/L 12/17/19 17:18 1 12
Xylenes, Total ND 0.50 ug/L 12/17/19 17:18 1
2,2-Dichloropropane ND 0.50 ug/L 12/17/19 17:18 1 13
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
4-Bromofluorobenzene 100 67 - 130 12/17/19 17:18 1
14
1,2-Dichloroethane-d4 (Surr) 123 72 - 130 12/17/19 17:18 1
15
LToluene-d8 (Surr) 100 70 - 130 12/17/19 17:18 1
Page 7 of 20 12/19/2019
Surrogate Summary 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
3
Percent Surrogate Recovery (Acceptance Limits) 4
BFB DCA TOL
Lab Sample ID Client Sample ID (67-130) (72-130) (70-130) 5
720-96481-1 275NEC-01AE 100 123 100
LCS 720-277577/5 Lab Control Sample 104 118 102 6
LCSD 720-277577/6 Lab Control Sample Dup 106 116 102
MB 720-277577/4 Method Blank 105 119 100
7
Surrogate Legend
BFB = 4-Bromofluorobenzene 8
DCA = 1,2-Dichloroethane-d4 (Surr)
Page 8 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 720-277577/4 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 277577
MB MB 5
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Methyl tert-butyl ether ND 0.50 ug/L 12/17/19 12:10 1 6
Acetone ND 50 ug/L 12/17/19 12:10 1
Benzene ND 0.50 ug/L 12/17/19 12:10 1
Dichlorobromomethane ND 0.50 ug/L 12/17/19 12:10 1
7
■9
Bromobenzene ND 1.0 ug/L 12/17/19 12:10 1
Chlorobromomethane ND 1.0 ug/L 12/17/19 12:10 1
8
Bromoform ND 1.0 ug/L 12/17/19 12:10 1
Bromomethane ND 1.0 ug/L 12/17/19 12:10 1
2-Butanone (MEK) ND 50 ug/L 12/17/19 12:10 1
n-Butylbenzene ND 1.0 ug/L 12/17/19 12:10 1 10
sec-Butylbenzene ND 1.0 ug/L 12/17/19 12:10 1
tert-Butylbenzene ND 1.0 ug/L 12/17/19 12:10 1 11
Carbon disulfide ND 5.0 ug/L 12/17/19 12:10 1
Carbon tetrachloride ND 0.50 ug/L 12/17/19 12:10 1 12
Chlorobenzene ND 0.50 ug/L 12/17/19 12:10 1
Chloroethane ND 1.0 ug/L 12/17/19 12:10 1 13
Chloroform ND 1.0 ug/L 12/17/19 12:10 1
Chloromethane ND 1.0 ug/L 12/17/19 12:10 1 14
2-Chlorotoluene ND 0.50 ug/L 12/17/19 12:10 1
4-Chlorotoluene ND 0.50 ug/L 12/17/19 12:10 1
Chlorodibromomethane ND 0.50 ug/L 12/17/19 12:10 1
15
1,2-Dichlorobenzene ND 0.50 ug/L 12/17/19 12:10 1
1,3-Dichlorobenzene ND 0.50 ug/L 12/17/19 12:10 1
1,4-Dichlorobenzene ND 0.50 ug/L 12/17/19 12:10 1
1,3-Dichloropropane ND 1.0 ug/L 12/17/19 12:10 1
1,1-Dichloropropene ND 0.50 ug/L 12/17/19 12:10 1
1,2-Dibromo-3-Chloropropane ND 1.0 ug/L 12/17/19 12:10 1
Ethylene Dibromide ND 0.50 ug/L 12/17/19 12:10 1
Dibromomethane ND 0.50 ug/L 12/17/19 12:10 1
Dichlorodifluoromethane ND 0.50 ug/L 12/17/19 12:10 1
1,1-Dichloroethane ND 0.50 ug/L 12/17/19 12:10 1
1,2-Dichloroethane ND 0.50 ug/L 12/17/19 12:10 1
1,1-Dichloroethene ND 0.50 ug/L 12/17/19 12:10 1
cis-1,2-Dichloroethene ND 0.50 ug/L 12/17/19 12:10 1
trans-1,2-Dichloroethene ND 0.50 ug/L 12/17/19 12:10 1
1,2-Dichloropropane ND 0.50 ug/L 12/17/19 12:10 1
cis-1,3-Dichloropropene ND 0.50 ug/L 12/17/19 12:10 1
trans-1,3-Dichloropropene ND 0.50 ug/L 12/17/19 12:10 1
Ethylbenzene ND 0.50 ug/L 12/17/19 12:10 1
Hexachlorobutadiene ND 1.0 ug/L 12/17/19 12:10 1
2-Hexanone ND 50 ug/L 12/17/19 12:10 1
Isopropylbenzene ND 0.50 ug/L 12/17/19 12:10 1
4-Isopropyltoluene ND 1.0 ug/L 12/17/19 12:10 1
Methylene Chloride ND 5.0 ug/L 12/17/19 12:10 1
4-Methyl-2-pentanone (MIBK) ND 50 ug/L 12/17/19 12:10 1
Naphthalene ND 1.0 ug/L 12/17/19 12:10 1
N-Propylbenzene ND 1.0 ug/L 12/17/19 12:10 1
Styrene ND 0.50 ug/L 12/17/19 12:10 1
Page 9 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: MB 720-277577/4 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 277577
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
5
1,1,1,2-Tetrachloroethane ND 0.50 ug/L 12/17/19 12:10 1
1,1,2,2-Tetrachloroethane ND 0.50 ug/L 12/17/19 12:10 1
6
Tetrachloroethene ND 0.50 ug/L 12/17/19 12:10 1
Toluene ND 0.50 ug/L 12/17/19 12:10 1
7
1,2,3-Trichlorobenzene ND 1.0 ug/L 12/17/19 12:10 1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
1.0
0.50
0.50
ug/L
ug/L
ug/L
12/17/19 12:10
12/17/19 12:10
12/17/19 12:10
1
1
1
■9
8
Page 10 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCS 720-277577/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 277577
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
5
- - - - - - - - - - - - - - -
Page 11 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
LCS LCS
Surrogate %Recovery Qualifier Limits 4
4-Bromofluorobenzene 104 67 - 130
1,2-Dichloroethane-d4 (Surr) 118 72 - 130 5
LToluene-d8 (Surr) 102 70 - 130
6
Lab Sample ID: LCSD 720-277577/6 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA 7
Analysis Batch: 277577
■9
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
8
Methyl tert-butyl ether 25.0 28.9 ug/L 116 70 - 130 1 20
Acetone 125 124 ug/L 99 61 - 147 13 30
Benzene 25.0 26.1 ug/L 104 79 - 119 1 20
Dichlorobromomethane 25.0 29.9 ug/L 120 81 - 130 0 20 10
Bromobenzene 25.0 27.4 ug/L 110 77 - 117 1 20
Chlorobromomethane 25.0 27.6 ug/L 111 81 - 122 0 20 11
Bromoform 25.0 31.2 ug/L 125 75 - 127 2 20
Bromomethane 25.0 27.5 ug/L 110 70 - 132 0 20 12
2-Butanone (MEK) 125 134 ug/L 107 66 - 133 2 22
n-Butylbenzene 25.0 28.1 ug/L 112 78 - 119 0 20 13
sec-Butylbenzene 25.0 28.5 ug/L 114 78 - 118 3 20
tert-Butylbenzene 25.0 28.9 ug/L 116 78 - 118 2 20 14
Carbon disulfide 25.0 26.4 ug/L 105 64 - 127 0 20
Carbon tetrachloride 25.0 35.2 ug/L 141 72 - 142 0 20
Chlorobenzene 25.0 26.9 ug/L 108 76 - 116 0 20
15
Chloroethane 25.0 25.7 ug/L 103 70 - 131 4 20
Chloroform 25.0 28.5 ug/L 114 82 - 119 1 20
Chloromethane 25.0 25.2 ug/L 101 49 - 134 3 20
2-Chlorotoluene 25.0 27.2 ug/L 109 75 - 115 2 20
4-Chlorotoluene 25.0 28.1 ug/L 112 73 - 119 2 20
Chlorodibromomethane 25.0 30.5 ug/L 122 77 - 133 0 20
1,2-Dichlorobenzene 25.0 27.2 ug/L 109 77 - 117 0 20
1,3-Dichlorobenzene 25.0 27.9 ug/L 111 76 - 116 2 20
1,4-Dichlorobenzene 25.0 27.9 ug/L 112 76 - 116 0 20
1,3-Dichloropropane 25.0 26.9 ug/L 108 77 - 117 3 20
1,1-Dichloropropene 25.0 28.4 ug/L 113 83 - 130 1 20
1,2-Dibromo-3-Chloropropane 25.0 27.7 ug/L 111 74 - 126 1 20
Ethylene Dibromide 25.0 27.3 ug/L 109 80 - 121 1 20
Dibromomethane 25.0 26.9 ug/L 108 79 - 117 1 20
Dichlorodifluoromethane 25.0 30.9 ug/L 123 21 - 150 1 20
1,1-Dichloroethane 25.0 26.3 ug/L 105 77 - 119 1 20
1,2-Dichloroethane 25.0 31.0 * ug/L 124 73 - 122 3 20
1,1-Dichloroethene 25.0 26.6 ug/L 107 69 - 119 1 20
cis-1,2-Dichloroethene 25.0 26.8 ug/L 107 77 - 117 1 20
trans-1,2-Dichloroethene 25.0 26.9 ug/L 108 79 - 117 2 20
1,2-Dichloropropane 25.0 24.6 ug/L 98 79 - 119 0 20
cis-1,3-Dichloropropene 25.0 27.8 ug/L 111 82 - 119 0 20
trans-1,3-Dichloropropene 25.0 29.5 ug/L 118 76 - 122 2 20
Ethylbenzene 25.0 28.5 ug/L 114 77 - 117 1 20
Hexachlorobutadiene 25.0 29.3 ug/L 117 78 - 140 0 20
2-Hexanone 125 126 ug/L 101 63 - 140 2 24
Isopropylbenzene 25.0 29.4 ug/L 118 77 - 130 1 20
Page 12 of 20 12/19/2019
QC Sample Results 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: LCSD 720-277577/6 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA 4
Analysis Batch: 277577
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
5
- - - - - - - - - - - - - - -
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene 106 67 - 130
1,2-Dichloroethane-d4 (Surr) 116 72 - 130
Page 13 of 20 12/19/2019
QC Association Summary 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
GC/MS VOA
3
Analysis Batch: 277577
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 4
720-96481-1 275NEC-01AE Total/NA Water 8260B
MB 720-277577/4 Method Blank Total/NA Water 8260B 5
LCS 720-277577/5 Lab Control Sample Total/NA Water 8260B
■9
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Page 14 of 20 12/19/2019
Lab Chronicle 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Client Sample ID: 275NEC-01AE Lab Sample ID: 720-96481-1
Date Collected: 12/10/19 10:45 Matrix: Water
3
Date Received: 12/10/19 14:19
4
i Batch Batch Dil Initial Final Batch Prepared
5
L- - - - - - - - - - - - - - -
Prep Type
Total/NA
Type
Analysis
Method
8260B
Run Factor
1
Amount
10 mL
Amount
10 mL
Number
277577
or Analyzed Analyst
12/17/19 17:18 AJS
Lab
TAL PLS
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919
7
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Page 15 of 20 12/19/2019
Accreditation/Certification Summary 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
Laboratory: Eurofins TestAmerica, Pleasanton
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report. 3
Authority Program Identification Number Expiration Date 4
California State 2496 01-31-20
■56
USDA US Federal Programs P330-18-00328 11-06-21
7
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Page 16 of 20 12/19/2019
Method Summary 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
3
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL PLS
5030B Purge and Trap SW846 TAL PLS
4
Protocol References:
5
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
6
Laboratory References:
TAL PLS = Eurofins TestAmerica, Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919 7
8
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12
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Page 17 of 20 12/19/2019
Sample Summary 1
Client: Locus Technologies Job ID: 720-96481-1
Project/Site: NEC 2
3
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
720-96481-1 275NEC-01AE Water 12/10/19 10:45 12/10/19 14:19
4
5
6
7
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Page 18 of 20 12/19/2019
••·OCUS
...
7Z~· l//?"HJ Atf'3[?1.~ SERIAL NO.
TECHNOLOGIES CHAIN-6F-CUSTQOV"lfECQRD (See Reverse for ,;tfuctions) .?'_,I 151'1~
PROJECT NAME _lf/'£C.. SAMPLERS _ _ _ _ _ _ _ _ _ _ __
SAMPLE CONTAINER SAMPLE DESCRIPTION CODES TAT CODES
(PRINT}
PROJECT NUMBER C, f?-c) 0 '7 -9 9 -~;J..-& 0 DESCRIPTION CODES
fA') 40-ml VOA Vial
~ Ground Water
Surface Water
F.
G.
Oil
Waste ~ Standard
(SIGN)
RECORDER ~..rf=A-'1-1- €rt-~ ½{ Glass Liter
C. Plastic 500-ml
E. Brass Tube
F. Other _ __
C. Leachate
D. Rinseate
H.
I.
Blank/Spike
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2. 48 Hour
3. 24 Hour
(SIGN} D. Plastic Liter E. SoiVSediment 4. Other _ __
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Page 19 of 20
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I I I I I · I____ _ ILU-!:!o4~1 Chain of Custody ,I
16 I I I I I I II 1 lr
NOTES/ MISCELLANEOUS Field/ Container Temp. 1Reli~gnature) ~f1'ed ~: (Sig~ Date Time ,,-
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Time I
Container Sealed with Custody Seal: Yes D No0
Method of Shipment I Description of Other Chains-of-Custody Dispatched By: (Signature) Date Time Date Time
Transport Container Transported with this
~~e~ /.2-itJ--t?
Chain (by Serial No.)
ll-ro--1~\ t f / 9'
Send Lab Results to (Name): /V'«l"'-o/ 0e~4~ Le ..Pev--re/4Ltv~':1:4-. (Check Office Below) Verbals Requested: Yes D No D
0
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MOUNTAIN VIEW• 299 FAIRCHILD DRIVE• MTN VIEW, CA 94043 • TEL (650) 960-1640 • FAX (650) 960-0739 ,
12/19/2019
WALNUT CREEK• 1701 N. CALIFORNIA BLVD• WALNUT CREEK, CA 94596 • TEL (925) 906-8100 • FAX (925) 906-8101
0
0
SACRAMENTO• 1100 MELODY LANE• ROSEVILLE, CA 95678 • TEL (916) 677-1751 • FAX (916) 677-1760
OTHER _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ TEL _ _ _ _ _ FAX _ _ _ __
I.be
REV.6/02
WHITE: Laboratory Copy YELLOW: Project Copy PINK: Database Copy
15
14
13
12
11
10
9
8
7
6
5
4
3
2
1
1
Login Sample Receipt Checklist
2
Client: Locus Technologies Job Number: 720-96481-1 3
■
Sample containers have legible labels. True
Containers are not broken or leaking. True
15
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Table D-1
Comparison of Analytical Laboratory Quality Control Results
2019 Annual Progress Report
501 Ellis Street, Mountain View, California
Accuracy Accuracy
Date Laboratory Precision
Method Analyte Spike % Duplicate % (2)
Analyzed Batch Number RPD
REC (1) REC (1)
EPA 624 3/8/2019 268441 1,1-Dichloroethene 99 94 4.6
Batch Spike Benzene 105 105 0.4
Trichloroethene 98 98 0.1
Toluene 95 93 2.2
Chlorobenzene 98 96 1.2
EPA 8260B 3/8/2019 268441 1,1-Dichloroethene 99 94 4.6
Batch Spike MTBE 90 92 3.1
Benzene 105 105 0.4
Trichloroethene 98 98 0.1
Toluene 95 93 2.2
Chlorobenzene 98 96 1.2
Ethylbenzene 94 93 0.9
m,p-xylenes 96 95 0.7
o-xylenes 97 98 1.1
EPA 624 3/11/2019 268494 1,1-Dichloroethene 106 105 0.7
Batch Spike Benzene 109 107 1.3
Trichloroethene 104 103 0.9
Toluene 92 91 1.5
Chlorobenzene 95 94 0.3
EPA 624 6/20/2019 555711 1,1-Dichloroethene 104 -- --
Batch Spike Trichloroethene 93 -- --
Chlorobenzene 98 -- --
EPA 8260B 6/20/2019 268680 1,1-Dichloroethene 86 85 0.9
Batch Spike Trichloroethene 93 92 0.4
Chlorobenzene 96 92 4.2
EPA 624 9/11/2019 569819 1,1-Dichloroethene 94 -- --
Batch Spike Trichloroethene 104 -- --
Chlorobenzene 107 -- --
EPA 8260B 9/11/2019 272829 1,1-Dichloroethene 93 91 1.7
Batch Spike Trichloroethene 97 97 0.4
Chlorobenzene 94 93 1.3
EPA 624 12/10/2019 586032 1,1-Dichloroethene 117 -- --
Batch Spike Trichloroethene 108 -- --
Chlorobenzene 97 -- --
EPA 8260B 12/10/2019 277577 1,1-Dichloroethene 107 107 0.7
Batch Spike Trichloroethene 113 111 2.1
Chlorobenzene 108 108 0.0
Project Average 100 97 1.4
Project Goals 40-150 40-150 <35
Notes:
(1) % REC - Percent recovery
(2) RPD - Relative percent difference between the batch spike and batch spike duplicate.
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Appendices\Appendix D - Quality Assurance Report\AppD_QAQC Tables_2019AppD_QAQC Tables_2019
Geosyntec Consultants
Table D-2
Summary of Blank Sample Results
2019 Annual Progress Report
501 Ellis Street, Mountain View, California
Notes:
-- - not available
µg/L - micrograms per liter
ND - non detect
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Appendices\Appendix D - Quality Assurance Report\AppD_QAQC Tables_2019AppD_QAQC Tables_2019
Geosyntec Consultants
Table D-3
Duplicate Quality Control Results
2019 Annual Progress Report
501 Ellis Street, Mountain View, California
cis-1,2-Dichloroethene 26 29 10.9
3/4/2019
trans-1,2-Dichloroethene 2.5 2.9 14.8
Trichloroethene 20 21 4.9
Notes:
1
RPD = relative percent difference = |X1-X2|/X3 x 100
where:
X 1 = concentration of the sample
X 2 = concentration of the duplicate
X 3 = average of X1 and X2
µg/L - micrograms per liter
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2019 Annual\Appendices\Appendix D - Quality Assurance Report\AppD_QAQC Tables_2019AppD_QAQC Tables_2019
APPENDIX E
VOC Concentration Mann-Kendall Trend
Analysis
Table E-1
Mann Kendall Statistical Test Summary Table
501 Ellis Street, Mountain View, CA
Notes:
VOC = volatile organic compound
CL = confidence limit
TCE = trichloroethene
cDCE = cis-1,2-dichloroethene
VC = vinyl chloride
< RL = concentrations below reporting limits
P:\PRJ2003REM\NEC_501 Ellis Street\WR0434\EPA Annual Reports\2018 Annual\Appendices\App E Mann Kendall\TblE-1_MannKendall Summary.xlsxTblE-1_MannKendall Summary.xlsx
VOC Concentration Trend Analysis Geosyntec Consultants
501 Ellis Street, Mountain View, California