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Construction and Building Materials 250 (2020) 118890

Contents lists available at ScienceDirect

Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Technical feasibility of using recycled aggregates to produce eco-friendly


urban furniture
Zoraida Sánchez-Roldán a, María Martín-Morales a, Ignacio Valverde-Espinosa a, Montserrat Zamorano b,⇑
a
Department of Building Construction, University of Granada, High Technical School of Building Engineering, Fuentenueva Campus s/n, 18071 Granada, Spain
b
Department of Civil Engineering, University of Granada, High Technical School of Civil Engineering, Fuentenueva Campus s/n, 18071 Granada, Spain

h i g h l i g h t s

 Recycled aggregates were maximised in manufacturing eco-friendly urban furniture.


 Using recycled aggregates is technically feasible to produce concrete benches.
 Recycled benches put into service were as durable as conventional ones.

a r t i c l e i n f o a b s t r a c t

Article history: The construction sector is characterised by high resource consumption and waste production.
Received 21 October 2019 Consequently, current European policy aims for maximum use of available resources through converting
Received in revised form 23 March 2020 waste into new raw materials. In this context, using recycled aggregates in less demanding technical
Accepted 24 March 2020
applications, such as pieces for urban furniture, could help to maximise the use of these granular mate-
Available online 3 April 2020
rials. In this research, partial and total replacement of natural aggregates has been used to produced eco-
friendly benches that meet technical requirements, for surface characteristics, compression strength and
Keywords:
water absorption. Putting benches into service for 24 months has shown a slight decrease in compression
Recycling
Construction and demolition waste
strength and water absorption values for pieces produced with recycled aggregate; nevertheless, the val-
Recycled coarse aggregate ues were always within the technical requirements limits. These results and the small hanges measured
Recycled fine aggregate in other properties, such as density, carbonation, rebound index and ultrasonic velocity with similar val-
Total replacement ues to those pieces produced with natural aggregate, lead to the conclusion that using recycled aggre-
Urban furniture gates to produce urban furniture is technically feasible.
In-situ tested Ó 2020 Elsevier Ltd. All rights reserved.
Industrial scale

1. Introduction society towards a circular economy [3,4]. In fact, member states


must recycle 70% of construction and demolition waste (C&DW)
The construction sector is the higher consumer of non- for 2020. Consequently, transforming C&DW into secondary mate-
renewable natural resources, demanding nearly 2700 million tons rials represents a great opportunity [5] that contributes to optimal
of aggregates each year [1]; in addition, it produces a large quantity waste management [6,7], improves resource efficiency and reduces
of waste, estimated at 923 million tons in 2016 [2]. For this reason, costs [3].
this sector’s sustainability is crucial in the environmental policy of Currently, the use of recycled aggregates (RA) is widely studied
the European Union (EU), which has the objective of promoting a for its differences to natural aggregates (NA). One of the most
important differences is the greater water absorption of RA that
restricts its use to producing concrete, especially for fine fractions,
Abbreviations: EU, European Union; C&DW, construction and demolition waste;
RA, recycled aggregate; NA, natural aggregate; RC, recycled concrete; NFA, natural
as a consequence of the cement mortar adhered to the surface [8–
fine aggregate; NCA, natural coarse aggregate; RFA, recycled fine aggregate; RCA, 10] and the presence of ceramic material and impurities [11,12].
recycled coarse aggregate; P-HR, bench manufactured with RA. Higher absorption reduces the amount of water available to be
⇑ Corresponding author at: High Technical School of Civil Engineering, Fuente- combined with cement, with the consequent loss of fluidity and
nueva Campus, 18071 Granada, Spain.
negative effect on the mechanical properties of recycled concrete
E-mail addresses: zorisaro@ugr.es (Z. Sánchez-Roldán), mariam@ugr.es
(M. Martín-Morales), valverde@ugr.es (I. Valverde-Espinosa), zamorano@ugr.es
(RC), among other deficiencies [13]; for this reason, the absorption
(M. Zamorano). value is limiting for both aggregate and concrete [14].

https://doi.org/10.1016/j.conbuildmat.2020.118890
0950-0618/Ó 2020 Elsevier Ltd. All rights reserved.
2 Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890

Consequently, optimizing the concrete production process could structural concrete balustrades, is presented as a highly interesting
make up for the negative aspects related to the use of RA, so results application field due to its great presence in any urban environ-
of laboratory experiments could be transferred to a real or indus- ment. In addition, its lower technical requirements would guaran-
trial scale [15,16], mortars [17,18] or in road works [19,20]. The tee a greater possible use of recycled materials without
application of RA in structural concrete requires the observance compromising final performance [42]. Finally, these pieces would
of some technical requirements which often differ from country be recyclable at the end of their useful life, allowing a growth mar-
to country. For example, the Structural Concrete Instruction ket for RA and some environmental benefits, such as reduced pri-
(EHE-08) limits the use of RA in Spain to those exclusively from mary raw materials consumption, increased C&DW recycling
concrete residues; it also establishes a maximum replacement per- rates and reduced waste disposal in landfills.
centage of 20% by weight of coarse RA for the manufacture of con- Consequently, and to encourage society towards sustainability
crete with a compressive strength value of 40 MPa [14]. in the field of urban furniture through recycling C&DW, this
Comparable restrictions are also included in the standards or research focused on producing non-structural concrete benches
guidelines of other European countries, such as the United King- incorporating RA on an industrial scale and putting them into ser-
dom (BS 8500–2 [21]), Portugal (LNEC E 471 [22]) or Norway (NB vice to assess their technical feasibility under conventional use
26 [23]). conditions over two years. For all that, this research represents
Consequently, the need to explore other possible construction an important contribution to the field of knowledge, as no pub-
applications in which the type and characteristics of the RA are lished full-scale experiences have been found to date.
not so limiting is justified, such as vibro-compressed prefabricated
concrete, paving stone, kerbs, blocks, tiles or hollow blocks [24– 2. Materials and methods
27]. The studies consulted have shown the possibility of replacing
100% of NA with RA, both its fine and coarse fraction; in addition, 2.1. Materials
using recycled materials of highly variable composition, such as
ceramics [24,28], mixed [29,30], concrete [31,32], waste marble The materials used to produce concrete benches are described
[33] or the combination of various types of waste [29,34], is possi- below:
ble. However, to maintain the mechanical requirements, using
greater quantities of cement [25,35], or incorporating mineral  Aggregates. Two types of aggregates were used, natural (NA)
additives, either as a substitute for the cementitious material or and recycled (RA), both fine (0/4 mm) and coarse (4/16 mm),
as a supplement [36,37], is necessary, resulting in increased CO2 which were identified by the acronyms NFA, NCA, RFA and
emissions during the manufacturing process. Only a few studies RCA, respectively. The physical, mechanical and chemical prop-
have assessed the characteristics of structural or prefabricated con- erties, constituents of RCA, and the standards applied are sum-
crete produced with RA on an industrial scale to research its beha- marized in Table 1, according to the specifications established
viour in use conditions, put into service in the short and long term in Article 28, Annexes 15 and 18 of EHE-08 [14], and the tech-
[24,28,30,38–40]. In this context, experimentation is necessary for nical requirements of standard EN 12,620 [43,44]. NA was pro-
using RA for alternative applications on an industrial scale, which duced from limestone crushing from a local quarry in the Sierra
would allow maximizing the use of the resources available in Elvira mountainous massif in Atarfe (Granada, Spain). RA was
C&DW within the framework of the circular economy [3,41] with- obtained from different C&DW by crushing and screening, from
out compromising the final products requirements. In this sense, unselected mixtures and with unknown origins, deposited at
urban furniture, understood as the set of elements for decorative the Inertes Guhilar S.L treatment, recovery and elimination
applications in public space, such as benches, flowerpots or non- plant, located in Alhendín (Granada, Spain). C&DW was

Table 1
Tests for characterising aggregates and reference standards [46–53]

Test EHE-08 [14] EN 12,620 [44] Standard


Particle size Designation Particle size domains for sand/D > 4 mm* – EN 933-1; EN 933-2;
Particle size distribution <1.5 CA; 6–16 FA 0.5–4 CA; 3–22 FA EN 933-2/1M [46,47]
Assessment of fines Fines content (<0.063 mm) <5 RCA* –
Particles smaller than 4 mm <10 RCA* –
Sand equivalent index >70 class of exposure type I, IIa ó IIb;>75 <30 to > 65 EN 933–8:2012 + A1;
other cases EN 933–8:2012-A1:2015/1M [48]
Constituents of RCA Rc – concrete – > 90 to < 50 EN 933–11; EN 933–11:2009/AC [49]
Ru - natural stone – –
Rb - clay masonry units < 5 RCA* < 10 to > 50
Ra - bituminous materials < 1 RCA* > 95 to < 1
Rg – glass –  2 to  25
X – others < 1.0 RCA* <1
FL - floating material in volume – < 0.2 to < 10
Oven-dry particle density (kg/dm3) – > 2.00 EN 1097–6 [50]
Water absorption, WA24h  5 5 RCA1* –
Resistance to fragmentation. Los Angeles test 40 15 to > 60 EN 1097–2 [51]
Water soluble chloride content <0.05 (reinforced concrete);<0.03 presstressed – EN 1744–1:2010 + A1 [52]
concrete;<0.15 consrete in mass
Water soluble sulphate content of RA – –
Acid soluble sulphate content – < 0.2 to > 1.3
Total sulphur content 0.8 < 0.2 to > 1.0
Organic matter Exent –
Acid soluble chloride content of RA <0.5 FA;<1 CA;1 RCA* – EN 1744–5 [53]
1
WA24h not exceeding 5% in ACR used in RC with>20% RA; (*) Limit value given in Annex 15 of EHE-08, applicable only to RA; (-) There is no restriction for this parameter
Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890 3

identified with LER code 17 01 07, according to the European urban furniture, benches were manufactured on an industrial scale.
Waste List [45]. The results of the tests carried out on the aggre- Fig. 1a. shows the shape and dimensions of manufactured benches
gates (Table 2 and Table 3) show that RA quality is similar to that were placed in a public area at the Fuentenueva Campus of the
NA, in all cases complying with the limits established. Despite University of Granada to evaluate the evolution of their properties
RA having shown a slightly higher value of bituminous material over two years.
than permitted by Instruction [14], the low ceramic material
content and absence of organic matter would guarantee its 2.2.1.1. Concrete manufacturing. First, laboratory work was under-
use. Consequently, RA could be used to produce concrete for taken to determine the optimum dosage to obtain the characteris-
non-structural applications. tic strength, 35 MPa [59], recommended for prefabricated urban
 Cement. A white Portland cement with between 6% and 20% furniture [42]. Second, three types of concrete were produced
limestone addition, resistance class 42.5 and high initial using NA, recycled concrete replacing the coarse fraction (RC-C)
strength, designated as BL II/A-L 42.5R UNE 80305, was used. and RC with total replacement of aggregates (RC-T). RA was used
Its characteristics are defined in standard UNE 80,305 [54] without pre-soaking, so a previous adjustment in additive content
and in agreement with the harmonized standard in force: EN was necessary to make up for the loss of free water in the mixture
197–1 [55], Instruction for the reception of cements [56], as due to the higher absorption and ensure a soft consistency for all
well as in the Instruction on Structural Concrete [14]. concrete samples, according to the results obtained in previous
 Additive. A new generation superplasticizer based on modified works [60]. Table 4 shows the dosage, by weight, established for
polycarboxylate, ChrysoÒfluid Optima 227, was used in accor- each type of concrete manufactured. Finally, three types of con-
dance with EN 934–1 [48] and EN 934–2 [57] and EN 934–2 crete benches were produced using the optimal dosages previously
[58]. It has been used to increase workability without modifying determined for NC, RC-C and RC-T, which were called P-NC, P-RC-C
the water content, as established in Article 29 ‘‘Additives” and and P-RC-T, respectively, as shown in Table 5. Two units of each
Annex 15 of the Instruction on Structural Concrete [14]; in addi- type were manufactured following the standard production line
tion, it was allowed to maintain the soft-type consistency used in the factory. For its production, the requirements that must
design values to compensate for the water demand required be satisfied by precast concrete products and finished products are
by the RA. in EN 13,369 [61] and EN 13,198 [42] standards, respectively.
 Steel. To avoid cracking in the concrete pieces manufactured on Pieces were demoulded one day after pouring and were stored
an industrial scale, electro-welded mesh type reinforcing bars, inside an industrial warehouse with relatively constant tempera-
15  15 mm and 8 mm in diameter, were used; this material ture and humidity conditions (Fig. 1b). To guarantee the best per-
complies with the requirements in Article 32 ‘‘Steels for passive formance and durability of the prefabricated benches, they were
reinforcement” of EHE-08 [14]. put into service between the third and fourth month (Fig. 1c).

2.2. Methods 2.2.1.2. Technical feasibility of concrete benches. Two categories of


tests were carried out to technically evaluate the benches pro-
2.2.1. Manufacture and technical feasibility of concrete benches duced; one was performed on the concrete produced and the other
A great variety of products are usually produced for urban fur- on the benches themselves. These tests, the standards used and the
niture; one of the most commonly used are benches. So, to assess limit values recommended by EN 13,198 [42] are summarized in
the feasibility of producing precast concrete with RA to be used for Table 6. In the case of concrete produced for manufacturing the

Table 2
Results of tests for geometrical, mechanical, physical and chemical properties of aggregates.

Test/Aggregates RFA RCA NFA NCA


Geometrical properties
Particle size Designation FA-0/4-T-R CA-4/16-T-R FA-0/4-T-N CA-4/16-T-N
Particle size distribution Continuous Continuous Continuous Continuous
Assessment of fines Fines content (<0.063 mm) (%) 2.10 ± 0.18 0.30 ± 0.03 0.50 ± 0.002 0.09 ± 0.001
Particles smaller than 4 mm (%) – 6.65 ± 0.84* – –
Sand equivalent index 100 ± 2 – 70 ± 1 –
Mechanical and physical properties
Oven-dry particle density (kg/dm3) 2.26 ± 0.12 2.54 ± 0.02 2.61 ± 0.04 2.72 ± 0.06
Resistance to fragmentation. Los Angeles test – 34 ± 2 – 31 ± 1
Water absorption, WA24h (%) 5.2 ± 0.41 2.1 ± 0.11 1.0 ± 0.10 0.4 ± 0.05
Chemical properties
Water soluble chloride content (%) 0.021 ± 0.005 0.014 ± 0.001 0.001 ± 0.001 0.008 ± 0.003
Acid soluble chloride content of RA (%) 0.014 ± 0.003 0.012 ± 0.004 – –
Water soluble sulphate content of RA (%) 0.53 ± 0.09 0.48 ± 0.12 – –
Acid soluble sulphate content (%) 0.54 ± 0.10 0.43 ± 0.11 0.04 ± 0.01 0.10 ± 0.03
Total sulphur content (%) 0.63 ± 0.13 0.63 ± 0.09 0.10 ± 0.02 0.50 ± 0.04
Organic matter No contain No contain No contain No contain

(-) Test not performed or no restrictions for this parameter; (*) Value outside the established limits

Table 3
Results of classification test for the constituents of recycled coarse aggregate, and the category assigned using EN 12,620 [43]

Constituents of RCA Rc Ru Rc + Ru Rg Rb Ra X X + Rg FL**


Percentage passing by mass 89 ± 3 9.1 ± 0.9 98 ± 4 0.0 ± 0.0 0.2 ± 0.0 1.8 ± 0.2* 0.1 ± 0.0 0.1 ± 0.0 0.0 ± 0.0
Assigned category [43] Rc80 – Rcu95 Rg2- Rb10- Ra5- X1- XRg0.5- FL0.2-

(-) Test not performed or no restrictions for this parameter; (*) Value outside established limits; (**) Floating material, its content is measured in cm3/kg
4 Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890

Fig. 1. (a) Concrete bench dimensions; (b) Benches curing; (c) Putting in service and concrete core extraction.

Table 4
Concrete mixtures dosification (dosage in weight).

Concrete NCA RCA NFA RFA Cement Mixing water Effective w/c Admixture (% respect cement Mixing time Slump
(kg) (kg) (kg) (kg) (kg) (kg) ratio weight) (min.) (cm)
NC 1200 – 800 – 350 158 0.45 0.50 10 6–9
RC-C – 1183 800 – 350 158 0.45 1.75 10 6–9
RC-T – 1183 – 800 350 158 0.45 3.00 10 6–9

Table 5
Designation of the concretes studied.

Concrete type and designation Fine fraction Coarse fraction Concrete Concrete core type
replacement, replacement, benche type by age = N*
NFA by RFA NCA by RCA
NC Natural or reference 0% 0% P-NC P-NC/N
RC-C Recycled 0% 100% P-RC-C P-RC-C/N
RC-T Recycled 100% 100% P-RC-T P-RC-T/N

(*) N = 1, 3, 6, 9, 12 or 24 months

benches, it was necessary to determine water absorption and com- ignation for the type of concrete followed by the age of the
pression strength, according to EN 13,198 [42]; in addition, con- concrete in months (1, 3, 6, 9, 12 or 24) was used, explained in
crete had to comply with the requirements included in Annexes Table 5. Six concrete core extractions and tests were conducted
15 and 18 of Instruction EHE-08 [14]. to obtain the mean value and deviation of each property.
Eight tests were carried out on the benches put into use, either
in situ or on extracted core specimens, as seen in Table 6. The tests 3. Results and discussion
on the finished product, according to EN 13198, allowed the eval-
uation of the geometric characteristics or dimensions, surface 3.1. Concrete characterisation used to produce benches
appearance, compression strength and water absorption of
benches. In addition, the non-destructive tests of rebound number This section summarises and analyses the values of the two lim-
and ultrasound velocity, included in the general standard for pre- iting properties of concrete used to produce non-structural prod-
fabricated products [61], were carried out to develop a better ucts, water absorption and compression strength. The mean
understanding of possible material alterations over time; likewise, values and their standard deviations are shown in Table 7 and they
it was considered of interest to include the modulus of elasticity, have been analysed below.
density and natural carbonation, as these are significant tests
according to studies carried out by various authors [39,62]. For 3.1.1. Water absorption
all this, a follow-up programme was established, which involved Table 7 summarises the water absorption results for the con-
a core extraction taken 1, 3, 6, 9, 12 and 24 months after manufac- cretes produced, showing average values of 1.8, 2.3 and 1.7% in
ture (Fig. 1c); to do this, a drill with a diamond tubular crown was the case of the RC-C, RC-T and NA samples, respectively. These val-
used perpendicular to the direction of concreting, as far as possible ues are below the maximum 6% established by the standard for
from the ends of the piece and in areas where there was no rein- prefabricated elements EN 13,198 and they represent an increase
forcement, in accordance with EN 12504–1 [63]. The slenderness in absorption of 5.8 and 35.3%, strongly conditioned by the fraction
of cored specimens was similar to that of cylindrical specimens of the aggregate replaced and by the quality and nature of the
(length/diameter ratio = 2) to be able to compare the results granular materials used [24,25,66]. The increases observed were
obtained [64,65]; they were also conserved by immersing them lower than those referenced in the literature consulted, with val-
in water at 20 °C + 2 °C for the 48 h before the test, as per the tech- ues ranging from 8.5% [67] to around 30% [68,69] in the case of
nical regulations [63]. For identifying the core specimens, the des- using RCA. The smaller increases in the parameter are related to
Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890 5

Table 6
Control tests for concrete benches.

Requirements Standard Límit EN 13,198 [42] Elements tested


Geometric and surface characteristics EN 13,198 [42] – In-situ
Hardened-state density 4 EN 12390–7 [62] – Concrete cores
Water absorption EN 13,369 [61]  7.5% 1 7%2 6%3 Standard samples/
Concrete cores
Mechanical Compressive strength EN 12390–2 [63], EN 12390–3 [64]; EN 12390–3:2009/ Exempt 1 30 MPa 2 Standard samples/
behaviour AC [65]; EN 12504–1 [66] 35 MPa 3 Concrete cores
Dynamic modulus of elasticity EN 14,146 [67] – Concrete cores
(resonance frequency) 4
Natural carbonation resistance 4 – – Concrete cores
Non- Surface hardness (rebound number) EN 12504-2 [68] – In-situ
destructive Ultrasonic pulse velocity EN 12504-4 [69] – In-situ
testing

(-) No restriction for this parameter.


1
For products for external use, not subjected to freeze–thaw conditions.
2
For products for external use, subjected to freeze–thaw conditions and without melting salts.
3
For products for external use, subjected to freeze–thaw conditions and with melting salts.
4
Requirement not contemplated in the EN 13,198 [42], nor in EN 13,369 [61].

Table 7
Results of the tests carried out in the laboratory phase.

Concrete Water absorption (%) Compressive strength 7 days Compressive strength 28 days Strength development,
(MPa) (MPa) 7–28 days (%)
Mean value Deviation Mean value Deviation Mean value Deviation
NC 1.7 0.06 41.97 0.74 49.15 1.79 85
RC-C 1.8 0.07 40.61 0.51 42.64 0.07 95
RC-T 2.3 0.08 34.76 1.05 39.08 0.68 89

the quality of the aggregates, as has been explained in the previous 3.2. Bench characterisation and follow-up
section.
The laboratory results previously discussed showed the techni-
cal feasibility of using the selected RA to produce non-structural
3.1.2. Compressive strength concrete. For the tests carried out on the benches, the results have
The compression strength of the concretes manufactured was been summarized in Table 8 and Fig. 2 to Fig. 11, and they have
evaluated at 7 and 28 days (Table 7). The results showed a lower been analysed bellow to evaluate their behaviour over time under
value of strength in the case of RC. In fact, the compressive strength real conditions, as well as finding other complementary informa-
of the concrete RC-C was reduced by 3% and 13.2%, compared to tion including geometric and surface characteristics.
the values obtained in NC at 7 days (41.97 MPa) and 28 days
(49.15 MPa), respectively. In concrete RC-T, the percentage reduc-
tion was increased to 17.2 and 20.5% after 7 and 28 days, respec- 3.2.1. Geometric and surface characteristics
tively. The values obtained are within those published by other The surface finish characteristics are considered an important
authors, which ranged from 46% [70] to + 29% [71] at 7 days property in the case of prefabricated urban furniture due to its dec-
and 37% [72] to + 40% [39] at 28 days in the case of the coarse orative function. In this sense, the results showed that the dimen-
fraction replacement with RA. When the NA was totally replaced, sions of the manufactured benches (Table 8) had no changes
the loss of strength ranged from 4% [73] to 44% [74] in the first between natural and recycled pieces, exhibiting parallelism and
few days of age, while after 28 days it decreased from 6% [75] to flatness in the external volume and in the internal walls (Fig. 2).
30% [76,77]. The decreases obtained in this mechanical property Using RA did not affect the external appearance, homogeneity
are attributed to the lower resistance to fragmentation observed and uniformity of colour and texture of the finished product;
in the RA, in addition to its lower density and greater absorption except that a slightly darker colour was detected as RA content
[78], as shown Table 2. Despite this, all the samples of concrete increased (P-RC-T) and negligible surface imperfections at two
manufactured with RA reached the compression strength required, meters distance [42].
35 MPa to 28 days.
In relation to the evolution of resistance over time, the
growth observed at 7 days was faster than at 28 days. In the 3.2.2. Hardened-state density
case of RC, growth values reached 89 and 95% for RC-T and The results show, as in other studies [67,80], that the density
RC-C respectively; both values were higher than the 85% of NC. of RC was not affected by the incorporation of recycled material,
The results in agreement with other researches that have even and did not progress after the first months of curing. Fig. 3
shown higher development percentages using super-plasticizing shows the average density values of the cores extracted from
additives [74], which confirms that the use of additives has a the benches in service for two years of monitoring; it highlights
positive effect on the development of RC initial strength, as well that after 28 days of fabrication, the density of concrete pro-
as over time, working as an extended curing [38,79]. It is also duced with recycled coarse fraction (P-RC-C) and total replace-
considered positive for the demoulding process and putting ment (P-RC-T) was, respectively, 3.8 and 4.8% lower than
pieces into service because it reduces the time interval between pieces manufactured with NA (2,516 kg/dm3). However, at the
production and use, making the production process of prefabri- end of the monitoring period, these percentages were negligible
cated pieces more competitive. for both types of concrete.
6 Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890

ates new cement hydration products beyond those already formed,


which is equivalent to extended curing, as other authors confirmed
[79,81].
If the values of absorption are related to climatic conditions
(Fig. 5) of the area where the pieces were put into service
(Fig. 4), it was possible to observe that their evolution was condi-
tioned by curing, both in the factory and in use conditions. During
the first 3 months, the evolution was marked by curing carried out
in the factory (periodic irrigation with water, under conditions of
stable humidity and temperature, similar of the laboratory). How-
ever, after it was put into service, the absorption values were
affected by environmental conditions; the rainfall in the 6th month
led to a turning point in its development, with a decrease in the
values obtained, mainly in RC. From the 6th to the 12th month,
the absorption coefficients showed few significant changes in all
cases. Finally, from the 12th to the 24th month, water absorption
in NC hardly varied, while in RC there was a sharp decrease. There-
fore, the percentage of variation obtained from 28 days (Fig. 4) to
the two-year follow-up was a decrease of 45 and 48% in P-RC-C
and P-RC-T, respectively, and of 15% in P-NC. The result obtained
is justified because, in addition to the possible effect that climatic
conditions may have had on the curing process and the effect of the
additive, with the passage of time, the natural carbonation of the
material began, decreasing porosity at the edge of the carbonated
samples mainly due to the precipitation of calcium carbonate
inside its porous system, and consequently, reducing the water
absorption capacity of concretes manufactured with RA [82,83].

3.2.4. Mechanical behaviour


The analysis of the mechanical behaviour of the material con-
tained in the manufactured pieces was evaluated using the com-
pressive strength test on the extracted cores and the resonance
frequency method [84], results shown Fig. 6 and Fig. 7 in
respectively.
Fig. 6 shows the influence of using RA, and the evolution of
Fig. 2. Bench images at two meters distance.
compression strength over the two years of monitoring. A strength
decrease was observed in the case of the P-RC benches in compar-
ison with the P-NC. The decrease was higher with total NA replace-
3.2.3. Water absorption ment, reaching a reduction of 9.3% for P-RC-T after 28 days, while
Fig. 4 shows the water absorption coefficients of the cores this value was only 4.7% for P-RC-C; after 24 months similar values
extracted from the prefabricated benches. All values were lower were reached (11.7% and 10.3%, respectively). The observed
than the 6% established in standard EN 13,198 [42] (Table 3), decrease in strength has been explained by the presence of a
although increasing with the percentage of NA replaced. However, greater number of weak points in the RC (aggregate-paste interfa-
at 24th month, a large decrease in water absorption was shown, cial unions), among other factors [85,86]. Despite this, the values
which was 30% lower for both P-RC-C and P-RC-T benches, com- obtained in P-HR benches exceeded the minimum value required
pared to P-NC (3.06%). This result is explained mainly by the higher (35 MPa) [42].
additive percentage used in the industrial process (2.5% in P-RC-C The values of compressive strength were also related to the
and 4% in P-RC-T) to get adequate concrete workability. The dis- climatic conditions (Fig. 5) of the area where the pieces were
persing effect of additives based on modified polycarboxylate cre- put into service (Fig. 6). As in the case of water absorption, the

Table 8
Dimensions of the manufactured benches (value declared by the manufacturer).

Dimensions (m) Declared value P-NC-1 P-NC-2 P-RC-C-1 P-RC-C-2 P-RC-T-1 P-RC-T-2
Mean Dev. Mean Dev. Mean Dev. Mean Dev. Mean Dev. Mean Dev.
Plant Width 0.600 0.603 0.001 0.602 0.005 0.603 0.003 0.603 0.004 0.605 0.000 0.604 0.003
Long 1.900 1.899 0.001 1.901 0.001 1.896 0.002 1.900 0.000 1.899 0.001 1.901 0.001
Elevation Outside height 0.500 0.500 0.005 0.499 0.001 0.503 0.009 0.500 0.002 0.499 0.001 0.501 0.005
Interior height 0.380 0.379 0.005 0.376 0.003 0.381 0.007 0.377 0.002 0.378 0.003 0.379 0.004
Rear left leg thickness 0.120 0.116 0.004 0.118 0.005 0.118 0.005 0.117 0.004 0.117 0.005 0.117 0.004
Front left leg thickness 0.120 0.116 0.006 0.118 0.005 0.117 0.005 0.117 0.005 0.117 0.005 0.117 0.005
Rear right leg thickness 0.120 0.116 0.005 0.117 0.004 0.116 0.005 0.118 0.005 0.116 0.004 0.115 0.005
Front right leg thickness 0.120 0.117 0.005 0.116 0.005 0.116 0.005 0.115 0.005 0.117 0.005 0.115 0.005
Interior rear length 1.660 1.667 0.010 1.666 0.008 1.662 0.009 1.665 0.010 1.666 0.008 1.669 0.008
Interior front length 1.660 1.666 0.010 1.668 0.010 1.663 0.010 1.668 0.010 1.664 0.010 1.668 0.009
Rear seat thickness 0.120 0.122 0.003 0.124 0.003 0.123 0.002 0.124 0.001 0.121 0.002 0.123 0.001
Front seat thickness 0.120 0.121 0.001 0.121 0.001 0.121 0.001 0.121 0.000 0.121 0.001 0.121 0.002
Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890 7

Fig. 3. Density of cored specimens tested.

Fig. 4. Water absorption of cores and the maximum value established in EN 13198 [42].

Fig. 5. Rainfall (mm and days) and maximum relative humidity during the monitoring period in the city of Granada (http://www.ugr.es/~velilla/meteo-albayzin/resumen.
htm).
8 Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890

Fig. 6. Resistance of the cores extracted from each concrete analysed. Minimum strength limit of 35 MPa for the most unfavourable condition [42]

Fig. 7. Modulus of elasticity for the evaluated concretes, calculated on the test cored specimens.

evolution of the resistances was conditioned by the curing sys- 3.2.5. Carbonation weathering
tem, first in the factory, and after, by its exposure to use condi- To analyse the durability of the pieces manufactured and
tions, with a turning point at 6th months with the maximum exposed to use conditions, their natural carbonation was analysed.
values of strength (due to precipitations). The percentage of total The natural carbonation of the concrete surface, exposed to the
variation obtained, from 28 days to 24th months, was 11.5% in P- open air without any type of protection, is a slow but progressive
RC-C, 8.6% in P-RC-T and 6.1% in P-NC (Fig. 6). In-situ concrete physicochemical phenomenon; in the case of pieces without struc-
gains little strength after 28 days [87,88], but its evolution over tural reinforcement, the densification of the hydrated cement
time can also depend on the stability in the particular test site matrix and the pores structure refining (due to the precipitation
conditions and the possible deterioration of the recycled material of the formed calcium carbonates) can improve surface hardness,
over time [89]. strength and impermeability [82,83,94].
Finally, the analysis of the values obtained for the elasticity Fig. 8 shows the irregular carbonation front of some of the cores
dynamic modulus (Fig. 7) in the cores extracted confirmed the extracted from the tested pieces after breaking and applying 1%
results discussed for compressive strength. This parameter phenolphthalein. The presence of coarse aggregates, close to sur-
decreased with the percentage of RA used and was affected by face, prevented its progress as a perfectly straight line [87,95].
curing conditions [73,89–93]. This result was explained by the Likewise, the lower portions of the cores show greater carbonation
important rigidity loss in the case of concrete manufactured with than the upper ones, which corresponds with the area of the bench
recycled fine fraction (P-HR-T), due to the increase of weak most protected and not directly exposed to rain.
points inside pieces. Likewise, the degradation of the mortar Fig. 9 shows the measured carbonation depth and the forward
adhered to the RA produced discontinuities between the cement speed of the front at 12 and 24 months; previous measures were
matrix and the aggregates, generating a greater number of fragile not included because this phenomenon is non-existent in
points and, consequently, favouring the deterioration process of younger ages. The results show higher carbonation resistance
the material over time and the worsening of its mechanical in the case of RC compared to HN, with the improvement per-
behaviour. centages of 35% for P-RC-C and 20% for P-RC-T. In relation to
Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890 9

Fig. 8. Natural carbonation of the cores extracted from the seat of the manufactured benches.

Fig. 9. Speed and depth of natural carbonation of the cores tested at 12 and 24 months.

Fig. 10. Rebound number of the tested concretes obtained in-situ.

the development of the carbonation over time, the highest speed sons [79,80,87,96]: the use of superplasticiser, the carbonation
was observed in the P-HR-T bench, with an increase of 20% after of the RA closest to the surface prevents the access of CO2
two years, compared to 14% for P-NC and 10% for P-RC-C. The (Fig. 8), the longer factory curing time of the pieces and the
improvement observed in RC could be justified for several rea- age of exposure progresses.
10 Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890

Fig. 11. Ultrasonic pulse velocity determined in-situ on the tested benches.

3.2.6. Non-destructive testing rioration produced and the surface carbonation of the material,
The study of surface hardness, thanks to non-destructive tech- respectively. The trend in the changes observed in the rest of the
niques applied in-situ, has made it possible to analysis of the matu- properties analysed (density, carbonation, rebound number and
rity of the concrete over time [62,97,98]. Fig. 10 and Fig. 11 show ultrasonic velocity) were not significant and their values were sim-
the evolution of the results obtained for measuring the rebound ilar to those obtained from pieces made using NA. Despite this,
index and the speed of ultrasonic impulses in the studied precast benches produced with RA complied with the technical require-
concrete benches. ments established by the specific regulations in terms of shape,
Fig. 10 shows the insignificant influence of RA on the rebound external appearance, weather resistance, compression strength
index, both after 28 days and two years. In relation to the evolution and water absorption.
over time, in the bench P-NC, the rebound index grew up to This research demonstrates the technical feasibility of manufac-
6 months, then gradually decreased until the end of the monitoring turing pieces of urban furniture with total or partial replacement of
period. In the case of benches P-RC, a slight increase (9%) in this the NA by RA and increases the field of applications of RA, with the
parameter was detected from 28 days to 24 months, with higher consequent environmental benefits according to the Circular Econ-
values with total replacement of NA. Nevertheless, this test only omy strategy established by the European Union.
measures the properties related to the surface area of the material
(2–3 cm) [62,99], so these results were attributed to the carbona-
CRediT authorship contribution statement
tion observed in the tested pieces, which increased the hardness
of the bench surface.
Zoraida Sánchez-Roldán: Conceptualization, Methodology,
Fig. 11 shows that the ultrasonic velocity slightly decreased
Investigation, Formal analysis, Writing - original draft, Writing -
with incorporation of RA, with percentages of variation insignifi-
review & editing, Visualization. María Martín-Morales: Conceptu-
cant for both types of RC in comparison to NC at 28 days; at the
alization, Methodology, Investigation, Validation, Formal analysis,
end of the two years, a 5% maximum observed in the piece P-HR.
Writing - review & editing, Visualization, Supervision. Ignacio
Compared to the over time, the ultrasound speed showed little sig-
Valverde-Espinosa: Conceptualization, Methodology, Investiga-
nificant changes; in the case of the piece manufactured with NA,
tion, Validation, Formal analysis, Writing - review & editing, Visu-
the speed tended to decrease, with a final value 2% lower than that
alization, Supervision. Montserrat Zamorano: Conceptualization,
obtained after 28 days. Instead, a slight gradual increase of ultra-
Methodology, Investigation, Validation, Formal analysis, Writing -
sonic velocity was observed at the end of the monitoring period
review & editing, Visualization, Supervision, Project
for P-RC-C and P-RC-T, compared to the values obtained at 28 days.
administration.
This improvement is directly related to the anomaly presented in
the water absorption coefficient of RCs at 24 months, resulting in
a more compact material that allowed waves to pass through it Declaration of Competing Interest
quickly [62,100].
The authors declare that they have no known competing finan-
cial interests or personal relationships that could have appeared
4. Conclusions to influence the work reported in this paper.

The conducted study revealed the technical feasibility of the Acknowledgements


RAs selected to produce precast concrete for non-structural uses,
even in the most unfavourable external use conditions; generally, We would like to thank the staff of INERTES GUHILAR S.L.
using the coarse fraction showed better behaviour compared to (Alhendín, Spain), and PREFADUR (Padul, Spain) for their help in
the results obtained when using together RFA and RCA. this study. Also, the Departments of Building Construction and
Exposing the benches under real use conditions for 24 months, Civil Engineering and research group TEP-968 ‘‘Tecnologías para
showed a decrease of compression strength and absorption in the la Economía Circular” (Technologies for Circular Economy) of Gran-
case of pieces manufactured with RA, as a consequence of the dete- ada University.
Z. Sánchez-Roldán et al. / Construction and Building Materials 250 (2020) 118890 11

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