Universidad de Guadalajara

Centro Universitario de Ciencias Exactas e Ingenierías

Departamento de Química

Sample Information
Acquired by : Propietario
Sample Name : JC85B-2ba
Sample ID :
Injection Volume :1
Method File : Catá lisis ciclohexanona - integració n.gcm
Batch File :
Date Acquired : 09/05/2018 18:13:33
Date Processed : 09/05/2018 18:24:52
Chromatogram
uV
300000
1FID1
3,464 / Ciclohexanol
3,613 / Ciclohexanona

200000

100000
2,999 /

0
1 2 3 4 5 6 7
min
Peak Table
FID1
Name Ret. Time Area Height Area% Unit
2,999 4026 1678 0,896
Ciclohexanol 3,464 258604 118500 57,582 ppm
Ciclohexanona 3,613 186479 80374 41,522 ppm
449109 200552 100,000
<<Injection Port SPL1>>
Injection Mode : Split
Temperature : 250,0 C
Carrier Gas : N2
Flow Control Mode : Velocity
Pressure : 27,3 kPa
Total Flow : 28,4 mL/min
Column Flow : 0,50 mL/min
Linear Velocity : 17,6 cm/sec
Purge Flow : 3,0 mL/min
Split Ratio : 50,0
High Pressure Injection : Off
Carrier Gas Saver : Off
Splitter Hold : Off
<<Column Oven>>
Initial Temperature : 80,0 C
Equilibration Time : 0,3 min
Temperature Program : Total Program Time : 9,20 min
Rate(C/min) Temperature(C) Hold Time(min)
------ 80,0 2,00
1 8,0 112,0 0,00
2 15,0 160,0 0,00

<<Column Information>>
Column Name : SH-Rx1-5ms
Column ID :
Film Thickness : 0,00 um
Column Length : 15,0 m
Inner Diameter : 0,25 mm ID
Column Max Temp : 320 C
Activation Date : 2016/08/31

<<Detector 1 FID1>>
Temperature : 270,0 C
Signal Acquire : Yes
Sampling Rate : 40 msec
Stop Time : 9,20 min
Delay Time : 0,00 min
Subtract Detector : None
Makeup Gas : N2
Makeup Flow : 30,0 mL/min
H2 Flow : 40,0 mL/min
Air Flow : 400,0 mL/min