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First Page PDF
First Page PDF
1. Introduction 114
2. Sulfation of Alcohols 116
A. Sulfuric Acid 116
2-1. Preparation of Sodium Lauryl Sulfate Using Fuming Sulfuric Acid . . .120
2-2. Preparation of Neopentyl Sulfate . . . . . . . .120
2-3. Preparation of Sodium Ethoxylated Tridecyl Sulfate . . . . .120
B. Sulfur Trioxide 121
2-4. Preparation of Sodium Lauryl Sulfate . . . . . .122
a. The Properties and Safe Handling of Sulfur Trioxide 123
C. Chlorosulfonic Acid 124
2-5. Preparation of Sodium Tridecyl Sulfate . . . . .125
2-6. Preparation of Sodium Lauryl Sulfate . . . . . . .125
2-7. General Procedure for the Preparation of Sodium A Ikyl Sulfates of Secondary
Alcohols 127
D. Sulfur Trioxide Complexes . . . . . . . . . 127
2-8. Preparation of Pyridine-SOi Complex . . . . . . .130
2-9. Preparation of Trimethylamine-SOi Complex . . . . .131
2-JO. Preparation of Barium and Lithium ά-2-Butyl Sulfates . . . .133
2-11. Preparation of Sodium Lauryl Sulfate Using the Pyridine-SO i Complex 133
E. Sulfamic Acid 134
2-12. Preparation of Ammonium Ethoxylated Tridecyl Sulfate . . . .134
3. Miscellaneous Methods . . .136
References . . . .137
1. INTRODUCTION