Temperature Measurement and Calibration:: What Every Instrument Technician Should Know

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Temperature measurement

and calibration: Application Note


What every instrument technician
should know

Introduction require four to six inches when


inserted into a liquid or snug
Temperature may be the most fitting well, depending on the
commonly measured physical diameter of the probe. Best
parameter. Yet there have never results in terms of accuracy and
been so many ways to measure it stabilization time occur when
as there are today. With so many the probe can be inserted into
options it’s natural to have a few a stirred liquid. Air pockets
questions. How do I measure between probes and solid sur-
temperature? How accurate is my faces lead to longer stabilization
measurement? What temperature times and require more immer-
range is required? What type of sion than would be required in
device best measures tempera- a liquid. Specialized thermom-
ture? Does my instrument require eters are needed for measuring
certification? temperatures on surfaces and for
These are very common ques- situations where the probe cable
tions when confronted with the will be exposed to extreme
need to measure temperature. A temperatures.
variety of measurement devices Often devices that measure
may be used for temperature; and display temperature need
liquid-in-glass thermometers to be verified or calibrated
(LIG), thermocouples (TCs), against a reference thermom-
thermistors, resistance tempera- eter. Accuracy is improved when
ture detectors (RTDs), platinum the distance between the two
resistance thermometers (PRTs) thermometers is reduced. A best
and standard platinum resistance practice is to align the centers
thermometers (SPRTs). This appli- of the sensing elements of the
cation note focuses on electronic reference thermometer and the
temperature measurements, and device under test. Be aware that
helps clarify the answers to some the location of the center of the
of these nagging questions. More sensor depends on the sensor
information on these subjects is type and model (i.e. PRT, ther-
available at www.fluke.com. mocouple, bimetallic).
A common method of calibrat-
How do I measure ing temperature sensors is to
temperature? remove them from where they
After inserting a temperature are installed and place them in
sensor into the area to be a dry-well calibrator or a Micro-
measured, it takes time before Bath. These calibrators provide a
the temperature reading is stable temperature environment
stabilized. For the thermom- over a range of temperatures to
eter to stabilize at the correct compare the thermometer under
temperature, the probe must test to the calibrator display or
be sufficiently immersed. Some to a reference thermometer for
thermometers require more more accuracy. Alternatively,
immersion depth than others. temperature sensors may be
Most precision thermometers calibrated or verified without

F ro m t h e F l u k e D i g i t a l L i b r a r y @ w w w. f l u k e . c o m / l i b r a r y
removing them from their TUR Accepted False Accept Rejected False Reject
installed location. Usually this
is done by inserting a reference 1:1 843 17 157 128
thermometer into a thermowell, 2:1 925 12 75 41
immersion well, or thermometer
pocket installed next to the ther- 3:1 941 9 59 22
mometer to be tested. In other 4:1 947 8 53 15
cases the sensing element of
the reference thermometer must Table 1. What-if table summarizing false accept and false reject risk for a hypothetical scenario of 1000 instruments
be placed inside of the freezer, that are truly 95 % in tolerance. A normal distribution without guard-banding is assumed.
oven, or environmental cham-
ber being verified, calibrated or Thermometers are specified by same accuracy as the thermom-
adjusted. design engineers for tempera- eter under test, then the TUR
In these cases it is often ture monitoring or control. These is 1:1. The latter TUR is never
necessary to record data over specifications should include recommended for calibration
a period of time such as a few the accuracy of the thermom- and would produce unreliable
hours to verify performance. eters. A design engineer, quality results.
Statistics such as average value, engineer or metrologist should With a more accurate calibra-
maximum and minimum, or also specify the calibration tion standard you can identify
standard deviation are some- requirements. However, it is not more actual out-of-tolerance
times recorded. uncommon for instrument tech- field devices. Table 1 illus-
Testing the energy perfor- nicians to receive a calibration trates the expected frequency
mance of steam systems, cooling job and little or no information of making mistakes at various
towers, heat exchangers, and about calibration requirements. TURs. Table 1 is based on a
refrigeration systems, turbines, A common calibration strategy scenario where 950 of 1,000
and internal and external is to reduce mistakes by keeping instruments are truly in toler-
combustion engines requires the uncertainty of the calibration ance. For example, if all 1,000
measuring differences between standards to a low percentage are calibrated with a 2:1 TUR
inlet and outlet temperatures. of the accuracy of the thermom- then we expect that 926 will be
Sometimes these measurements eter under test. This percentage found in tolerance (accepted), 12
have to be made from outside is usually described as a Test of which are truly out of toler-
the pipe using thermocouples, Uncertainty Ratio (TUR). For ance (false accept). Of the 74
thin-film sensors, or infrared example, the 4:1 TUR used by expected to be rejected, 41 are
temperature measurements. the military and other industries expected to be truly in tolerance
However, the best accuracy will keeps the collective uncertainty (false reject). The cost incurred
be achieved when a thermowell of the calibration standards to for each of those falsely rejected
has been properly installed in 25 % of the thermometer under instruments could range from
both the inlet and outlet pipes so test accuracy. For comparison, $50/each for a calibration house
that a probe can be inserted and a TUR of 2:1 means that the to $10,000/each in down time in
sufficiently immersed. Because uncertainty is 50 % of the the chemical process industry.
pipe diameters are sometimes a thermometer accuracy, and if the
limiting factor for immersion, the reference thermometer has the
best location for a thermowell is
at an elbow in the piping so that
Temperature range Accuracy Cost
the probe can be inserted parallel
to fluid flow with as much immer- Noble-metal R, S: –50 °C to 1760 °C > ± 0.6 °C Med
sion depth as needed. thermocouples
(Special tolerances)
How much accuracy is Base-metal B: 0 °C to 1820 °C ± 0.25 % Low
needed? thermocouples E: –270°C to 1000 °C > ± 1 °C Low
Decisions about accuracy should (Special tolerances) J: –210 °C to 1200 °C > ± 1.1 °C Low
be made carefully. Inaccuracy K: –270 °C to 1370 °C > ± 1.1 °C Low
leads to mistakes and mistakes N: –270 °C to 1300 °C > ± 1.1 °C Low
cost money. Mistakes may lead T: –270 °C to 400 °C > ± 0.5 °C Low
to down time, excessive energy PRTs and SPRTs Industrial: –80 °C to 480 °C ± 0.05 - 0.1 °C Low - Med
costs, high product defect rates, Reference: –200 °C to 660 °C ±0.001 – 0.02 °C Med - High
safety hazards, and public health High temp: 0°C to 1000 °C ±0.01 – 0.02 °C Med – High
threats.
Precision thermistors 0 °C to 100 °C ±0.002 °C Med

Table 2. Temperature sensor tradeoffs among temperature range, accuracy and cost. The most accurate sensors are
the most expensive. Often accuracy is sacrificed for wider temperature range.

2 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know
Thermometer probe is not based on the absolute thermocouple wire is usually
types temperature of the measurement connected directly to the ther-
junction, but rather a temperature mocouple readout binding posts
There have never been as many difference between the measure- at room temperature. Automatic
temperature sensor (probe type) ment junction and the reference reference junction compensation
choices available for your mea- junction. is needed to compensate for the
surements as there are today. Thermocouple types are dis- deviation from 0 °C. A therm-
With so many choices, the task tinguished by the metals used istor bead is usually used to
can become time consuming and in each leg of the thermocouple. measure the temperature of the
difficult without some help. The Noble metal thermocouples all junction. The readout measures
most important factors are tem- contain platinum in one leg of the resistance of the thermistor
perature range, accuracy and cost. the thermocouple and include and calculates a correction for
Table 2, on the previous page, Type S, Type R, Au/Pt, and Pt/ the thermocouple temperature.
illustrates the tradeoffs among Pd. Base metal thermocouples In Figure 2, thermocouple wire
these factors for several thermom- include Type B, Type E, Type meets with copper wire at the
eter types. J, Type K, Type N, and Type T. binding posts of the meter form-
These thermocouples come in ing the reference junction (J).
Thermocouples (TCs) two accuracy classes: standard The temperature in the region
Thermocouples are temperature limits of error and special limits surrounding the binding posts
sensors that measure temperature of error. The special limits of (TJ ) is usually measured by
by generating a small voltage error thermocouples are the most a thermistor. Automatic refer-
signal proportional to the tem- accurate. Letter designated ther- ence junction compensation is
perature difference between the mocouple tables are available accomplished by measuring the
junctions of two dissimilar metals. from NIST on the web or in NIST difference from 0 °C at the bind-
One junction (the measurement monograph 175. A thermocouple ing posts (TJ) and compensating
junction) is typically encased in voltage and sensitivity calculator for it digitally. The accuracy of
a sensor probe at the point of is also available on the web at this measurement has a signifi-
measurement; the other junction www.fluke.com. cant impact on the accuracy of
(the reference junction) is typi- Reference junction com- the overall temperature mea-
cally connected to the measuring pensation is one of the most surement.
instrument. The measurement significant contributors to the
instrument measures two things: accuracy of a thermocouple Resistance based tem-
the voltage signal and the refer- measurement. Thermocouple perature measurement
ence junction temperature. From tables like those in NIST mono-
An RTD is a temperature sensing
those two things the instrument graph 175 are based on a
element that relates tempera-
computes the temperature at reference junction temperature
ture to its own resistance. There
the measuring end of the probe. of 0 °C. Although external refer-
are several kinds of RTDs. RTD
It is important to note that the ence junctions can be used to
sensing elements include coils of
voltage generated by the sensor achieve this with an ice bath,

A C
T1
T2
V

B C
Figure 1. Model of a thermocouple circuit where A and B are dissimilar thermocouple wire, T1 represents the temperature at the measurement junction, and T2 repre-
sents the temperature at the reference junction. The absolute temperature at T1 does not produce the voltage measured at V; rather, the temperature difference between
T1 and T2 produces the measured voltage.

3 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know
+ VJ1(TJ)
+ VJ1(TJ)
+
VTC(TTC) VJ2(TJ) Vo=V (T(T
V TC ) TC)+[VJ1(T J)+VJ2(TJ)]
+
Vo=VTC(TTC)+[VJ1(TJ)+VJ2(T
- V (T )
TC TC
J2 J
-
-
-
TJ

TJ

Figure 2. Reference junction compensation is one of the most significant contributors to the accuracy of a thermocouple measurement.
Caution: some manufacturers may not advertize this important part of their accuracy.

platinum wire (PRT), nickel wire,


copper wire, thin films and more.
the results of both sets of
measurements. This technique
RL1
Another resistance based sensor
is the thermistor which is made of
used by many modern instru-
ments improves measurement +
semi-conducting material. Figure stability and reduces significant
3 illustrates a simple 2-wire errors that are common in other
measurement circuit. The sens- instruments.
ing element is labeled RT. The
lead-wires have finite resistances
RT
labeled RL1 and RL2.
When current passes through
the sensor, the environment
RL1 RL2
is going to get a little warmer -
because of power dissipation.
The more resistance or current
there is, the more power gets Platinum resistance
+
Figure 3. Current is passed through the sensing element to produce
a voltage measured by a meter. Lead-wire resistance in two-wire
measurements causes potentially large temperature measurement
dissipated (P=I2R). The self- thermometers errors. Other types of resistance measurements include three-wire
and four-wire resistance measurements. Four-wire measurements are
heating will be higher in air A platinum resistance thermom- preferred in temperature applications because they eliminate lead
because the heat will not flow eter (PRT) element contains coils wire resistance from the measurement.
away as efficiently as it would of highly-pure platinum wire. The

RT
in a stirred fluid. Self-heating
errors can be minimized by
using the same level of current
used during calibration. Using
resistance of a PRT element varies
more linearly with temperature
than any other temperature
sensor. A Standard Platinum
the correct current is particu- Resistance Thermometer (SPRT)
larly important in thermistors is the most accurate temperature
because they can have very
large resistances causing greater RL2sensor available and is used in
National Standards Laboratories

-
self-heating. and in industry for traceability
Current

Current reversal is a very to the International Temperature


effective technique used in Scale of 1990 (ITS-90). The full
resistance measurements to text of the ITS-90 is available at
eliminate errors associated with www.bipm.org.
thermal EMFs. Thermal EMFs Temperature measurement
are unwanted voltages in a with a PRT requires correlating
resistance measurement circuit the resistance of the sens-
caused by the same principle ing element with temperature
that produces a voltage in ther- using the correct equations and
mocouples. The measurement is coefficients. Fortunately, most
made with the current flowing thermometer readout devices
in one direction and then again have support for these equa-
with the current flowing in the tions, so the calculations are
other direction. Thermoelectric handled automatically. Examples Figure 4. Current is required to measure resistance. Current that
EMFs are removed by averaging passes through a resistance dissipates power and generates heat,
include ITS-90 equations, causing temperature errors.

4 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know
Callendar Van Dusen (CVD) Readout device Requirements
equations, and polynomial equa-
tions. Best performance with Thermocouple readout Good accuracy from –10 mV to 100 mV
PRTs can usually be achieved Low noise floor
with the ITS-90 equations. Older Very low thermal EMFs
readouts and uncalibrated PRTs Good reference junction compensation
may use CVD equations. PRT readout Excellent accuracy from 0 Ω to 400 Ω
The coefficients used with Current reversal
these equations are customized Four-wire resistance measurement
through calibration and can be 1 mA excitation current
found on individual calibra-
tion reports along with a table Thermistor readout Reasonable accuracy from 150 Ω and 500 kΩ
that describes the resistance Better accuracy required below 1000 Ω
vs temperature relationship. 2 μA to 10 μA excitation current
Some inexpensive PRTs used Table 3. What to look for in electronic thermometer readouts.
for industrial measurement are
intended to operate even with-
out calibration. Out of the box may be the most important
they should conform to a stan- factor affecting the accuracy
dard such as IEC 60751 or ASTM aside from calibration.
1137. These standards specify Accuracy specifications can be
values for the CVD coefficients structured several ways. Speci-
and tolerances that depend fications will usually be divided
on temperature. However, the into ranges and may be given
accuracy of these probes can be in base units of temperature,
significantly improved through resistance or voltage. Simple
calibration. specifications will either be
a variable or fixed value, and
Thermistors complex specifications will be
A thermistor element is made of a combination of both. When
semi-conducting material and variable type specifications
has an electrical resistance that are used, the allowed error
varies non-linearly with tem- increases when the magni-
perature. Thermistors are widely Thermometer tude of the reading increases.
used because of their sensitiv- accuracy, repeatability, Calculations are required for
ity, small size, ruggedness and and resolution a numeric result. Examples
low cost. Thermistor accuracy include percent of reading or
Two important components of parts per million (PPM). On the
depends greatly on design accuracy are repeatability and
and construction. Inexpensive other hand, fixed value specifi-
resolution. They should be con- cations remain constant over a
thermistors are commonly used sidered along with other factors
in electronics applications while range. Examples include percent
affecting accuracy. Repeatabil- of scale or span and numeric
precision thermistors are cali- ity refers to the consistency in
bration standards rivaling the constants.
values of repeated measurements. You can convert specifica-
accuracy of SPRTs. Regular calibration is helpful for
The resistance vs tempera- tions in base units of resistance
establishing instrument repeat- or voltage to temperature. The
ture relationship in thermistors ability. Another important method
is described by a few differ- conversion depends on the
of verifying repeatability in sensitivity of the temperature
ent polynomial equations. One thermometers is to measure peri-
form of the equations is used sensor. For example, change
odically in an ice point or triple temperature 1 °C and it will
take resistance as an input to point of water cell and record the
calculate temperature T(R) and result in a 0.4 Ω change in resis-
results. tance for a 100 Ω PRT and result
another form of the equation Resolution on a digital ther-
takes temperature as an input in a 0.1 Ω change for a 25 Ω
mometer is often user selectable. SPRT, but it may cause a 1000 Ω
to calculate resistance R(T). The A digital thermometer should be
standard version of these equa- change in a thermistor. This
chosen with sufficient resolution means a one degree change in
tions take four coefficients, but to achieve the desired accuracy;
the Steinart-Hart version only temperature may have a very
however, resolution is not the big or very small impact on the
requires three. same thing as accuracy, it is change in resistance. Conse-
merely a limiting factor in the quently, a meter with ± 1 Ω
accuracy. In a liquid and glass or
dial thermometer, the resolution

5 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know
accuracy will be most accurate To ensure that temperature
for those sensors with the high- measurements around the world
est temperature sensitivity. are consistent each country has
Each of the thermometers adopted the ITS-90, a tempera-
listed in Table 2 requires a ture scale defined by the BIPM
digital readout. The best digital (International Bureau of Weights
readout is going to be designed and Measures). Instrument accu-
specifically for temperature racy is determined by comparison
measurement. Table 3 lists some to measurement standards of
of the requirements for good higher accuracy. These mea-
electronic thermometer readouts. surements are part of a chain of
Reference junction com- comparisons that extend from end
pensation is one of the most user measurements in the field to
significant contributors to the secondary calibration laboratories
accuracy of a thermocouple and then all the way to national
measurement. Thermocouple (i.e. NIST) and international
tables are based on a reference standards.
junction temperature of 0 °C. In addition to traceability, What to look for in a
Although external reference sometimes calibration customers temperature calibration
junctions can be used to achieve have an additional requirement equipment solution
this with an ice bath, thermo- for accreditation. Accredita- provider
couple wire is usually connected tion provides assurance that an
When choosing calibration equip-
directly to the thermocouple appropriate quality program is
ment solution providers there are
readout binding posts at room in place and that training and
many factors to be considered.
temperature. Automatic reference procedures meet the technical
Here are a few of them.
junction compensation is needed requirements for the calibra-
to compensate for the deviation tion service provided. A logo
A complete solution: Make sure
from 0 °C. A thermistor bead appearing on accredited calibra-
that the company you choose has
is usually used to measure the tion certificates distinguishes
a complete range of products so
temperature of the junction. The them from other calibration
that your options can be based on
readout measures the resistance certificates. There are many
your needs and not just what they
of the thermistor and calculates accreditation programs avail-
have available. If you’re consider-
a correction for the thermocou- able. NIST sponsors the National
ing using automation software in
ple temperature. Voluntary Laboratory Accredita-
the future to improve productivity
tion Program (NVLAP).
you should plan to stick with one
NIST and calibration supplier because the manufactur-
NIST is a National Metrology Maintain your standards er’s software will likely only work
Institute (NMI) responsible for Maintenance of calibrated with their own equipment.
United States national stan- equipment is an important part
dards. Metrology is the science of quality assurance. There is Experience: You probably don’t
of measurement and includes no guarantee that a calibrated have time to be an expert in
basic research, activities that thermometer will remain cali- temperature calibration along
ensure adequate functioning of brated over time. Changes in the with everything else you do. It’s
measurement instruments used in temperature relationship of used important to get help from the
industry, and also measurements thermometers over time need experts, so look for a company
that ensure economic transpar- to be corrected by calibration at that specializes in temperature
ency, public health, and safety. regular intervals. When thermom- calibration so you won’t have to.
Traceability to NIST or another eters are found repeatedly out of
NMI is established through cali- tolerance remedial actions need Support: Expertise is great, but
bration. The three main reasons to take place, such as shortening make sure you have access to the
for having an instrument cali- the calibration interval or replac- experts. You are in good hands if
brated are: ing the thermometer. It is a good they answer their phones, treat
1. To ensure readings from an idea to keep records and monitor you respectfully and get answers
instrument are consistent with certified thermometers between to all your questions. You’ll also
other measurements calibrations using an appropri- want to make sure they can
2. To determine the accuracy of ate method such as an ice bath, resolve any equipment problems
the instrument readings or triple point of water cell. This for you quickly. Ask about service
3. To establish the reliability of will limit or prevent expensive turnaround times. If your equip-
the instrument consequences should a certified ment must be sent to a different
thermometer be found signifi- continent for repairs you could be
cantly out of tolerance. in for some serious delays.

6 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know
Accreditation: Even if you don’t Fluke Calibration
have a specific requirement for
accreditation it makes sense to Fluke Calibration provides the
work with a company that has an broadest range available of
accredited laboratory. Here’s why. calibrators, standards, software,
An accredited laboratory has been service, training and support
inspected very carefully to make solutions. Our customers work in
sure they have the organizational electrical, temperature, pressure
capability to do what they say and flow calibration laboratories
they do. In the case of NVLAP around the globe, as well as in
accreditation the laboratory has manufacturing test, research and
passed a technical assessment development, and service.
performed by experts from NIST. The Fluke Calibration tem-
perature calibration division
A guarantee: Calibration is all makes everything needed for
about confidence. First, make sure calibrating temperature sensors,
accuracy specifications are pro- from constant temperature baths
vided. Second, make sure those and dry-well calibrators with
specifications are guaranteed. The unmatched stability to primary
last thing you need is to wind up temperature standards used in
with a piece of equipment taking national metrology institutes
up space that doesn’t perform as around the world. For precision
promised. thermometry, Fluke Calibration
thermometer readouts and
probes are exceptionally accu-
rate and easy to use, and our
temperature and humidity data
logger eliminates the need for Fluke Calibration. 
paper chart recorders. In addi- Precision, performance, confidence.™
tion Fluke Calibration also offers
temperature calibration train-
ing courses from experienced
instructors and expert service
from its NVLAP-accredited labo-
ratory (lab code 200348-0).

Fluke Calibration
PO Box 9090, Everett, WA 98206 U.S.A.
Fluke Europe B.V.
PO Box 1186, 5602 BD
Eindhoven, The Netherlands
For more information call:
In the U.S.A. (877) 355-3225 or
Fax (425) 446-5116
In Europe/M-East/Africa +31 (0) 40 2675 200 or
Fax +31 (0) 40 2675 222
In Canada (800)-36-FLUKE or
Fax (905) 890-6866
From other countries +1 (425) 446-5500 or
Fax +1 (425) 446-5116
Web access: http://www.fluke.com
©2011 Fluke Corporation.
Specifications subject to change without notice.
Printed in U.S.A. 3/2011 3996588A A-EN-N

Modification of this document is not permitted


without written permission from Fluke Corporation.

7 Fluke Calibration Temperature measurement and calibration: What every instrument technician should know

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