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...... ..... .... " . . . ' WELDING PROCED)URE NO.

WESERvicEs, INC
WELDINGwps- NC'
WE-(GPRCEUEO 1
REVISION A0317 4-N
1
1 432
LDING
..... .. .. _PAGE 1 OF 2

WELDING CODE SUPPORTING PQR(S)

WELDING PROCEDURE SPECIFICATION A03N432


ASME B & PV
SECTION IX

WELDING PROCESS(ES) i. Gas Tungsten Arc Welding TYPE Automatic (Machinbe)


2.. Code cape N 432 TYPE. ,Temper Bead

BASE METALS (OW-403) POSTWELD HEAT TREATMENT (OW-407)


P No. - Gr. No. 3 to P No. 2 Gr. No. . Type Electrical Resistance

Thichness Range Maximum 3" IN. Temperature 450OF to 550'F OF


Pipe Dia. Range none IN. Time Range 2 hours
Range for Fillet. Thk. none Die. nnne IN.
Max Deposited thickness 3"
GAS (OW--408)
FILLER METALS (W-4O4) "Shielding Gas 1. Argon
FNo. 1. 6 2. N/A PercentComp. )9995%
ANo.1. See Chemial AnarJsis N/A Shielding Gas Flow Rate 40 to 50 CFH(min)
SFA Spec. No. 1. I _28 2. N/A PurgeGas none - Flow Rate none CFH(min.)
AWS Class. No. 1. FR8nl,05,-D2 2. N/A Trailing Shielding Gas Composition -none
Size of Electrode 1. N/A 2. N/A IN.
Size of Filler 1. .035" 2. N/A -IN. -ELECTRICAL CHARACTERISTICS(OW-409).
Electrode - Flux Class none . Current1. DCEN 2.- N/A
Consumable insert none Amps Range 1. * 2. N/A
Pass thickness less than 0,50" Volts Range l. * 2. .. /A
Tungsten Mec. Size/Type -125" 9WTH 2%

POSITION (OW-405) TECHNIQUE (QW-41 0)


welding Position 2( Stringer of Weave Bead 1. Stringer 2: N/A
Welding Progression Horizontal ; See parameter Bead Width See Page 2
sheets, Orfice or Gas Cup Size #4 (.250") IN. (min.)
PREHEAT (OW-406) Initial and Interpass cleaning: Welding surfaces shall be wire brushed or ground
Preheat Temp. 300 OF OF (Min.) as requied to remove slag, scale or other contaminants.
Interpass - Temp. Range 45 0 °F Max OF Method of back gouging none
PreheatMaint. '30F Min: Preheat 30 minutes
prior to start welding, Oscillation 1. Not ,allowed 2. N/A IN. (max.)
Contact Tube to work distance N/A IN.
JOINT DESIGN (E-402) Mutipleorslngle Layer I. Multiple Layer
GrooveDesign Weld Repair Code Case N432 . (PerSde) 2. N/A
Joint Type OB -none C none BS none Multiple or single electrodes Single
Backing Mati Type none Travel Speed (Range) 1. * 2. N/A IPM

REMARKS
* Parameters are restricted for layers 1 thru 6, see attachments QW-409 and
QW-410, for each layer parameters. Range is given for all layers beyond
the sixth.

8911220164 89111-7 °
PDR ADOCK 05000247
@ PDR

• i/I2t/i Fab.Codes: ASME B&PV Codes 1981 Edition, Sections


III & IX
Project: Indian Point II - Con Edison
Materials Engineering
SobNo.... .____________________
Quality Assuince
WELDING TECHNIQUE SHEET WELDING PROCEDURE NO.
TOPNO. 3 GROUP 3' WPS- A03174-N432
PNO. 3 GROUP.13
I. REVISION 1
.
•R Eu M
THK. RANGE "Maximum " ., IN PAGE OF 2
2
TYPICAL JOINT DESIGNS PERMITTED Plate Dimensions 12"x30", ROOT OPENINGS O.B. IN.
7 1/4" thick. BS.
e!
B ., IN.

NObT TO

WELDING PARAMETERS - SINGLE VALUES ARE MINIMUM

WELDING SIZE-
FILLER METAL
-
GAS ELECTRICAL DAT A fMAX.
T
LAYER PROCESS (AWS CLASS TYPE LOW.RATE (CFH) TYPE/ AMPERAGE VOLTS SPEED WIDTH
(IN.) SHIELD lYPURGE POLAR. RANGE RANGE (IPM) (IN.)
1 GTAW .935 ER80S-D2, ,0 nonet9 DCEN P180- zP9.7 3.2 .375"
.. ... .. - .. .. . . B220 B8 .9, -
2 GT 0/',
GTAV4>LT 35 -L ": A oE5R80S'2
'none- N " Y--
125
P194 " B9.1
9. 3.2

,___',L«-:
.L 5. o"- B13B150 "'3.2B9.2
P9'.8
4t) GTAW .P220 P9.9
. . . "'3,B140 B9.4 13.4
7 t:) 885- to -250 2.7-5.0

PREHEAT TEMP. . 0.i__________________


01 L " 1- n 4)-BACK GOUGING
overlap 40-60% none
METHOD- T __ __

INTERPASS TEMP.. _490 Max OF CONTACT TUBE TO WORK DIST. N /A IN. (min.)
PREHEAT MAINT.0 . min,,prior-tc.welrdanjL OFIFI EORCUPSIZE -1: #4 (.250!!) IN.(min.)
TUNGSTEN ELECT. SIZE & TYPE . 1 25. . IN. WELDING PROGRESSION See technique sheets
EWTh .2% Wee; t-ech!gique sheets
'N ''~~

INSTRUCTIONS >.i.:T .52k ' *'::c.it ~.. £ . : F, -,;

Preheat to 300OF 30 minutes prior to start of weldinj 10" ar 6nd ar4-to'be welded.
Thermocouples and recording instruments shall be used to monitor preheat, interpass
and pQst..weid-hqat tr at me nt....o..pd..r....., . -,
No oscillat'ion is to be used on layer, lt.hiugh,... cr5 .
Peening is not permitted.
5. Parameters for layers 1 thro uh 6 s~stated inQW409.pd.QW410 .hall,.be strictly
adhered 6 ,.d. ( 2~.C - I'. - . I' ..
6. Weld heat iTn bu OCoi yi-si taisough" ahl l'e +09
+i10of QWsA and W41OI
7. Travel speed shall be measured at the work .irfce.' '
8. Welding power supply shall be Gold Track II or equivalent.
9. When welding is done remotely, optics for weld puddle shall begin working order.
10. After welding, no non-destructive examination shall be performed for 48 hours.
11. The finished surface of. the repair shall be substantially flush with the surface
of the component surrounding the repair.
1. 7 . .

~
-2C~,~

K, .~**Wel. P~
4 WZ ?- 2Ti3,Z )
.. , I .. NC.
WELDING SERVICES, INC. :'

,ELE:TNG PROCEDURE SPECIFICATION

"S }'CIAL INSTRUC I..NS


... . -i - A

We1Cdng of the- re-ai-r- area- :hall- b -


foll.wJ. ng insftu bns, and ;delin :

1. The area to be repairedby weiAdng,-f :nd a n, ghe


area, shall'e prelhet-d to "-30Q dec"rees ,. i ,
tempirature shall 45e I ainaiLa at-least- 3 , d-tAes
before welding is started, dur ng w:lding, and' u til .
starting the postweld heating *as: dqscribe3 below.

2. The width of: the Preheat (band shall be at 1 ,a t three


times thb thicknessfof the cynpbnrit to be w l.ded!apd :as
neEded to--accommsdate -hermocb'jae--at achmcnt- and" --tr -a
tion application, -but need.>.co,
' .,: ee-d t.t.( .. ncbes_ ..

3. The into as7 t,1_peratur4 sh e i45

4. Thermo&cup -es and fecordrig nstrmments sha-r be used to


--monitor - pret-h ,--intoerpa.T.... t.; tE:per6ature. ... .
Thermocouples may be attb.ch :d by mechanical methods or
apaLtor, s charge- ,".. .

5. The first six (6) layers of woldjbde0Vtit--- shall : appj.i-,;Li


as shown on the attah~d- , .ctcha,.- .
' *. z,. rj ,. ....

6. The' Weld heat in~ruit f'dr each of etl ,.'-irst six () laye~z~.-..b-i
shal!.be controled to w thin f.;,- h p
.ein tae, :_.-w
p r o ce diaur e . c ati p .. * .- , . - * .C, i L ,q'
''I

JJ Z -_r T~
-'. , ,L U.
Welding Procedure No.
WPS-A03174-N432
Page 2 of 2

7. The remainder of the weld deposit shall be completed with


the heat input equal to or less than that used for layers
beyond the sixth in procedure qualification.

8. At the :D!,pletion of wCe71.ng, the heated bend described in


#1 and #2 above, shall :je maintained in the r-ange of 500
decrees F +/'- 50 degrees for two (2) hou -s miinua.
WELDING SERVICES, INC.
WELDING PROCEDURE SPECIFICATION

Welding Procedure No. WPS-A03174-N432

STEP 1: Deposit layer one with


first layer weld parameters
used in qualifications.

STEP 2: Deposit layer two with


second layer weld parameters
used in qualifications.

STEP 3: Deposit next four layers


with layer three through six
weld parameters used in
qualifications.

STEP 4: Subsequent layers to


be deposited as qualified.

AUTOMATIC OR MACHINE (GTAW) TEMPERBEAD TECHNIQUE


(. lO
Temper Bead GTAW
Ref. Code Case N-432

AttachmenL_
Electrical Charecteristics (QW-409)

Layer_

Current: DCEN Pulsing Current

Low Pulse Frequency__20

Low Pulse Width 6_6

Machine Mode Pulse Arc


Amperage: .Primary 180 Wire Feed: Primary.__35.

Background 120 Background _

Voltage Primary 9.7

Background 8.9

Tungsten Size .125a

Type EWTh 2%

Technique (QW-410)

Layer 1

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed_ j M

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS


Temper Bead GTAW
Ref. Code Case N-432

Attachment 2
Electrical Charecteristics (QW-409)

Layer 2

Current: DCEN Pulsing Current

Low Pulse Frequency__

Low Pulse Width 66

Machine Mode Pulse Arc


Amperage: Wire Feed: Primaryl..
Primary.
Background y
Background
Voltage Primary 9.6

Background 9.1
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)

Layer 2

Stringer Beads Only


Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed 3 ZTpM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS


Temper Bead GTAW
Ref. Code Case N-432

Attachment I
Electrical Charecteristics (QW-409)

Layer 3

Current: DCEN -Pulsing Current

Low Pulse Frequency_ 0

Low Pulse Width 66


Machine Mode_ , Arc
Amperage: Primary___ 2 m ......... -Wire Feed: Primary .._5_0_

Background BackgroundJLQ

Voltage Primary 9.8

Background 9.2
Tungsten Size .125"

Type EWTh 2

Technique (QW-410)

Layer 3

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed _Z._


2 PM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS


Temper Bead GTAW
Ref. Code Case N-432

Attachment 4
Electrical Charecteristics (QW-409)
Layer--- thru 6

Current: DCEN Pulsing Current

Low Pulse Frequency__2

Low Pulse Width. 66

Machine Mode Pulse Arc


Amperage: Primary_ . . Wire Feed: Primar.YL ..

Backgrou.dj . Background 50

Voltage Primary 220

Background 140
Tu\ngsten Size .125"

Tv.e :,71-i 2/%

Technique (QW-410)
Layer 4 thru 6

Stringer Beads Only

Gas Cup Size #4 (.250") Min.


Multiple Layer

Single Electrode

Travel Speed -. 4IJPM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS


d

Temper Bead GTAW


Ref. Code Case N-432-

Attachment 5
Electrical Charecteristics (QW-409)
Layer 7 thru Remainder

current: DCEN Pulsing Current

Low Pulse Frequency 2.3 to 2.

Low Pulse Width U_to 60

Machine Mode Pulse Arc

Amperage: Primary 2= to 260 . Wire Feed: Primary 10-90

Background_1_0-Q.._
Backgroupd IM to 170
Voltage Primary_90-1 . 5
Backgrou4 _8.j_ 5.5. 0
Tungsten Size .125"

Type EwTh 2%

Technique (QW-410)

Layer

Stringer Beads Only


Gas CupSize #4 (.250") Mn.

Multiple Layer

Single Electrode

Travel .Speed 7

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS

-
?--- , .

"-.
[ 2 : -
QW-483 SUGGESTED FORMAT FOR PROCEDURE QUA-LIFICATION RECORD (POR)
(See QW-201.2, Section IX, ASME Boiler and Pressure Vessel Code)
Record Actual Conditions Used to Weld Test Coupon.

Company Name Welding Services Inc.


Procedure Qualification Record No. A03N432 Revision 1 Date 6-22-89
-WPS No. A03174-N432
Welding Process(es) Gas Tungesten Arc Welding
Types (Manual, Automatic, Semi.Auto.) Automatic (Machine)

JOINTS (QW-402)

tA
!! 60
N

INOTTO &C4. _ __ __ _

Groove Design of Test Coupon


(For combination qualifications, the deposited weld metal thickness shall be recorded for each filler metal or process weld.)
BASE METALS (OW-403) POSTWELD HEAT TREATMENT (QW-407)
Material Spec. SA 102 Temperature 500°F
Type or Grade _B Time 2 Hours
P-No. 3 toP.No. Other Cool to ambient temperature for 48
Thickness of Test Coupon 7.25 " hours prior to any testing
Diameter of Test Coupon none
Other

GAS (QW-408)
Type of Ggs or Geses Argon
Composition of Gas Mixture 99 .995%
Other

FILLER METALS (0W-404) _


Weld Metal Analysis A-No. See Chemical Anya1sis
Size of Filler Metal .03l" Dia ELECTRICAL CHARACTERISTICS (OW-409)
Filler Metal F-No. 6 Current Direct
SFA Specification 5.28 _ j Polarity Straight
AWS Classification ER80S-D2 Amps. Volts *
Other Tungsten Electrode Size - 125"
Max Deposited thickness 3" Other * See Attachments for QW409
Parameters are restricted for layers 1
through 6 ,
POSITION (QW-405) TECHNIQUE (QW-410)
Position of Groove 2G Travel Speed *
Weld Progression (Uphill, Downhill) Horizontal String or Weave Bead Stringer
Other Weld bead placement is restricted for Oscillation Not allowed
1--thru6- See attachments
-_.layers Multipass or Single Pass (per side) Multipass
Single or Multiple Electrodes Single Electrode
PREHEAT(QW-406) Other * See attachments for OW-410
Preheat Temp. 3000 F 30 minutes prior to welding Parameters are restricted for layers
.InterpassTemp. 4500F max 1 thru 6
Other Temperatures to be monitored by a
srin chart recorder.

(6/82) This form (E00007) may be obtained from the Order Dept., ASME, 345 E. 47th St.. New York, N.Y. 10017
NOTE: This PQR was revised for editorial reasons.
OW-483 (Back)
A03 N432
POR No. Rev 1
., Tensile Test (OW-150)

. .' - Ultimate Ultimate Type of


Specimen . , . ..: ; Total Load Unit Stress Failure &
No. Width Jhickness Area lb. psi Location
___2M _,_2_4_7_7 - 0.0482 __4530 9.S4000 BMD
___3 ... 0_ 5.--Q_ - 0 0491 ....4780 _ 97500 BMD
M 0.288 - _0 0486 477Q 7 98000 _. BMD
6B 0.2496 - 0.0489 480 98000 BMD

Guided Bend Tests (OW-160) 21

Type and Figure No. . Result

S 224),, 1 ___q pal


" 1: PF£. ;£ . - -
'-. : :-- 3 .-. .- ...

Toughness Tests (QW-170)

Specimen0o. NotchuJr, s- Notch' iTe t .f . CL'mpact ., LateriIE3p rp.Weight


No. Location . .ye Tem. Values % Shear Mils Break No Break

- SEE ATTACHMENT A-- -,._ __

Fillet Weld Test (QW-180)

Result -Satisfactorv- Yps. - ,.No Penetration into Parent MetalYes No


Macro-Results ..

-Other Tests

Type of Test MT, UT, 4ble


loept
Deposit Analysis c~iI~
Other

. .u
K .0sa *-- "9110vI. '.1
.51
.... .i. .. ....:
e. ..::' ... .
: ..E . ..........
.. .. ... .. .. .. a ...
V 5.. . .
K. Buba~h/e.YV' t~rt11we1 kLi..........jJE7575
Welder's Name . Harmon C
. 0. e 1 /ScH6517
Tests conducted by: APPLIED TECHNICAL SERVICES Laboratory Test No. AO-O394&HO 0516
We certify that the statements in this record are correct and that the test welds were preprared, welded and tested in accordance with
the requirements of Section IX of the ASME Code.

Manufacturer WELDING SERVICES INC.

Date 'By ' '. '


(Detail of record of tests are illustrative only and may be modified to conform to the type an4 number of tests required by the Code.)

(6/82)

L .-j,:'"
ATTACHMENT A
22 1.. TPQR1V(5T. A03N'43'2
V
t nfl. ToughnessI Tests
....
..... 5'y A
...x_ ... .. .. . . .. < . . ...
:. -. .j ,..- . .. . - .
r~ I

3A
- r

Drop Weight 9rests j : A ., T t, c4b,.-It -1

Base Meal T
'
ASTM E208 Type p3,:Specim4ns Weld M~tal-"Specimen-_
Specimens -40 degrees F: Break -10 degrees-F:
No-Break . ....
-10 deqve 4ti-grF 1N brr-eF:
No break
+20 Degreps. F: iT
uf]
+30 degrees F .Nil.. e DuctiLty - .. .
. 0-degre:s F:.No Preak Tempe__ature/= 20:

_+40 degrees F: No--Break.-. ,- --


Nil--Ductility- - .. .......
.....Te erature-=--30 -d geree F .... .

CV Tests

Weld Metal
3-. .... 2- : '163 :ft.lb , : . . . tc -4O
--
egre s
. . 63---m i l s- l at .- ex p .
.. .. -.... . . . . . . . .....
40% shear

2: 105 ft-lb RT NDT = Tcv -60


62 .mils- latex. - 'h7
-- 705% shear .- .Ai.q'

3: 80 ft-lb RT NDT: -20


62 mils lat. exp. ",-gr-eS,
&M,,,q~.shear - - l ?'~LN

4 3~aY~
17
7 7'v~ y~?1o

~~ U . "I C1 ')'n beriborn Sr. ' F'M Of, virv3 li~ EMS O~O
10 ) '1~~J
ATTACHMENT A
PQR No. A03N432
Toughness Tests
(QW-170)

Heat Affected
Zone
1: 46 ft-lb Tcv = 90 degrees F
39 mils lat. exp.
20% shear T NDT = 30 degrees
F (base metal-drop
test)

2: 51 ft-lb
46 mils lat. exp. 29 mils lateral
20% shear expansion and 28 ft
lb. average for base
metal at T vc = 90
degrees F

3. 35 ft-lb
32 mils lat. exp.
20% shear

Base Metal
3 C1:27 ft-lb Tcv: 90 degrees F
28 mils lat. exp.
10% shear

C2:31 ft-lb T NDT: 30 degrees F


28 mils lat. exp.
10% shear

C3:39 ft-lb
37 mils lat. exp.
10% shear
ATTACHMENT A
PQR No. A03N432
Toughness Tests
(QW-170)

Base Metal
3 D1:39 ft-lb Tcv: 120 degrees F
36 mils lat. exp.
20% shear

D2:27 ft-lb
27 mils lat. exp.
30% shear

D3:34 ft-lb
34 mils lat. exp.
30% shear

Heat Affected
Zone
1: 61 ft-lb Tcv = 120 degrees F
45 mils lat. exp.
50% shear

2: 52 ft-lb
47 mils lat exp.
50% shear

3: 49 ft-lb
45 mils lat. exp.
50% shear
Temper Bead GTAW
Ref. Code Case N-432

AttachmenL__
Electrical Charecteristics (QW-409)

Layer__

Current: DCEN Pulsing Current

Low Pulse Frequency _2_0

Low Pulse Width 66

Machine Mode Pulse Arc


Amperage: Primary 180

Background 120
Voltage Primary 9.7

Background 8.9
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)

Layer 1

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed_ pM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS

I-
Temper Bead GTAW
Ref. Code Case N-432

Attachment 2
Electrical Charecteristics (QW-409)

Layer 2

Current: DCEN Pulsing Current

Low Pulse Frequency _


2

Low Pulse Width__6_

Machine Mode Pulse Arc

Amperage: Primary__

Background__

Voltage Primary 9.6

Background 9.1
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)
Layer 2

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed . 2 T.IPM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS


Temper Bead GTAW
Ref. Code Case N-432

Attachment -_
Electrical Charecteristics (QW-409)

Layer 3

current: DCEN Pulsing Current

Low Pulse Frequency__2 0

Low Pulse Width 66


Machine Mode 2,.se Arc
Amperage: Primary_ 2n

Background ,
Voltage Primary 9.8

Background 9 2
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)
Layer 3

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed 3,?JPM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE PARAMETERS

//
Temper Bead GTAW
Ref. Code Case N-432

Attachment 4
Electrical Charecteristics (QW-409)

Layer-A- thru 6

Current: DCEN Pulsing Current

Low Pulse Frequency-_


2

Low Pulse Width 66

Machine Mode Pulse Arc


Amperage: Primary__22s

Background4j
Voltage
Primary 220

Background 140
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)
Layer 4 thru 6

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed -LAIPM

HEAT INPUT SHALL NOT EXCEED ± 10% OF THE ABOVE


PARAMETERS
lit Temper Bead GTAW'
Ref. Code Case N-432

Attachment 5
Electrical Charecteristics (QW-409)

Layer 7 thru Remainder

Current: LkxN Pulsing Current

Low Pulse Frequency 2.3 to 2.6

Low Pulse Width 50 to 60

Machine Mode Pulse Arc


Amperage: Primary_20 to 260
Backgrund- 1 to 170
Voltage Primary

Background
Tungsten Size .125"

Type EWTh 2%

Technique (QW-410)

Layer

Stringer Beads Only

Gas Cup Size #4 (.250") Min.

Multiple Layer

Single Electrode

Travel Speed

HEAT INPUT SHALL NCT EXCEED ± 10% OF THE ABOVE PARAMETERS

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CASE
N-432
CASES OF ASNIE BOILER AND PRELSSUR VESSEL CODE

Approval Data: February 20. 1916

See Numeric Index for expiration


- '" ed conoeafflrmptiondreC&

Case N-432
IX and additional requirements of Section Ill, as niudi.
Repair Welding Using Automatic or Machine Gas
Tungsten.Arc Welding (GTAW) Temperbead Technique fled by 2.1,2.2, and 3.0(c) and (J).
Section XI. Division 1

Inqfliry: Ma) tile' ailtiamatic or machim 2.1 Procedure Qualifications


I;i'TAW pro.
ces* ie u1sed as an alternative to the SMAWR' process for (a) Tlme test assembly materials feir the wcllineg iro.
perfomitig the teniperh,.ad technique on Ua.s I corn cedure qualification shall be of the salie speiricatitin
pollenth? type, grade, and class as the materials being repaired.
The test assembly shall receive a poitield heat treatlseist
Reply: It is the opinion of the Committee that repair that is at least cquivalent to the time and temperature
to P-Nos. 1, 3. 12A, 1211, and 12C base material and applied to the materials being repaired. The procedure
associated welds may be made by the automatic or and perfunnance qualification tests may be osmtbip,.d,
machine TAW lemperbead techniqe without thespeci. provided Section IX requirements are met. The test as
fled postweld heat treatment requirements of Section sembly dimensions, including joint details, shall be docu
III, provided the requiremenLs of 1.0 through 5.0 below mneeted on the PQIi.
are met. The depth otf repair is not limited provided the . (b)Th.. test assembly thickness shall be at lert
rte
teet as smicll mrets the rrequin'me.nt lf2.1. times tile depth of repair, but nveed iit exceed tile thick
sloes. t [ime material to lie repaired preividd thi re-quiired
test slt.cimei can be removed. Wien'i lite thit Lee-,iSif
1.0 GENERAL REQUIREMENTS tlst la-e iirtal to be repaired is greater tlia.. 2i i.. Ih,
deplth iltie cavity in tie test asbrinlly seall le tie
(a) Tle requirei. gith or IWA4(Xi(1, as apliceable,
greater tof I in. or the depth of the cavity Its
loe'rel-liail.
shall Iet'int.
lowev.r, in no case shall the pr(ceellre ilualilicatitan test
(b) Only the automatic or ma,-hine (;TAW proecss
using cold wire fee~d shil be used. No arc oscillation asenbly be less than 2 in. thick, nor shall tile h lih of
the cavity in the test assembly be less than I ins.
iall be used.
(c) W.'Idig material! shall be coontrolle'd during re (c) The te t assenitly diniensiuns semrrmiidiiig thai:
pair so that thae'y cavity shall be al least lice tIickness of the cwaili.oit at
arc identified as acceptable material
the' location of the repair or 6 in., whichever i.gr,-ate-r.
until vomsunmed.
If the re-'air weld is to be prrfir.d rm:etmt'i,. i1,' lai.
(d)TIl..eae'mtrinm fluuem in te"repair art-as shall be
al,-si inito
ce'dure, qualification, lest assembly shall be- ,'u.,iel,,te.d
arccmnt %fhrs r'.tablibhi.g the weld metal
with tile salmi t duplicate irenming andel eiee lrIleqiiij.
compisetieara linmie.
nmellotlia t, use'il fir the' repair. Ti le' t'sa.'saill hall
(P) Pe'miimg *11al nitl I permie d.
Aniielatl' t-e pitilii and bstructictnrm eelisti- ait-il
Ie'imair.
(d) h'lereott width arid time'immi'hld aii.,' il tIhr
2.0 WELDING QUALIFICATIONS
I'ati ii ill' 'llart
ab. eibl) ,hall hi,sie gre'at-'r d.
hli tam
Th," W'i~iing Pr.'.dore Sl,,.rifivation aoid the we'ldisig ililmli ii sp'cifieid Ill lin'u.o-ed
il il, re.'ir.
ool,'rateors shal b. q ialifieel in ar:,irdair', with Se'elien (e) "l'ii6 te',t Ue.s'ill nai)i) li . .4 ltee 4 h iai r0 ,
eitn'e. etr #eIehl buildup sof prrir., rllaiiiiii ai ateril,...
'P.No. 12A. 1210. and 124: dr'iaeli,re. rr'.r t s,,l'ifr mihetrial pooir tim.milliatiellm. tihe' do'1 1 tipe i,-eas'vit) hiall littl toe.
ecfireaiois,erindnallh i..ififi,.d in,Se-iin Ill. ald .wilowtqe.'ie. h', Ililiih,tlist- irkiil. lt 111e'vll lellilill.
i)rrrlaeii'ed in a li'r ediliN, 401 Set'11m Al. ir I ilm..
wioil'ievr i;Ngr'allr. Itsailijiem. tImt are's uelIlle 10i1

A-I.2

noppiWN--N-wwmmm-.
CASE (continued)
N-432
CASES OF ASME BOILER AND PRESSURE
VESSEL CODE

shall not be less than the area of tile well buildup to b.


applied or 54 sq in., whichever is less. e Also, if tile repair weld is to be performed
() For all applications, the lest remotely, the
assembly and cavit) . pec..vmance qualification test shall
shall be of sufficient size be coilipleted with
to obtain the required lesi lthesame or duplicate sensing and control
equipmelt to
specime:ns. be used for tie repair. For
these applicatiolis, only non.
(b,) Welding material shall destructive examination
mee.t the reqlireneni i of the weld is required.
Seetions IX and Ill, and the Editiun and Addenda of Tile
be mtated in tie repair program. shall procedure and welding opcrateir performance qalifia.

h~ hess tetiiig requirements


Th,. appropriate tough.
of NI-2000 rhall be completed
for tili: uld materials used.
ion tests may be combined, provided ection IX require.
ments are met.

N (h) Wdling procedure qualification


2.-h-,ll lIeperfer,,med ill
Ill fior groove %rlds, and
be, stat.d in tile repair
destructive tests
accordan.,. it i Sec tiori
the Edition and Addenda
program. Dropweight
IX ell
shall
tests,
3.0 REPAIR WELDING
impact tests. side bend
tests, and all weld metal tension Welding of the cavity or area
being repaired shall be
tests of the welI deposit
are required. A reference in accordance with the following.
ductility transition temperature (RtTDT) nil (a) The cavity or area to
--"wz of the weld he repaired by welding and
metalInl-se
NB 00 metal f, shall •be established a band around the cavity or
area
- with 0 f RTN is less than in accordance 300*F minimum. This temperatureshall be preheated to
or equal to 60 0 F, shall be maintained
tilequa ification test shall be for at least 30 min before
RT.VDT is greater than 600F, conisidered acceptable, If weldinf, said until starting
welding is started, during
the qualificatiun test shall the postweld heat treatment
le rijt'cte.d and a requalificaimn of 450 F to 550*F described
of the procedure shall in (e) below. The width of
be performed. Test specimens the Land shall be at least three

Ii
shall lie obtained from the times the thickness (37)
completed test assenbly
at the maximum practical
of the component to he welded,
depth but need not exceed 10
of rtpair. in. The component thickness
(7) shall be determined for
(i) Impact tsting of the the area to be welded prior
procehre qualification test to formation of the cavity.
as.,'nbl% HAZ shall be conducted The interpass temperature shall
as follows. not exceed 450°F.
The TNDT of the unaffected (b) Thermocouples and recording
based material shall be instruments shall
detrmined by dropweight be used to monitor the preheat,
test to establish the test interpass, and postweld
temlerature for the C,tests. heat 'treatment temperatures.
The Ce specimens represent. Thermocouples shall he at.
ing tile IIAZ material and th. tached by welding or mechanical
m.thods.
sall b, tested at the (T.'DT unaffected base material (c) The first six layers of the
cavit" shall be buttered
+ 60°F) temperature of
unaff,.ct,.d base material. the as shown in Fig. 1, Steps I through
The HAZ.C, absorbed energy 3.
aill lateral expansion shall (d) The essential welding variables
be equal to or greater than shall be controlled
Ill, uiafft'ct,.d ba.e material at as follows.
the (N 7')T + 60UF) t'n
lieratlrc of the haze' material. (I) Tile weld heat input for each of
tile first six
layers shall be controlled to within
±IO'/A of that used in
the procedure qualification test.
(2) The remainder of the Weld
deposit shall be
comleleted (see Fig. I, Step 4) with
2.2 Performance Qualification the heat input equal
to or less than that used for layers
beyond the sixth in
Til, weldiing operator shall be the
prc-'edore qualificationi.
qualified ill accerlao.e
will Sction IX andi Ih. (3) Th. finished surface of th,.
f-Jl, ing addition.ul reqoire. repair shall be sub
t'o.-. . If til r,.pair %,.Ild stantially fl.-h with the surface
is to lir perfoni d W.her. of the. component sur.
I111.- i,'al.lltnie.jtimiimpair ihe' w,'lding roindui./ig tIII"
re'pair.
thp,'rfnii , ti," operalor'b abilit)
w,'ling ,'liratr shall al. (4) 'l,. ti'einhilur descril,wel
o d,:nin.,trath. in this plaragralpls
thI,. abilil tI',, e,.' .i- shall he-perfin.,.dl in the procedur,,
uil'I o 4-'l,l ei'tal ill t qualificatin, t'st.
rt"l'lir'e , i..if,_ i..o
Je.,itioll.
ihl i. sat,'
, partel,.t,.rs ami oiiiillhd (P) At tll'. compl,.ion of
weling. tlia! 37' land1 a.,
Ih. ial -h.-Inietitins tIhat
~ are inoh'd ill tia- r'pair.
d,'fiul'd il (a) aie eve i all
be maitaned in the rang: ,if
4l50°1- toa5500F1 ..
for at lea.tI 2 hr.

A-1.3
CASE (continued)
N-432
CASES OF ASME BOILER AND PRESSURE VESSEL CODE

layer one with


Step 1,:Deposit
lirsl'ayer weld
parameters used in
quail fications.

Step 2: Deposit
layer two with
second layer weld
Parameters used in
qualifications.

Step 3: Deposit
next four layers
with layer three
through sixweld
parameters used in
qualifications

Step 4: Subsequent
layersto be
deposited as
qualified.

FIG. 1 AUTOMATIC OR MACHINE (GTAW) TEMPERSEAD


TECHNIQUE

A-1.4
CASE (continued)
N-432
CASES OF ASME BOILER AND PRESSURE VESSEL CODE

4.0 EXAMINATION
(a) The repair area and the 3T band as defined in
3(a) shall be nondestructively examined after the com
pleted weld has been at ambient temperature for at least
48 hr. The nondestructive examination of the repair
welded region shall include radiography (if practical),
ultrasonic examination, and surface examination.
(b) Areas from which weld-attached thermocouples
have been removed shall be ground and examined using
a surface examinatioi, method.

5.0 DOCUMENTATION'i
The use of this Code Case shall be recorded on Forn
NIS.2 or other applicable docunients.

71.11

'1

A-1.5
* ' STRUCTURAL
INTEGRITY
ASSOCIATES, INC.
3150 Almaden Expressway
Suite 226 M 3ssil 8S P,1 Operations
San Jose, CA 95118 May 31, 19896. uM er R d
(408) 978-8200 AJG-89-035. Sute I0
TELEX: IM17 STRUCT A(o ) o 4313
FA: (408) 978 894 (216 8 8 6
FAX: (216) 869-5461

Mr. S. Burkhalter
Welding Services Incorporated
3276 Marjan Drive
Atlanta, GA 30340
Subject: Revision to Letter AJG-89-031, dated May 19, 1989,
"Consulting Support for Qualification of Welding
Technique for Temperbead Welding on Indian Point Unit 2
Steam Generator Shell"

Dear Steve:
The purpose of this letter report is to document my review of the
results of the subject temperbead welding qualification test
program conducted by Welding Services Incorporated (WSI) for
Consolidated Edison Company. The temperbead qualification was
performed for the Indian point Unit 2 (IP-2) steam generator
shell. The shell material is SA302 Grade B low alloy steel,
designated by the ASME Code as P-3 Group 3 material.' The purpose
of the temperbead qualification was to be prepared to perform a
cavity weld repair to one or more of the IP-2 steam generator
shells using this welding approach, such that an elevated
temperature (11500F) post weld heat treatment would not be
required. ASME Code Case N-432, issued in February, 1986 [1],
provided guidance for the temperbead qualification activity at
WSI. Both weld parameter trial tests (on a thinner plate of
SA302 B material) and procedure qualification tests (on a thicker
plate) were performed in order to select a weld procedure and
then to qualify it. Although a dilemma arose wherein the thicker
plate was not entirely representative in terms of toughness, the
results on the thinner and thicker plates, taken together,
demonstrate that the procedure should be technically acceptable
for use on the 3.5 inch thick steam generator shell at IP-2, as
discussed in the following sections of this report.

Weld Trials
In the technical program undertaken for the qualification, WSI
performed a technical evaluation of eight (8) different automatic
gas tungsten arc welding (GTAW) approaches for welding the SA302
B cavity. The welding approaches included a welding technique
which reproduced the Babcock and Wilcox approach which formed the
basis for ASME Code Case N-432 [2], as well as modifications to
that approach to improve the ease of welding in the field.
Page 2 May 31, 1989
S. Burkhalter
AJG-89-0 3 5

Following the welding of eight test


using these eight different welding coupons of SA302 B plate
techniques,
microhardness measurements were performed metallurgical and
[3]. on the test coupons
The microhardness measurements revealed
welding techniques produced a weld that three of the
hardness well below Rockwell C heat affected zone (HAZ)
hardness
reference hardness used for selecting 37, an upper bound
suitable for use in the temperbead a welding process as
These three welding techniques included procedure qualification.
and two approaches where the travel the Reference 1 approach
speed
for greater ease of welding. WSI selectedwas adjusted to provide
the two travel speed adjusted welding technique P-6, one of
qualification techniques, for procedure
in accordance with Code Case
microhardness results for the P-6 N-432. The
in Table 1 [3]. welding approach are presented
One notes from Table 1 that the maximum
in the HAZ in the technique P-6 plate hardness
Rc 37 target value. is Rc 33.5, well below the
Thus, this procedure appears quite
of meeting the HAZ requirements capable
of this representative base
material.
One additional weld trial was conducted
parameters. using the P-6 weld
A single bead weld was deposited
plate and the hardness measured in. on the SA302 B
test would compare the untempered the HAZ of the plate. This
hardness with the tempering
,anticipated using the P-6 welding technique.
single bead weld are presented in Table The results of that
observes from Table 2 that the untempered2, from Reference 3. One
maximum hardness of Rc 49, more than weld HAZ contains a
than the tempered P-6 process HAZ. 15 hardness points higher
These results confirmed the
fact that the temperbead process
technique is representative of adeveloped using the P-6 welding
welding process which should
produce a base metal weld HAZ which
an untempered structure. is substantially softer than
Based upon these results and the ease
of application of this welding
was selected as the preferred process, the P-6 welding approach
approach for the temperbead weld
procedure qualification.

Weld Procedure Qualification


The Weld Procedure Qualification Record
inch deep groove weld into a 7.125 [4] specifies welding a 3
material. inch thick plate of SA302 B
The material type and minimum thickness
and the groove for procedure qualification of the plate
Case N-432 and by Section XI of the were specified by Code
ASME Code [5]. The required
tensile, side bend, drop weight and
Charpy
removed from the plate following welding v-notch specimens were
Technical Services, Inc. and tested at Applied
The tensile test results and the side
bend test results were certified to
the Applied Technical Services, Inc.be acceptable as presented in
certified test reports [6].

ellMM
Page 3 May 31, 1989
S. Burkhalter
AJG-89-035

The base metal drop weight specimens


condition in duplicate-specimens at +40OF produced a no break
produced a no break condition at -10°F. whereas the weld metal
the reference nil ductility transition The Code Case requires
metal and the base metal to be no greater temperature of the weld
weld HAZ to have Charpy v-notch absorbed than +600F, and the
expansion equal to or greater than the energy and lateral
unaffected base metal at
the nil ductility transition temperature
plus 600F.
Since the reference temperature from
the all weld metal drop
weight specimens was -206F, the Charpy
+40°F and the requirements of the Code tests were conducted at
Case and the Code were
met. Since the reference temperature from
weight tests was +300F, the Charpy v-notch the base metal drop
metal and the HAZ were performed initially tests for the base
metal specimens did not meet the 1980 ASME at 900F. The base
determining reference NDT at +900F. Section III values for
absorbed and lateral expansion were However the HAZ energy
far superior to the base
metal properties, thereby meeting that
Case. requirement of the Code
The Charpy v-notch results for these tests
are presented
in Attachment 1 [6).
A second series of base metal and HAZ
impact tests were performed
at +120°F in an attempt to meet the Code
at the maximum temperature allowed by of repair requirements
metal. The results of these tests are the Code Case for the base
presented in Attachment 1.
The base metal tests again failed to
requirements at the maximum temperature meet the Code toughness
alIowed
However, note that the HAZ impact toughness by the Code Case.
the base metal toughness at 120°F, attesting is still superior to
to the adequacy of
the weld procedure.

Conclusions
The properties of the base metal
qualification program did not meet allused in the temperbead
Code Case N-432 and the Code of repair. of the requirements of
these requirements in this case is overly However, application of
was constructed to ASME Section III, restrictive. The plant
1965 with addenda through
1966, a Code which prescribed less
in the way of toughness
requirements for this material than either
Code Case N-432. The intent of Code Case the Code of repair, or
the weld procedure which is qualified, N-432 is to assure that
representative material which provides qualifies a process on
assurance that the welding
process has not degraded the base metal.
energy absorbed and lateral expansion The HAZ Charpy v-notch
those of the unaffected base metal in were clearly greater than
7.125 inch thick SA302B plate used this test program. The
in this test program is
representative material in that section thickness. One

ASSCIATES M
Page 4 May 31, 1989
S. Burkhalter AJG-89-035

characteristic of this material is its poor through


hardenability, thickness
thereby resulting in plate which in this
thickness, may have poor notch toughness in the
1/4t to
region. In reduced section thicknesses, this material 3/4t
is
expected to have better toughness.
The steam generator shell at IP-2 is significantly
inches thick, and has superior Charpy v-notch impact thinner, 3.5
compared to the test plate as would be expected for properties
this grade
material. The steam generator shell impact strength exceeds of
minimum construction code requirements of 30 ft-lbs the
contrasted to approximately 30 ft-lbs at 120°F for at +10°F as
thick test plate. the 7.125 inch
Were the test -plate a more representative
thickness, I believe that the notch impact properties
been significantly improved. would have
This observation is substantiated
by the weld trial tests in the thinner plate (2.25
where hardness measurements revealed a softened inches thick),
with increased toughness for a representative HAZ consistent
restrictions of Code Case N-432 required a thickermaterial. The
to plate than is
be welded to in the field thereby restricting
qualification program to use of a base metal which the
could not be
reasonably expected to meet the notch toughness requirements
the Code Case. in
Consequently, while all requirements of Code
Case N-432 cannot be literally adhered to, I believe
considering both the trial weld .tests and that, when
the
qualification tests taken together, a clear demonstration procedure
been made that the HAZ properties have not been degraded has
SA302 B plate and that the temperbead process in the
is technically
qualified for use at IP-2.
I trust that this document meets your requirements
regarding the
qualification of this process. If you have additional
or require additional information, please do not questions,
hesitate to
call.
Very truly yours,

A. iannuzzi, Ph ,P.E.
Ass 6Siate

/mc
enclosures

ASSOCIATES INC
Page 5 May 31, 1989
S. Burkhalter AJG-89-035

References
1. Cases of the ASME Boiler and Pressure Vessel Code,
N-432, Repair Welding Using Automatic or Machine Case
Tungsten Welding (GTAW) Temperbead Technique, Section Gas
XI,
Division 1, February 20, 1986.
2. EPRI Report NP-3614, Repair Welding of Heavy-Section
Components in LWRs, Babcock & Wilcox Company, July, Steel
1984.
3. Report CMS 405-89, Subject: Microhardness Testing of
Various
Welds Involved in Temper Bead Pass Welding, Consulting
Metallurgical Services, Inc., April 27, 1989.
4. Procedure Qualification Record A03N432, Welding Services
Inc.
5. ASME Boiler and Pressure Vessel Code, Section
XI, 1980
Edition Including All Addenda Through Winter, 1981.
6. Report AO-0394, Applied Technical Services, Inc., Inspection
and Metallurgical Test Reports, Purchase Order No.
207593,
May 9, 1989.

STRCTE L
I

TAFI1,E 1
11-6 Weld Process Microhardness Restilts

Distance
inches A B C p
Filars FLI_ KIlN 5 0KIN500 ars500 F i lars KIIN 5 0
.002 347 268 338 282 336 286 338 282

.004 335 287 321 313 323 I 309 333 291

.012 345 271 331 294 323 I 309 322 312

.020 329 297 330 296 321 313 322 312

.028 333 291 322 312 313 330 334 289

.036 336 286 329 298 309 338 348 266

.044 338 282 327 302 318 319 350 263

.052 335 287 337 284 322 312 342 276

.060 346 269 338 282 320 315 342 276

.076 350 263 340 279 329 298 338 282

.084 356 254 318 319 335 287

1I08 352 260 354 257 330 296

iKIIN ----- -- 5 0 0 W. (cony.

A-297 28.9

B-319 31.1

C-338 33.5

D-312 30.0
TABLE 2

icrohardness Resul ts on Single Bead Weld


Using 11-6 Weldi ng Process

Distance from Filars KILN500 Filars KHN 500 Filars KILN500

fusion

0.005" 255 495

0.015" 257 486

0.025" 255 495

-0.045" 248 525

0.065" 252 508

0.085" 254 500

0.105" 254 500

Iligh Hardness

A - KIIN Rc (cony.)
--525500
49.0
ATTACIDIENT 1

SUMARY OF WELD METAL, HAZ


AND BASE METAL CHARPY V-NOTCH
TOUGHNESS TEST RESULTS

Attachment to AJG-89-035
APPLIED TECHNICAL SERVICES, INC.
MARIETTA. GA.
METALLURGICAL TEST REPORT
Ref. HO-0516 Date May 11, 1989 Page 4 of 10
PURCHASE ORDE; # 207953

Welding Services, Inc.


MAT:IAL: SA 302
3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432
L Attention: Steve Burkhalter

Metallurgical Test Procedure

Hardness Specifications: Tested in accordance


Case Depth with AS.!_ BPVC Sec
tion I7I; NB-2331 and
Impact Ca.,V-orch
ASME BVC Section IX;
Coating Thickness QW-171 35 mils lateral
expansion and 50 ft-li
Coating Weight
minimum.
Bend Test Ref. Case Code N-432
Other-.---.

Metallurgical Test Results


PART IDENTIFICATION QUANTITY RESULTS REMARKS

Weld Metal 3 1i: 63 ft-lb 0


T 4 r
-cv .
63 mils lat. exp.
40% shear

2: 105 ft-lb RTNDT Tcv -60°F


69 mils lat. exp.
70% shear

3: 80 ft-lb RTNDT: - 20°?


62 mils lat. exp.
60% shear

.AA - - _____________

Witnessed by

L Preopared by: >iV .Armnistead


0 bTes: Engineer
Approved by: /"-_v R. W. Dunning
Mana or
APPLIED TECHNICAL SERVICES, INC. MARIETTA, GA.
METALLURGICAL TEST REPORT
Ref. HO-0516 Date May 11, 1989 Page 5 of 10
PURCHASE ORDER # 207953 ..

Welding Ser:ices, Inc. MATERIAL: SA 302


3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter

Metallurgical Test Procedure


Hardness Specifications: Tested- in -accordance
CaseDept ,'
C ase epthtion with AS E BPVC Sec
III; NB-2331 and
Impact -iarpy, V-Notch
ASME BPVC Section IX;
Coating Thickness _
0W-171
Ref. Case
Coating weight Absorbed energy and lateral Code N-432
expansion
Bend Test E equal to or greater than base metal
Other- - . at TNDT + 60F of base metal

aRI -a - . .? * - -

ivetaliurglcal I est Res ults


PART IDENTIFICATION OUANTITY RESULTS REMARKS
RESULTS
Heat Affected 1. 46 ft-lb Tcv =90°F
Zone 39 mils lat. exp.
20% shear TN-DT = 300F (base metal
drop test)
2. 51 ft-lb
46 mils lat. exp. 29 mils lateral expansion
20% shear and 28 ft-lb average for
base metal at T vc =90°F

3. 35 ft-lb
32 mils lat. exp.
20% shear

A. t1.68

Witnessed by

,1 Prepared by: . Armistead


Test Engineer
LI...
Approved by: R. '.Dunning
DDR.
.~. ,.anaerer
*,I* *'~. - -
/~~DP j "rrijr wwvkvif-
APPLIED TECHNICAL SERVICES, INC.
MARIETTA, GA.
METALLURGICAL TEST REPORT
Ref. HO-0516 Date May 11, 1989 Pa e 8 of 10
PURCHASE ORDER # 207953

Welding Ser-,ices, Inc. ,MATE;IAL: SA 302


3276 Marian Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter

Witnessed by
- y Prepared by: . -W .Armistead
.~, -'-
'-~ ~: Test Engineer
Aporoved
^100by: / R,M W. Dunn i-.-
nAun
e-n
a 9-
ager
hl ,.T- '- :" TIE 1 ' F L I E D T E-:H E F.:-. I; E
P. .-
,

APPLIED TECHNICAL SERVICES,


INC. MARIETTA, GA.
METALLURGICAL TEST REPORT
R~ef. Ho-0S 6-2 Date may 5, 198 9
.FC 6- OCj; #.207953

Veldirg Services, inc.


3276 Marian Drive
L,:rE-!! L SA - 02
Arlanta, Georgia 10340 Grade B
FilR No: A05;3422
L Aen:'0n: Steve Burkhalter

Metallurgical Test Procedure


Hardness - Specifications: Tes eq. In acrnce
Case Depth _ wh AS.:E BPVC Sec-
Impact C-jary, V'- -- ti.on IiI; N2-2331 ar< d
AS.E B:VC Section !X
Coating Thickness 7--1 QW-171
Loating Weight Re . Case Code N-4i2
L Absorbed energy and lateral expansion
Bend Test - equal to or greater han b-e neal
Other . 7 a-, TND T ,, 60cF of base mee:a

Metallurgical Test Results


EART [DONTI;1CATION CUANTITY RESULTS
REMAK9
Feat Affected 3 1: 61 fbc-lb - z;
Zone
"45 mils lat. exp.
50% shear

2: 52 ft-lb
L7 mils lat. exp.
507 shear

3: 49 £t-lb
45 mils lat. exp,
50D% Shear

a., 1.54

WVinessed bv

Prepa' ed by: 4ZAAZm -2 .


M ' Ar .stead
'4
APPLIED TECHNICAL SERVICES, INC.
MARIETTA, GA.
METALLURGICAL TEST REPORT
Ref. H0-0516 Date May 11, 1989 Page 9 of 10
PURCHASE ORDER # 207953

Welding Services, Inc.


MATERIL: SA 302
3276 Marjan Drive
Grade B
Atlanta, Georgia 30340
PQR No: A03N432

L Attention: Steve Burkhalter

Witnessed by
Prepared by: .M. . Arm tead
t,'.'.
L ""
A."" " ";" ". ':f "
h!.:
" 'J~; '"-
E; t ", - ,."-'" Test Engineer
Approved by: _, R. W.. Dunnin,
SMana2er.
APPLIED TECHNICAL SERVICES, INC.
Dr. Anthony J. Giannuzzi, P. E.
Associate

Education

BS, Physics, LeMoyne College (1964)


MS, Solid State Science.and Technology, Syracuse University (1967)
PhD, Solid State Science and Technology, Syracuse University (1969)

Professional Associations

Professional Corrosion Engineer, State of California

Professional Experience

1983 to present Structural Integrity Associates, San Jose, CA


Vice President
1979 to 1983 Electric Power Research Institute, Palo Alto, CA
Project Manager

1978 to 1979 NUTECH, San Jose, CA


Project Manager
1972 to 1978 General Electric Company, San Jose, CA
Principal Engineer

1969 to 1972 Aerojet Nuclear Systems Company,


Sacramento, CA

Summary

Dr. Giannuzzi has been involved in solving materials and corrosion problems for the
nuclear industry since 1969. One of the world's leading authorities on intergranular stress
corrosion cracking of stainless steel in aqueous systems, Dr. Giannuzzi was employed by the
Electric Power Research Institute in the Nuclear Systems and Materials Department for
three and one-half years prior to joining Structural Integrity Associates in 1983. At EPRI,
Dr. Giannuzzi was task leader and principal investigator involved in development and
qualification of all the Boiling Water Reactor IGSCC piping remedies. This activity
included primary responsibility for qualifying and producing material specification for the
alternative materials (Types 316NG and 304NG stainless steels), qualifying the induction
heating stress improvement (IH1SI) remedy, qualifying heat sink welding, last pass heat
sink welding and the weld overlay and performing the investigations to determine the
causes of and remedies to IGSCC in Type 304 stainless steel pipe.
In addition to his BWR IGSCC responsibility at EPRI, Dr. Giannuzzi has had the lead
responsibility for investigating the causes of low pressure large steam turbine stress
corrosion cracking in nuclear and fossil steam turbines and has been involved in projects
associated with bolt and fastener reliability, steam and water piping erosion-corrosion and
has been active in projects related to primary and secondary side corrosion of steam
generators. Dr. Giannuzzi has also been the lead project manager responsible for all
materials related failure analysis activities in the Nuclear Systems and Materials
Department and was a member of the EPRI Three Mile Island Unit 2 task force.

INTEGTTr
AESOCATES. INC.
Page 2
A. J. Giannuzzi

Prior to his employment at EPRI, Dr. Giannuzzi was employed as a senior consultant at
NUTECH. While at NUTECII, he formed the stress corrosion cracking group and
developed the methodology used to estimate likely locations of IGSCC in stainless steel
piping systems. He also was involved in the earliest investigations involving PWR boric
acid corrosion and assisted in the final formulation of the NRC I-E Bulletin 79-02 which
established criteria for inspection of the boric acid system piping.

From 1972 to 1978, Dr. Giannuzzi worked as a principal development engineer at the
General Electric Company. Nuclear Energy Division. His responsibilities while at GE
involved investigation of alternative materials and processes to alleviate the IGSCC
problem in stainless steel piping. He managed the initial weld residual stress measurement
and analyses activities which lead to the development of the residual stress remedies to
IGSCC.

From 1969 to 1972, Dr. Giannuzzi worked for the Aerojet Nuclear Systems Company
developing materials for use in the nuclear rocket engine (NERVA).

In 1983, Dr. Giannuzzi founded Structural Integrity Associates with Dr. P. C. Riccardella
and Dr. T. L. Gerber. His activities at Structural Integrity have included nuclear plant life
extension studies, temper bead welding development on low alloy steels and selecting of
remedies to IGSCC in BWRs.

ST,CTU AL
~INTEGBMY
ASqSOCTS INC.
~o (9 ye i 7~4
I-0 2
/'_'Uf 989
)~~1 Docket"..i No.
aA/ f nt.
50.247
Ulf iL
, NO. e

Document Control
U.S. Nuclear Renlii.Desk ^- de
Washington, D.C. 20555 V
SUBJECT: Relief Request Regarding Temperbead Welding on
Indian Point Unit No. 2 Steam Generator
Shell
9, /4/A
As a contingency measure for the 1990 mid-cycle outage
for Indian Point
Unit No. 2, Consolidated Edison has been planning
the development and
qualification of an automatic gas tungsten arc welding
(GTAW) temperbead
process to be available for steam generator girth
weld repair. The
automatic GTAW temperbead process is a welding process
which produces a
tempered, as deposited, heat-affected zone microstructure
properties which are similar to that of GTAW weld and weldment
deposits which have
been post weld heat treated. The qualification requirements
for the GTAW
procedure cannot be met to the letter of the applicable
ASME code case
due to the unavailability of the test material required
as stated.
Attachment A contains a brief discussion and
basis upon which
Consolidated Edison hereby requests that the NRC
grant
10 CFR 50.55a subparagraph(6)(i), from strict interpretation relief, per
of Code Case
N-432 for this repair procedure.

Attachment B contains the detailed weld procedure


qualification package
for your review. I
Should the staff have any questions on this matter,
Mr. Jude Del Percio, Manager of Regulatory Affairs and please contact
Safety Assessment.

Attachment

_7% '-/55 ' ~ J c~n 2~7 $z~

6~2&@ t~A14
ATTACHMENT A

Regulatory Input Related to Relief Request


Regarding Temperbead Welding of
Low Alloy Steel Vessel Materials
Using GTAW

Consolidated Edison Company of New York, Inc.


Indian Point Unit No. 2
Docket No. 50-247
July, 1989
In anticipation of need, Consolidated Edison has developed a temperbead
weld qualification program for the Indian Point Unit
No. 2 steam
generator shell. The shell material is SA302 Grade B low alloy steel,
designated by the ASME Code as P-3 Group 3 material. The
purpose of the
temperbead qualification was to be prepared to perform
repair to one or more of the IP-2 steam generator shells a cavity weld
using this
welding approach, such that an elevated temperature (llSOOF)
post weld
heat treatment would not be required. ASME Code Case N-432,
issued in
February 1986, provided guidance for the temperbead
qualification
activity. Both weld parameter trial tests (on a thinner
Grade B material) and procedure qualification tests (on plate of SA302
a thicker plate)
were performed in order to select a weld procedure and
then
it. Although a dilemma arose wherein the thicker plate was notto qualify
entirely
representative in terms of toughness, the results on the
thinner and
thicker plates, taken together, demonstrate that the procedure
should be
technically acceptable for use on the 3.5 inch thick
steam generator
shell at IP-2, as discussed below.
The properties of the base metal used in the temperbead
qualification
program did not meet all of the requirements of Code Case
N-432 and the
Code of repair. However, application of these requirements
in this case
is overly restrictive. The plant was constructed to ASME Section III,
1965 with addenda through 1966, a Code which prescribed
less in the way
of toughness requirements for this material than either
the Code of
repair, or Code Case N-432. The intent of Code Case N-432 is to assure
that the weld procedure which is qualified, qualifies
a process on
representative material which provides assurance that the
has not degraded the base metal. The HAZ Charpy v-notch welding process
energy absorbed
and lateral expansion were clearly greater than those of
base metal in this test program. the unaffected
The 7.125 inch thick SA302B plate use
in this test program is representative material in that section
thickness. One characteristic of this material is its poor through
thickness hardenability, thereby resulting in plate
,which, in this
thickness, may have poor notch toughness in the 1/4t to 3/4t
region. In
reduced section thicknesses, this material is expected
to have better
toughness.
The steam generator shell at IP-2 is significantly thinner,
3.5 inches
thick, and has a superior Charpy v-notch impact properties
compared to
the test plate as would be expected for this grade of
material. The
steam generator shell impact strength exceeds the minimum
construction
code requirements of 30 ft-lbs at +lOOF as constrasted ;to
approximately
30 ft-lbs at 120OF for the 7.125 inch thick test plate.
plate a more representative thickness, we believe that the Were the test
notch impact
properties would have been significantly improved. This observation is
substantiated by the weld trial tests in the thinner plate
(2.25 inches
thick), where hardness measurements revealed a softened,
HAZ consistent
with increased toughness for a representative material. ;
The restrictions
of Code Case N-432 required a thicker plate than is to
be welded to in
the field thereby restricting the qualification program to
use of a base
metal which could not be reasonably expected to meet the
notch toughness
requirements in the Code Case. Consequently, while all requirements of

a'I
Code Case N-432 cannot be literally adhered to, we believe that, when
considering both the trial weld tests and the procedure
qualification
tests taken together, a clear demonstration has been
properties have not been degraded in the SA302 Grade made that the HAZ
B plate and that the
temperbead process is technically qualified for use at
IP-2.
In addition, the ASME Section XI Special Working
Group on Repair by
Welding will formally include the use of automatic GTAW
temperbead in the
code. This will be addressed during the summer 1989 meeting.
Additionally, the ASME has realized that the present
N-432
automatic GTAW temperbead, as it now exists, is unworkable, code case for
specifically
for thick section plate qualification. As a result,
the committee is
recommending the following changes to the weld qualification
requirements:
o The test assembly shall be of the same "P" number
and Group
number as the component being repaired.
o The base metal impact properties shall meet the design
specification.
o The average of the three charpy V-notch HAZ results
shall be
equal or greater than the average of the three base
metal
impact values.
In conclusion, Consolidated Edison believes that the strict
interpretation of Code Case N-432 for this temperbead
Grade B steam generator shell material is clearly repair of SA302
impractical and that
the weld procedure, as prepared, is technically adequate.

Consolidated Edison, therefore, requests relief from the full


requirements of Code Case N-432 such that the weld
procedure already
developed is acceptable and qualified.
STRUCTURAL
INTEGRITY
ASSOCIATES, INC.
3150 Almaden
Expressway
Suite 226
May 31, 1989 ossil Plant Operaton
San Jose, CA 95118
AJG-89-034 Sou er Road
(408) 978-8200AkonOh..
Suite 10
TELEX: 184817 STRUCT Aron,Oho 44313
FAX: (408) 978-8964
(216) 864-8886
FAX: (216) 8M-5461
Mr. S. Burkhalter
Welding Services Incorporated
3276 Marjan Drive
Atlanta, GA 30340
Subject: Additional Information Regarding Through
Thickness
Properties of A302 B in Thick Sections

Dear Steve:
As a result of our telephone conversation
your request for additional data of May 25, 1989, and
regarding the through-thickness
properties of A302 Grade B pressure
sections, I have performed an additional vessel steels in thick
the assistance of Fred Copeland, literature review, with
of lowalloy steel. -As you know, of the properties of this class
pressure vessel steel which is not A302-B isrepre-s-entativ-. off -a'
nuclear vessel applications due to generally used today inthick
hardenability. its lack of through-thickness
Consequently, -a literature review
examination of relatively old data involves
reference documents were located from limited sources. Two
was prepared (References 1 & 2). from which this letter report
Reference 1 is a background
technical report from Lukens Steel
Steels for Nuclear Service". entitled "Heavy Gage Plate
Reference 2, appended to this
letter report, is entitled "Utilization of
Tempering for Improvement of Low Quenching and
Alloy Steels in Heavy Thickness
for Welded Construction".
One of the characteristics of most
solid state, minor changes in steels is the fact that in the
treatment can produce dramatic composition and/or in heat
changes
steel. For example, in a carbon or low in properties of the
cooling from. above the austenitizing alloy steel, a rapid
very strong bainitic or martensitic temperature can produce a
cooling will produce a ferrite-pearlite structure, whereas slower
bainitic or martensitic structure, microstructure. The
once properly tempered, will
produce a high yield strength, high-toughness
the ferrite-pearlite structure will material, whereas,
lower yield and ultimate tensile have lower toughness and
only fabrication differences betweenstrength. One notes that the
toughness structure and the low strength, the high strength, high
is cooling rate. low toughness structure
This cooling rate from austenitizing
treatment temperature. is a function heat
thickness and location in the plate of quench medium, plate
(surface vs. mid-wall, etc.) through-thickness direction
However, for a given cooling rate
Page 2
S. Burkhalter
May 31, 1989
AJG-89-034
(defined by the above parameters), the
transform to bainite and/or martensite cantendency of a steel to
be enhanced by further
increasing the alloying or carbon content
hardenability of the steel. to increase the
Hardenability, therefore, can be
defined as an index of the depth to which
can be formed in a given steel as the resultmartensite or bainite
of a given hardening
treatment and cooling rate.
The A302 Grade B low alloy steel pressure
somewhat limited hardenability in: thick vessel material has
in Figures 1 through 3, from Reference 1. sections as illustrated
1 for One notes from Figure
A302-B plate with additional nickel,
Charpy-v-notch that the.
toughness decreases dramatically as
thickness is increased. plate
Figures 2 and 3 illustrate that the
yield and ultimate tensile strengths
decreased as plate thickness increases.
are also dramatically
tempered condition, the notch toughness Even in the quenched and
of the
degraded in thicker sections as illustrated A302-B steel is
in Figure 4
(Reference 2).
As a result of the toughness and hardenability
sections., steel producers developed problem in thick
a second -generation _of__.
reactor steels (Reference 1), steels which
A542 and A533.designation of low alloy steels. included the A543,
became the modern generation replacement The A533 Grade B
material to A302 Grade
B. The basic difference between A533-B
fact that the second generation material steel and A302-B is the
which lowers the nil ductility transition contains some nickel
improves notch toughness of the A533-B (NDT) temperature and
Although some through-thickness problems material (Reference 1).
the second generation A533-B materials, thedo indeed still exist in
the NDT temperature (typically to less dramatic reduction in
than 0°F), and the large
improvement in notch toughness due to the
than compensate for the through-thickness nickel addition, more
hardening deficiency in
thick sections.
In summary, the through-thickness hardenability
exists in A302 Grade B low alloy steel problem which
pressure vessel material
also exists to a lesser degree in
replacement material, A533 Grade B. However,the modern generation
produces such a dramatic increase in upper the nickel addition
and dramatic decrease in NDT temperature shelf notch toughness
that the hardenability
problem can be tolerated in this modern material.
applications involving For
thick section plates, the residual
elements, such as Cr, and other elements
mainatined near the top end of permitted are also typically
limits, in order to get
an additional "boost" in hardenability
through-thickness strength and toughness. and, thus, in
A302-B material does not provide the toughness The lower toughness
the A533-B. It is for that reason that margin provided in
the base metal toughness requirements we had difficulty meeting
in thick sections in the
A302-B material.
Page 3
S. Burkhalter May 31, 1989
AJG-89-034

I trust that this report


your needs in the subjectandarea.
the accompanying paper will meet
information, or further clarification,Ifpleaze
you require additional
do not hesitate to
call.

Very tr ,y yours,

A.IJ Giannuzzi
Associate

/mc
enclosures

References
1. "Heavy Gage Plate Steels for Nuclear Service",
R. H. Sterne,
Jr., Lukens Steel Company, June, 1966.
2. "Utilization of Quenching and Tempering
for-Improvement.-in-_i
Properties of Low Alloy Steels in Heavy
Welded Construction, R. E. Lorentz, Jr., Thicknesses for
Welding Research
Supplement to the Welding Journal, October,
1962.

STIRUCTURAL
EN w-EGFdrrY
ASSOCIATE& INC
60
WATER QUENCHED &TEMPERED
3T X 3T OR LARGER

rn
I:
z

040 N
z0

z 30

0
z 20
K

U10 N\

I I I
I I
10 15.
PLATE THICKNESS INCHES
Figure 1. Effect of Plate Thickness on Charpy V-Notch Energy at NDT
ASTM A302 GR. B + 0.50 - 100% Nickel
I

100

90

80

70

60

50
2.0 2.5 3.0 3.5 4.0 4.5 5.0
CRITICAL BAR DIAMETER, D1, INCHES
Figure 2. Effect of Hardenability on Yield Strength
ASTM A302 GR. B Steel
120

110

100

90

80

70-
2.0 2.5 3.0 3.5
4.0 4.5 5.0
CRITICAL BAR DIAMETER, D1, INCHES

Figure 3. Effect of Hardenability on Tensile Strength


ASTM A302 GR. B Steel
I

RANGE OF CHARPY V
NOTCH IMPACT PROPERTIES

QT DEOxIDATION
QUENCHEDPLATE FORGING MAT'L PRACTICE
& TEMPERED

Me-Mo 4LBS AL
A-3028 A-ZIZB CASE PER TON
1236

NC AL

M NORM. B EMDERE

- A-2128
40[I

0
-60 -4
-60

"-3" 3"-6 6€'C 1""4"


3OFT L3. TEMP
15 FT LB. 4 "- 6"
TEMP 20 FT LB. TEMP

THICKNESS OF PLATE
.OISTA NCE BELOW
OUENCHED SURFACE PLATE THICKNESS

Figure 4. Charpy V-Notch Impact


and Tempered Plate Data for Different
Metals Quenched
STRUCTURAL
INTEGRITY
ASSOCIATS, INC.
3150 Almaden Expressway Fssi Plant Operaton
Suite 226FoslPatOetin
SanJose, CA95118 May 19, 1989 66SouthMillerRoad
(4) 978-82 AJG-89-031 Suite 10
TELEX: 19- 2s0u Akron, Olio 44313
TLX: (48) 978964 (216) 864-8886
FAX: (216) 8M-5461

Mr. S. Burkhalter
Welding Services Incorporated
3276 Marjan Drive
Atlanta, GA 30340

Subject: Consulting Support for Qualification of Welding


Technique for Temperbead Welding on Indian Point
Unit 2 Steam Generator Shell

Dear Steve:
The purpose of this letter report is to document my review of the
results of the subject temperbead welding qualification test
program conducted by Welding Services Incorporated (WSI) for
Consolidated Edison Company. The temperbead qualification was
performed for the Indian point Unit 2 (IP-2) steam generator
shell. The shell material is SA302 Grade B low alloy steel,
designated by the ASME Code as P-3 Group 3 material. The purpose
of the temperbead qualification was to be prepared to perform a
cavity weld repair to one or more of the IP-2 steam generator
shells using this welding approach, such that an elevated
temperature (1150 F) post weld heat treatment would not be
required. ASME Code Case N-432, issued in February, 1986 [1],
provided guidance for the temperbead qualification activity at
WSI. Both weld parameter trial tests (on a thinner plate of
SA302 B material).and procedure qualification tests (on a thicker
plate) were performed in order to select a weld procedure and
then to qualify it. Although a dilemma arose wherein the thicker
plate was not entirely representative in terms of toughness, the
results on the thinner and thicker plates, taken together,
demonstrate that the procedure should be technically acceptable
for use on the 3.5 inch thick steam generator shell at IP-2, as
discussed in the following sections of this report.

Weld Trials
In the technical program undertaken for the qualification, WSI
performed a technical evaluation of eight (8) different automatic
gas tungsten arc welding (GTAW) approaches for welding the SA302
B cavity. The welding approaches included a welding technique
which reproduced the Babcock and Wilcox approach which formed the
basis for ASME Code Case N-432 [2], as well as modifications to
,-"that approach to improve the ease of welding in the field.
Page 2 May 19, 1989
S. Burkhalter AJG-89-031

Following the welding of eight test coupons of SA302 B


using these eight different welding techniques, metallurgicalplate
microhardness measurements were performed on the test coupons and
[3]. The microhardness measurements revealed that three
welding techniques produced a weld heat affected zone of the
(HAZ)
hardness well below Rockwell C hardness 37, an upper
bound
reference hardness used for selecting a welding process
suitable for use in the temperbead procedure qualification. as
These three welding techniques included the Reference 1 approach
and two approaches where the travel speed was adjusted to provide
for greater ease of welding. WSI selected technique P-6, one
of
the two travel speed adjusted welding techniques, for procedure
qualification in accordance with Code Case N-432. The
microhardness results for the P-6 welding approach are presented
in Table 1 [3]. One notes from Table 1 that the maximum hardness
in the HAZ in the technique P-6 plate is Rc 33.5, well below
Rc 37 target value. the
Thus, this procedure appears quite capable
of meeting the HAZ requirements of this representative
base
material.
One additional weld trial was conducted using the P-6
weld
parameters. A single bead weld was.deposited on the SA302 B
plate and the hardness measured in the HAZ of the plate.
This
test would compare the untempered hardness with the tempering
anticipated using the P-6 welding technique. The results of
that
single bead weld are presented in Table 2, ofrom Reference 3.
One
observes from Table 2 that the untempered weld HAZ contains
a
maximum hardness of Rc 49, more than 15 hardness points higher
than the tempered P-6 process HAZ. These results confirmed the
fact that the temperbead process developed using the P-6 welding
technique is representative of a welding process which
should
produce a base metal weld HAZ which is substantially softer
than
an untempered structure. Based upon these results and the ease
of application of this welding process, the P-6 welding approach
was selected as the preferred approach for the temperbead
weld
procedure qualification.
Weld Procedure Qualification
The Weld Procedure Qualification Record [4) specifies welding
a
inch deep groove weld into a 7.125 inch thick plate of SA302 3
material. The material type and minimum thickness of the plate B
and the groove for procedure qualification were specified by
Case N-432 and by Section XI of the ASME Code [5]. Code
The required
tensile, side bend, drop weight and Charpy v-notch specimens
were
removed from the plate following welding and tested at Applied
Technical Services, Inc. The tensile test results and the
bend test results were certified to be acceptable as presentedside
,-the Applied Technical Services, Inc. certified test reports in
[6).
The base metal drop weight specimens produced % --- a
/STU CTdMU
• .- TE IIM
Page 3 May 19, 1989
S. Burkhalter AJG-89-031

condition in duplicate specimens at +40°F whereas the


weld metal
produced a no break condition at -10°F. The Code Case requires
the reference nil ductility transition temperature
metal and the base metal to be no greater than +600of the weld
weld HAZ to have Charpy v-notch absorbed energy F, and the
expansion equal to or greater than the unaffected and lateral
base metal at
the nil ductility transition temperature plus 600F.
Since the reference temperature from the all weld
weight specimens was -200F, the Charpy tests were metal drop
conducted at
+40°F and the requirements of the Code Case and
met. the Code were
Since the reference temperature from the base metal
weight tests was +30°F, the Charpy v-notch tests drop
for the base
metal and the HAZ were performed initially at 900F.
metal specimens did not meet the 1980 ASME Section The base
determining reference NDT at +90°F. III values for
However the HAZ energy
absorbed and lateral expansion were far superior
to the base
metal properties, thereby meeting that requirement
Case. The Charpy v-notch results for these tests of the Code
are presented
in Attachment 1 (6].
A second series of base metal and HAZ impact tests
at +1200F in an attempt to meet the Code of repair were performed
at the maximum temperature allowed by the Code Case requirements
for the base
metal. The results of these tests are presented in
Attachment 1.
The base metal tests again failed to meet the Code
requirements at the maximum temperature allowed by toughness
the Code Case.
However, note that the HAZ impact toughness is still
the base metal toughness at 1200F, attesting to the superior to
adequacy of
the weld procedure.

Conclusions
The properties of the base metal used in the
temperbead
qualification program did not meet all of the requirements
Code Case N-432 and the Code of repair. However, of
application
these requirements in this case is overly restrictive. of
was constructed to ANSI Code B31.1 which prescribed The plant
the way of notch toughness requirements for this much less in
material. The
intent of Code Case N-432 is to assure that the weld
which is qualified, qualifies a process on procedure
representative
material which provides assurance that the welding
process has
not degraded the base metal. The HAZ Charpy v-notch energy
absorbed and lateral expansion were clearly greater
than those of
the unaffected base metal in this test program. The
thick SA302B plate used in this test program is 7.125 inch
material in that section thickness. representative
One characteristic
material is its poor through thickness hardenability, of this
,-resulting in plate which in this thickness, may have poorthereby
notch

ASSOCIATES RTC
Page 4 May 19, 1989
S. Burkhalter AJG-89-031

toughness in the 1/4t to 3/4t region. In reduced section


thicknesses, this material is expected to have better toughness.

The steam generator shell at IP-2 is significantly thinner,


inches thick, and has superior Charpy v-notch impact properties3.5
compared to the test plate as would be expected for this grade
material. The steam generator shell impact strength exceeds of
minimum construction code requirements of 30 ft-lbs at +10°F the
contrasted to approximately 30 ft-lbs at 1200F for the 7.125 as
thick test plate. inch
Were the test plate a more representative
thickness, I believe that the notch impact properties would
been significantly improved. have
This observation is substantiated
by the weld trial tests in the thinner plate (2.25 inches thick),
where hardness measurements revealed a softened HAZ consistent
with increased toughness for a representative material.
restrictions of Code Case N-432 required a thicker plate than The
is
to be welded to in the field thereby restricting
qualification program to use of a base metal which could not the
reasonably expected to meet the notch toughness requirements be
the Code Case. in
Consequently, while all requirements of Code
Case N-432 cannot be literally adhered to, I believe that,
considering both the trial weld tests and when
the procedure
qualification tests taken 'together, a clear demonstration
been made that the HAZ properties have not been degraded in has
SA302 B plate and that the temperbead process is technically the
qualified for use at IP-2.
I trust that this document meets your requirements regarding
the
qualification of this process. If you have additional questions,
or require additional information, please do not hesitate
to
call.
Very truly yours,

A.J Giannuzzi, Ph.D, P.E.


As ociate

/mc
enclosures

01

STRUT URAL
ENTEGRI .
Page 5
S. Burkhalter May 19, 1989
AJG-89-031

References
1. Cases of the ASME Boiler and Pressure Vessel
N-432, Repair Welding Using Automatic Code, Case
or
Tungsten Welding (GTAW) Temperbead Technique, Machine Gas
Section XI,
Division 1, February 20, 1986.
2. EPRI Report NP-3614, Repair Welding of Heavy-Section
Components in LWRs, Babcock & Wilcox Company, Steel
July, 1984.
3. Report CMS 405-89, Subject: Microhardness Testing
Welds Involved in Temper Bead Pass Welding, of Various
Consulting
Metallurgical Services, Inc., April 27, 1989.
4. Procedure Qualification Record A03N432, Welding Services
Inc.
5. ASME Boiler and Pressure Vessel Code, Section
XI, 1980
Edition Including All Addenda Through Winter,
1981.
6. Report AO-0394, Applied Technical Services,
Inc., Inspection
and Metallurgical Test Reports, Purchase Order
No. 207593,
May 9, 1989.

IRTEGRTY
ASSOOIATEh flr
TABLE 1
P-6 Weld Process Microhardness Results

Distance B C
Inches A
Filars KIIN Filars KHN 0'C Filars K Filars KHN500
-500 H N500 3 -50

268 338 282 336 __286 338 282


.002 347
309 333 291
335 287 321 313 -
333
.004 323

393 309 322 312


345 271 331 294 323__ _-+-
.012
321 313 322 312
329 297 330 296.
.020 I * T
334 289
322 312 313 330
333 291
I
334 28
.028
329 298 309 338 348 -266 __ _ _ _ _ _ _

336 286
.036
302 318 319 350 263
338 282 327
.044
284 322 312 342 276
335 287 337
.052 1 1
282 320 315 342 276
346 269 338 ~ I
.060 320 1
298
338 282
350 263 340 279 --29
.076 329~ 298__ _ _

R7
356 254 318 319
.084 33 287I-.I

OU -viA 2q6
354
.108 352 2 60 1 25 330' 296-~ J

Highest KHN 5 0 0 Rc (cony.)

A-297 28.9

B-319 .31.1

C-338 33.5

D-312 30.0
TABLE 2

Microhardness Results on Single Bead Weld


Using P-6 Welding Process

Distance from Filars KHN 500 Filars KHN 5 0 0 Filars KHN 500
fusion

0.005" 255 495

0.015'" 257 486


0.025" 255 495

0.045" 248 525

0.065" 252 508

0.085" 254 500

0. 105" 254 500

High Hardness
A - KHN 5^ Rc (cony.)
525 49.0
I I'

ATTACHMENT I

SUMMARY OF WELD METAL, HAZ


AND BASE METAL CHARPY V-NOTCH
TOUGHNESS TEST RESULTS

Attacment to AJG-89-031
APPLIED TECHNICAL SERVICES, INC..
MARIETTA, GA.

FRef. H0-0516
METALLURGICAL TEST REPORT
D~ate may 11, 1989 Page 4ofo
PURCHASE ORDER # 2079.53

Welding Services, Inc. MATERIAL: SA 302


3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter

Metallurgical Test Procedure


Hardness -- Specifications: Tested in accordance
Case Depth Etion with ASN BPVC Sec
III; NB-2331 and
Impact Charpy,v -Notch
ASME BPVC Section IX;
Coating Thickness '- QW-171 35 mils lateral
Coating Weight expansion and 50 ft-lb
[l minimum.
Bend Test El Ref. Case Code N-432
Other_ ...

Metallurgical Test Results


IbADT I I l'llP . -+Iq'
.. .
rA ' M0111lr-.lI lidAI gI QUANTITY RESULTS REMARKS
1 1 RESULTS 9* REMARKS
Weld Metal .3 1: 63 ft-lb Tcv: 40°F
63 mils lat. exp.
40% shear

2: 105 ft-lb 0
RTNDT = Tcv -60 F
69 mils lat. exp.
70% shear

3: 80 ft-lb RTNDT: - 20*F


62 mils lat. exp.
60% shear

A.t1-S6 - - _____________________________ I _______________________________________

Witnessed by
Prepared by: w- W. Armistead
/ .P .,I ..t ,'.L . Test Engineer
Approved by: 9. Dunning
l~l'lmlt
l~q =l=L='w'=t
m ww P m= " ) Manager
='=- 'W,%-- ... .
APPLIED TECHNICAL SERVICES, INC. MARIETTA, GA.

METALLURGICAL TEST REPORT


Ref. HO-0516 Date May 11, 1989 Page 5 of 10
PURCHASE ORDER # 207953

F Welding Services, Inc. MATERIAL: SA 302


3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter _

Metallurgical Test Procedure


Hardness LI Specifications: Tested in accordance
Case Depth with ASME BPVC Sec
tion III; NB-2331 and
Impact Charpy, V-Notch [] ASME BPVC Section IX;
Coating Thickness II QW-171
Ref. Case Code N-432
Coating Weight L] Absorbed energy and lateral expansion
Bend Test 0I equal to or greater than base metal
Other------- F-- at .TNDT + 60*F of base metal

Metallurgical Test Results


PART IDENTIFICATION QUANTITY RESULTS REMARKS
Heat Affected 3 1. 46 ft-lb Tcv = 90°F
Zone 39. mils lat. exp.
20% shear TNDT = 30°F (base metal
drop test)
2. 51 ft-lb
46 mils lat. exp. 29 mils lateral expansion
20% shear and 28 ft-lb average for
base metal at Tvc = 90 *F

3. 35 ft-lb
32 mils lat. exp.
20% shear

A-11-88

Witnessed by
Prepared by: ° ". W. Armistead
Test Engineer
Noty
Approved by: R. W. Dunning
MYCommission Exuires Jan. 29, 1992 Manager
APPLIED TECHNICAL SERVICES, INC.
APPLIED TECHNICAL SERVICES, INC. MARIETTA, GA.
METALLURGICAL TEST REPORT
Ref. HO-0516 Date May 11, 1989 Page 8 of 10
PURCHASE ORDER # 207953

Welding Services, Inc. MATERIAL: SA 302


3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter

Metallurgical Test Procedure


Hardness El Specifications: Tested in ac.cordance
Case Depth [- with ASME BPVC Sec
tion III;
Impact~harpy, V-Notch Fx1 ASME BPVC NB-2331 and
Section IX;
Coating Thickness E3 QW-171 35 mils
Coating Weight M] lateral expansion
and 50 ft-lb minimum
Bend Test El Ref. Case Code N-432
Other El

Metallurgical Test Results


PART IDENTIFICATION QUANTITY RESULTS -REMARKS

Base Metal 3 'i: 27 -ft-lb Tcv: 90*F


28 mils lat. exp.
10% shear

2:31 ft-lb TNDT: 30OF


28 mils lat. exp.
10% shear
;3: 39 ft-15
37 mils lat. exp.
10% shear

A-Il-OS

Witnessed by
/C -\ z
Prepared by: 7k a- M W. Armistead ,ir
. j A
.... "fi
t
Approved Apprvedby:
by: 9-- Test Engineer
R.-W. Dunning
II
* Manager
6-G:. TUE 1z. :9 AFFL IEt TECH SE .. ICE P . 0

APPLIED TECHNICAL SERVICES, INC.


MARIETTA, GA.
METALLURGICAL TEST REPORT
R~ef. H0-0516-2 Date May 15, 1989 Page 1 of I
PURCHASE ORDER # 207953

Welding Services, Inc.


h;,ArE-,AL- SA 302
3276 Marjan Drive
Atlanta, Georgia 30340 Grade B
PQR No: A03N412
Attention: Steve Burkhalter

Metallurgical Test Procedure


Hardness U Specifications: Tested .i.p .a.ccioird_ njce
Case Depth 1-1 with ASME BPVC Sec
tion III; NB-2331 and
Impact cvtrpy, V-_\.Otch [ ASME BPVC Section IX;
Coating Thickness E. QW-171
Coating Weight 0 Absorbed energy andRef. Case Code F-432
lateral expansion
Bend Test j equal to or greater than base metal
Other- at TNDT + 60'F of base metal

Metallurgical Test Results


PART IDENTIFICATION CUANTITY RESULTS REMARKS
Heat Affected 3 1: 61 ft-lb
Zone
Tcv 120'F
45 mils lat. exp.
50% shear

2: 52 ft-lb
47 ml1s lat. exp.1
50% shear

3: 49 ft-lb
45 mils lat.
50% Shear

A-I 161

Witnessed by.

Prepared by: M.M W Armistead


APPLIED TECHNICAL SERVICES, INC.
-- - --.

METALLURGICAL TEST REPORT


Ref. HO-0516 Date may 11, 1989 Page 9 of 10
PURCHASE ORDER # 207953

Welding Services, Inc. MATERIAL: SA 302


3276 Marjan Drive Grade B
Atlanta, Georgia 30340 PQR No: A03N432

L Attention: Steve Burkhalter

Metallurgical Test Procedure


Hardness
Li Specifications: Tested in accordance
Case Depth with ASME BPVC Sec
tion III; NB-2331 and
Impact
ASME BPVC Section IX;
Coating Thickness E QW-171 35 mils
Coating Weight El lateral expansion and
50 ft-lb minimum.
Bend Test Ml Ref. Case Code N-432
Other- -. -

Metallurgical Test Results


PART IDENTIFICATION -GUANTITY RESULTS REMARKS
V --
aJs Metal D1: 39 ft-lb Tcv: 120°F
36 mils lat. exp.
20% shear

D2: 27 ft-lb
27 mils lat. exp.
30% shear

D3: 34 ft-lb
34 mils lat. exp.
30% shear

A-Il-Se

Witnessed by
Z''111,00Enfi.
t A. zn 2..PJ Prepared by:
-
- 00 M W. Arstead
Test Engineer
Approved by: - . R. W. Dunning
Manager
APPLIED TECHNICAL SERVICES. IUnr_
Dr. Anthony J. Giannuzzi, P. E.
Associate
Education

BS, Physics, LeMoyne College (1964)


MS, Solid State Science and Technology, Syracuse University (1967)
PhD, Solid State Science and Technology, Syracuse University (1969)

Professional Associations

Professional Corrosion Engineer, State of California

Professional Experience
1983 to present Structural Integrity Associates, San Jose, CA
Vice President
1979 to 1983 Electric Power Research Institute, Palo Alto, CA
Project Manager
1978 to 1979 NUTECH, San Jose, CA
Project Manager
1972 to 1978 General Electric Company, San Jose, CA
Principal Engineer
1969 to 1972 Aerojet Nuclear Systems Company,
Sacramento, CA
Summary
Dr. Giannuzzi has been involved in solving materials and corrosion problems for the
nuclear industry since 1969. One of the world's leading authorities on intergranular stress
corrosion cracking of stainless steel in aqueous systems, Dr. Giannuzzi was employed by the
Electric Power Research Institute in the Nuclear Systems and Materials Department for
three and one-half years prior to joining Structural Integrity Associates in 1983. At EPRI,
Dr. Giannuzzi was task leader and principal investigator involved in development and
qualification of all the Boiling Water Reactor IGSCC piping remedies. This activity
included primary responsibility for qualifying and producing material specification for the
alternative materials (Types 316NG and 304NG stainless steels), qualifying the induction
heating stress improvement (IHSI) remedy, qualifying heat sink welding, last pass heat
sink welding and the weld overlay and performing the investigations to determine the
causes of and remedies to IGSCC in Type 304 stainless steel pipe.
In addition to his BWR IGSCC responsibility at EPRI, Dr. Giannuzzi has had the lead
responsibility for investigating the causes of low pressure large steam turbine stress
corrosion cracking in nuclear and fossil steam turbines and has been involved in projects
associated with bolt and fastener reliability, steam and water piping erosion-corrosion and
has been active in projects related to primary and secondary side corrosion of steam
generators. Dr. Giannuzzi has also been the lead project manager responsible for all
-materials related failure analysis activities in the Nuclear Systems and Materials
Department and was a member of.the EPRI Three Mile Island Unit 2 task force.

*~2:STHUCTRAL
'- . '

Page 2
A. J. Giannuzzi

Prior to his employment at EPRI, Dr. Giannuzzi was employed as a senior consultant at
NUTECH. While at NUTECH, he formed the stress corrosion cracking group and
developed the methodology used to estimate likely locations of IGSCC in stainless steel
piping systems. He also was involved in the earliest investigations involving PWR boric
acid corrosion and assisted in the final formulation of the NRC I-E Bulletin 79-02 which
established criteria for inspection of the boric acid system piping.

From 1972 to 1978, Dr. Giannuzzi worked as a principal development engineer at the
General Electric Company Nuclear .Energy Division. His responsibilities while at GE
involved investigation of alternative materials and processes to alleviate the IGSCC
problem in stainless steel piping. He managed the initial weld residual stress measurement
and analyses activities which lead to the development of the residual stress remedies to
IGSCC.
From 1969 to 1972, Dr. Giannuzzi worked for the Aerojet Nuclear Systems Company
developing materials for use in the nuclear rocket engine (NERVA).
In 1983, Dr. Giannuzzi founded Structural Integrity Associates with Dr. P. C. Riccardella
and Dr. T. L. Gerber. His activities at Structural Integrity have included nuclear plant life
extension studies, temper bead weldinig development on low alloy steels and selecting of
remedies to IGSCC in BWRs.

~INTEGM~Y
ASSOCIAEZ R\C
R"ese ch; Sponsored by the Welding Research Council
of the Engineering Foundation

'PLEMENT TO THE WELDING JOURNAL. OCTOBER 1962

1962 ADAMS LECTURE


lization of Quenching and Tempering for
,)rovement in Properties of Low Alloy Steels in Heavy
cknesses for Welded Construction
Successful welded construction with low alloy steels
in heavy thicknesses requires closer control of tech
niques and procedures than those generally required
for annealed and normalized and tempered material
:. E. LOR ENTZ. J R.

ager-Metallurgical Research and several significant articles to the'


Development. technical literature, the last being
The affiliations of Mr. L.orentz "The Eddystone Story" which he
include membership in the AMER co-authored with E. C. Chapman
CAN WELDING SOCIETY, the Ameri and which was in the ASME trans
can Society for Metals, the Ameri actions.
can Society for Testing Materials as
well as the Chattanooga Engineers FOREWORD. I wish to expres my
Club. He has held the position of appreciation to the officers and mem
chairman as well as other offices in bers of the AMEJUCAN WELDING SOCI
E'Ty in being invited t) present this. the
local sections of AWS and ASM. 20th Adams Lecture. I appreciated
He is the Past Southeastern District the friendship and high principles of
Representative of AWS and was a Comfort A. Adams over a period of
member of the National Nominat several years. His enthusiasm and
ing Committee of AWS for 1956- interest in the SO(:IET-Y were ntt..sted io
1957 as well as 1961-1962. by his regular atlendance at thv techni.
Lorentz. .,.. was born 46 Mr. Lorentz is presently a mem cal sessions (usually in the front row
ago in Champaign. Ill. Fol ber of several technical committees. and participation in the dLscussions.
, his early schooling in Illinois These in'lude the ASME Sulwom In those earlier year,. it was posqible ti
tended the University of Illi attend all of Ihe s.esSions.
mit tee on Welding, ASTM Com
-here he received a Bachelor of mittee-7 on Nondestructive Testing, Introduction
.p degree in Metallurgical En the WRC High Alloys Committee., This broad subject is one which is
ing in 1939. A year later he the 1'VRC Pressure Vessel Fabrica receiving increasing attention. The
ed .' masters degree in science tion Committee, the AWS Com Pressure Vessel Research Commit
-Metallurgical Engineering mittee on Standard Qualification tee of the Welding Research Council
*high University and immedi Procedures, and the ANVS Com foresaw the need many years ago
ioined Combustion Engineer mittee for Section IV Chapter 75 of for basic study in this field and has
ic.. where he has since been the WELDING HANDBOOK 'Clad sponsored University research which
here he is now District Man- Steels). He has also contributed has been the forerunner of industrial
.A
WELDING RESEARCH SUPPLEMENT I 433I-s

~ i .-.. -
'- .-
" ' 1'.:3
*Z
m

~I.

RELATIVE CALCULATED specifications in the American


HARDENABILITY
ciety for Testing Materials and
PER
development of fabrication saf
GROSSMAN CRITERIA rules in the American Society
Mechanical Engineers. Ioth gro
MIN. MAX : have set up committees study
various aspects.
- SPECIFIC ANALYSES
Present Usage
High strength quenched and tE
10- pered plates up to 2'.. in. maximi
thickness are presently recogni:
by the ASME Boiler and Pressi
Vessel Code in its Case Nos. 12

f
1297 and 1298. This recognitior
limited to particular chemical an
2 - 21".
2'

2129 2258
32
3028
" ., ' "
yses of material and is predicai
on the material exhibiting maxin-i
1204P !297 1204 Ni-C-Mo and minimum required tensile pr,
299 2030 3878 1298P 387D 1298
PROPOSED LOWER ALLOY MODIFICATIONS TO ASME
erties throughout its thickness.
CODE CASES
Fig. 1-Hardness ranges calculated from chemical analyses is also predicated upon the mater
of several pressure vessel steels being heat treated by the matei
manufacturer. In addition, 1
development. The work of Profes fabricator is required to limit a
temper embrittlement has been
sor Stout and his colleagues at Lehigh pertinent.l,-,r Pertinent informa forming and stress relieving heat
University has been and is continu tion on the subject has been pre
ing to be particularly progres to a temperature below the n
sented in previous Adams Lec tempering temperature. Other li
sive.1 -10 The continuing work of tures.: "I Many others have also
W. S. Pellini and his colleagues at its are also assigned.
contribuntt.d "-'-1,; to the extent that The ASME Code also presen
the United States Naval Research the subject is now receiving broad
Laboratory in illuminating con recognizes use of "accelerated cc
study aimed toward the develop ing" in several case numbers (12
ditions affecting brittle f-acture and ment of base material purchase 1241, 1243, 1255, etc. applied

Table 1--Chemical Analysis and Multiplying Factors for


Determining Hardenability
A212B A299 A225B APfRr) ll:
Min Max 302B 1204 P A
Min Max Min Max Min Max Min Max
C iax Mur Max
0.15 0.35 0.15 0.31 0.10 0.20 0.10 0.20 0.15 0.25 0
Factor 0.14 0.22 t; p 0.1;
0.15 0.20 0.13 0.17 0.13 - 0.17 0.15 0.19 0 .23
.18 :; 0.If
Mn 0.60 0.90 0.86 1.45 0.90 1.45 0.60 0.90 1.10 1.55 1 .05 0.6!.
Factor 3.5 4.5 4.5 0.36
6.8 4.5 7.0 3.5 4.5 5.5 7.3 55.1 2.5 3.9
P 0.010 0.035 0.01 0.035 0.01 0.035 0.01 0.035 0.01 0.035 0 .035
Factor 1.03 1.1
0.01 0.0"
1.03 1.1 1.03 1.1 1.03 1.1 1.03 '1
1.1 .1 1.03 1.1
S 0.01 0.04 0.01 0.04 0.01 0.ko 0.01 0.04 0.01 0.04 0 .04 0.01
Factor 0.96 0.99 0.01
0.96 0.99 0.96 0.,w 0.96 0.99 0.96 0.99 0 .99 0.96 0.9
SI 0.13 0.33 0.13 0.33 0.13 0.32 0.13 0.32 0.13 0.32 0 .37
Factor 1.08 1.25
0.13 0.3;
1.08 1.25 1.08 1.25 1.08 1.25 1.08 1.25 1 .27 1.08 1.2!
Ni ... ... ... .. ... 3.18 3.82
Factor ... ... 2.8 3.8
Cr ...
Factor
... ... ... ... ... ... ... 0.36 0 .69 0.74 1.2
... ... 2.0 2 .95 3.15 4.7
Mo
0.41 0.64 0.12 0 .28 0.40 0.7
Factor
2.25 2.90 1.38 1.85 2.2 3.2
V ... ... ... ... 0.07 0.16 ... ... ... 0.02 0.09
Factor ... ... . ... ..
... 1.35
1:3
1.40 ... ... 1.25 ...
Ti ... ... ... ... ... ... ...
... ... 0.01 0.03
Factor
... 1.05 1.08 ...
Zr
Factor
Cu
...
°.. ... .... ... ... ... °. ... ... ... °. ... ... °
... ... ... ...
Factor ... ... ... ... ... ... . o . °

B ..... .. ... ... ... ... ... ... ... 0.0005 0.005 ...
Factor ... ... ... ... ... ... ... ... ... ... 1.02 1.48 ...
Harden
ability 0.58 1.28 0.74 1.85 0.85 2.27 1.36 3.96 1.98 5.48 1.72 14.4 2.13 12.1
4 4
3 -s I OCTOBER 1962
-igher .nsile properties which may , ,u ,IIU;e structures exhibiting these quenched" and tempered condition
esult. This approach is limited to properties has awaited developments
which would exhibit improved me
in procedures for welding and in
iata&riaJFiof reLatixvi'y low hardena chanical properties. Some of these
procedures of control for assurance
,ility. materials would exhibit this im
Quenclk-d and tempered steels of
of required properties. ASME Code provement throughout thicknesses
eavier thieknewes than 2' 2 in. approval of the quenched and tem
heavier than 2';: in. Most would
.ave been used t,, fabricaite "non pered materials to limited thick. exhibit variation in properties from
,ode" type pr-4%ure -,gels for nesses was 'given only after exten center of thickness to surface. What
mbient and low t'mper:ature ser sive testing was performed, in are the maximum thicknesses which
ice. Large Cylitdrical pressure volving not only tests of welded would exhibit improved properties
easels of thi-. t-yjl up t. approxi samples but also tests to destruction throughout their thickness? What
lately 4 in .,nd I'..vier thickness, of relatively large vessels. Service variations are exhibited? Is it pos
f single tlii knem material; have experience of these materials has sible to utilize any improved tensile
een built to ,tllow:,ile slrlt; values now been obtained with pressure properties in design?
f up to ' : the yielil stretirth. vetisel and structural applications. There is a present need for large
Large tonniges of quenched and Lower alloy modifications of the diameter vessels of an operating
mpwred st&44 hay, be(, used for materials have been proposed for pressure which requires thickness of
ressur, vea.i and :tructur"I appli. use for the thinner thicknesses, heat plates of present ASME Code ma
itions.:: .11 .arg. tonn~iges have
treated to the same strength levels, terials heavier than the capabilities
caen used I,. marine applications to allow use of more economical of mills to produce iwith sufficient
-quiring bih lihili strength and materials. Conversely, the original degree of hot working; but which
(celitionallv high notch toughness. alloy range has been proposed for may be produced in usable thick
hese have 64m built to Govern usage at thicknesses greater than neses and sizes with quenched and
,ent material .,nd fabrication speci 2' 7 in. Requests for ASME Code tempered materials. Although sat
:ations.3: -X. approval of other low alloy steels up isfying this need is not entirely lim
to various thickness levels have been ited by economics, the wider use of
ossible Future Usage made. quencied and tempered materials
The properlies available through Several of the ASME Code ma may allow more economical finished
terials presently used in the normal- products for other needs through

I
Ible 1 lContinu*,41
1298P' 1297,2 1204-9 A387D 1298-2 Ni-Cr.Mo
Min Max Mm Max Min Max Min Max Mm Max Min Max
0.11 0.22 0.13 0.22 0.08 0.22 0.08 0.15 0.10 0.22 0.10 0.23
0.125 0.17. 0.14 0.17 0.10 0.17 0.10 0.15 0.12 0.17 0.13 0.175
0.36 0.74 0.75 1.15 0.55 1.05 2.07 0.63 0.36 . 0.74 0.10 0.40
2.5 4. C 4.0 5.7 3.0 5.1 2.0 3.7 2.5 4.0 1.3 2.3
0.01 0.01 0.035 0.01 0.035 0.0i 0.035 0.01 0.035 0.01 0.035
1.03 1.1 1.03 1.1 1.03 1.1 1.03 1.1 1.03 1.1 1.03 1.1
0.01 0.0" 0.01 0.04 0.01 0.04 0.01 0.035 0.01 0.04
0.96 0.01 0.04
0.96 0.99 0.96 0.99 0.96 0.99 0.96 0.99 0.96 0.99
0.18 ,.37 0.44 0.86 0.13 0.37 0.15 0.50 0.18 0.37 0.15 0.35
1.12 .27 1.3 1.6 1.08 1.27 1.1 1.35 1.12 1.27 1.08 1.28
0.67 1.03 2.0 3.25
1.2 1.35 1.8 2.8
0.79 0 4- 0.84 0.36 0.69 1.88 2.62 1.34 2.06 0.90 1.85
3.2 3.35 2.0 2.95 6.3
2 8.4 4.8 6.8 3.5 6.3
0.12 .1 10.31 0.36 0.64 0.85 1.15 0.36 0.64 0.23 0.60
1.35 ;.90 2.05 3.0 3.6 4.6 2.05 3.0 1.6 2.8
0.02 0.09 .... 0.03
1.25 1.3
(1 03
... 1.35
0.03 0.11 •... 0.02
1 08
1.08 1.1 1.05
04 0.16

L: 7]
0.12 0.53 0.17 0.43
i 15 0.25
1.03 1.2 1.05 1.15 • . 1.]
015 C - 0.002 0.006
:tor 1.4 0. 0015 0.005
1.1 1.48 1.2
rdenabiity 4 1. 1.48
-,4 i.4 2.84 33.2 4.47
h 4.4 35.8
IM'Dr.0' "1 med,.. "1, I. .4 I,1 h.,
kSr~t f:.-"€"{' • "la.

WELDING RESEARCH SUPPLEMENT I 435-s

4
' --- I - -- . "

.3 T C

8 T100. 4
j4 32"x32

A3C2
t
Ot

L_
. L C ..

~O~f
*r
I 4ix 33'X23"
A387D7
49 '

Fig. 2-Location of thermocouples DIP 0UE'_HE


test plate to aetermine on CENTER ToCKNESS
PLATES
cooling rates
5 6 71
use of thinner and lighter INCHES FROM OUEN-MEC EDGE 3141 67
rnterials
The heavy thick ni-,; Fig. 3 -Time required to reach
are most economi(All%. -46awd material specific ti-moera~uwc: during dip quenching
pressing rather thai by ho
.,lidor warn
pressing. - 4' ; "'h. Ir,.sentlv
materials require norm., ilzing, UsecI either by the material producer or
whic I by the material fabricator. r anat.,.
can be performed eit h.. This also emphasizes in
applied to flat plate or
at the milI ditionally this has been a function
Tra. - need close analysis control the
I-rged shapeE the Arnerit'an -ociety of ini . .ln of segregation of
or at the fabricator's for Testing anal
shop. The Materials.
fabricators generally
find it more It aL , h.ls resul.ed in a ys is
economical, with hc.a-v need for re, -(r :204 and
,:,Ifle
;.,,; 1298 steels
Of meeting are
90,000
plates, to hot form duringthickness further devlpmient of codes
regu
cooling lating safe '",islruition to Ii., ik I's minimum
from the normalizlc
and to warm size -ir,',lId
temper:tur, procedures.
rules and trengti.,. a II1,,. center of the yield
size follow. [raditionally this has thick
ing hot forming in o,'der been a funclion of the tness ol 4 .i or heavier material.
to American
distortlorLQ in shape --lused remove Society of Mechanival Engineers
The 3871.) material is capable of
cooling from n,,rmali7meL by .air Boiler and Pressure Vesse'l meeting I(0(, I. : minimum yield
Applica Code and strength
tion of this procedur,. various Government agencies. at th. I.... ,ofthe thick
t..:I quenched All ness of 6 in. or t... '.r
and tempered produ, of these groups are active rnaterial.4
fabricated in this The relativt
from thick plate requires subject. .. -- bility -data
fabricatorapply the quench
that the Development of high shown in Fig. -... - 4ulin estim
and tem strength ating depth ofh .t
per either to the formed weld metal deposits has ,,.. :',z capabilities
parts kept pace
welding or to the finished prior to with quenched and tempered for material .,., rhich
after welding. Both procedures vessel metal development.,
base cooled rpitdl.. ,'eiugh tocanallow be
may What re transfo,r,,.'
be applicable dependent mains to be done for heavy ., ol all or a portion of
upon the thick the mat,?-:.. I o martensite or
finished product. nesses is to determine bainite.
properties
Both procedures, however. which ar' a-vatable and possible, I-ea''. It .nesses of some materials
re determin,, limits of controls to cann,, In.cooled sufficiently
quire close control of 1
ables of the quenching
all the vari sary for n.suranre of these
neces to all,,% .tuc'h transformation.rapidly
process to ties, and to polie purchase proper tranr,!,rn:,-tion characteristics The
the same extent as those and of
the material producer
applied by fabrication such that these each "ut4+rial and the practical
at are ob coolin, ',Les possible for the
For some designs, it may his mill. tained. mate
tageous to apply quenching
be advan rial , regulate the degree of
to .Hardenability hardi.wtilit% which can be real
shapes prior to joining
welding than to apply them by ized..
quenching /7 An approximation of the depth of
a completed vessel. Distortion to hardening capabilities of various Design
due ImateriaLs can be obtained from
to heat treatment of shapes the
removed by cold or warm can be %workof M. A. Gro.ssmann.: Presently approved ASME
shaping. range of minimum and The quenched and tempered materials,
In either case, the weld maximum
metal must hardenability calculated as other Code materials, are assigned
he specifically tailored frrn the
for the ap range an allowable maximum design stress
plicable heat treatment of chemical analysis of *veral
ing only or quench of temper presently used and proposvd of i/,of their minimum ultimate
and type tensile strength to a specified
Also in either case, the temper. pressure vessel steels is
shown in tem
properties must also be required Fig. 1. The chemical analyses perature limit. Where allowable
met in the multiplying factors used and stresses are assigned above
heat-affected zone.
This sequence of events calculations are given in
in these limit, they are progressively this
has Table 1 of creased dependent upon criteria de
sulted in a need for development re the 'Appendix.
material procurement specifications of It appears obvious that based upon yield strength,
utiliza stress
specifically designed for tion of the higher hardenability rupture strength or creep strength
and tempered steels,
quenched steels to their ieaviest at each temperature.
heat treated capable The high strength quenclicd
thickness requires close and
control of tempered plate materials
4 approved
36-s I OCTOBER 1962
NN ~ 212 B 67 X6T DIP OUENCH FROM
0 ' 302e £ " 6 "T GE 1750*r.
20o T ' INlNITELY LAP
21 28 6T X76
AT CENTER THICKNESS
!287t 6'!.X 6
'A' - THICKNESS
10 "" " " " sI "
U -- THICKNESS
X NORMAL.IZI *.
' ...
5 i2

72 6 CS 24?T24T I RATIO
AVERAGE -F. PEP .ECON: .O LINW I IS
I~ 1714 1I 27.10 9
- 1". ZeF.
*,t 43 14 13 I1 25 1
10 AVERAGE* PER MINUTE COOLING RATE TO 825-r

Fig. 4-Cooling rates fur dip ul;ench and ........ -


normalized test pieces
Fig. 5-Cooling rate vs. ratio of surface
area to volume
by the ASME (:ode .- )ri"iItly
.assigned a maximLiiII
heat transfer conditions, vessel con
alI'wab.e and spray quenching cooling rates.
stress up to 2 in. t.hick,, s of ne,-tion requirements and practical
ity of nondestructive testing require Cooling rates obtained by dip
28,750 psi at minus 2(1 t,plu. -..0' F quenching of plates in agitated
and progressively les up te. '650 F ments. For many constructions, a
water and comparable cooling rates
at which the allowable Piress is single thickness material is required.
obtained by normalizing have been
limited to 25,000 psi. livlween 2 This requires a material capable. of investigated. This has been done
and 21'in. the alhet-.bh. '41ress is meeting minimum design strength
26 2 with various sizes and thicknesses
, 50 psi at minus eo1 to pIu- 150, F at the center of the thickness of the
of plates with thermocouples placed
and decrease.s to 22,80 1 psi at quenched and tempered single thick
at the center of the thicknesw and at
6500 F. ness material.
the' , thickness level at various
New design criteria, which con locations in the plates. These lo
Bider yield strength as well as Cooling Rate
cations varied from the center of the
tensile strength and which addition The means available for cooling width and length to near the edges
ally consider su perimlosed service from the auListenitizing temperature of the plates as indicated in photo
stresses such as thermagl stresses and consist of air cooling, oil quenching graph of Fig. 2.
low cycle fatigue and more rigor and water or brine quenching. The Figure 3 shows the time required
ously define allowshle design de quenchini can be acomplished by to reach a specific temperature
tails, are about to be lresented in a either a spray or by dipping in the during dip quenching at various
new ASME Code stction. This quenching medium. Dip quenching distanms from the quenched edge
section also more rigorously defines should be (lone in a medium which is for two heavy thicknesses of a range
destructive and nondestructive test agitated to avoid vapor blanketing. of thicknesses tested. This time
ing. With this approaclI. higher de Agitation can be accomplished by becomes uniform ata distan
sign stresses are to be allowed for circulation of the medium by pump rom
the quenched edgeof---ap proxji
specified materials and temlperature ing or by agitation with air. 1
Literature data is available con
'rr elvz_ t gthe _plate_ thick
limits. ..et. A test plate size of width and
The designer wisht.,, to -,lect tl. cerning cooling rates of various
shapes and sizes of samples sub length of three times the plate
least expensive steel ,a ,,,I. of thickness would exhibit a cooling
consistently meeting tie higlu-t d,- ject.ed to cooling in still air and rate at the center of its width, length
sign properties at the maximum various quenching methods:... and thickness approximating that
thicknet-s required iii ht design. The pertinent variables involved of a larger production-size plate.
The maximur \ in slprav and dip quenching are: A specimen of larger size than.2TY
individual ;elate
thickness in tll. design, among other 1. Austenitizing temperature and 3 would required, hoever, if
factors, ma* be dependent upon I ,me. any appreciabl.e volume of metal is
A'hether the d..sign is baseto on u4 \ 2. 'rime from furnace to start of required for re s.entatet ng
)f a single tlbikne&s mater:.d or a quench and temperature at start of samles. ''his is also dependent
nultilayer thickness mal,.ri;, The qiench. upon the hardenability characteris
atter. where it is allowed !,v " \.- 3. Surface condition tics of the material.
of the metal
.onstruc-tion code, will all,,% ..it! . r
degree of scale:. Figure 4 shows cooling rate data
he selection of a thin thirki, -,, I..;t \. 1.Volume of spray per unit time from 1750 to 825' F for both dip
o ?"" !TI
iigh strength J r unit area per side
and quenthed and normalized test
for dip
.he selection of economical
a more.exll'ns:.
in. -.!
... * ai'lli'ation the ratio of quenching
I)iecs. The data given are for the
I, thickness level and
iigher strength thin thickie".- n. ,n..djumvolume to metal volume. at the center
,erial, or the selectior of :1 1-..1 • d. degree of agitation and of the thickness and at the center
hickness more expensiv, n: .eri.. circula of the width and length of the test
li,.i and the temperature rise
isable in fewer layers to .I) ih- of samples. The majority of the test
It. quenching medium.
equisite thickness. Th:- al... ,at ' Time of application. samples consist of carbon steel ma
.; regulated by the. rahr.ti terial and the lines are djawn
)awa directly applicable to pres
,fassemblina the ,iu;" .. ay, slecifically to the carbon steel ma
iy whether operat jig I. ,diti,.. a-,'ar.
. . ve.-el part thicknesses and terial. Tle A__.2 Grade B material
uch as to allow this t%.- cni.. ru, ;,-.A is hmit,:d. Work most directly -and the A387 Grade- ateril in
jrkinew: ha:s been performed at
ion. This can I. delb .le- ..,. general are off the curve and are
1A4..gh I niversity, on normalizing better represented on the dip q _1jich

WELDING RESEARCH SUPPLEMENT j 437-s

I ,,
Table 2-Cooling Data
o
Point M. h
thick. Width Length --
- At center of width and length,-
no. terial ness, in. in. Average *F/min. to Start Location
in. A/V Cooling 400 from in
" I
] C.S. 600 825 1000 1200
1/, 6 6 8.7 Air
"400 *F thickness .,
133 182 238 268 317 428 1750 Center
2 C.S. i/I 6 6 4.6 247 . .,T
3 C.S. 3 Air 91 118 142'
/ 6 6 3.1 Ai 156 190 270 1750 Center
59 77 92 204 12T
4 212B 1 6 6 112 194 1750 Center
2.7 Air 40 53 8T
5 212B 2 12 66 73 79 160 1750
12 2.33 Air 18 Center 67 *6,
6 212B 26 31 32 '37
3 18 18 0.89 70 1750 Center 61 xbi
Air 13 17 20
7 2128 6,' 24 21 23 37 1750 Center
24 0.50 Air 6 7.7 61 x 6
8 2128 9.2 9.6 11 17.5 1750
1 6 6 2.7 Water 1258 Center 3.87 x 3 8T
9 1188 1110 1104 1104
2128 1 6 6 2.7 1230 1750 1/4T 6T x 61
Water 1122 1116 1050
10 212B 2 12 978 1032 1164 1750
17 1.33 Water 435 Center 6T x 61
.4
467 478 459 486
11 2128B 2 12 500 1750 1/4T 6T x 6T
12 1.33 Water '35
]2
1;: 2128 460 474 450 452
3 18 18 0.89 Water 477 1750 Center 6T x 67
r 284 294 303 302 330
3 212B 3 18 18 338 1750 1/4T 6T x 67
0.89 Water 272 280 283
14 212B 61/, 24 266 260 256 1750 Center
24 0.50 Water 103 110 6T x 6T
15 212B 62, 24 118 125 13] 116 1750
24 0.50 Water 95 1/AT 3.8T x 3.87
16 387D 101 100 91 79
4:/1 23 33 0.59 77 1750 Center 3.ST x 3. ST
Water 121 139 162
17 387D 4:/, 23 33 178 184 166 1750 1/4T
0.59 Water 113 120 5.IT x 7.3T
18 302B 132 143 162 146
81/i 321/: 32',. 0.36 Water 1750 Center 5.1T x 7.3T
39 47 55 67 78
302B 8/ 321/ 321/. 0.36 79 77 1750 1/AT
Water 42 45 46 50 3.8T x 3.8T
20 387D 4'/: 23 52 47 1750 Center 3.8T x 3.8T
33 0.59 Air 6.5
21 212B 8.1 9.7 15 18
, 8 "30 4.5 21 1750 Center 5.1T x 7.3T
Air 70 91 118
22 212B B 130 150 250 1650 Center
J/. 10 3.1 Air 161
23 2128
" 2 21B 40 54 66 73 75 125 1650 1 7 a 20T
1 10 2.5 12 ]50 Center
ener 61 xx 133
10.7 13.3T
Air 31 42 52
24 2128 1/1 8 10 56 60 100 1650 Center
1.8 Air 23 31 8T x 10T
25 2128 41 41 40 71 1650
1 30 30 2.13 Water Center 53T x 6.77
26 1127 1080 894 804
387D 1/, 9 9 1.78 798 810 1750 Center
Water 900 990 1176 30T x 307
27 3028 2-/, 15 1320 1176 954 1750 Center
15 1.16 Water 368 6 x 6T
28 387D 379 388 443 432
,: 8 10 4.45 .408 1750 Center 6 x 67
Air 54 70 83
29 387D 2/4 8 167 220 232 1750 Center
10 3.12 Air 38 51 16 x 20T
30 387D 1 59 116 157 175 1750 10
8 10 2.45 Air Center .7 x 13.3T
31 387D 28 34 34 68
p/! 8 10 1.78 85 100 1750 Center
Air 22 28 8 x 107
32 302B i/ 31 53 73 88 1750
33 302B 8
8 10 4.45 Air 58 Center 5.3 x 6.7T
3/4 10 3.12 Air 35 75 97 163 225
48 59 93 150 250 1650 Center 16 x 20T
167 1650 Center 10.7 x 13.3T
34 3028 1 8 10 2.45 Air 28 36
35 302B li/? 44 65 112 125 1650
8 10 1.78 Air 20
Center 8 x 0T
36 387B 26 32 43 69
1/1 8 10 4.45 Air 83 1650 Center 5.3T x 6.77
59.5 78 103 130
37 387B 3/, 8 10 150 250 1650 Center 16 x 20T
3.12 Air 41.5 54
38 387B 1 69 87 98 125 1650
8 10 2.45 Air Center 10.7 x 13.3T
31 42 50 63
39 1204 '/: 8 10 69 100 1650 Center 8 x 0T
4.45 Air 57 73
40 1204 100 188 250 380 1700
3/, 8 10 3.12 Air 44 Center 16 " 20T
4! 1204 55 71 118 165
1 8 10 2.45 234 1700 Center 10.7 x 13.3T
Air 32 44 53
42 1204 1I/1 8 10 76 128 146 1700 Center
1.78 Air 22 29 37 8 aIT
43 387D 71/i. 241/, 50 81 100 1700 Center
48s/8 0.405 Water 47 5.3 x 6.7T
49 51 54 1750 1/4T 3.4 x6
a 6.8?

i TablePoint
3-Material Check Analyses, %

numbers Material Si S P Mn C
,,C.S. Cr Ni Mo Cu
0.05 0.019 V
0.009 0.40 0.059
2 ... ... ...
C.S. 0.06 0.020 0.011 0.47 0.176 ... ... ... .. ......
3 C.S. 0.07 0.019 0.017 0.47 0.210 ... ...
4,8.9 ......
212B 0.20 0.021 0.016 0.72 0.298 ... ... "
5 10. 1] 212B 0.25 0.019 0.020 0.80 0.290 ... ... ... ... ... ...
6,12. 132128B 0.24 0.020
7, 14, 15 212B
0.003 0.79 0.281 ...
0.20 0.019 0.009 0.74 0.279
... ... .. ....
... ... ...
16, 17, 20 387D 0.28 0.029 0.014 0.53 0.13 2.40
18, 19 302B 0.21 0.023 0.017 1.57
... 0.98
1.5 0.256
0.256. ... 0. ..
21, 22, 23, 24 2128
... 0.50 ... ...... .
0.20 0.017 0.012 0.82 0.29
25 ... ... "..
2128 0.23 0.017 0.027 0.86 0.26 Nil ... Nil ..
26, 28. 29, 30. 31 387D 0.22 0.021 0.011 0.50 0.146 2.29
27 ... 0.98 ... ...
3028 0.20 0.025 0.041 1.20 0.23 ... ... 0.50 ...
.32. 33, 34, 35 302B 0.19 0.025
...
0.036 1.21 0.23 ...
36 37,38 ... 0.52
3878 0.25 0.023 0.011 0.50
39, 40. 41, 42 0.143 0.94 ... 0.47
1204 0.21 0.023 0.016 0.82 0.18 0.48 0.89 0.48 0.31
%; 43 387D 0.23 0.051 0.002/0.006
0.0.1 0.009 0.43 0.135 2.12 .. . .. ...

4
38.s j OCTOBER 1962
a fasterliverage rate th-,n the carlbr
steel material at t -l"tninh ner
a .d-at-a--Slower-ag -uragatp
at the
heavy .thicknets. 50 - 50
The size of the amnple with rela
tion to its thickne.im also may be DIP OUENCH IN
important with respect to cooling AGITATED WATER
rate. The snme data, therefore.
were plotted a diffiront wav. in
which the cooling rat- was pl,)tt.l
Vs. the ratio of surface aren to Vol
ume. This is shown in Fig. 5,. h'lis
figure shows the variati, of ratio in
area to volume of a -17'x 47'. a 67' x 0 50
6T, and an infinitely large plate .is 00

it varies with thicknr.s, o! plaic.


VOLUME RATIO ATER
Point 9 is the crenter of th,. thi,.k,.,.w,
of a 6 x 6 x 1 in. test sanilpe iv vun, a STEEL
ratio of area to volume ,I _".7.
Point 25 L also a I in. 'plat- ,-ut ,t
30 x 30 in. having a rtio of .,r, :, i.,
100O00
volume of 2.13. Th,. i-,oiij r.ite is 50C
Fig. 6 -Temperature rates of water vs. volume rate of water
lesser, and it is belived that the to steel
amount lea- ib limit.d to within the
degree shown on tile chart.
The data from which the Figi,.
4 and 5 were obLained, ani fiurtlivr
data for cooling to other I .chr and
lower temperntur.s of ?tie typ '
shown in Fizs. 4 and 5 are given in
Tables 2 and 3 and Figs. 17 through
31 of the Appendix.
Tile temp:erature rise ,,f wster ob
tained on dip quen-hiing of ,,,urse,
is dependent upin the relative
volume of steel and water, degree of
circulation and many other vari
ables. The data of rise in tem.ra
ture as atually obt-,i:,d on the
specific test samples art shown in
Fig. 6. The actual cooling curves
of temperature vs. tim* obtained
with the various test samples are
shown in the Api'undix, and -oie
are plotted superiinix)sed on '',n
tinuous cooling or isothermal tem
perature-time'ransformati, m curves 400
10 2
for several materiaL di..us.sed I* 0 10 105

low. TIME-SECONDS
Fig. 7-Cooling rate data superimposed
on carbon-steel isothermal
transformation data
Temperature.Time
Transformation
When the. c,,,linz rate ,roted that transformation takes
'if I,, pa-' provement in properties, but the
titular thicknes and size if fl;,,er..-. ,tlacv only at a high temperature.
dip quenching rates of ] in. thickness
is known and whien is)t hermai rani I.itti,. imptrovement in tensile prop
.. rti,-s can result from quenching and possibly heavier thickness
.ormation data or continu, of are
)ot sufficiently rapid to realize an im
ng transformation are a, is material. The dotted cooling
. urv,.s rcl)resent actual cooling rates provement.
ough estimation can be ina,. Figfure 9 shows similar data for
:he possibility of realizing in;.: y. SaI, cooled pieces of I ., .11,1 and
A387D material superimposed on a
nent in properties by qu(i%--Ii. . n. thickness test pieces which
:o, continuous cooling transformation
he combination of tlhic, ,,ss :m •,"rte later tempered at various
diagram. Air-cooled material of
naterial involved. I. nl--rattires and times and result
{'o,de, '-it . ! t4,-silh strength plotted as sub ' '-,I ,.I and I I in. thickness ex
'ontinuous cooling and is, 1h . ,a! hibit cooling rates sufficiently rapid
1 •u'...uetily illustrated.
ransformation inf,)rm ,lio, ar. in
Figure 8 to realize improvement as does watei
s':.,ws imilar d.,ta superimposed on
he literature.".-,a. quenched material of 7 in. and
Figure 7 shows -ot)l,,g r.,:, 1 't jnuot,t ,'o,,tling transformation possibly heavier thickness.
ti :A d. cr:ins of A3.'71 material. Here
uparimposed on hot ,.rm., rt. Figure 10 shows similar data for
3rmation data of ,arl- I st, . it n 1-. vi.-that air cooling rates
A302B material superimposed on an
ar to A212B i;,erib.
-.
"or and I ili. materials are too
1 •, isothermal transformation diagram.
-lo, t,,r-,aliz,, any appreciable
im- Here, again. some improvement can

WELDING RESEARCH SUPPLEMENT I 439-s


,4 .

a,'."•
.140

IA
I AC,1553*r'
,, ,
*' N
A a..
",33
.

-.
-+F+C
1," L
A'C tSRBSF.,
- AC '98
5
' ';i'"f ,
"''I' ''.
'
[ •
J '-:"'A=
. .
" "
- -
A
AAa73T,+F .\3 A . 1436-r DASEONE-
-01 u. e- -- A.,4-F4P" OAS
869-*,1 oo ,
.. \ r3
AIR0
COO 31
I '. . rt+C A*N4SIS
I AB
A.n 8 "
.• a-
IaL5
.19
25
62 0 - I
A ~ ~ S
. 36.9I
7
1000. STEIIANO3W
Ir
• - .. . . . . ,a.. "I
41LEI12N
20 -ErEENC! %C.
9

-.- .. ,. CR 80

[j4al MC 40
I
LooL ANALYSIS
- I
~N
60 S. C21

Dir O'IENZ .. . 600


- -. r . t NG105 :. 229 .6)P
S• AIR
"COOL .... A STE'".,NC
, e',. 'EMP
N. 0 14
ac "r 700 ICo
10, 50C , "0 0
K; ,3r
3
I12 10
T;ME - SECONDS
TME - SECONDS
Fig. 8-Cooling rate data superimposed on A387B continuous
Fig. g-Cooling rate data superimposed on A387D continuous
cooling transformation diagram
cooling transformation diagram
1400 4 0
1 c
I , PI'"I
.
A+F+C,
1200 A / A-F
/ ISe I-j -- - 2o
1200-
AIR COOL,
,a a
.
t A i
-I 200
A A+r

a , ao;
'
La. 100'
,A+F+C ,
F+C 100C
f
. 'a SA- 302B
Ia \, I RECERENCE N0. 06 * "a, asa A+F-+C .
IC I ANALYSIS
c oo- I 50%. -,a.a99%I-T
C O2C sOC
- l -a t
LI DASHED LINES 2 41 ,19 M,:74o.F. I
CE AIR COOL 32 aSi Dil
, ' 33
" N; 0.22 a ASME CASE 1204
600 SOLID LINES ' M1o 056 60C * REFERENCE NO. 107
DIP QUENCH a I , I £ 0005 aUSTENITIZING TEMPIAC16F.
G.S.6-7
I . - Is--C . AE,-,131'F.
400 , , c.l,
-11
", I I,,,,
I....
to 4
tO, 103 10 10 to O3
0e to' tO
;-.00
TIME- SECONDS
TIME- SECONDS
Fig. 10-Cooling rate data superimposed on A302B continuous
Fig. 11-Cooling rate data superimposed on ASME Code Case
cooling transformation diagram
1204 continuous cooling transformation diagram

AS
NORM O00F 1100F I20o*F NORM 1000 F IO" F 1200 -"F

aiim CAS 1204

I I
.. ASME. CASE 12014
C I

"' ,A-302"
2o
an

1C
, -'r" I . t
S LEGEND .
A,,.
-3 - L
D":' A-, 3 7, , ..'*,,* . * - .2 5,

I 5 C
2
&. a 5 10 20 i 5 I0 20
a " a
I !C 20 .¢ y

HOURS AT TEMPERATURE HOURS AT TEMPERATURE


Fig. 12-Effect of tempering temperature on tensile strength Fig. 13-Effect of tempering temperature on tensile strength
of A302B and A387B steels. of ASME Case 1204 and A212B steels

be realized to a relatively heavy It must also be kept in mind that Tempering Time
thickness. continuous cooling results in shifting
Figure 11 shows data for ASME the transformations generally to ihe and Temperature
Code Case 1204 material. Improve right and downward. The trans Material heat treated by tnJtei.
ment in properites can be realized in formation curves are taken from the tizing and quenching must he tem
heavy thickne&ses. literature. 104- ,o0 pered pripr to cold forming -)? cold
-9,
I
i x5

~. / e
z
-T
4¢ /
* ,.-9.: CENTER T 7-

-
100 16'IKA877-
* lcl 37 I UNCE-T4
u~HO T4

NON[ 5 o 20 I 5 Ii. 20 I 5 I 2.
"A* V- ATUR;
HOURS AT TEMPERATURE
Fig. 14-Effect of temperi, f-,g";era.utt or! tensile strength Fig. 15-Effect of tempering temperature on tensile strength
of A387D steel of 7/:,, in. thick A387D dip quenched steel

sizing. After welci:g the heix


thicknesses. it must also 1e i:-r,
Figs. 7 and 11 respectively. Here
A212B shows no improvement.
analyses are available and will de
posit sound weld metal exhibiting r
pered; in most inatmnces. this must whereas 1204 material does and it a variety of ranges of high strength
be done prior to cooling fron, te retains its strength after tempering tensile and impact properties in the
welding temperature t,,asur, :rt(e for 20 hr at temperatures of 1000 as-welded and as-welded and tem
dor from cracking l.rge ve.ws and 1100' Fand for5 hr at 1200' F pered conditions. These can be
constructed by sul-wively joining but loses appreciable strength at 10 chosen of various diameters and
several courses will mubject the first and 20 hr tempering at 1200' F. resultant operating amperages and
course to si.vral tempering heat Figure 14 shows similar data for used at selected travel speeds to
treatment-. \lthourh the time at A387D material cooled at rates regulate heat input to tolerances re
each temperitg heat treatment can shown ili Fig. 9. It exhibits an in quired for control of properties of
be short, the sum total plus that of a crease in strength on tempering at the base metal heat-affected zone.
final stress relig-ving heat treatment 1000 - F for up to 20 hr with strength Multilayer gas metal-arc auto
can be on the order id 10 to 201 hr. rapidly decreasing after 10 hr or matic processes are also available
Similar but possibly, lesser total time longer at 1100' F and 5 hr or longer and require similar heat input con
at temperature will be required for at 1200" F. The maximum strength trol for maintenance of heat-affected
materials heat tr..at,,d as flat plates level exhibited, however, is higher zone properties. Flux cored wires
and warm formed or heat ireated as than that exhibited by the Case and strips. are also available and
finish welded shells or lwiads and 1204 or A302B material. usable for alloy additions. Multi
then subjected to %,,ldini temper Figure 15 shows data for a 71, layer submerged-arc processes, using
ing and stress relieving. in. thick A387D dip quenched plate bare electrode of the proper alloy
The a-queri.hed ,nechanical at the center of the thickness and at content and. or alloy additions to
properties wil! hi.affected by these the I ',thickness level at the cooling the-flux or braided wires for regula
re
tempering and t reas relievino! tem rate of point 43 as shown in Fig. 9. tion of the alloy content, either as a
peratures and t;rne ,t t.enipera Here, also. an increase in strength is directly consumable electrode or as
t.ure. :* Till- )r(qm.rt ies may he exhibited at 1000' F temper for up an additive to the molten pool, are
adversely stilected by -one torn) of to 20 hr. This high strength is re also available. In all cases, how
temper embrittlemem - 2 The tained up to 10 hr at 11000 Ftemper ever, the use of these processes for
degree to which the p'r-periies itre but drops below 140,000 psi tensile welding on steels previously
affected must b4. known so tint th strength at the center of the thick quenched and tempered must ob *211

finished product will exhit, the i ss after 20 hr at 1100 " F. Further serve proper heat input control to
desired minimoi, proprtie*. decrease is exhibited after only 1 preserve the base metal heat-af
Th. *.fl,'i -i i'l) to 20t hr tfm. ai hr at 12000 F. These properties, fected zone properties.I. '.. .:1.'. 1:14
each t!w% era: temnperatures o01!ht however, are quite high for such Preheat and interpass tempera
tensile strength of several qi.en,:.d thick material. tures must also be closely controlled
low. alloy steels is gtv%,-? illV ,-'s ". In most applications, the finish -above a minimum to prevent
13. 14 and 15. ''ll t'.nsile oita a:, ';bricated pressure vessel will -be cracking and below a maximum to
been converted from f,,,kw. :hard ,.-adv for service after being tem prevent excessive loss of properties.
ness testing using 'onvvrsi,. c , .cregd or stress relieved for the rela Material, which is to be welded in
given in the literature. I - ,v,.v short time of up to approxi the annealed or normalized and
Figure 12 shows the strencti of i!,at !v 20 hr. Its subsequent ser tempered condition followed by
A387B and A302B mat-erial(,,.de,: at I'e ,na% be at low or intermediate quenching and tempering heat treat
rates shown in Figs. F and 10 re i..Inil.ra!jre. The effect of service ment of the welded part. requires an
spectively. It can be not,.d t i:at -. ,ml rat ,Ire over long time periods analysis of . weld metal, different
A387B material is not ti. m.,,ria! properties must also
v-iliy ti..: from that above, which will de
strengthened by these co,,lini ri i's velop properties equal to those of
but that the A302B matermi is. the base metal upon being subjected
Figure 13 shows similar d ,La - r Welding to quenching and tempering. The
A212B and ASME Cole 1-4
1 _.. M ,.;al %..eldingelectrodes of a high heat input welding proc
material cooled at rai.s ,. wi n id, .ari.tv of deposited metal esses of gas metal-arc, submerged-

WELDING RESEARCH SUPPLEMENT j 441-s

~'* .7 .I
RANGE OF CHARPY V-NOTCH IMPACT PROPERTIES have poorer resisuitice .t *'o'er
DEOYI)AT ON
0 T FORGING MArL PRACTICE temleratures, if an\ failure a: the
,Ot O'OENCHED 8 TEMPERED
lower temperature does not en tail
PLATE
M.- MO 4L.BS A.
exceasiv( risk of life and prolerty
CASE PER TON Tht. lower temperature may Ie at
A-302B A-212B the hydrostatic, test. or it may i6.all
:23C
unforseen impact loading. High
rebistance to brittle fracture may not
be necessary for materials whichi are
Nt. AL
stress relieved and are adequately
nondestructive tested to assure suf
ficient freedom from "crack starter"
type discontinuities. The carbon
NORM. S'EMPERED steel and low alloy steels, of a low
A- 212 B hardenability analysis not appreci
ably improved in tensile properties
by quenching and tempering, are
"" '
appreciably improved in impact
Y 3E: 6t-,C
I'-- .-4 I ., ;' - F"
properties in heavy thicknesses by
30c' -9 TEMP 15FTLB. W3r 'L P TEV 9 . 20FT LB TEMP
TEMP accelerating cooling. only if they are
melted to fine grain practice. Such
THICKNESS OF PLATE -DISTANCE BELOW PLATE THICKNEss
I OUENCHED SURFACE deoxidation practice also minimizes
deleterious effects from strain aging
Fig. 16-Charpy V-Notch impact data for different quenched and tempered
and quench aging.141
plate metals
The range of Charpy V-notch
properties of quenched and tem
pered plate of A212B and A302B
materials and similar forging ma
arc and electroslag or electrogas terial strength and resistance to terial analyses, tested in large pro
methods are usable for this type brittle fracture. duction quantities, are shown in
application. Fig. 16.
Heavy thicknesses subjected to
tempering or stress relieving heat
Service Criteria The more hardenable quenched
and tempeied materials, however,
treatments must be designed such Brittle Fracture generally show a greater degree of
that no welding is applied after the. Quenched and tempered materials improvement in impact property
final heat treatment, or such that are advantageous not only for utili values, although they also generally
welding is applied only to previously zation of higher tensile properties require higher impact values for
prepared attachment areas engi but also for utilization of improved equivalent degree of resistance to
neered so that the later applied as resistance to brittle fracture.'3-141 brittle fracture. The work of Pellini
welded attachment will not affect Whether such improved resistance and Puzak and their colleagues, and
the integrity of the part. This to brittle fracture is necessary or not Stout and his colleagues, has been
necessitates careful design and se depends upon several factors. It particularly illuminating to this
lection of weld metal and attach may not be necessary for materials subject.
ment material with respect to ma-
which operate warm, and which
Temperature Limits
The maximum temperature and
times at which quenched and tem
pered materials will retain their
1400 improved tensile properties is not
known precisely. Design is generally
based upon a factor of the yield
strength at temperature, the tensile
1200 strength at tempelature, the stress
rupture strength at temperature and
the creep strength at temperature.
The temperature at which each
000
criteria becomes controlling must
be determined for each material and
condition. It is generally believed
BOO
that, in the absence of such factors
as temper embrittlement, the tensile
properties are controlling up 'to
possibly 700 or 800" F and that
600 stress rupture and creep properties
become controlling at above this
temperature. At higher tempera
tures, the material will revert toward
10
-- 102 103 0 00400 its normalized and tempered or
annealed properties. Since most
TIME- SECONDS pressure vessels are designed for
Fig. 17--Cooling rates for Points 1-7 long life, on the order of 20 years or
more, quenching and tempering

442-s I OCTOBER 1962


*\ I,'
1204oj PN? Nos CARBON STEEL A, 317 D
II 12 5 DIP OUENCH I COOL'NG RATE
DIP OUENCH 1200

.0'0
\ I,,
COOLING RATES 1100
I SU$IIAC(
I 16i-I,

-000 1000
L.

4OjN223S- . '*',
,/4 7-DASHED LINES
Gool-
" 0.2 IY AIR COOL
1/2 T-SOLID LINES

F
I..0" . "
.... 20
Ia ,.t"X24;xo
4
I4.x 23x 33 k
N
, J ,,, [
I0 'C' K 9 5 so
IC, IC
"WE - SECONDS TIME - SECONDS
Fig. 18-Cooling rals for Puints 9,11-15 and
25 Fig. 19-Cooling rates for Points 16, 17, 20, 26
and 43

DIP QUENCHED COOLING RATE


-VS
1200
I'DIA JOMINY BAR
REFEENCE N0.96
AUSTENITIZNG TEMP I550*pF
SAE 4.40

- 23 Ia
OO

S " FROM OUENCHED 0.


• END OF JOMINY BAI 6o0

I\. i

to ,. 1 1000500
-! -SECONDS

Fig. 20-Cooling r!&s to, i.:-,,ny test bar-SAE TIME- SECONDS


4140 steel
Fig. 21-Cooling rates for Jominy test bar-SAE
4330 steel
applied 1.. _-Is to oper:it,. f,
high tem I,..r,,;.. Joes not ali..tr corrosion media must be retested
t,. resislant. The weld metal must
be highly priv::, 9 . for contemplated use in the also be resistant and not be chosen
In addition sw
quenched and tempered condition
ueptibility (I on only the basis of its mechanical
t4) assure that they are
quenched and I.-.. oert. material to sufficiently characteristics.
aging embritti..,m ,ver lnn1
periods of timi ' ol'erating tem
peratures from n I.,. 1ei;twrature up.
Is
must also be ki. ... ': Stnut 943 15
14 16
I? 3f2 I-7, O
and his ,',,ll,.:j
', -, test.d
i,,ve.r;,'
m,.,
--. ,,. tll

Coo ruw4CaI
Quell, t"
ust be ctr,-,.:.
n corrosive N
, tu-il'P Y~ ;I •
|'IJ)ll, . 0 ] ; l .,. |
ttr: ,lr
,. ,h-
f -- °it o 're
, l,- .,]

ge
cd 0i i ., ~,. u.- 'XV
it~h
ome h ,:i: , ..
:i*. ic'. s
Yherein the ri.in.......
,rihl CS 1T X12T -i
equired NORfIALIZE-.
fur .rr,. ,n ,, , Ice
juen'hi.d a.rd emi.- red lath'ial.
. 5 4 3 2 CS 24TX24T
niL!Ill 11-. h, -*d% ta 1us and
-VERAGE *F PER SECON COOLING RATE-,7"SOTO 4OC.0
-F
Allnt - .d,): rrm., 'ed .,id l,.n 1
, 'I I
.ered m:i ,rij4.. Irc?-s.
ly _A ;. .I ,I
ause of tiSeil --Sti ... t' tpe, .*re
10
FaR. 2-Thickness vs. cooling rate from 1750 to 400' F

WELDING RESEARCH SUPPLEMENT J 4 43-s


•, *5 .S' 7 . .

". •212f ,
AT CENTER O r WIDTH AND LENGTH

DP OUENCH * :; ".

NORMALIZE ""
- I

•~ ~~~~
S p, , ° S 2.3- X. ,4,

AVERAGE F PER SECONDCOCLING RATE FROM ITSC*TC 120C-;"

Fig. 23-Thickness vs. cooling rate from 1750 to 6000 F


Fig. 24-Thickness vs. cooling rate from 1750 to 10000 F

tI 16 122? 10 26 a
19 15 14 I .3 I 2! 1
I '-' .. S ~'.I "" I 302B
,os 3eX38*" " ~ ~
2120 38TX,3 "
AT CENTER O WIDTH AND LENGTH3

* 2128 6't 67
CENTER T 3028 6: 6

*387D 6SE
X

DIPO.ENCN- 2128 -
_G., ,
-""81
CS B' ST "
12 Tk 127 -- st NORMALIZE
* " CS '2" 1 2T

2C 6 5 4 ! 2 24T X24T 7 20 It 5 4 3 2 * '


,, Cs 24TX24 11
AVrR4E'F PER SECONDCOOLINGRA E -SC'SCF TC IOOO AVERAGE 'F. PER SECOND
F COOLING RATE F!ROM 1750r TO 1400"
.I I
A I JiIi . I
.... F

Fig. 25-Thickness vs. cooling rate from 1750 to 12000 F Fig. 26-Thickness vs. cooling rate from 1750 to 14000 F
-4.

Summary strength levels in heavy thicknesses als and to allow application of the
as well as light thicknesses. Wider quenching and tempering at the
Information is presently available use of such construction is awaiting fabricators shops. It also is await
to allow construction and use of the formulation of material pur ing the formulation of Code rules
welded pressure vessels of material chasing specification criteria to allow regulating safe construction pro.
quenched and tempered to high a wider selection of possible materi- cedures.
Successful construction is depend
S...
ent upon maintaining close control
lOP, THICKNESS- INCHES of material chemical analysis, heat
-FROM 1650' F. -, I...I treatment, welding procedure and
- 24 23 22 21
5.6 4 3 2 I - FROM 1750 F. all aspects of fabrication forming,
heating and cooling. This requires
closer control of techniques and
procedures than those generally
' ,INFINITELY LARGE DIP OUENCH FROM 1750-F. required for annealed and normal
*2
! ".,,-" - 67 X 6T
",, -,, , e AT CENTER T ized and tempered material. This
"AT 14 requires closer control in procedures
MALIZE "" 4 of obtaining test samples for destru.
NORI
tive testing which are representa
/I" tive of the larger mass of the prod ur
*'..THICKNESS tion materials. Information which
RATIO-- * will be helpful in determining degree
of control necessary in some oft hese
aspects is given.
19 1517 IS 11 9
43 14 16 12 27 10 26 8 It is believed that the quality
Is 25
control assurances necesar. for
AVERAGE *F PER MINUTE COOLING RATE TO 400* F.
proper application will cokint ul
. ,SI , , , I I. .. . ,i l..a. .. i I. ....."i iI
0too
.. . . . . . .
oo
specific rules regulating and de
fining material procurement specifi
Fig. 27-Ratio of surface area to volume vs. cooling rate to 400 ° F cations, design aspects, and Iuihrici-

444-s 1 OCTOBER 1962


,/I- FRood 1750 *F.
a
1. 23 17 ~ .2. 'ROM' 1650'F
FROM I750o*F
* ,- INFINITELY LARGE DI OUENCH FROMA
1750
.'IP' OLENC M
' 4T
'.4TX FROM
.Tx ST *ATCENTER Ti P 1750*
42IN74INITELV LARGE
AT 'Z T
-, ,6TXGT
0 -AT CENTER TI
ALIZE
T'4!CKNES
~0
* NORMALIZE- 1?.NS
RATIO-

w RATIO-
I -~

0 .9 1 IT 24 10
-. 43 259826
1 AVE6AGE -F P!.0 MINUTE COOLIW RATE To 600-F. AVERAGE-F. PEPI MINUTE COOLINGRATE TO 1000-.
IC .- ~. 0000

Fig. 28-Raticofa sur1m,':e arev. I- oooirre vs.


cooling rate to 600"1. Fig. 29-Ratio of Surface area to volume vs.
cooling rate to 10000 F
.~ INCHES _

TICKNESS - INCHES

-50 1. 7 6
.23 22
5 2
7, -- FROM.165C-F
-- FROM 1750*F

7
to

- dA
0IP QUENCHFRM 1750-F.I

CENTER 7
IDID
I.IN"IN'TELY LARGE
FROM 7C
OUENCH

70-T - ATX OTATr CENTER

746

1 NI~M.2ZE
0 7HICKNES

RAT!-

o2 Ia. 14.7.:6 3 , 2! 9
7 AVI2.GEFr PER w !.U1t1 24
;,N:
.ATE TO0100'F S AVERAGE*F PER MIN07E COC..ING RATE To I400*F
70 7(. 7000
Fig. 30--Ratio of surtac'- area to volume vs.
:ooling rat,- to 1200" F Fig. 31-Ratio of surface area to volume vs.
cooling rate to 1400' F

pr(lce!du7.
IticIf tiivolI.!f t;,eai nig II). PuzakL 1. I'.. An1.i ellini. WA.S.S"Effct of
7
and coo ii" "- .
It' I m".-L':'tli~ng' 77-1W.~Id 7 ijiljty of1 H 171-Sirerl Pr7717
i.7-7u77 V.
1towrntIure oin Ith1 I )ovIil itIv f H ittl Str.r171 1
-1 81,.- in Henvy Lid.. 36
A7.is .1-. I(,..
procedure quah'.. ,timl1s, anid 1 'lre! .,rchi"'pi..
57
1- -s to 167-m 97
Stitm7 rIl SI .,,'I Londw.l inl the Pr7.*n7. ..r Shiurpi
3ent4itive fiabri. '.-ion test p; rtes. ii Slul . R. D.. -l huh,.,-SIrt-nI Ii Zttn-k- br 17. 2.il I) t.. '*Fv,IuI in .I* fiI1171-nu
Nondestrili',,( -V.sting pJoctur('s
'I'III 7%ELIH7No3i71I'NA.. 36 -. 677-9.12 .t5j
must a 1917 :- d.l tied but -xi! ar.\ 7. Pens.. A. W.. Ir.,. .1. Ht.. and Stowl.
.7

iepe'ndingJ up.i - *he serv7-$(. IS,'... in I Ieavv-S.-iino Pre-waur,-V,,.,. Stm .I.C Aihd
Inti,. bund.. 39 1 I- 1.. tirchl 50171. I - In 197-.4
and slietific do. . 7
:19 ';;. II.'.4~.rch Suppli.. 2:Ii-.to 2fl;.R NII 71915!1).
I! I Jael-.- I' - - la. 517(n-i (.f Ar, Weldl
b,. Si 7701. It. ID.. -'I'he I'rf-huiling and7 Pi'Lst
i ng. Ib-id.. 39 4 . I o-.'w.' i, Ill I2-.. h
A cR-,. 4CdA7Pml'?t I I...Iting .,f Prt~,sire Vte .Simvlk.' Mhd.. 32 , 1). 14011-1.7-,. t.. I'61- ind7, 22-'- t,- 2301-s, - 1964)1).
litarch SupplI., 14-m-17,22 * 1953i.
'Ttie aid. in 'I-!aining I le 97. II . Jr.. aind S9tout. It. D)..
F7IcsnI.I.
211. 517,0. I. D.. -IIt:IIr-Si-1'7,l si.-I. f.'r
W04I SI ruo,'I7.*/ , 39 7'. I7'N.7rc
"IIT-f7. vtf MicrrUCLiUt. on Ni..rh Tougi2ne.-.
Iw. IV '7Iid..38 -11). It,-s-grch SuI..4.-,, lot 21. I;rt777777. Ib-ntri P.- '$IulI.w. .n (r.7ei:7i
1 4. . , 'I l
of itn, I'r71t*;,iwiniI io77 in St717'12I I )urinp!I 7VelL.
;earch mid H /77Yl~~ Ai7d.. 41 . 1..c,,h~7IIl.I, .i-,i7i
.
No1t7 'r-ogi,77 .. o.f St I ot71ural She5 il,.- Atin.. 22. (Iil.iv,,. J1 A. and io1,ni. .J. it.. ''Tiw
ASAI.ioI.44.
1 2: -?- M.%av1961). i-'ahrii-.ilion :snt1 Il-r SIri.rI
op7777*f ur- cif 81'-V
-,n7 .- I I1. jigijiiCitl7777 ' 1II.r 'I~e-.ts ft~r St"+' i-r:n77 I- .IV4-7,77
('w'.7p.
1- 1@0*77
77) *.ilmI.r-' SI(.-ls."'YHIIE 'AILnisii . 2-~w 17.
Fr 1 7ro-
g I-I....r,:P 1A.71.Iil,- i.na
'7e.i
aI Vabi.. *i. m I on -. I77
St.:..7~ Ndi,27. No kmI.)
I*S. . 35 6 W. S4~~I11
ani 077.. 2uo...R.
V.7 1. 7
245. I - . . 1 '77..'
I71771or noi I-%,
7 -
I77 .
Uto,7-. 1 'r.. -oa. ii 'I'vilitwo liril tItI'77771 in AII'iy Steo,
s... 7 .5.
'777777ure-Ve,...i Sio,.. I \vk.7,
:7 4 1. 1ti'(-a7rch Supid71.7 i i 3017 I:Irili
3 13: ;
*A 1 d.Ij.I. W. It.. JIr.. lDuopIh%. It. 1'.. and7 2 .'.7 'to\A.I ti rsilk..I-.-ri7747vt l 7 ?I~
2 . 171,. AIfH.I i I . . jr7i-lii I.-..I ., (4,'7-... and1 .... : Sitel f77r
it 611i,, ral olCrM., i.,I3
771 Heatvy S"Iior, Ir.', .. ~~. It".
777 7f -
-1-, -"
:77.17
WEr71.1cm4
I., G4-% ( 19154).
I'n7-ur.,,- 77e..7' 71 ',. 34 1!.I-$~7.i 0.7

Iim
: 1I).an
.4 -1 ~. 1 1'.. I&7Iio,I,,r. E. W . viol
42!7 ,.s :7,
!111. S. - 1771..tiO.i ,nil. 'l1ol77271i1n 71r
al Priri .. 7. .....
IA M. .i:j-f 5 Vi'n~el. 1'.1 'II (F7.'nih,-.. anti1 'I771 7.171SI .,I.
7 7 1 - 11I, . - 7ut7itral Sil. i,.31
*Iren;!th SI- Woo
' 77 (*, li777.. 34 ;'- .777 .I SUI 17..44-In - 19A70
,'o. 27 My-, .
4. (;ro.- . u I0.
irrnbunt,, ..r 11771. 2 '71tti. 1,,
I..7.. n. WlliritlI I I'roiItfl Servicv I ion." Ibi.d.. 34 .97,. I,.i',rch 8 u717., 449-m. * 19-751.
2'Ilil,I..r. . 4% H Iodge. J. M.. Altman.
1p., 1,."I?:' :I:
3' ..-- reb SupplI..
.LT 314-P to 4017-o It. V.. avidI 17,y. WA. D .. "7A Newv I-Iisl Yield
Strength11 Aliloy Sleel (771 W~elded Sirticlures."

WELDING RESEARCH SUPPLEMENT I 4.45-s


Wyelding
1952,. ltue..rclhCouncil Bull. No 11 IJuly
58. Jominy. W. L.. **AIHardenablility Teat
291. Nitl,.• E. F.. Savag,. W. for 92. Uidholm. C. A.. °Llri#tt,-nt^, S, ,.tte.
F.. and Alli. Shallow Hardening Steels," 7rns. ASf.
It. J.. "'Studiti of the Weld Heat-Affected 1072 Of Continjiou, Cooling Trsnsfurr-tiu.. ""-.,.
Zon. of (Dece-nmer 193).
*"-' Steel.'" THE WRLDING JOURNAL, 36 (12), ASM.38. 180 04947).
Ite. 59. 'ot. C. H.. Greene. 0. V.. and Fenster
"i'erch Supptl.• .5 3 1-a 11957,. macher. '. H.. "Hardenailiuy of shallow.ilard. 9:1. Steven. W .. and M ayer. I.,_ 'ti, ti -.
.30.Sillhcomniittie on lfigh-Strength Steels. ening Steels." Ibid.. 30. 1202 t19412). Dlia , s. alt S l..' - ""
I'VIWC. *'Lilera-ture Survey of 60l Atinvi.
('ooling
./nl. Iran Sterl /nat...matlon
'rans forn 147, .11 (1 7,3). '
High M.. and Grosmann. M. A..
Steei." Ibid.. 33 tS). Itea-Arch Suppl., Strength "'lirdenin tlaritctriatita of Various Shellas." 94 t'haPman It. ).. mad ,lominy. W. E..
A
251-a to
Ibid..2M. No. 4.949 "1),ttml.,r1140). Methusl for J)eterminin, the '.ontinu,.. cav,.,.
I1454). 'rransforimatsiori in Steel." Trunk. ASAI
31. Kihira. Iliroahi• Suzuki. Ilaruynathi, 1 ;i.T rm ian o. A . It., a nd K lin p her.L . J.. "Li 47, sa
and 1195;,.
Tamura. Ilirelni. "'Itt-earchem on Weldable Iuliina of the End-Quench lI:.rdenahility
Iligh 'est."
Strength Sleeks'" Welding I(asearch Ahrndd Ibid., 44, 77%5.1!,2). 95. t ratigi. It. A .. and K iif ir, J . M ..
S. 2 ,January 19591. Bull., formation of Austenite on (ontilnuou
i'. Freriting N. C.. and lowland. E. S.. t,1,',
32. I)a%%slan. 'larden.,lilily "'e-ting if Low Carbon Steels." and Its ItelAtinn to Transfurmation at t t'nst,.ti
T. J.. "'Quenched and Temlicr.d
Ibid.. 311. 22.t I 'J1 2;. Temperature," Ibid.. 29, 85 (19411.
Steels
40 (4),in Ship Structure."
R(esearch JOUHNAL, 96. Blickwedge, D. J., and Hem. It. V ., i oi
Suppl., 171",-x
VLDNt.
to hqI-p 14(I.l6
). 6. Frieh. It.J.. "Sote Aspecta of the Hard
enahility of Steels." Metol Prog.. 5. th;'Cooling Transformations in Some 0.41',
33. Kirkley. G. W., Jr.. "Weltiig of "T'riton. .505 (1949). 1 .r
64. Welchner. J.. Iowland, E. S.. and Ubben, bon Constructional Alloy Steela," Ibid.,
W\orlidP, rttt Nucluar-owered Sui6arin." 49, 427
(19571.
Iid.. 49 ;91. 843 !K)'- (19N)I J. Ii.. "EFffect of Time. T,'merAture and Prior
i4. l)awson. T. J..••Queiched and "emlaer.'d Structure on the flardenabilily of Several 97. Apilett. W. R.. Jr., Duntihy. It. P.. .nd
Alloy Pellini. W. S.. "'Franaformation of Cr-Mo Steel.
Steels in Ships Struclur.." Me-talt Enr. Steels." Tran.. ASAT. 32,. 521 1144).
ASAI.• 1 41,46i!NO-nilaer 1461). Quart.. During Welding." THE WELDING JOURNAL, 33
65. McMullan. U. W.. "A flardenahility Test
:t.'. Enmanuel. C. N.. Voung. 1). E.. and,) fair Low Carlinn land Shallow I lardening (1). litearrh S .7-
57l to 1)4-a (1954).
bid.. 3.5, !,4 Steel." 98. French, I. J., "Some Aslpect.s of Harden
Spalr. G. I... "'i, Metallturgy I!l 7, ..
fech-d Z.nt in HIY-HO tligh of Weld IIit-Af.
StrenLh Steel. " 66. Ill. M.. "I'n- End-Qu,,nch Test: able Alloy Steels." 1956 Howe Memorial l,:ur,
ducibility.'" Ibid.. 31. r - If4t 93. Itepro. of the AIME../nl. Metal., 'Jun( 195,6t.
Atfrl(d,% Fnj:. (uar).. A.A!,. I .,:. 82 -August
67. (irtitlan. J.. Ilenley. I. G.. Jr.. and Chris. 950. Hagel. W. C.. and Itunff. M. N.. "Trara.
:15.BaitIly. F. I.. ' E' rclm of Non-Mart tenson, A. L.. "Thermal Itetloducihility formation Structurm in Typoeutectuid Alliy
,-iI it of the Steels.' Trans. AS.Mf. 60. 1.4 (1958).
•. I lo'sinplion I'r'.lucts tn the Prolmerlie End-Quench 'esl." Ibid., 46, 928 i1954,.
of 100. Loria. E. A.. "Kinetics of the Attanit
Quenchel and Tnempered Steels," Trr,ns. 68. Carapella. L. A.. "A Ipl.ilinnhip Bet ween
ASAI. Transformation in Certain Alloy Steels.' "
46, 8O u1954j. ltardenaltilily and 'lenileStrengthr Norm aid..
dized 43, 718 1)151,.
:17. llollomon.1. II.. Jaf1es•L D.• MCarthy. Stet-ls.' Truns. AS f. 35, 4:1.", t 1451.
I). ..curl Nortn . Ni. It.,Effecta of Niirrostruc. 69. Zick. L. 1'.. "'l)-tignof Welded Pressure 101. Matas. S. J.. and Hehemann. Ri. F.
I -ar on Mechanicia l'rort.rt iea ofStel•"• Ibid., 38, Ve ulh Using Quenclitel antd Temliered Structure nf Bainite in Hypoeutectoid Si.-eLs."
Steel," Trans. Met. Souc. AI E, 221, 179 (February
141171947). THr. WELDoING JOURINAL. 34 (9), lItearcb Suppl..
.11. Hertz. S. A... mad l.oirig, C. H., 'Influence 442-a (1t95). (1981,.
of Metallurgicl Factor, on the Mechanical 70 . Murlthy. J. J.. Sotlerlerg. C. It.. Jr.. 102. Cohen, M., "'14eLained Austenite." 7rans
Plt, and ASM. 41. :5 (19491.
Prlie of Steel,' Iid.. 40. 77r, .194hi. Romheim. I). It.. "("'isiderations Affecting
Fu 103. Grifliths. W. T.. Pfeil, L. B., and Allen.
"19. Lodge. J. W., and Manning. G. K., ture Plrt-&-4ure--Vem.I ('odes." Ibid.. 35
'Ph. 5 (12), Re N. P., "'The IntermediateTransformation in Allty
Mi-chanicl I'roperlie=s of Quench,) and
Tem. se.rch Suppl.. 82-s tO 5 96-a (1956).
71. Carlson. W. H.. "Presgure Vesasel Design Steels.'" JnL. Iron Steel Insi., Second Report of
I.-r..d Mediur-Carbon Alloy Steels." Contribu. I hw
tions to the Metallurgy of Steel ••No. 49. Roquirements in OI,- Future." Ibid., 40 Alloy Steel, Research Committee. Special Report
Ameri 7 i6). ]e 24. Section XII. p. 343--Abstracted in
can Iron and Steel Institute (O.totier 1954). search Suilitl.. 26!,-s 1.0 2 1- (19I'f i. ,f-tud
40. Vajda, J.. and Busby, I'. E.. "Transverse 72. Marin. J.. and Ifimmtu. E. I'. J., "Design Progr.. 158 (August 1939).
Me'hanical Prnperties of SlacL-Quenched if Thick-Walled l're-ture Vitaels Ilaau' 104. Supplement to Atlas of Isathermal Trvan
and Upon the formation Diagrams. United States Steel. p. 3
Tempered Wrought Steel." Trian. ASM. 46, l'lmastic lijtnge.' Welding Besearch 'ouncil
1331 BuLl. (19;53).
1954). No. 41 (July 1958,.
41. Vadja, J. and Busby, 1'. E.. "Effect 73. Waring. H. W. A.. "Sti-els for Reactor 105. Weaver. Rose, Peter, Strassburg and
of Rademacher. Atlas Zur Warmebehandluni Der
Composition on l'runsverse Properties of Prtiure Circuits." .Ini. Iron .'t1.l Inst..
Slack 199, 1 Stable. Max-Planck-lntitut Fur Eili-nfor.
Quenched Steel." Ibid.. 47. 408 (1955). iSeptember 1961).
42. MacKay. K. P., Coldren. A. P.. Hush. 4. "'Ten Years of 'rogruem in Preaure Vesel schung. Verlag Stachleiten M. B. H., Duasa-ldorf
A. (1958) p. I1-323A.
1.. and Freeman. J. W., "A Survey of the Effect Research (1948.19",8l." Welding Itesearch Coun
of 106. Pellini, W. S.. Isothermal Transformation
Auslenitizing Temperature and Itateof Contin cii Bull. No. 45 (December 19581).
ioux Cooling on the Structure and 700' 75. Canonico. I). A., Kottcamp. E. IH.. and Diagram for SA302H. U. S. Naval Research L.ab.
F to oratory. Private Communication.
12(Xl F Properlies ofl'hre,- Low-Alloyed St,.,la.• Stout, lt. D.. "Acc'lerated Cooling of Carlbon
WADC Tech. Report 5r,-:18 iJanuary 1956). Stilia for Pressure Veuse'la.". 107. Doty, W. D'Orville. "Properties and
WeLDINtC JOURNAL. Characteristics of a Quenched and Tempered
43. Carlenter. 0. It.. and Floyd. C.. "Heat 40 tt), IResearch Suppltl., 40)-s to 414-s t1961}.
Treatment of :arhon and Low Aloy Premature 76. Carney. D. J.. 'Another I.onk at Quench. Steel for Pressure Vesels." THE WELDING Jntta
Vessel Steels.' Tom WELDING JOURNAL. .nLs. Coling lIale. and Hardennhility." TranA5. NAL. 34 (9). Research Suppl., 425-s to 44 1-a
36 12,. 11955).
I(-esarch Suppl.. 6 7 -P to 7 6-a (1957,. ASAf. 46, M82 ,197,41.
44. Bar, W.. "Progress in the l)evelopment 7.. Siebert. C. A.. "'The Why and Hon of 108. Weaver, Hose. Peter, Stramuburg and
anti Application of Steel PlaLe@." Jal. Iron Qut-oriting." Mfetal Treating. 10 14,. 4 t 1959,. }iademacher, Atlas Zur Warmebehandlung Der
S-l Stable, Max---Planck-lnstitut Fur Eisenfor
Inst.. 192. 109t (June 1959). 7)88.'Quenching of Steels." A Compilation of
45. "Heal Treatment and Forming'• Data Paler reire'tnt- at the National Metals schung. Verlag Stachilisen M. B. H., Dusseldorf
Boiler And Premaure Vemal far Con ;1958). p. 1I-322A..
THE WELnING JOURNAL. 29 (12) Sttw, • iChart)
Research Suppli..
gresa. ASAf. October 27 -31. 1158.
79. Steinherg. S.. "Itelalionship Bet ween Hate 109. Smith. E.. and Nutting. J.. "The Temper
nf Cooling. ]tate of 'i'ransfnratifn. l1ndercool ing of Low-Alloy Creep-Resistant Steels Contain
622-a (1950 .
46. Bunk. A. P., "Welding ing of Austenis- tint Critical ltai of Quenching.' ing Chromium, Molybdenum and Vanadium."
of High-Strength
Presure Vesal Steels in Heavy Sections." .in. Iran Steel lnst., 187, 314-329 (December
TH. Altallurgia, 13, 7 11938) or BruteLher Translation
WELDING JOURNAL. 36 (2), Research SuppL.. 6 19571.
2 No. ,77.
110. Constant, A., and Delbart, G.. "Study of
to R-s f1957). 0. I'it. '. B.. Fetzer. M. C.. and Fenster.
the Influence of Tempering on the Microstructur
47. Grosmann. M. A.. Elements of Harden. mttcher, W. H.. "Air Hirdenability of Steels."
ability. ASM and Room- and Elevated-Temperature Mechani.
Puhllcatii,n, Cleveland, Ohio Trans. ASM.35, -,;1945,.
81. Lw. '. F.. "'Eff,-t of Miuts on 1leat cd I'ropert les of Chromium-Molybdenum St"aLs,'
(1952). • Ret. Mc.. 51, 777 (195741.
48. Griffin. It. C.. anti Emmanuel. G. Treatmi'nt. " .1nl.Imn St.'•l Ins:.. g7. :333 •1918).
N.. Ill. Irvine, K. J.. Pickering. F. B.. '1 e
"l'roperti-i and Fabrication of High Strength M2. Zimnii-rschied. K. W.. "Influenc- of Masat
Tempering Characteristics of Low-Carbon Low.
21 '; Chromium -I; Molybdenum Miaterials." in He:it Trveltmenl of Stevl.' loin Trode Rev.,
WELDIN; JOURNAL. 40 (9), 53, M-1'19131 Alloy Steels." -Int. Iran Stel Inst., 194, 137-153
lta-arch Suppl., (February 1960).
:t)1:1.,to
399-a (11I61). 83. Straub. T. G.. "lu-lativ,, Siie in Iheal
49. Gromannm n. M. A.. •llardensbility as Treatment." Ieon Aer. 104. 167 (]ll!
112. Hollonn. J. If., and Jaffe. L. D.. "Time
It l , Temperature
Affets Heat Treated })arta." Metal Progr. R4. i'ortpvin. A.. R-t. Met., 14, -t7 ,1917,. Relations in Tempering Steel."
373 Trans. AI M E.162,223 (1945).
April 1938). 95. French. I. J.. "A Study of the- Quinching
113. Jaffe. 1.. D.. and Gordon. E.. "Temper
,M. Jominy. W.' 1.. and iloegehold. A. In..
"A of Steels." Tran. Am. Sn,..Ste'l Trming. 17, ability of Stels." Ibid.. 49, 359 (19571.
Hardenabiiliy 'est for Carburized Steel,' 646. 798 19;W),1.
'irans. 114. Manning, G. K.. and Krunlauf. G. P..
ASM 26. 574 (938) anti 27, 1072 119:19). 86. French. I1.J., Tr.a. Am. Stra. Stee Treat "Effect of Tempering no Mechanical Properties."
51. Jominy. W. J., "IHardenabilily Te t." ing. 21. M)t9 19:13).
in Iron Age. 158, 44. October 24;
V'tlume Ilardenattility of Alloy Steels. ASM, 87. French. I1. J.. and IRQue. F. ... "Ajloy 0. Octobter 31
6 11946).
Constructional Shrs's." 7"Ons. A.Af '9421.
52. Burns. J. L.. Miatre. T. I... :and Arche'r. 115. Engel, E. H.. "The Softening HatA f I
138. ScOtt. H.. 'Trans. ASM. 22, 68. 577
It. S.. "Quantitative Steel When Tempered from Diffe-rent Initial
Ilardenaltility." Trans. 119.34).
ASM. 26, I (March 19384). Structures." Trans. ASM, 27. 1 !1939).
89. Nipf. s. E. F.. "nti Nilun. E. C.. "Ct
3. Burns. J. L.. and Ilegel. G. C.. "'|ardun 116. Pense. A. W., Gross. J. H.. tnd Stout,
tinuous Cooling Tranfirntaion Characteristio.
.ility of Plain (-nrlin Slt.shl." in Volume R. D.. "Effect of Elevated-Temlxwrature lFi .ure
Hard. of "''hrop Tyes of Weld Metal." THE WKLDING
enahility of Alloy Stwla. ASMf. 261 19.319. JOURNAL. 37 on Heavy-Section Pressure Vessel S tl.-'
l). Iesearrh Suplil., 30-a to 36-a W.LDING JOURNAL. 39 (6). Re,a.arch Suppl., 2.it .o
b4. Janitzky. E. J.. tund BHayerlz. M.. Metals 1958). 23
Ifandbuaok• AS f. .515b 1193.q) to 5-s (19601.
55.) Pat ton.W",.G(.. Mete Ilrulr•..43. 726 t194"3). 90. LiedlIm. C. A., "l)iagram of Transfor
117. Willer, A. B., and Light. J. 0.. "'I .,n:
mllion During Continuuus Cooling of Steel."
56. Gromman. M. A.. Asitnow. M.. and Time Elevated Temperature Tet of Chr..... ..
Ur. Afetal PrnWr.. 46, 111)97(1944).
han. S. F.. "lHardenatility of Alloy Steela," 91. L.ielholni. C. Molybdenum Steels." Trans. ASM, 43
A., "Cintinunua Cooling - J3
ASM. 124 1193 9. 11951).
,7. Grommrann. M. A.. Trans. AlME.150, Transf.iv nimtion )iagran friim Mo:lifitd End
227 118. Waiatnan. J. L.. anti Snyder. v T..
Qutench Mu-'lug." Metal I'ruxr.. ASM, 45, No.
11142). ! 14 ,114 1). I "PredicLing Iht Effecl of Complex "reui.t.-iir
'ycleau," Ibid., 41, 1400 (l449).

446-s I OCTOBER 1962


M.t4L EnAg. Qi,.rt.
120. Len,,t. It s.. 1961).
AM' . I . ). yi.hruitry w'lded to the test prlte as shown in
.r,,,I ... I 141)..I ul .. an
;td ,I .
bea. Mori..'irorwu.IIl~ig
'NOtch TJ*,
.|..
1 :tl I , Fig. 2. The tuhing plrevented water
Pering Iron Corl'.,n Alit hn 1 l ,4
46. 1 (21 5M Al/ty 14(';1;. rtur.l lii'.PLA." Ibd.. from 'ontacting the thermocouple
851 t1.j
141. Arrm.tirong.
"*l1.-bw.h. I I.. "lrnitc 'T. N..from
K.hn. N. ,,A..Brim
Durl ih. i...l
junction and leads. Hot junctions
l.
.d.. 36, 47:! 113 were made by peening the wire into
122. Nllini. WV S.. ,illQo... fi.ehns,m in I'ro~qulp \'titl
vel.,Pieni of I 111 llritthjl.,.
it .I ",..rth S.upl. ;1..
3 t l-s I-
StelKt." 31 81.It.
,I1 52).
adjacent holes at the base of . 4 in.
klIny
142. NleG,,,v J.. J. . ni lotTr.mi...r.tur. nominal diameter access holes. The
12.3. Tahe-r. A. 1'.. Th1ornllo. .1 * tii lIlh,.vior or Ir"'.ur7
J. P.. '*1nfioOll,,,. of (
plpf R ~ .rth
;i SUllJl." 1 - t 1)V 11-"
,,.sl S11114.'"
l 'l 11id., 340, above pro(edure exhibited satis
ti. Tt owit.r Brit.
-11i~o~
14,1 W-,(Chiir
'racturt. I.=lericj¢
T.. nti ifl'ryle. W. II.. Pi-%ure.
a |{eweitr 'Hritth. factory reliability.
124. Htidrf. 1I %%
.. rlr Ilntlelle..., \',-,-,ie| SivI.'" Ib,,d.. 40 11). |{:4tearch SUlil]. Each test plate was grit blasted
a-I 41.-, ,
25. 24 1 43 to 144.
4 3 il,.
4.-.
I'tw,.k 1'. 1'.. and Bal ,cki. A. J.. "N r
before entering the furnace. Heat
ing time to austenitizing tempera
Flure ViPm'i Svw,.- Trn~v.Ut, toiliention Procedur fir NI1. I)rol,.-W.ihl
34 (31 fr.o. "P,'.i~l.,.1. oii..,g~
JOultsA,.
Tm.t," ii,d.. 38 ',. i.-.arch SuIppi., 20!P-. to
ture was dependent upon the maxi
21 8~-F- I IK,9I;.
126. J'l.i..It.. andI I 'lnn J1.. Chang. i. 14 5 . 1 - h9r r . C . . u ui m e n t
mum rate of the furnace and a hold
feet of (""""A~gi Corfo.. in ott
ofsil,l. I -i-ti lrot itt w I
SuAcept iii,
for Low.Iemii' ra un .- rvic
ing period was maintained until
on,.1'11.
AS.,I2 4 Iid., 38
t..' 11).
129" 1-4.,4.. equilibrium was obtained.
127 4uene~u. B1 I; J463. Thi,L:h. II.. "Sir:i. At:ingi
b mrti*i.~ , of 'ri-ur. All dip quenching was done in
12e ll-ch. J1. F.I ~. A.E. oIl,.U.
It, 2:1:).K , IW51 t. water agitated with air. Quench
7ran... ASM. 44, hri.. l4,%-. ing was done in a water volume of
129g.Steven. W live y, K .-Th.- hill,"
Balai either 69 or 131 cu ft. Air cooling
pance or Minor n ....e tin the 1...h.ernial
hnitllement of st-.. . I.Irn...1i,.19
F. consisted of suspending each piece
,2).141 i'Octcla-r
130. Wentw,.
'n-Io "- -. 9
Appendix in still air.
itP. CAnit,h.ll. 11C.
'lemper Hiiti.... in IAow Alloy Si..Weld AL the cooling data were ob Figures 17, 18 and 19 show cooling
Metal..Ni"*F -l--, -1kNAL.31 I!I t-,m
tained from time-temperature traces rate data for the specific point
131- Metal.. llml...'th Ed . .tI Prop. produced with an oscillograph re numbers described in Table 2 and
ertim. and Slisi. .- f %1.meriij,6
ciety fur Met,,l. :-el
n.,~.t So.
corder. Time zero was chosen as mnterial analyses described in Table
132. Stout 1:I it ~.t~uljllh-.i lo.
133. Niptw.. i 1.. and Ne!...,, I f* Pr..dt,.
the moment just before immersion 3. Cooling rate curves for other
ticlu of Weill l4.-...Affoc, l Zot.. 't 1 -r-ructures
0
in the quenchant. Depending upon point numbers described in Tables
from Conts- olittjg Tran1Inpi,*.
*i... ' Data." specimen size, chart speeds of 3 to 2 and 3 are shown in Figs. 7 through
289-it ti, ?41, -
30 ipm were used. Recording 11. Figures 20 and 21 show com
134 N,,.,..
Zone." 1.w, 31.
ceased, when the center thickness parable cooling rate data obtained
(1959).
-"-rch Supi.: , t. 19 of the plate reached 400: F. from the literature at various dis
1.5. Puzak. I- I
-I'lini. W
The oscillograph recorder was in tances from the quenched end of
-
iinn or th- Sito,%
Charps
ls
itially calibrated with a millivoltage
(11mwh-J and T
Ii- rc'hSupl, ;°
-Af t.or
Source to establish a correlation be Jominy test bars.
Sl-iq. "1 l'. 3 61
1-36.Sheehan. tween deflection and temperature. Figures 22 through 26 show
"'Impanct Prul)ert
Subsequently, zero settings Were thickness vs. average 'F per
Ailny St-eel,." p1.
1:I. "Effcl.' checked and adjusted, if necessary, second cooling rate from 1750 to
n,- I t '.I..I..
prior to each cooling cycle. In all 400, 600, 1000, 1200 and 1400: F
* .. AINII
(-ss, 32' F was used as a reference respectively.
Auxuxt J9 .;, 21N.
1:1K Koti'm, Junction. Figures 27 through 31 show the
"'Eflf,-t of Mi. intl Si......I All thermocouples were of the same data plotted with relation to
'--tch 'I -in
Part IV." \V.
°. 38 ;II I:.
standard -chromel-alumel type, in ratio of surface area to volume vs.
Supril.. 43 .
sulated with ceramic beads and cooling rate.

LOC" NG AHEAD INTO 1963...


T! 6? AWS Nation,2 l Fall Meeting will be held
,at. - 42t)n in Buston. at the Hotel
Massachusetts, during September 30
:t. For authors who may wish to present papers
ei :.-. nuary 15, 1963 will be the deadline at this
for submitting the
OF' "papers
, which you may wish to have
re-.. a! considered for
Tr
:te,. -_sary forms, "An Invitation to Authors"
:tior Form," appear as a detachable insert
:pp and "Author's
ft on
ss.,e of the Welding Journal. Additional copiespages 921-922
na. o-
011,ined through AWS Headquarters. 345 East of the insert
47th
4e. ,irk :. New York. Stre~at,

WELDING RESEARCH SUPPLEMENT I 447-s


_ASME Control Traveler
Material Control. Weld Joint Control
Item Description Coded Weld Welding Heat Treat NDE NDE Welder QUALITY CONTROL AUTH. INSP.
# # # Procedure Procedure Rqd Proc. Name
& Rev. & Rev. Fit-up Corn NDE Fit-up Corn NDE

REV.A C-OIE CASS.Y ________ _ _ _

V) - J- -.. K4,6n __

ISSUE CONTROL PRESSURE TEST A.N.I. REVIEW


at _P.S.IG.
' QC. Project
A.I. ---- , po 'T
Customer Customer
SYSTEM

PIECE MARK X=HOLD POINT


O ORIGINAL ISSUE ,,
PROJ. QA DAN CKD Sheet
Rev. Description MGR, MGR.
QA 0015. 9,2
ASME Control Traveler
Weld Joint Control
Heat Treat NDE
Procedure Rqd Proc.
& Rev.
1 -5.

PRESSURE TEST
at _P.S.I.G.
0.C.
Project
A.I.
Customer
Customer
SYSTEM

nA nni-A. o,2
ASME Control Traveler
Material Control Weld Joint Control
Item Description Coded Weld Welding Heat Treat NDE NDE Welder QUALITY CONTROL AUTH. INSP.
# # # Procedure Procedure Rqd Proc. Name
& Rev. & Rev. Fit-up Corn NDE Fit-up Corn NDE
PIA-_
T -aca.3 ,______ 1O03043 8 ' R V. )(,
I l , .o;-
~. "' ,
_,

5k% iV -32 .

± + -4-
-t +
1 1 I-i 1 4 4______ ______ ______

T t I I I I t I J- I ___ I __

_____________ I _____________

ISSUE CONTROL
__________ ___ I ________ I
_______________

PRESSURE TEST
_____

A.N.I. REVIEW
I _____

at .P.S.I.G.
Q.C.
Project
A.I.
Customer
Customer
SYSTEM

X= HOLD POINT
PIECE MARK
0 ORIGINAL ISSUE

PROJ. QA DAN CKD Sheet


Description MGR. MGR.
_________________ * .1_________ L 307
ASME Control Traveler
Weld Joint Control

PRESSURE TEST
at P.S.I.G.
Q.C.
A.I.
Customer
SYSTEM

Description
ASME Control Traveler
Material Control Weld Joint Control
Item Description Coded Weld Welding Heat Treat NDE NDE Welder QUALITY CONTROL AUTH. INSP.
# # # Procedure Procedure Rqd Proc. Name
& Rev. & Rev. Fit-up Corn NDE Fit-up Corn NDE

_____P_ RV. A. C66


N-43z- 3.0
eAse I
w__',,
s 1_b

ISSUE CONTROL PRESSURE TEST A.N.I. REVIEW


at P.S.I.G.
Q.C. Project
A.I.
+ I
Customer Customer

I_______
SYSTEM
Con. PL.
X=HOLD POINT
PIECE MARK
_____ _______________
0 ORIGINAL ISSUE 4-'PF q
4 t I I
DAN I CKD Sheet
PROJ. QA
FLev. Description MGR. MGR. So1c7
ASME Control Traveler
Material Control Weld Joint Control
Item Description Coded Weld Welding Heat Treat NDE NDE Welder QUALITY CONTROL AUTH. INSP.
# # # Procedure Procedure Rqd Proc. Name
& Rev. & Rev. Fit-up Corn NDE Fit-up Com NDE

)i P/
_ - - L"O . .c I
___ etk dL) ___ t43?- 3.0____ ___ _

W_ __ _ __ __ "4~,~A o.,_ ___ _

ISSUE CONTROL PRESSURE TEST A.N.I. REVIEW


at _P.S.I.G.
Q.C. Project
A.I.
4 4 1- t t
-~
Customer Customer
4 4
4
SYSTEM
*1-
Con. h.
X=HOLD POINT
PIECE MARK
0 ORIGINAL ISSUE Z ,31
DAN I CKD Sheet
PROJ. QA -6het
Description MGR. MGR.
(~) ASME Control Traveler (j
Material Control Weld Joint Control
Item Description Coded Weld Welding Heat Treat NDE NDE Welder QUALITY CONTROL AUTH. INSP.
# # # Procedure Procedure Rqd Proc. Name
&Rev. & Rev. Fit-up] Corn NDE Fit-up Corn NDE

I iv jwjiJjt&1 F'ok 0,JT- (403046 '~ r.'~j.


rA~
_______ -~-.~--- + ~-~~-f 4 4
I ~
L_ F.6.
__3_ !_ I I I __K ,
EAJvik---.) q.43L 3.0
1A

ISSUE CONTROL PRESSURE TEST A.N.I. REVIEW


_ I
___ Iii _

Q.C.
at .P.S.I.G.

1. II
Project
A.I.
;-r-b ;, "
_ _ ____ _ _ Customer Customer

I
SYSTEM
.o,, . E.

____ _____________ ______


__ I ______

ORIGINAL ISSUE
I I__ __ PIECE MARK
X=HOLD POINT

4 4. DAN CKD
I QA
....7,7,__._
n Sheet
Description i PROJ.
MGR. MGR. __-
FILLER MATERIAL LOG

Project V-P 6 90 4-67 Dwg Control Traveler# 17

Weld No. Procedure # Welder Date Material Material Quantity


Type Ident.
4&,5o13 OV -'SZI75- 4-z4' E--U b t#;f'0319 2S5o

oujpok' 34-So

SI Lrz v~JE-(-t

RL 631-14o _

IA~ar~.t
THIS CMTR COVERS WELDING SERVICES
• ' TICKET N908630 INC. PO#N908630; WELDSTAR NUCLEAR
SHIPPING
AWPO. Welding
Bo 0 Materials Plant
, Mlddle Road
AafaOt~Q#j00#
Wa NG cu MUS....
October 23, 1986

CERTIFIED MATERIALS TEST REPORT


WELOSTAR CUIMPAiY'S OU"AlIY SYSILt TIFICATE
(MATERIALS) QSC- 229
EUPIRATION DATE JAN. 5, 1991
CUSTOMER: Weldstar Company
1750 Mitchell Road YOUR ORDER NO.: 8117-A
LINDE S.O.
Aurora, IL. 60504 QUANTITY: NO.: 898117 A 01
1,452 lbs.
MATERIAL: Linde 83 - Heat No. 083195 - .035" Diameter - 44 lb. Spools
This is from
shipped to certify that
one heat Linde has
83 Class
number,
of AWS A 5.28-79 and ASME been ER80S-D2 as supplied under the above order number,
tested using the test assembly specified
SFA5.28 specifications. in Fig. 1
impact property requirements The wire met all the mechanical
process with C02 shielding of these -specifications using and
gas. This is also to certify the gas-metal arc welding
are correct and accurate that the contents of this
and the material conforms report
and ASME Section III, 1983 to ASME Section II, Part
Edition, Subsection NB-2400, C, SFA5.28
was manufactured free of Summer 1985 Addenda. Above
Mercury or any of its compounds. material
LWLIAkT
vav . ...
SwjL RUERTIES OF WELD PER TABLE 4
Weld Test Number AS-WELDED
REQUIRED
All-Weld Metal Tensile U1002-IAW
Yield Strength, psi
Ultimate Strength, psi 92,300 68,000 min.
Elongation in 2", 100,700
Reduction of Area, 80,000 min.
24.0 17 min.
61.7
CHARPy V-NOTCH IMPACT
STRENGTH @ -20F (Ft./Lbs. LATERAL EXPANSION
(MILS) DUCTILE FRACTURE AREA
As-Welded (PERCENT)
As-Welded
As-Welded
44
75
45
65
42
SS
46
60
(Avg. 3) 50 65
Required 20 ft./lb)so
REDIOGRAPHIC TESTS: X-Ray met the requirements of Fig. 2
APPLICATION CONDITIONS: of AWS/ASME SFAS.28-79.
340 Amps, 28 Volts, 13
IPM
CHEMICAL ANALYSIS:
C Mn p S si
.09 1.82 Ni Mo Cu Cr
.014 .014 *04 .0
.07 1.60 4- .15 .04 V
.025 .025 .S0 .15
.12 .40 .S0 <.01 - Actual
2.10 max. max. .80 max. '-60 max. - - Require d

ASME Quality Systems Certificate:


QSC-323
Expires March 17, 1987
Sworn to before me this

-~day

KAIHLLSN A. SIMONS, Nalory Public


My comm~liian axplies Jan~owy 31, 1991
Aecor~ee in AA--$,I, 0---nt
"WELDERS SERVICE CENTER,
P.O. BOX 711 AURORA, ILL 60507
•PHONE (312)8659-3100

April 24, 1989

Welding Service Inc.


3276 MarJan Drive
Atlanta, GA 30340

Gentlemen:
The attached CMTR (one
copy) covers the following
your purchase order number material shipped against
0207887; Weldstar Nuclear
shipping ticket N908630:

132 lbs. .035 ER80SD2 L-TEC bare filler


rod
Heat #083195

The above materialis in compliance with your purchase order number 0207887,
and will meet or exceed
code requirements of 1986
Edition, 1988 Addenda.
Sincerely,

WELDSTAR COMPANy

James R. Berry

Quality Assurance Manager

/ck

Attachment

HOME OFFICE: 1750 MITCHELL


ROAD, AURORA, IL 60504
BRANCH OFFICE: 1000 E. MAIN PHONE (312) 859-3100
STREET, LOGANSPORT, IND.
BRANCH OFFICE: 2650 BOND 46947 PHONE (219) 722.1177
STREET, UNIVERSITY PARK,
IL 60466 PHONE_ (312) 5.)A.A,
- L.. USTOMER Copy...

'tJULEAR SHIMPNG TiCKET DA!f2aq

'"WELDERS SERVICE CENTER"


P.O. Box SHIPPING DATE 4124189
11--AURORA, ILLINOIS 60507-(312)
859-3100

SOLD TO ELD IG SUVMCKsS - H'"


3276 XRjAN DRIVSHIP TO -I ilc WynI v 1
ATLAnTA CA 303,40
3202IAJAII DXIV
-ATLANTA CA 303,4o.oooo
PW Chorle CAccont v rse Ord Number Job Nmbr

E CERTI 1
WYTHAT MATERIAL SHIPPED HAS BEEN HANDLED
COMPLIANCE UNDER OUR IDENTIFICATION IN
& VERIFICATION PROGRAM.
"The Test Report(s) of which copies
ore attached hereto were prepared
by t TO
(Manufacturer). Each Item in this shipment
celved under the original lest report is a portion or all of the materials
applying to such material. The original re- TA
of each test report is kept on file
at Weldstqr Company."
DAMAGE CLAIMS When this equipment isshipped, litle posses to
the purchaser upon receipt by the PA'
carrier. Consequently, claims for material
damaged In shipment must be mode
by the purchaser against the
transportation company. AN
CUSTOMER SIGNATURE

NO. N908630 NOTE: AN INVOICE MAKING REFERENCE


TO THIS DELIVERY TICKET
WILL BE MAILED FOLLOWING ALL CMAmr-. e: ,,e
RECEIVING INSPECTION REPORT
JOB NUMBER ITEM(S)

INFORMATION ITEM 1 ITEM 2 ITEM 3 ITEM 4 ITEM 5


MANUFACTURER L
P.O. NUMBER o-o8078
VENDOR WC-4b 3TS74.
MATERIAL -e8 05/t)
HEAT NUMBER
09 / 5
MATERIAL MILL TEST REPORT i- ~
LENGTH

WIDTH
NOMINAL DIAMETER O3
DIAMETERCHECK A 0 3
B .03_g"
B o3 "
C 03&
D
NOMINAL THICKNESS
THICKNESS 1
2

3
4
5
VISUAL INSPECTION
REMARKS
L.. .. ..

NCR#
D A TE. -( - }
Welding Services Inc. 0
Welding Services Inc. Mfg. Div. g PURCHASE ORDER t
3276 KiAwIaW",
Adsta. Googia 30340 AcC.Weft Psyablo
o h (404) 452-.o (404) 4S-WU

785900
WELD STAR, INC H WELDING SERVICES, INC.
Ip SHIPPING & RECEIEVING
3202 HARJAN DRIVE
00000 0000 ATLANTA, GEORGIA
L 30340-0000
IDER DATE TERMS F.O.B. SHIP VIA I ~ 5
JOIPO
o
i
I V-S I :

') 1012 inl a .rlp rv ~,a .wrnr.


i . .
.J0_1.J[1"o-c.LI I~ JN €, WELD INV.
W: 13754,2663
'I CTY. IWHSEI WS, MI NO. SPEC/VENDOR DESCRIPTION
U PAH PACT NmJ PRICE UNIT I EXT..
| !
MATERIAL TO BE SUPPLIED ON 2#
SPOOLS AND HUST CONFORM TO
ASHE SECTION II, SFA 5.18.
50.00 ,07 17631 !ER7053/.035 DIA WIRE, WELDING, ER7053, .035 7.520 LB 376.000 0401
121-02-00 DIA.* SPOOLED, 2#, 10#, 25# ETC
MATERIAL SUPPLIED ON 2# SPOOL
AND MUST BE IN ACCORDANCE WIT
NB2400 & NCA3800 REQUIREMENTS;
SECTION III, ASHE B & PV CODEr
CURRENT EDITION; PART 21
APPLIES; CERTIFIED HILL TEST
REPORTS REQUIRED.
WELDING SERVICES, INC. RETAIN
RIGHT OF ACCESS. |
.00 .07 Q.A. APPROVAL Q.A. APPROVAL Q.A. APPRQVkL/DATEo )49)4,k .000 EA .000 0401:
400-02-00 SIGNED
CERTS/TEST REP CERTS/CHTR'S CERTS/HATERIAL TEST REPORTS .000 EA .000 0401:
400-02-00 REQUIRED

E
CONFIF LS 1 1,229.2001

DECKER
PURCHAMNQ CEPT.
@ Welding Services Inc. Mfg. Div.. En
Welding Services Inc.
32 7
TephW4 (404) 42-(4
0 A

SS-O
PURCHASE ORDER NC
O0o788 7

785900 S
WELD STAR, INC H WELDING SERVICES, INC.
p SHIPPING & RECEIEVING
T 3202 MARJAN DRIVE
00000 0000 0 ATLANTA, GEORGIA
L 3034e-0000

-R DATE TERMS I F.O.B. ISHIP VIA

3/89 NEET 30 DAYS S/P FED EXP P-i/UPS INDINA POINT/CON ED; WELD
PRICE
TWV. 1179;4
UNIT
.1
" I
QTY. WHSE IWS
M F
G PART NO. SPECNENDOR DESCRIPTION EXT.I I[."

ER80SD2/.035 DIA WIRE, WELDING, ER80SD2, .035, 3.750 LB 495.000 69041-


132.00 I5 17626
121-02-00 DIA, 10#, 25# ETC. SPOOLS
MATERIAL HUST BE IN ACCORDANCE
WITH NB2400 & NCA3800 REQUIREr
HENTS. PART 21 APPLIES; SECT.,
III, ASHE B & PV CODE; CURRENT
EDITION; CERTIFIED HILL TEST
REPORTS REQUIRED.
WELDING SERVICES, INC. RETAINP
RIGHT OF ACCESS.
NOTE; MATERIAL IS BEING
SUPPLIED ON 44# SPOOLS.
.00 IS Q.A. APPROVAL Q.A. APPROVAL Q.A. APPROVaL/DATE,'--L .000 EA .000 69041
i400-02-00 SIGNED, ________- _ ._
.00 .000 EA .000 69041
I5 CERTS/TEST REP. CERTS/CHTR'S CERTS/HATERIAL TEST REPORTS
; 400-02-00 REQUIRED
1.650 LB 165.000 04011-
100.00 07 !17631 ER70S3/.035 DIA WIRE, WELDING, ER70S3, .035
.121-02-00 DIA. SPOOLED, 2#, 10#, 25# ETE
MATERIAL TO BE ON 2# SPOOLS;
A$D HUST CONFORM TO ASHE SECT'
II, PART C, SPA 5.18.
1.610 LB 193.200 04011
120.00 07 ;4767 'ER70S3/.045 DIA WIRE, WELDING, CARBON, ER70S3
.121-02-00 .045 DIA, 25#, 10#, 2# SPOOLS t~~~~
CONFIRMATI ION TO CONTINUED |
NE
NO
Y hoNO
=
PURJCNA44NG O4PT.
__,_,___AMERICAN ALLOY STEEL, INC,
7721 PINEMONT INVOICE NO.
RO. BOX 40469 -. INVOICE DATE:
HOUSTON, TEXAS 77240-0469
(713) 462-8081
TELEX 76-2806 05265O
l 72)6S
TERMS: 1%-15 days-NET 30 DAYS

SOLD TO: EHE.Y STEEL r SUPPLY COMIPANY SHIPPED TO: SAME (313-3774.! )
2715 PALO A, ITYE
AUK194 HILLS, MlCHtJM U62S7 327 D}IV.
33340

VIA: AIR EXPKRSS -COLECT

PACKING LIST
RUSH SHIPMENTS - OUR
THIS IS A PACKiNG SUP - NOT AN INVOICE
SPECIALTY AROUND THE CLOCK.
marathon 6% Letourneau compang
Testing Ltaboratory DEGIHAL FLE COJ
h ,-o
reA C~
peport of CHEMICAL °nd eYSCA TESTS
and PHYSICAL ~.. .................
ESTSoof.......STEEL....... .... "....." Dote,
Mll O .e 9-36 . . .......
.72 . 1 1.9
.D) NOT REMOVE
Mill Order No....4! .. ...............
Shipped To ... 7N = CA.. U A . TM. ;RC ............... ...............
AMEB1CAN ALLOY
Custoer's Orde N. 12505 ..
PLATE4~
2". Gage_.
CHEMICAL ANALYSIS __ Yzeld j
16
M.LS S61, Sp- C". M.". 1 30p6. Ph".. SWL . Pe.6 3w.gA '*, .t SIZI Of PLATT
.
HH. F./Lb.. P.L 1. P.j . 0. T.u"

21629 A323 SA302B .18 1.15 .016 .013 .26 .55 77,500 97,500 19.0 7 1/4 X 106 X 106

S-4 79,500 100.000 19.0 _

Norm. @ 17000F for I hr. per Jnch of thickiTss ta. an qtj11 ir cool-d.

_with 9-1 additiln tnrigr tt ulta qnni -ally I -pmct er = 'AL77.2.


T-e_-1

,r.n inns

TEST iEPORTAPP OVEDODE . I IA.._?_____I___,


ASST QUALITY CC TROL RECTOR u_
I

C4Z~id a ime copy.

I Hereby Certify that the Above Tests Are Correct to the best of My Knowledge .AMCAR ALLOY STEI
and Belief.

martho-&Leoueau~
~I4U. U3.L

3:C A *Ir X D: k4
ENERG STEE an%'
. ++
. + ++
++ CERTIFICAT O + * CERTIFICATION OF COMPLIANCE +
.......... 4. .4 4.4.4
..... .+ . 4 ...

Auburn Hill, M

WELDING SERVICES
MANUFACTURING DIVISION
3276 MARJAN DRIVE
ATLANTA, GA 30340

Your Order Number Our Order Number Date

207866 WELSEO04377 01 4/21/69

Item# Prod# Qty Deacription Grade-Spec. Heat Number


------------------------------------------------------------------------------
a, I. C0050 I PLATE 7-1/4X12X30 ASME SA302 GB 21629

'K -.

This is to certify that the material furnished for your order and described
'I
KS...
above, has been reviewed and complies to requirements of the applicable
material pecifications, and meets all requirements of your purchase order.

Energy Steel & Supply Co.

Quo ity Ajsurance.Specialist

I,'.~

1,.
*I
#
PURCHASE ORDER NO.
Welding Services Inc. Mfg. Div. [ o&' 7c%(e
3276 Ma&a Ot
Welding Services Inc.
AUda*. 0'gw 30340
Tea.an (404)452-O0S [] Accounts Pwymabe
(404)46&O

)90
ENERGY STEEL &.SUPPLY CO. S
H WELDING SERVICES, INC.
SHIPPING & RECEIEVING
2715 PALDEN DRIVE P 3202 HARJAN DRIVE
AUBURN HILLS,
ATLANTA, GEORGIA
MICHIGAN
48057-0000
L 30340-0000

..E TERMS FOB./SHIP VIA


INDIAN POINT II/CON ED. 13735
I NET 30 DAYS SPAIR BEST
SPECNENOOR DESCRIPTION PRICE UNIT
I EXT.
fl'v'-
-.----
ITY
WHSE
1WHSE1P
P
II *tJL ULJtJr No.
WSI ~FGy~J
WSIMFGPARTNO.
G/L %Xw-
OAO~ M %
LOU.L L3
I
3,900.000 SEA 3,900.000 69041-1-1
.. 00 :15
401-01-00
ISA302/GR.B
I PLATE,
SA302/GR B STEEL
7-1/4" X 12"
X 30".
.000 .000 69041-1-1
;Q.A. APPROV AL Q.A. APPROVAL Q.A. APP VAL/ ATE, L-2-L.
.00 15 ,
400-02-00 SIGNEDs - ,".
.000 .000 69041-1-1
CERTS/TEST REP. CERTS/TEST REP. CERTS/HATERIAe TEST REPORTS
.00 1I5
400-02-00 REQUIRED

IT,.A-- . ]1.. 3,900.0001 1


I NO y~p I NO I L J, a

EMING
i
rURKHALTER"
-
I I I PURCHASING 09PT.
AMERICAN ALLOY STEEL, INC.
7721 PINEMONT INVOICE NO.
P.O. BOX 40469 -.
INVOICE DATE:
HOUSTON, TEXAS 77240-0469
(713) 462-8081
TELEX 76-2806 04521550
S/ 7i 6S
TERMS: 1%-15 days-NET 30 DAYS
SOLD TO: E nE.GY STEEL Z SPPtY COMAIAW SHIPPED TO: SAME (313 3774.)
ins PL.otA mIUVE le VLDVMU SERVICES. 13C.
AUB094 lUILLS. M4C)IJGMk 4M5S7 W.7MRJ.
DIV.
3276 MIRJAXI OUR'. ATLA.%TA* GEORGIA
_333A0
VIA: Atl EVMSS -CL.ECT

RUSH SHIPMENTS - OUR PACKING LIST


SPECIALTY AROUND THE CLOCK. THIS IS A PACKING SLIP - NOT AN INVOICE
RECEIVING INSPECTION REPORT

INFORMATION
MANUFACTURER
P.O. NUMBER
VENDOR
MATERIAL
HEAT NUMBER
MATERIAL MILL TEST REPORT
LENGTH
WIDTH
NOMINAL DIAMETER
DIAMETER CHECK
IWSJ . I "-3HP . ...

,,t , ? .. s * ....

, ~ e tibJ ---

1.5

........
. ... . . . . -___.
. ... ___

...-...
- - -:; --..... -. .- . _ _ I-P ...
OPERATOR LOG
WELD NUBER LAYER NUMBER

OPERATOR LAYER PASS# START STOP NOTES I of

90)

( lk. AhM ___ Av 4______0__

-y

3 f ",M 7;3l 11
i

_-T ,0 " 7' r,;2 Al 7' eC

'TO
A A)) __ 2

5~~~
14A0 .,.. , 6~-e
u, 2;
fie75 I
: /iU 7/Q16A,
-
2 ____lO 79, /I:IIgf i~
t
( 110 "
_

5~ ~ 2/6
~ - ~16:&,7,4 7~7
,,,.s I~//1e9o
// ol I9!:1 : //: I~7~t~t~O7t
. .

/1. A !60/
5 ,s{'~1 e,-~no ~
OPERATOR LOG
WELD NUMBER
LAYER NUMBER
OPERATOR LAYER PASS# START STOP NOTES I, o+ 3

S5. 4,iir,--,,o _ __ ___ /2i "33/ '¢


/ .60
__ __5./, _9 - __ / '5 /."2 63

_ t - .2 &2 __/. _ /7
I, 62d_
- *- //e p WcbJ't IlI

__
_ _ _ _ _ .__
_
o,~ 2:2 A) , /,'2
3.nO
/ .M
w' __,_.,_,__._.

__, ____ = 4>:c/cS.t ___.'_ _ _ _ _ _ _ _

/' ( A _ _ _ _ _ _ _ _ _ _ I_

14 .5 ~o 5.S MONSOON
__

I\ C A)

c{\ \K~~ '4


1L6)s5 7; o
OPERATOR LOG

WELD NU ERLAYER NTUMBER

OPERATOR LAYER PASS# START STOP NOTES O- 3


OiC
6.

___I 0 CI

_ Y,, \K;,c -S
dbfd
9.. ____ o ,. ,' _ __ _ __ _

___I __

_______,,., _ _ _ _ _ O\As5
a3I o._ ___ __

_
SK~Yrrv~ _ _ _ _ _ _ _ _ _ __ _ _

mo
I _ _ _ _ _ _ _ _
OPERATOR LOG
WELD NUIER_
LAYER NJMBER
OPERATOR LAYER PIASS# START STOP NOTES

C4 I2 _ I_ 7 _ _ _ ~ F fp

rq \A
-- IL

- _____ ____s 1:o50


Cy Y ) _ !JS1 _ _ _ _ _ _ _

,m _4 - 6oc __ ______

\s\ ___ ,/ ,_,L%1


IVA e/7_ 7 Lj
751______ i __ 1

_ _ _ _ _ _ _ _ _ _ _ _ z 3 0 1
4)Q ____

,c11\& 6R e76____ ii 9 o .

_§- /IA 1A,,. 3 --


/,.'4/ 'S.o-7 I_ _ _

5"//(i ,m ,, in/j7 /d 2 /___,'__

/@p . ____ L L /0 :4,,'S //i.'o)i _ _ _ _ _ _

I A d/ " n 7 _ _ _ _ _ l/1/~

x 3
OPERATOR LOG
WELD NUBERL d, ,/ LAYER NUMBER 3
OPERATOR LAYER PASS# START STOP NOTES

_ ._
_- _ _ _ __ 3 _ _ _ _ 6~:'od ~1 -"

,k.
i %Z:A,,
r/ 3 -/7 <4 _ __._ .
I~c~i~,
_._

,. 37 __" _ ,___ , __
_7

D134
_l?. L-1 715 _-_4

J ,r[A /,
u'd _ _ __.I /_ _ _ _ _ _ _ _ __q

X! i'b s '7_7 ____ 0(__ __-__,"__


X t 3 oA kA _ _ _ _ _ _ _ _ _ _ _ _ q_ _ _ _ _ _

_l,f? 4sA f4
1 !

K _ _ A _ 17 --.7
OPERATOR LOG
WELD NUMBER/, fcv, 7- LAYER NUJMBER J
OPERATOR LAYER PASS# START STOP
NOTES /6V'/o.
K /2 ,hAs/ 7 ~ ____ -o ? .'

*4i f.,/As 4 . l a :f / .L
? .L __ __ _ __

I-I
OPERATOR LOG
WELD NU9E N LAYER NUMBER_____
OPERATOR

< c_.
LAYER PASS# START STOP NOTES ' O'

IL ______ ____o

(.0x 17 o '

_ _ _ _ _ _ _ _ _ _ _ _ _ _ _
Z_
)Kt e-6O
4I
-5 O

koi

6D(.,
K

III

y f ro/.1
tv9 d
OPERATOR LOG
~'4
WELDNURERTA/>A ~LAYER 7 NUMBER
OPERATOR LAYER PASS# START STOP NOTES 11o 7

_0_7 ex 33.17 7
2-1l~ u-/ -- -°'1
67/Td,---

76

_r " _ _ _ _ _ _ _ _i

I'/. 00 0~

-70 170

_I__ _l__ I_
_-_i_ _ /3/ I I5 _ _,__ _ _ _ _ _ _ __ ,

! i i o-ojo
0,- )L/o

j0 _5-_4 oI.,H "_._,_

i - oi 4.,1 1, 17",-)
S I r
.177(o *1
170

_ _ _D_ _ _ _ _ _
_ _ now]__
(0- iq.
p PA r,,, F~O Win'
OPERATOR LOG
WELD NUMBER
LAYER NUMBER
OPERATOR LAYER PASS# START STOP NOTES

9 9,L
0i

1 L _ __ I 1__

i Jsl

C :S I ?- I -9

| IMONO
OPERATOR LOG
WELD NUMBER LAYER NUMBER

OPERATOR LAYER PASS# START STOP NOTES

__ -/__ .-
__. 3- /2%, d /€o3i: ____ ____
/ I l P7 I -.

____/_,_,. ___ / /5 J*?ec<(


/f,,,

:' /glA',/ 1 3- /z13 7 I

2 Ile

//".
6V-/
¢,,o.. :.or .>.o. S<.Wq
_ ._ -,,,, -.
_,_, _ _ _ Vi2:/. 'ape
_ _ _ _ _ _

2~e'
J427O A1 '1 6:i :
KY' ,U, _-_ __- <__' _ _ _, _ _ _ _ _ _ _ _ _ _

M ILvv I I__ _

mT I -I+Cd V q-V.1.L\ cjj~


OPERATOR LOG
WELD NUBERT#/)/.
LAYER NUMB ERL2
OPERATOR LAYER PASS# START STOP NOTES CC ,

SK. /YCA, S F . .
9,t.7 c7'f,7
_,__-__,____

114. _

K, 4S -L /(2' , '7 /A~' _______

_ K . Oa g~ A.- 7 1_ _ _

oli
_ _ __1,'_ _ _ _ _

Kt c ,Ar % _ _ ;_ _ _l _ _ __,_ _ _

_AK 6134 1L 1 I.,'


==/_ ,_

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_K, &,6A'-A -JecA4j 0,4,'

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_ _ _ _ _ _

_ )4" C?--
o~k4J4
I? 5-..ol .1
/.

1< /3(4454 ¢(<-"p Y4cil ~9~W&~ ~J~A 4 ~


OPERATOR LOG
WELD NUfIBER LAYER NUBER

OPERATOR LAYER PASS# START STOP NOTES

rf J _ _ _ _II__ _ _ _

, _ _ _. 6 _ _ .,...,,..,
435 5Y"
---- _
__I
_ " _ o___ ..
_ oL~soL

( \M,\uJ
d, r,, ___ \Z,< 7 IC3: l/ __ __

Th ld - -~~C',
___ _ ___ g-o, ,,
I_____.___ ____ _

p Aqe1,-,, 44 1 64 L: /C 00
OPERATOR.LOG
WELD NUBER
LAYER NUMBER
OPERATOR LAYER PASS(# START STOP NOTES

.. 7:'-7. _ ¢ _ __ _
q-70

p• _ i _ _ __ i_ _ _ __

:~~ I ~ i ~-- l4!y, o: .a,,,

'q,aw'
Y3
aI1
PCa
_ __ __ __ _ _ _ _-__ _ 95 _ _ _ _ _-_

-r
Z I _ _ __
_ _ _ _ _ _ _ __:_
__
_,-

A
a'.1

2.~og -04 __.o_ 3


_ _ _ 00
mam

Q? - A (15 Thr ,<'q*7 11,160


>90X
OPERATOR LOG
...."-ELD NUMBER
LAYER NUMBER

S OPERATOR LAYER

_,-/_//__7__
PASS# START
r.oAJ
STOP
/_'_"/_--
, _
NOTES
_ _ _ _ _ ,

.1o

- ._ _ cIQ __ ___ I__

s-a~

_ _ _(
i ni , I__
n ('I_
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_ _ _ _ _
_ _ _
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60'.:

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""9
OPERATOR LOG
WELD NUFIBER
LAYER NUMBER
OPERATOR LAYER PASS# START STOP NOTES

_______ __ &~A 7:o7 ac __ _ _

71 ti
page .Of /
APPLIED TECHNICAL SERVICES, Rer.
Blanch 0101.
INCORPORATED t ofnv:
Mdi Ole*
1213 Onoalds" Road Branh ONl.
1190 Atlanta Induetlal Olve
Oreonyl. Bouth Calritna 2960 10'-A Cattl I..lv*
Modetta, OeoIai 3006
(803) 290-0525
404) 423,"1400
Madison, Alablr~m 357H
(255) 77
Purchase Order #" 75 _.
FA (4TI44 GN PAR24-64TI
MAGNETIC PARTICLE
INSPECTION REPORT
MATERIAL: 5+ea / f. 3
PART SIZE: 30" )

. .
Specification(s) INSPECTION PROCEDURE
"' :I I ' '& 2 .0 0 ( "5 0

l - 15 y
WET.. M.T~
r.hi
..E.....
0~ 1 .I1iC ...
M.T. EQUIP. IAA\c
'"'" "
PARTICLE MFG. Af
j DA 0O
o RECTIFIED " .
.
PARTICLE BATCH NO.3c3+e[
iMC
PARTICLE COLOR Re .
..... , ..PROD.SPACING
o CENTRAL CON. (AMPS) All
" AMPERAGE
o HEAD (AMPS) 1\'l,..
METER CAL DATE "
0 COIL (AMPS) . "
o DEM AG _ _ _._.. .__
__ _
YOKE CAL DATE.
...
'.

INSPECTION RESULTS "".


IDENTIFICATION
ACCEPT REJECT QUANTITY
REMARKS
-- ---------
" :I Jc '~ -GT'" h
C. C.

Ae Irrl

A-2-88
Client Inspection Performed By:
Approval
APPLIED TECHNICAL SERVICES, INCORPORATED Page.L.. of L...
Branch 0111ce Main Of fice
Ref. J.)
1218 Donaldson Rload 1190 Atlanta Industrial Dr.
Branch Office P.O. No. 2 )
Greenvil. South Carolina 29605 Mahietta. Georgia 30086 108-A Castle Drive 5*9
(803) 298-0525 (404) 423-1400
Madison. Alabama 35758 Date '
(205) 837.7777
Fa 44US.RADIOGRAPHIC
INSPECTION REPORT
- '-
Part No.: - M'
Part Name: ,Q'~
PJ ~~F r
Material:
_j T yp e wkn '*5.
v * T
llcdi:
Radiographic Inspection Technique..
Specification (s) T\S\T AV Set-Up
Isotope 560". tT)7~~
C (,tN. Film Size IA-
Curies
X1C7'
__ _ __

KV
_ __ _ __ _ _ irFilmType irt .'
t4______________
A Sensitivity,. 9- - F~ CV.Cl
MA N i ~ n' if
'Penetrameter 16
Time ,;s(;.Shim (s)
',FD
..... Develop:Temp:QJi~o~c Time:*
zOD775" Screen(s)'61 '~.......
ource Size (Physical) -A 11 -....Effective
Geometric Unsharpness Ug =Fd/D 6......

INTERPRETATION " I:.s.

N01'1
0
PART I.D./
,I 5.5y 1.
FILM VIEW.~''. *

REMARKS.

8. r

LL),
0

5 s, '~ Irs I~sC.' *.

A-6-88 NcTL SU1b C> 1 L/1\L1-1 VI tkLQ

Client ~ 10I-IL *lCU


TO tirOMERadiographec(s).
.u

Approval
Level . -T R.T.
Interpreter: ...
_______ I Ti:
___ Pag e _ of
APPLIED TECHNICAL SERVICES, INCORPORATED
Branch Office
IN
P R
O T DPurchasePe
Main Office
Order #t ,O 75-9.._ L
1218 Donaldson Road 110 Atlanta Induafdal Drve Branch Ohioe
Oreenville, Sourn Carolina 29s05
Mraeta, Georgia 30064
109-A Castle ,.o
Ma'ison, Alabama 35754
Date _ 5 -
(903) 29.525 F (404) 423-1400 (205) $37-77
FAX 0 (404) 424-6415

ULTRASONIC INSPECTION REPORT


WI- )l~l Ve_ . jvn. -MATERIAL: ST L / P-5

L_ _j
INSPECTION PROCEDURE
Specification(s): A 5SM, E Se
& z_ (-l i.E:T t L .- lAI A -ECT iL I T EL
ml, 5" . c . r?.c . 4x Dt--ro, ST'RA(&HT eC-At,, ,4-,'
1o SHEAR 0 SURFACE 9 CONTACT TRANSDUCER FREQUENCY-
O'LONGITUDINAL Z,,1,,
0 THICKNESS 0 IMMERSION
n SKETCH ATTACHED
TRANSDUCERSIZE v? " LA
TRANSDUCERANGLE 'AAIG w
SCANN ING METHOD HM %L REFERENCE STD.:'S/N Ao>,J4>Z,
SURFACE CONDITION SHoP-r " MATERIAL SIZE: THICK./DIA. SO
U.T. EQUIPMENT lo~?RTC/DT11 12-" ' "
,/M~ ZCOUPLANT/BATCH NO.
TRANSDUCER: MFG. S/N IHAJR l.,OJ 'L1LT1\.kL
C--
e- 2O-0 DAC METHOD oi45"...aaeni
:)
INSPECTION RESULTS
IDENTIFICATION ACCEPT REJECT INDICATION REFERENCE
LEVEL LEVEL REMARKS
_MULT
A _ !LId R ,ik zIgoks f?&j 2.:
.ro o
• .t•
; - ;; •! " ..
, - ..t.

SKETCH AND TECHNIQUE DESCRIPTION:


TY-?, IscL. LC ,? TbP. i r

0 a rAl~a

A-3
THICKNESS MEASUREMENTS tj /A.
MIN. THICKNESS REQUIRED
ACCEPT 0 .
MIN. THICKNESS RECORDED
REJECT

Client Inspection Performed By:


Approval Level .U.T.
Level . U.T.
I

PREPARED BY I
Applied Technical t ,
CHECKED Services, Inc. 2 - CF
PAOr

DATE 9
APPROVED TITLE A5 /8
IMDICATION MAP FOR. -T.AIC-HT LS'A4 £c.AdJ

7"

+ 2+ 44-<4-o 7+ 8+ 9+ 10+

'5

1'~ J]'2T HOLE


.. _
"r " W.. -- 7. , -.'1'_ ,.
-.
,.~ 2o. V -, - - ,-

IN4DIaio)w No. %DAC DEPTH4 INC)CtwioN No. %DA_ DEPTH


2 7o
'2
>100 ,

>/00

7
0 70
'/0
.,.10

---------.
PRCPARro oy

R..2rE, IrsrtL~ Applied Technical .. r

°,,o,,o Services, Inc. ... .


.... r.=
4 IA&
,T..5-
t I DSATC
S-8'7
j. I-LLf= j .A .C . ? I ST.-SETTING5 FOR .TRAIC Ir IW-AIr - -
A O -o
I -
(- o
Rc
3 qT
9
0.
-

joI-

0 1 2 3 1- " 6 7 8 10

/-TI00 e1 tI lb
'T 105
DELAY CAL1e6. 217
4T. 2.5 C'(o d-b RANGE CAL18, 17
3/ r 2! RANJ&E 10
DELAY

RE2EC.
AuEE LEVffL : to cjb
FIL'rER.
-CAJING LEVEL db PREM.
TEt4 P.
DZ13. FiN-E

DAMP.
Rep. RATE HIGH
.
Page - oft
APPLIED TECHNICAL SERVICES, INCORPORATED Ref. A o-02,a>94
Purchase Order # 207-592l
1190 Atlanta Industial Drivg Branch0111cs
M1 l,0 Geo.
(0III), '. gi 300,.6
(404) 42orgia
423-140020066
L"enhardl Road
Piedmont, South Catolina 29473 Date
(0)2902
Fax 6 (404) 424-6415 (03) 29"525

ULTRASONIC INSPECTION REPORT


F- WELc -E1IF-a cM.-'ll_. MATERIAL: STEL / P

L .
INSPECTION PROCEDURE
Specification(s): ,NtE._EC.TjO& 1 ART..L E 5 A/R IAv\A AsmF- E-.io,,4 TJ
M83303. DAc0. FReQ. 4- DIEC-bILPJS -QrP.A1GH- BEAM I :6
91 SHEAR 0 SURFACE [] CONTACT TRANSDUCER FREQUENCY - ___.2.
o LONGITUDINAL _
0 THICKNESS 03 IMMERSION TRANSDUCER SIZE 9-8
o1 SKETCH ATTACHED
TRANSDUCER ANGLE 450
SCANNING METHOD MANLAL REFERENCE STD.: S/N Ao3NI'_ 7_
SURFACE CONDITION SMOOTH MATERIAL SIZE: THICK./DIA.OO*x 12x "7
U.T. EQUIPMENT ,r
JoRTEC. t, DT I1I 4JS-P? COUPLANT/BATCH NO. ULTRA&EL
TRANSDUCER: MFG. S/N )'oAE1rOc. .J S15Z/21
DAC METHOD 00 S .R JE
INSPECTION RESULTS
IDENTIFICATION ACCEPT REJECT SINDICATION
LEVEL REFERENCE
LEVEL REMARKS

H"Lrel~
-E ?~cv- I L2Ot
t~ J L EVEbOL - LEVE A*R 7o
DAC.

SKETCH AND TECHNIQUE


DESCRIPTION: ,

WELDC
J' PLAT-_.JTop v Evw sJ
1 1000).
A-3
THICKNESS MEASUREMENTS iJ/A
MIN. THICKNESS REQUIRED
ACCEPT 0]
MIN. THICKNESS RECORDED__
REJECT

Client Inspection Performed By:


Approval ' "Level U.T.
-_Level JL.U.T.
PREPARED BY

,/r

'I
' ...
.. . .

TL+ 6+
9+0+ J-- /Z+ /,+

V
2'4
2L
' -''21
Y9t
.T HOLE
b
."
...
:;"...
-- ......
.'x--.--.--.--
..
:7 - -,;,,. _28, '

INDIATIb)j Nio. % DAC DEPTii N) INDICATION No. % DAC. DEPTH


2.'/5"
2o
,/o
J3 2.945
5-0 /28
410 3 .,_

7
70 ', y
_l0
9
5o0
/
--
--
1.2 90
-I

MoPmtrrEor.APARif rr
F
it-li,--, j
kiDICATIO .
PR EPARE
A Y
EA
F?Et<oL<riony Applied Technical
Services, (0 aF J!
Inc. DATE

.J.J-^i-LL-S
APPROVED
.A.G. IMT.SETTING5 FoR 45 REPORT NO.

A 0 -oM4-
0

0 1 2 4r
3 5 6 7 8 7 10

'/4T 80 e Lb DELAY ('ALI6 . :O120


RAMGE CALIS :7?_.
V. T S0
P ANG E
3 /4T 26 DELAY
:0

RE7ECrT
REr-ertJCE LEVEL 55%Ilb
&c" db FILTER
-CAIN& LeVEL 71 A :5
rREA.
TEI P.
74"*
FNE
D01. COARSE
: 50
DAM P. OFF
R'p. RATE HIGH
Page 7 of
o_ L
i--i ""Ref. A O "O,_,% k
APPLIED TECHNICAL SERVICES, INCORPORATED Purchase Order #
Branch Offie
7-To
Q-0
Man Office
1216 Donaldson RoW Branh OfP
Ofeenvlila South Carolina 296N
(1031 290-O625
1190 Atlanta indutia Driv
MadoeLa, Georgia 30004
105-A Castle Drive
Madison, AJabalrm 3$75@
Date aee
5 '
(404) 423-1400 (205) $37-77r7
((404) 424-64111

F-- w c " SV e ULTRASONIC INSPECTION REPORT


. ,.lI..
MATERIAL: -.TiEL I P-3

L I
INSPECTION PROCEDURE
Specification(s): A-Er ..5E'TIOl =i A e-.LSe. AlI? I' At, SE:-"---_.rlCM 2l1 .
)J, .5-3 0 . )Ae. IR:. 4" DIRTIOkc iG.- TRAI&--A M-.9 -F- t:oo
W3SHEAR 0 SURFACE' 2CONTACT TRANSDUCER FREQUENCY '.25
O LONGITUDINAL 0 THICKNESS 0 IMMERSION. TRANSDUCER SIZE " "5/&,'
o SKETCH ATTACHED TRANSDUCER ANGLE
SCANNING METHOD M U,ALt'' REFERENCE STD.: S/N LAO'.J 5*1Z
SURFACE CONDITION SM2ooT MATERIAL SIZE: THICK./DIA. 20S(/Z C 7Y " T
U.T. EQUIPMENT JCrQo.T--_- I515/1 1A 419 COIUPLANT/BATCH NO. ULTPA&EL
TRANSDUCER: MFG. S/N 1 IS/14 (3Z,
-)-ZI
I DAC METHOD OK E 04--E
'
INSPECTION RESULTS .
IDENTIFICATION INDICATION REFERENCE
ACCEPT REJECT LEVEL LEVEL. REMARKS

' ". - 'I ' . ,. . ." * *"" . . . ..

- ,.. QA C

SKETCH AND TECHNIQUE DESCRIPTION: 5 4 -


" j ,)
•k cTc '4.

A-3
THICKNESS MEASUREMENTS M/A

MIN. THICKNESS REQUIRED ------------ ACCEPT 0


MIN. THICKNESS RECORDED
REJECT 0

Client Inspection Performed By:


Approval
_
10J. Lv
1ILLS Level1Z U
U.T.
P~p . y Applied Technical
Services, Inc.
HEC.KE
, DATE

APPROVED TITLE
RrPORT NO.
J. [AIILLS I.MDICATION MAP FoR * (oO .- 5ciA Ao)-o394

..... 7+ AI
T.
' Y!+ -I
J /3--
/S 1+17+ /8+ 1H +

B oz
T
V2m OLE
k- ~ ... ....
2'
................
... .........
'
"..
.. ... ..... . ...z

IIDILTILNhJ N.o, % DAC. DEPT


..1.
... .... 2 0 INDICATION No. r%DAC_ DEPTH
2 2 /00 /.20
2.6? 17 0.30
lb
40
o o./5o
!-._ _ -79
-J .. .__
1./0
9
r
lq

z
(A
0
z . ...... . -.. .... . _. -
2.29
C)
m

1"o
0
* 11 -/o 1.30
1/2. /00
0.z-x-.
in

_____ /00 0.55


. .3_
.._...
25 .....IO
.. ,.
/00

J.
L
...... ......Applied
rF__r i '0M.L
L2.' Technical
Services, Inc. ,OF DATE
9

APPROVED T LPORT NT.

J. RILLS .A.C. i IWlST..SETTING.5 FOR (O°.-tAR WAVE AO-O)394-

oH

_L I , I I,, I I ! I I. I
0 1 2 3 j- S.* 7 8 9 10)

/4- T RD e a~7b DELAY CALIM .

/2T 25 RA.mrGE CAL18,


Co- 657 d-6 TT4.
R.AN& E
/T io e 0 db DELAY :60
RE7ECr
r-rpjCi LEVEL : 67 b
FjorT
"CAMING LEVEL • 7 db
. TEMP. :7
13. FINE (D&O
DIAM P.
Hico)F
REP. RATE
Consulting Metallurgical
\"A&.4

April 27, 1989

Welding Services Inc.


3276 Marjan Drive CMS 405-89
Atlanta, Georgia 30340
Attn: Mr. Steve Burkhalter

Subject: Microhardness Testing of Various


Welds Involved
in Temper Bead Pass Welding.
Dear Steve:
At your request we have performed
microhardness surveys
through the HAZ of various weld samples
welded with different parameters that you had
in order to determine
the required technique for proper
temper bead welding
of SA 302 grade A with ER 805-D2
filler metal.
We used a Knoop indenter with a 500
gram load, observed
at 200 x magnification, in locations
A, B, C, and D
as shown in the attached sketch.
In addition we performed microhardness
A, B, and C on P-2 and P-6 single surveys in locations
bead
order to determine the highest hardness weldments in
the HAZ without tempering. produced in

Photomacrographs and photomicrographs


of the areas that
you requested are enclosed.

Respectfully submitted,

William .Jo es III


Consultin tallurgical Services

WFJilc

1700 CUMBERLAND POINT DRIVE, SUITE


10, MARIETTA, GA 30067* (404)
952-0038
Fax. (404)955-7310
I
/
A.
Id4A

~s j

.,

*,,* ~.

~ '~lA * ~

[',1.,' ~' I
1
* . *** L****~*
* I g~ '~~'

*~ .~r4 ..1. I
t~I L~,

* * *.J

~ I&*t

* *. . *,.i I

* *1'~*
* ~AIt~ f
A ~- I- I
Sketch .of.Microhardness Survey
and Sample'.Locations. * ~ I

5*

U.

'I
P-2 Single Bead Weld

High Hardness

A - -t.25oo0
KHN Rc (cony.)
49.0
P6 - Si-gle Bead Weld

A
Distance from Filars KHN500 Fila :s
KHN500 Filars
fusion KHN500
-5 00
0.005" 255 495

.1
0.015" 257 486
0.025" 255 495
__________
0.045" 248 525
_____

0.065"

0.085"
252

254
508

500
I
__
___
I
0.105" 254 500
I _______________________________________

_ _ _ _ _ _
I -_

High Hardness

A - KHN Rc (cony.)
2500 49.0
P-6 -Weld

A
.Distance from
,,.urface Filars KHN500 Filars KHN 500 Filars
I KHN50
0.005"
328 299
0.025" 269
348
0.045 "
350 26
0. 065"
354 256
0. 085"
373 231 I
0.1651f 4
358 251
r t
0. 145"1
365 241
0.185'"
368 237
0. 225"
354 256
0.265"1
358 251
0.345 "
248
360

High Hardness
A - KHN
f-9500 Rc (cony.)
28.3
P-2 SINGLE BEAD

High Hardness

A- KHN Rc (cony.)
492 46.8

B - KHN Rc (cony.)
508 47.9

C - KHN Rc (cony.)
525 49.0
P- 6 SINGLE BEAD

Base Metal 367 239

HIGH HARDNESS

A - KHN Rc(conv.)
512 48.1
B - KHN Rc(conv.)
473 45.4
C - KHN Rc(conv.)
459 44.5
P-6 A

Distance
Inches
Filars KHN Filars KHN Filars KHN500 Filars KN0
.002 312 331 320 315 325 304 315 324
.004 304 348 310 335 326 303 298 363
.012 304 348 328 298 320 315 295 370
.020 298 *363 305 346 325 304 313 328
.028 348 328 298 315 324
.036 305 346 315 324 328 298 320 315

.044 304 348 295 *370 351 262 328 298

.052 308 340 330 296 338 282 322 310

.060 304 348 332 292 323 308 313 328


.076 348 266 326 303 323 308 293 *380
.084 345 270 325 304 319 316 296 368
.108 343 273 314 326 329 297 310 335
.116 298 363 330 296 305 346
.132 295 370 320 315 310 335
.148 304 348 318 318 358 251
.164 304 348 314 *326
.180 306 344 325 304
.188 300 358 354 257

.196 'An A Base Metal High Hardness


323
M;L kL;UI1 I
363 36.3 326 32.0
B - KHN Rc(conv) D- KHN
.7
1* 7 A 1 - n' Q- -Rc (cony.)
P-I

Distance
Inches A B, C
P4 I 1 ~ ~
'.- -.
Filars KH__50 0 Filars
37
32•7 -500
302 KHN500 Filars KHN500
.002 304 349 298 II364
29 64 27 00
366
.004 37
325
25 3055 293
293 68 29 36 8
.012 318 319 298 363 A

310 1 Q
6
.020 02 354154 314 327 " A

I 310 34
q._ _ _ _

.028 324 308 319 317 " AQ


317 30 12 33
.036 32.0 316 296 368
qlQ
312
318 319Q
.044 327 36R
2302 296 327
33 296 302
3 368
325
.052 329 298 315
325 30 9 368 238
2
.060 314 327 271 qK '9" "7
345

4 f
271 67123
.076

.084
313
332
329
294
J376
I381
228 T 300 -5'
A
356 _25
38l __ _ _ _ -I.._ _ _ _ _ _ __ _ _ _ _ _ _ _ _

.108 374 231 355 256 • 9A9


256

Highest KHN 5 00 Rc(conv.)


A-354 35.3
B-375 37.5
C-368 36.8
D-368 36.8
P-2
Distance
Inches

Highest KHN 0 Rc (cony.)


50

A-361 36.1
B-371 37.1
C-430 42.3
D-366 36.6
P-3
Distance
Inches
Filars KHN00 Filars KHN 5 0 Filars KHN500 Filars KHN
5 -500 -H500
.002 342 276 318 319 345 271 318 319
.004 330 296 300 358 316 324 296 368
.012 335 238 315 326 315 326 299 361
.020 321 314 297 366 312 332 307 340
.028 320 315 313 329 312 332 318 319
.036 332 293 316 323 .308 340 304 349
.044 332 293 325 305 308 340 304 349
.052 331 295 310 336 305 347 298 364
•.060 325 305 304 349 302 354 293 375
.076 334 289 295 371 297 366 294 373
.084 333 291 297 366 300 358

.108 365 238 360 249 377 226

Highest KHN 5 0 0 Rc (conv.)

A-315 30.6

B-371 37.1

C-366 36.6

C-375 37.5
P-4
Distance
Inches
irH HNKHN s KHN Filars Filars KHN50
.002 351 262 316 324 305 347 315 325
.004 344 273 306 345 298 _ 364 325 305
.012 329 298 304 349 303 352 322 312
.020 1_325 305 321 313 302 355 310 336 A.
.028 334 289 318 319 318 319 320 315
.036 326 303 314 327 320 315 320_315
320 315
.044 328 300 318 319 303 352 315 325
.052 326 303 314 327 298 364 306 345
.060 326 303 304 349 306 345 298 364
.076 376 228 326 304 304 349 297 366
.084 378 226 356 254 335 288
*108 366 241 350 263 364 243

Highest KHN 5 0 0 Rc (cony.)

A-305 29.1

B-349 34.8

C-364 36.4

D-366 36.6
P-5
Distance
Inches A B , , C
Filars KHN500
Filars KHN5 Filars KHN500 Filars KHN500
.002 340 279 340 340 279
279 238
3408 238
.004 352 260 333 326 303 353
291
r I I
.012 348 266 340 326 303 344 27R
279
.020 3262303 344
348 266 324 2.7
347 268 307
.028 356 254 332 91
348 266 327 302 342 276
.036 276
346 269 273
329 298 326 303 342 2
.044 347 -268 336 286 334 289
338 282
.052 345 271 337 IQA
S 280 JUU 333 291
.060 348 I 266 33.
7 284 329 298 328 300.
.076 384 218 334 4289 326 303 330 296
.084 384 218 345 271 312 32
.108 365 242 -325

Highest KHN 5 0 0 Rc (cony.)


A-279 25.2
B-305 29.1

C-332 32.8
D-300 28.4
P-6
Distance
Inches
Filars KHN500 Filars KHN5 0 Filar -- KHN0 Filars KHN
-500 -H50.5
00
.002 347 268 338 282 336 286 338 282
.004 335 287 321 313 323 309 333 291
.012 345 271 331 294 323 309 322 312
.020 329 297 330 296 321 313 32i 312
.028 333 291 322 312 313 330 334 289
.036 336 286 329 298 309 338 348 266
.044 338 282 327 302 318 319 350 263
.052 335 287 337 284 322 312 342 276
.060 346 269 338 282 320 315 342 276
.076 350 263 340 279. 329 298 338 282
.084 356 254 318 319 335 287
.108 352 260 354 257 330 296

Highest KHN 5 0 0 Rc (cony.)


A-297 28.9
B-319 31.1
C-338 33.5
D-312 30.0
P-7

Distance
Inches
Filars
Fila KHN Filars KH NH5
50 0Flr H N500 Filars
Flr H
KHN500
.002 337 284 339 281 343 271 341 277
.004 362 246 337 284 334 289 322 312

.012 345 271 335 287 337 284 322 312

.020 351 261 322 312 328 300 327 302


.028 384 I 218 330 296 327 302 333 291
.036 325 306 337 284 340 279 339 281

.044 340 I 279 328 300 323 I 309 372 233


.052 327 302 335 287 323 I 309 499 139

.060 332 293 330 296 336 286 343 271

.076 328 300 337 284 344 272 350 263

.084 328 300 335 287 328 300

.108 351 261 322 312 388 214

Highest KHN 5 0 0 Rc (conv.)

A-302 28.5

B-311 30.0

C-309 29.7

D-311 30.0
P-8
Distance
Inches I-,
Filars KHN500 Filars KHN500 Filars KHN500 Filars KHN50

.002 308 340 359 250 389 213 346 269


.004 302 354 340 279 358 252 346 • 269

.012 312 332 337 284 349 264 341 277


.020 345 271 337 284 345 271 336 286

.028 356 254 334 289 343 274 327 301

.036 350 263 332 293 335 1 287 330 296

.044 356 254 315 326 333 291 335 287


.052 343 274 326 303 348 266 335 287
.060 366 241 329 298 340 279 338 283

.076 366 241 331 294 345 271 339 281

.084 367 239 330 .296 337 284

.108 394 230 327 302 335 287

Highest KHN 5 0 0 Rc (conv.)

A-354 38.1

B-326 32.0

C-291 27.1

D-301 28.5
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Relief Request 29

I. Request for Which Relief is Requested

(a) Name: Automatic Gas Tungsten Arc Welding


(GTAW) Temperbead Process
(b) Function: Facilitate repairs involving welding on ASME Section III
Class I Components
(c) ASME Section XI Code Case N-432,
Repair Welding Using Automatic or
Machine Gas Tungsten - Arc Welding
(GTAW) Temperbead technique Section
XI, Division 1.
2. Reference Code Requirements That Have
Been Determined to be Impractical
The Code case weld procedure qualification
required the test material
be of the same specification type,
grade, and class as the material to
be repaired. Indian Point 2 steam generators
requirements of ASME Section III 1965 were built to the
edition including addenda through
summer 1966. The steam generators
were fabricated from ASME Section
III SA 302 Grade B material which has
an impact value requirement of 30
ft-lbs absorbed energy (N-330). The
test specimen also used SA302
Grade B material and met the 1965
code edition of Section III impact
requirement of 30 ft-lbs. However,
the operative Section XI Code
edition is 1980; the corresponding ASME Section
imposes a 50 ft-lb requirement I1 (1980 edition)
from which relief is requested.
Achievement of this impact strength in a
thick test piece is
impractical.

3. Alternative proposal

It is proposed that Automatic Gas


Tungsten Arc Welding (GTAW)
Temperbead Process be accepted on
the premise that the qualification
procedure utilized test material
whose properties correspond to the
original code, ASME Section III, 1965
edition. Furthermore, the test
results verify that the impact strength
of the heat affected zone (HAZ)
of the base metal is enhanced, as
illustrated by the following test
results:

Weld Metal HAZ


(400F) (90°F) Base Metal
(90°F)

Ft-lbs 83 44 32
Lateral exp 65 39 31
Material records on file indicate
that the impact strength of the
material actually used in steam generator
construction corresponded to
values ranging from 55 ft-lbs to
105 ft-lbs. Based on the test
results, any repair using the GTAW
method should result in improved
values.
I

It is understood that the difficulties presented by Code Case N-432 are


acknowledged by ASME personnel and that
a Code change is currently
under way incorporating the current proposed
code modification for
Shielded Metal Arc Welding (SMAW). The proposed
changes in the code,
as presently stated for SMAW, and as
are to be proposed for GTAW,
include:
o The test assembly shall be of the same P
number and Group number
as the component and will be post weld heat
treated in a manner
which is similar to the component (on the
order of 80% of the heat
treatment time at temperature).
o The Charpy-v-notch impact requirements of
the test assembly shall
meet the following:
- The base metal impact properties shall meet the design
specification.
- The impact properties of the heat affected
zone shall be taken
at or below the lowest service temperature.
- The average of the three charpy-v-notch
heat affected zone
results shall be equal or greater than the
average of the three
base metal test results.
The results of the qualification process for the proposed GTAW in
general meet these requirements.

4. Basis for Requesting Relief


Consolidated Edison has developed a temperbead
program for the Indian Point Unit No. weld qualification
2 steam generator shell. The
shell material is Section III SA302 Grade
B low
by the ASME Code as P-3 Group 3 material.alloy steel, designated
The purpose of the
temperbead qualification is advance preparation
for performing a cavity
weld repair to one or more of the IP-2
steam generator shells using
this welding approach. ASME Code Case N-432,
issued on February 1986,
provided guidance for the temperbead qualification
activity. Both weld
parameter trial tests (on a thinner plate
of section II SA302 Grade B
material) and procedure qualification tests
(on a thicker plate) were
performed in order to select a weld procedure
Although the thicker plate was not entirely and then to qualify it.
representative in terms of
toughness, the results on the thinner
and thicker plates, taken
together, demonstrate that the procedure
is technically acceptable for
use on the 3.5 inch thick steam generator
shell at IP-2.
The properties of the base metal used in
the temperbead qualification
program did not meet all of the requirements
of Code Case N-432 and the
Code of repair. However, application of these requirements
case would be overly restrictive and unnecessary. in this
constructed to ASME Section 111, 1965 with The plant was
addenda through 1966, a Code
which prescribed less in the way of toughness
material than either the Code of repair or requirements for this
Code Case N-432. The intent
of Code Case N-432 is to assure that the weld
procedure is qualified as
a process on representative material which
provides assurance that the
welding process will not degrade the base metal. The HAZ
Charpy-v-notch energy absorbed and lateral
expansion were clearly
greater than those of the unaffected base
metal in this test program.
The 7.125 inch thick SA302B plate used
in this test program is
representative material in that section thickness.
of this material is its poor through thickness One characteristic
hardenability, thereby
resulting in plate which, in this thickness,
toughness in the 1/4t to 3/4t region. In reduced may have poor notch
section thicknesses,
this material is expected to have better toughness.

The steam generator shell at IP-2 is significantly


thick, and has superior Charpy-v-notch impact thinner, 3.5 inches
properties compared to
the test plate, as would be expected for
this grade
the test plate of a more representative thickness, of material. Were
the notch impact properties would have been it is believed that
significantly improved.
This observation is substantiated by the
weld trial tests in the
thinner plate, 2.25 inches thick, where hardness
measurements revealed
a softened HAZ consistent with increased toughness
material. The restrictions of code Case N-432 for a representative
required a thicker plate
than is to be welded to in the field,
thereby restricting the
qualification program to use of a base
metal which could not be
reasonably expected to meet the notch toughness
Code Case. Consequently, while all requirements requirements in the
could not be literally adhered to in this of Code Case N-432
instance, the trial weld
tests and the procedure qualification tests
taken together demonstrate
that the HAZ properties have not been degraded
in the SA302 Grade B
plate and that the temperbead process is technically
qualified for use
at IP-2.

Enclosed are records pertaining to the test plate.


RECEIVING INSPECTION REPORT.

JOB NUMBER ITEM(S)

INFORMATION ITEM 1 ITEM 2 ITEM 3 ITEM 4 ITEM 5


MANUFACTURER gno., .rUL__

P.O. NUMBER
VENDOR
MATERIAL AS _ ___"

HEAT NUMBER
MATERIAL MILL TEST REPORT Rma-v av "
LENGTH " " x 4"
WIDTH
NOMINAL DIAMETER
DIAMETERCHECK A
B
C
D
NOMINAL THICKNESS
THICKNESS 1
2
3
4
5
VISUAL INSPECTION
REMARKS

NCR#
DATE.
BY..__
RUSH SHIPMENTS - OUR, PACKING LIST
SPECIALTY AROUND THE CLOCK. THIS IS A PACKING SUP - NOT AN INVOICE
marathon Lttqtoumeau companU
Testing tabora.tory
am1NL .TIL Col
Report of CHEMICAl. and PHYSICAL TESTS f. S.. PLATE . . Dae 9 ....
3.. .86...
.. ... .. ........ ID NOT REMOVE

Sh;pp.d To ...NP' c&w. =t.


L.X. ;c.. ..... ......................... hull Ofjder No. .L.147221
. . . . . . .. *r.N.......................
. I1
c,,,.,', o, .. .. 12505 ..
AbfM~cA ALLOY
PLATE A.'1-54
2".Gage....
- - 1---- --r-- - E-ct ANALIII
1I
Y" 11- %
C",. *I~ I ~ ' 0- F.6f S--jA 26-V- 11-41 S- t Of PLIT!

21629 A323 SA302B .18 1.15 .016 .013 .26 .55 _ 7_7,500o 97.500 19.0 7 1/4 X 106 X 106
10
S-4 79,500 100,000 .0

°
Norm . 17000 for hr. n.er 1111 of thickiwig 0 tnn. an tj1j ir e-ol1 .. .'.

- - tint 9 11 w If,,
-wt -- I±*r
AAJLt 4n~ ln tpt -11I A& mniS
2j -'y j x-- 2 r

_ _ ._ I _..... __.

0D

00
-. ASST QUALITY CCITROL WRECTOR _

- ______ I --.....
1 .'
-htt A_ - A--
cagnru~oafe 1m.
a 7
a.orrocl Io iris boil of. My Kno-Iod
and- Belief. AaWGECANI ALLoy SM
rm'thonA Labw.oumew
*m**. a e.***** lob . *N. .1**wu
ROO ,e m . . * .
40 : . Eb

+ CERTIFICAT '-01 CERTIFICATION OF COMPLIANCE


ENERGY STEEL an
2715 Peidan
Auburn Hills, I

WELDING SERVICES
MANUFACTURING DIVISION
3276 MARJAN DRIVE
ATLANTA, GA 30340

Your Order Number Our Order Number Date


207866 . WELSEO04377 01 4/21/89

ItamN Prod# Oty Deacription Grade-Spec. Heat Number


----------------------------------------------------------------------------- --------
w' 1 C0050. 1 PLATE 7-1/4X12X30 ASME 5A302 GB 21629

•fhia in to Certify
that the material furnished for your order end decribed
L..above, hae been reviewed and complica to requirements o'f the applicabla
...material apecifications, and meets all requirements of your purchase order.

>>> En.ergy Steel & Supply Co.

I Vtu;EtyAurance Specialit

. 'e

rde %J C
#
190
Welding Services Inc. Mfg. Div. I
2276 Uw)-n Dift
Welding
AM. .Gw.0 4dO
T.I.c, +.Services Inc.
(404) DS2-DW
ONw
A3.'o Py
(4) 4 40m 0
PURCHASE ORDER NO.

ENERGY STEEL &.SUPPLY CO. S WELDING SERVICES, INC.


2715 PALDEN DRIVE S SHIPPING & RECEIEVING
AUBURN HILLS, 3202 MARJAN DRIVE
MICHIGAN ATLANTA, GEORGIA
48e57-0000 L 30340-0000
.J
E TERMS I F.O.B.. SHIP VIA *: -. XABL

NET 30 DAYS S/P AIR BEST INDIAN POINT II/CON ED. ' 13735
IY. WSI MFG PART NO.
,--'--1°" SPECENDOR DESCRIPTION PRICE 'NI"
. PART NOD,2/ R PTEL 3,Ie UNT ET.
.so .15 SA302/GR.D SA302/GR 9 STEEL I3,900.0e EA 3,90000O69041-1-1
i 1401-01-00 PLATE, 7-1/4" ,
X 30'.
12

.15 iQ.A. APPROVAL Q.A. APPROVAL Q.A. APPF4VAL/ QATEs.a2... .000* EA .000 69041-1-1
!400-02-00) SIGNED.
I5 CERTS/TEST REP. CERTS/TEST REP. CERTS/HATERIA.X TEST REPORTS .000 EA .060 69041-1-1
400-02-00 REQUIRED

I I ~ ~ annnnl

R AT'W."
NTO ..... .. :nf ' -I"" :-', I. I
wm '

J f i~ i 1 , wll
ILS OT -4
*..EING
~EURECHALTER 110. *~* -o
P.C.Ajih DaFT.

--------------------------------------
ATTACHMENT 2

RELIEF.REQUEST 29

CONSOLIDATED EDISON COMPANY OF NEW YORK, INC.


INDIAN POINT UNIT NO. 2
DOCKET NO. 50-247
NOVEMBER, 1989

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