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Strength and Compressibility Characteristics of Amorphous Tropical Peat
Strength and Compressibility Characteristics of Amorphous Tropical Peat
ABSTRACT
Peat is viewed to deflect from the standard guidelines of soil behaviours due to the influence of structural fibres and high
compressibility. Hence, the laboratory strength behaviour of peat is often complex, and the geotechnical test results may be doubtful.
Amorphous peat is expected to behave differently since the fibres have been broken down into smaller organic contents and humus
material. Laboratory tests such as scanning electron microscopy (SEM), one-dimensional (1D) oedometer tests and isotropically
consolidated undrained (CIUC) triaxial tests were conducted on amorphous peat samples obtained from a site in Kota-Samarahan,
Malaysia. The microstructure of amorphous peat indicates colloidal amorphous-granular particles with no visible evidence of
hollow cellular connections. The measured compressibility and strength properties reflect the effect of decomposition and are
somewhat different from that of fibrous peat. Interestingly, the strain hardening characteristic which complicates the interpretation
of strength results is less significant, and the tension cutoff line is not reached. Based on the outcome of this study, strength and
settlement behaviour of amorphous peat can be reasonably measured in the laboratory for design and construction of highways,
embankments and other infrastructures.
Key words: Amorphous peat, decomposition, shear strength, microstructure, compressibility, triaxial test.
organic-based material in soils, and fibre content is the degree of minimise soil disturbance induced by soil displacement. The
the organic substance that is yet to be humified. Peat is described picture of the undisturbed sampling is presented in Fig. 2. The
as soils with organic contents higher than 35% by soil scientists. disturbed samples were collected by scooping method and put
For geotechnical engineers, Landva et al. (1983) specified peat to into plastic containers for reconstitution in the laboratory. The
have organic content above 80% from loss of ignition test, and containers were sealed with silicone sealant to avoid disturbance
Von post used the state of decomposition and wetness to classify and loss of moisture. Index tests were carried out on the peat
peat into ten broad categories. The Unified Soil Classification samples, and the summary is presented in Table 3. Visual exam-
System (USCS) combines all soils that are composed primarily ination of the sample indicates a dark brown coloured organic
of plant tissue in all stages of decomposition, colours and odour material with a smooth texture. The von-Post squeeze test on the
as peat (ASTM D2487 2011). The Public Works Department, peat sample did not show any recognisable plant structure on the
Malaysia has improved the on the various existing classification hand after squeezing out the peat paste in between fingers. Al-
works, by combining factors of organic content and degree of most all peat escaped through the fingers except for few un-
decomposition for a comprehensive classification of tropical decomposed fibres. The nearly complete decomposed peat is
peats (Zainorabidin and Wijeyesekera 2007; Zulkifley et al. classified to be Von-Post index H8-H9 (Sapric).
2013). Table 2 shows the Extended Malaysian Soil Classification The loss of ignition was measured in the laboratory by heat-
System (MSCS) for peat. ing few peat samples at a temperature of 450C until there was
no significant change in mass (ASTM D2974 2014). The esti-
mated loss of ignition ranges from 92% to 96%. Other peat sam-
4. SAMPLING AND INDEX PROPERTIES
ples were soaked in a dispersing agent (5% sodium hexameta-
The undisturbed samples were collected with thin-walled phosphate) for 15 hours to determine the fibre content (ASTM
PVC sampler at 1.2 m depth. The PVC sampler measures 100 D1997 2013). After the samples were washed through a No. 100
mm in external diameter and 150 mm in height with a cutting sieve, and oven-dried at 110 5°C, the measured fibre content
edge angle of 30. The area ratio of the PVC tube used for un- was within 3.5 to 6.2%. The specific gravity was determined
disturbed sampling is 10.8% with no clearance ratio, which is using pycnometer tests (ASTM D854 2010) by using kerosene
within the ASTM D1587/D1587M (2015) recommended ratios to instead of distilled water. Note that kerosene was used instead of
Table 2 Malaysian soil classification systems (MSCS) for peat (Adapted from Zulkifley et al. 2013)
water because peat may be lighter than water. The measured spe- The reconstituted peat samples for use in oedometer and
cific gravity ranges from 1.69 ~ 1.71. The moisture content of triaxial tests were prepared in the laboratory by hand mixing the
peat was determined by oven-drying samples at a temperature of disturbed samples obtained from the field. The hand mixed
800C until there was no further change in mass. The water con- sample was pre-consolidated in 400 mm height cylinders as
tent ranges from 378% to 620%. shown in Fig. 3(a) until primary consolidation has been achieved.
Based on the index tests results in Table 3, the peat can be One of the cylinders has an inside diameter of 38 mm (for triaxial
considered as highly humified with less fibre. Note that humus test samples), and the second, 100 mm (for oedometer test
materials are the product of secondary synthesis of peat and are samples). The pre-consolidation stress applied for each triaxial
chemically active due to their small sizes and high electrical sur- test samples in the steel cylinder was 5 kPa less than the isotropic
face charge (Santagata et al. 2008). These humus materials are consolidation pressure to be applied during the tests. Once the
also referred to colloids of organic soils similar to fine clay in primary consolidation is reached, the pre-consolidated sample is
mineral soils because of their comparable chemical characteris- extruded and trimmed into the required sample height for the
tics (Huat et al. 2014). triaxial testing. Figure 3(b) shows a pre-consolidated sample for
the triaxial test. Each sample was carefully wrapped with poly-
thene and kept in an airtight desiccator for preservation. The
5. SAMPLE PREPARATION same procedure was followed for the preparation of reconstituted
samples for oedometer tests, except that the samples were all pre-
Air drying technique was employed to remove the pore
consolidated with 5 kPa vertical effective stress. The undisturbed
fluids of peat samples for use in SEM analysis. The sample was
samples were cut with the particular test mould from the undis-
air dried at room temperature for two weeks instead of putting it
turbed samples for the tests.
in the oven at a high temperature. The air dry option is prefered,
because heat may affect the microstructure of peat, which is from
plant remains. The air-dried sample was pulverised using a rub- 6. SCANNING ELECTRON MICROSCOPY
ber hammer and stored in an airtight polythene bag.
(SEM)
The imaging of peat microstructure was carried out with the
Hitachi TM 3000 Tabletop scanning electron microscopy to under-
stand the morphology and spatial arrangement of the peat constit-
uents. Figure 4 shows the setup of the electron microscope used for
carrying out these investigations. The pulverised sample was
sprinkled on a 5 mm aluminium stubs (sample holder). Before the
sprinkling of the sample, the stubs are overlaid with double-sided
carbon tape as a form of adhesive to gum the sample to the stubs.
Then the sample was coated with a thin layer of gold in a
sputtering diode system for 10 minutes. The gold coating is to al-
low repulsion of the scattered electron that hits the surface of the
sample when it is placed into the Scanning Electron Microscopy
(SEM) for observation. Various samples were prepared according
to the explained method and examined with the SEM.
Figures 5 and 6 present representative images from SEM the colloidal structure has no intra-assemblage pore space, but
micrographs of the peat samples that were taken at different pore water bounds their surfaces. Peat with colloidal microstruc-
magnifications. Majorly, the observed microstructure shows ho- ture is referred to as amorphous granular material and are in the
mogeneous non-crystalline micro-particles that are colloidal in range of H8 to H10 in the Von Post and Granlund (1926) classi-
structure and jelly-like in texture. Figures 5(a) to 5(c) are a fication. Organic colloids are very small in size (less than 2μm)
different magnification of the same sample while Figs. 5(d) to because it is formed from humified peat with fewer fibres (Huat
5(f) are also a different magnification of another sample. Looking et al. 2014; Kazemian et al. 2011).
at the higher magnifications (Figs. 5(c) and 5(f)), it is clear that
a d
b e
c f
Fig. 5 Scanning electron micrograph of amorphous peat samples showing colloidal structures
90 Journal of GeoEngineering, Vol. 14, No. 2, June 2019
a c
b
d
Fig. 6 Scanning electron micrograph of amorphous peat samples showing sheet-like structures
The second type of microstructure particles observed is cut with an oedometer ring with an inner diameter of 75 mm and
sheet-like microstructure, existing in some of the samples height of 20 mm as shown in Fig 3(c). The inner side of the ring
investigated (Fig. 6). The microstructure appears in the form of was lightly lubricated with silicon grease to reduce sidewall fric-
honeycomb intra-assemblage with a solid intraparticle arrange- tion. The undisturbed samples were cut from the undisturbed
ment without any discernable water-holding cells or voids (Figs. sample while the reconstituted samples were cut from the 100
6(b) and 6(d)). The sheet-like particles have no direct contact mm diameter pre-consolidated sample. Each sample was trimmed
with one another. It is also not possible to observe any distinct at both faces and placed into the assembled oedometer apparatus.
leaf structures, which means they are highly decomposed. Peat Filter papers and porous stones were placed at the bottom and top
with sheet-like microstructure are mostly stemmed sheaths (in- of each sample before placing the top cap. After setting each
teguments) and are classified as H7 organic materials (Landva sample in the apparatus, it was soaked in water for about 24
2007). hours to allow full saturation before loading the sample for
The SEM results complement the data of the index proper- settlement observation. A series of load increments from 10, 20,
ties. The SEM micrograph shows that the hollow perforated cel- 40, 80, and 160 kPa was used for the test, and the change in
lular structure of fibrous peat has been lost. Hence the peat could settlement for each load increment was recorded for 24 hours.
become more gelatinous and compact, relatively high specific Three samples each were tested for both the reconstituted and
gravity (Hobbs 1986; Boylan 2008). It is also noted that there are undisturbed tests in this study.
no significant cavities for storage of water in the intraparticle Figures 7(a) and 7(b) show the cumulative axial strain with
spatial arrangement of the peat samples. Hence, water is stored elapsed time for each loading steps employed for both the recon-
mainly in between the interparticle voids only. Thus the moisture stituted and undisturbed samples respectively. Three tests were
content is lower than that of fibrous peat (Haut et al. 2011). Note conducted for each set of incremental load (10 to 160 kPa), and
that two-thirds of the water content in fibrous peat are mostly each test is represented with alphabet A, B, and C. The repeatabil-
stored within the hollow cellular fibres while one- third is stored ity of the results is generally good as depicted in the two plots and
in the interparticle voids between the fibres (Landva and Pheeney both the reconstituted and undisturbed are somewhat identical. The
1980; Mesri and Ajlouni 2007; O’Kelly 2014). Given that signif- reconstituted tests results are more consistent than the undisturbed
icant part of the fibre has been humified, the fibre content is also samples. From the e-log(t) curves of the reconstituted samples, the
on the low side. axial strain for the first and last (10 kPa and 160 kPa) incremental
loads is approximately 9.5% and 48% respectively, while that of
the undisturbed sample is 9.7% and 53.1% respectively. The un-
7. ONE-DIMENSIONAL COMPRESSION TESTS
disturbed amorphous peat samples are slightly more compressible
One-dimensional tests were conducted using a conventional than the reconstituted samples, although the initial settlement for
oedometer apparatus to observe the compressibility anisotropy of both samples is high. The end-of-primary consolidation for each
amorphous peat through the settlement behaviour of both test was determined by the Casagrande’s e-log(t) curve method.
undisturbed and reconstituted samples. The peat samples were The duration of primary consolidation for the first two loadings
Amuda et al.: Strength and Compressibility Characteristics of Amorphous Tropical Peat 91
in the undisturbed tests is relatively shorter than other tests be- secondary compression index, and it is measured from the slope
cause of the high initial permeability of the virgin peat deposit of the secondary consolidation line (C = e/ log t). Note that
with high void ratio and expulsion of entrapped biogas (Mesri the C changes with time for each level of v while Cc changes
and Ajlouni 2007). with only the v. Therefore, the rate of change in C with time is
The compressibility curves (e vs. log of vertical effective proportional to the rate of change in Cc with , . The estimated
stress, v plots) for all the amorphous peat samples tested in this mean of C for each set of incremental loading ranges from 0.2 to
study are shown in Fig. 8. The data are superimposed with test 0.31, while the ratio of C / Cc is from 0.044 to 0.056 (see Table
linear fit lines. All the e-log v plots converge with an increase 4). Given the close range values of the ratio of C / Cc for the
in the vertical effective stress. The average compressibility and reconstituted and undisturbed sample, it can be said that com-
deformability parameters of amorphous peat estimated from this pressibility and deformability anisotropy is lower in amorphous
study are presented in Table 4. The compression index, Cc repre- peat than that of fibrous peat. Lower deformability, permeability
sents the slope of e vs. log v for each set of incremental loading anisotropy is often reported for amorphous peat than fibrous peat
test (Cc = e/ log v). The average Cc for the reconstituted and (Lee et al. 2015; Mesri and Ajlouni 2007; Yamaguchi et al.
undisturbed tests are 4.4 and 5.4 respectively and are within the 1985a; Yamaguchi et al. 1985b).
lower range of Cc for peat in the literature. The range of com-
pression index of peat in the literature according to Huat et al.
(2014) is within 2 to 15. Also, the difference between the values
of Cc in the reconstituted and undisturbed samples less significant.
The estimated Cc agrees with the empirical correlation of Cc =
w/100 suggested by Mesri and Ajlouni (2007) for normally con-
solidated and fully saturated peat deposits. Recall that the esti-
mated moisture content, w of the amorphous peat samples uti-
lised in this study range from 378 to 620.
The deformability of amorphous peat particles was
estimated from the ratios of C / Cc, where C is defined as the
Undisturbed B 5.45 0.24 0.044 Fig. 8 Void ratio vs. vertical effective stress curves for both
C 5.49 0.31 0.056 reconstituted and undisturbed samples
92 Journal of GeoEngineering, Vol. 14, No. 2, June 2019
Figure 9 plots C vs. compression index, Cc for each effec- sample). Each sample was then carefully placed on the triaxial
tive stress level. It also includes data from the most relevant past pedestal. Another set of filter paper and porous stone is placed at
reports, namely James Bay Peat, Middleton Peat and organic clay. the top end of the sample. The sample is enclosed with a rubber
Santagata et al. (2008) reported an average value of C / Cc to be membrane by a membrane fitting tool to reduce sample disturb-
0.095, though some of the data are as high as 0.122. The author ance (for low effective stress peat sample) during preparation and
stated that the reason for high values of C / Cc is because most installation. Hard Gabo “O” ring seals were used to fasten the
of the samples tested are high in fibre content. Mesri et al. (1997) upper and lower ends of the rubber membrane against the top cap
also reported that the average relationship of C / Cc is 0.052 and and the pedestal respectively before the cylindrical chamber is
0.035 for amorphous peaty clay (Zhang and O’kelly 2013). used to cover it.
Generally, a mean value of 0.06 ± 0.01 has been reported for peat The chamber surrounding the sample was then filled with
and mean value of 0.04 ± 0.01 for organic clay without fibre distilled water and placed on the automated Geocomp triaxial
(Santagata et al. 2008; Mesri and Ajlouni 2007). The average C testing machine. Once the sample is in place on the Geocomp
/ Cc results obtained from this study is 0.056 with some of the triaxial machine and all the required test conditions are selected,
data as low as 0.041. Based on the reviewed works of literature the system automatically runs the entire test from saturation to
and Fig. 9, we propose that the value of C / Cc might decrease consolidation and shearing without the intervention of the opera-
with the decomposition of peat. tor. Hence the back pressure, Skempton’s B-value, consolidation
pressure and strain rate were input into the machine at once be-
fore the test started. A back pressure adequate to remove all the
8. CONSOLIDATED UNDRAINED (CIUC) air (100 kPa) was applied to all the peat sample throughout the
TRIAXIAL TEST consolidation and undrained shear stage. The B-value was set to
0.95 for full sample saturation check. Once the desired B-value
Undrained triaxial tests were performed on reconstituted is reached, the test moves to the consolidation stage. The ma-
samples to establish the strength behaviour of amorphous peat in chine automatically stops consolidation when the time to end of
triaxial test. It was not possible to trim and place the undisturbed primary consolidation, t100 is reached, then the test moves on to
sample collected for the undisturbed triaxial test without disturb- the shearing stage. Each of the samples was isotropically consol-
ance because the sample kept deforming during the trimming idated to various consolidation pressure ranging from 10, 20, 30,
process. The in-situ effective stress of the samples obtained at 1 50, and 100 kPa.
m depth below the surface is very low, and the sample deforms Faster strain rate in a constant strain rate triaxial test in-
under own weight even when the sample was collected with a 38 creases the measured strength (Hanrahan 1954; Boylan 2008). In
mm diameter PVC tube (Hayashi et al. 2012). Hence undisturbed this test, the strain rate was estimated by dividing the estimated
triaxial test is not included in this study. The test was conducted failure strain (15%) by 10 t50 (where t50 is the time required to
with an automated CIUC apparatus with a LoadTrac-II and two achieve 50% consolidation). The estimated strain rate used for all
FlowTrac-II systems manufactured by Geocomp Corporation the triaxial tests is 0.18%/hr to allow for full equalisation of
(Geocomp triaxial manual 2013). The picture of the automated shear-induced pore water pressure within the sample. The mem-
triaxial system is shown in Fig. 10. One of the FlowTrac-II con- brane stiffness correction, qm is calculated using Eq. (1) (ASTM
trols the cell pressure and volume while the other one controls D4767 2011).
the sample pressure (back pressure) and volume. Before the
placement of sample on the pedestal, the sample is underlaid with
a filter paper and porous stone (of the same diameter with the
Fig. 9 Secondary compression index (C) vs. compression index Fig. 10 The automated triaxial LoadTrac-II and FlowTrac-II
(Cc) for peats System
Amuda et al.: Strength and Compressibility Characteristics of Amorphous Tropical Peat 93
(a) Deviatoric stress vs. axial strain, a (b) Change in pore water pressure (u) vs. a (c) Deviatoric stress, q vs. mean
effective stress
Fig. 11 Results from CIUC triaxial testing of reconstituted peat samples
94 Journal of GeoEngineering, Vol. 14, No. 2, June 2019
c = 4 kPa
= 33.3
and that obtained by Yamaguchi et al. (1985b) shows that the 9. CONCLUSIONS
effect of fibre is negligible in this present study. High friction
angles within the range 50 to 85 have been reported from This study involves series of various experiments conducted
previous studies on undrained triaxial compression tests of peat on highly decomposed amorphous tropical peat samples. The
(Den-Haan and Feddema 2012; Farrell and Hebib 1998; Hebib relationship between the microstructure, index properties,
2001; Yamaguchi et al. 1985b). Den-Haan et al. (1995) stated strength, compressibility and deformability properties of amor-
that the effective friction angles decrease with increase in density phous peat is explored to understand the engineering behaviour
of peat. of amorphous tropical peat. The outcome of the experimental
The critical state condition at failure for the reconstituted work is summarised below:
samples tested in this study can be compared with the state of the 1. The index properties of the amorphous peat indicate that the
peat at normal consolidation in the e-ln p plane as shown in Fig. peat is dominated by organic contents that are highly
13. Included in the plot is the data obtained from Yang et al. decomposed. The humification process has led to the
(2016) for organic clay. Figure 13 shows linearly fitted values of relative increase in specific gravity and reduction in water
void ratio after consolidation against the mean effective stress for content. The measured index properties are relatively stable.
both normally consolidated and critical state conditions. A simi- 2. The microstructure reveals that the peat morphology is more
lar linear relationship is found in the present study and the Yang of compact amorphous-granular particles with no physical
et al. (2016) data with a slight difference in the estimated slopes. evidence of hollow cellular connections or fibre entangle-
However, the amorphous peat from the present study is low in ment. Higher magnified views reveal homogeneous
density (high void ratio) than the later. The critical state line, non-crystalline micro-particles that are colloidal in structure.
CSL appears not to be parallel to the normal consolidation line, Traces of some solid sheet-like structure are also found.
NCL due to the organic nature of the particles and structural Though the studied peat is made of about 94% organic con-
arrangement which is different from that of fine-grained soil tent, the SEM images hardly show evidence of plant-derived
(Budhu 2010). microparticles.
3. The tested amorphous peat displayed high initial void ratio
and compressibility characteristics. Comparison of the com-
pressibility behaviour of reconstituted and undisturbed sam-
ples suggests less significant structural anisotropy. The av-
erage compression index, Cc for the reconstituted and un-
disturbed tests are 4.35 and 5.37 respectively and the aver-
NCL - Present study
age ratio of C / Cc measured in this study is 0.05. The
CSL - Present study similar compressibility and deformability characteristics of
NCL - Yang et al. (2016) both reconstituted and undisturbed sample in the
CSL - Yang et al. (2016) one-dimensional compression tests can be linked to the in-
significant effect of fibre that has been decomposed.
4. The stress path of amorphous peat samples did not touch the
tension cutoff line throughout the triaxial test, which is due
to significantly low fibre content. The samples were able to
achieve a relative peak failure at higher strains, and the pore
water pressure generated at the end of each test is lower than
their corresponding applied cell pressure. The subsidence
of the strain hardening effect is evidence of high decompo-
Fig. 13 Critical state (CSL) and normally consolidated (NCL) sition of the fibre. The angle of friction (33) estimated from
lines in e-ln p plane this study is relatively low as compared to fibrous peat.
Amuda et al.: Strength and Compressibility Characteristics of Amorphous Tropical Peat 95
5. The comparison of the critical state condition at failure with University College Dublin.
the state of the peat at normal consolidation in the e-ln p Budhu, M. (2010). Soil Mechanics and Foundations. 3rd Ed., John
plane exhibit a typical stress path for normally consolidated Wiley & Sons, Inc. http://doi.org/10.0470556846
undrained soils. Cola, S. and Giampaolo, C. (2005). “The shear strength behavior of two
peaty soils.” Geotechnical and Geological Engineering, 23(6),
This study demonstrated that the complexities in the 679-695. http://doi.org/10.1007/s10706-004-9223-9
laboratory test of peat, especially triaxial testing are less DenHaan, E.J. and Kruse. G.A.M. (2007). “Characterisation and En-
significant in amorphous peat and laboratory strength estimation gineering Properties of Dutch Peats.” Proceedings of Characteri-
can be reliable for amorphous peat. sation and Engineering Properties of Natural Soils, Singapore:
Taylor and Francis, 2101-2133.
http://doi.org/10.1016/j.jada.2008.10.064
ACKNOWLEDGEMENTS DenHaan, E.J., Uriel, A.O., and Rafnsson. E.A. (1995). “Special
Problem Soils/Soft Rocks.” Proceedings of the 11th European
The work presented in this paper is supported by the UNI- Conference on Soil Mechanics and Foundation Engineering-
Theme, Copenhagen, Denmark, Danish Geotechnical Society, 7,
MAS small Grant Scheme (grant No. FO2(S165)/1198/2015(02)) 139-180. http://doi.org/8789833007
and the Fundamental Research Grant Scheme (Grant No. DenHaan, E.J. and Feddema, A. (2013). “Deformation and Strength
FRGS/TK01(02)/1302/2015(19)). The first author acknowledges of Embankments on Soft Dutch Soil.” Proceedings of the Insti-
the guidance of Professor Amir Azam Khan of the Department of tution of Civil Engineers — Geotechnical Engineering, 166(3),
Mechanical and Manufacturing Engineering, UNIMAS on the 239-252. http://doi.org/10.1680/geng.9.00086
use of SEM. Edil, T.B. and Wang. X. (2000). “Shear Strength and Ko of Peats and
Organic Soils.” Geotechnics of High Water Content Materials,
ASTM STP 1374, West Conshohocken: ASTM, Edil, T.B. and
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