NO. DOKUMEN FLB-7.2.1.14.

1
EDISI 3 ASH ANALYSIS
NO. REVISI 00
TANGGAL TERBIT 1-Mar-19 BY ATOMIC ABSORPTION SPECTROFOTOMETRIC
HALAMAN 1 Dari 1 PT. IOL INDONESIA - LABORATORIUM BANJARBARU

JOB NO. :
STANDARD METHOD : ASTM D3682
ANALYST :
DATE :
Balance Number :
Balance Correction :

Sample ID Sample ID
Weight Weight Repeatability (r)

(a) (b) (c) (d) % Element % Element (a) (b) (c) (d) % Element % Element
Element Dillution b x c x 100 Element Dillution b x c x 100
Conc.(ppm) Chem.factor e = (a x d) % e x 100 Conc.(ppm) Chem.factor e = (a x d) % e x 100
factor 100 factor 100 Conct r
100 - LOI 100 - LOI
LOI LOI

SiO2 0.5000 2.139 1.070 SiO2 0.5000 2.139 1.070 33.14 - 57.73 0.33 + 0.04x

Al2O3 0.5000 1.889 0.945 Al2O3 0.5000 1.889 0.945 11.32 - 31.83 0.80

Fe2O3 2.0000 1.429 2.858 Fe2O3 2.0000 1.429 2.858 2.93 - 41.11 0.01 + 0.06x

CaO 2.0000 1.400 2.800 CaO 2.0000 1.400 2.800 1.46 - 22.19 0.21 + 0.04x

MgO 2.0000 1.658 3.316 MgO 2.0000 1.658 3.316 0.45 - 7.12 0.04 + 0.03

TiO2 0.2000 1.667 0.333 TiO2 2.0000 1.667 0.333 0.57 - 1.44 0.13

Na2O 2.0000 1.348 2.696 Na2O 0.2000 1.348 2.696 0.14 - 7.15 0.06 + 0.03x

K2O 2.0000 1.205 2.410 K2O 0.2000 1.205 2.410 0.45 - 2.99 0.03 + 0.03x

0.01 - 1 0.059
P2O5 P2O5
1 - 5.0 0.250
0.01 - 1.0 0.01
SO3 SO3
5 - 15 0.1
TOTAL

x = mean of analytical result Analyzed By : Checked by : Date :

Note : TiO2 use 3 dilation factor
in astm standard = 1
1 : 3 = 0,333
NO. DOKUMEN FLB-7.2.1.8.2
EDISI 01 ASH ANALYSIS
NO. REVISI 00
TANGGAL TERBIT 1-Feb-20 BY ATOMIC ABSORPTION SPECTROFOTOMETRIC
HALAMAN 1 Dari 1 PT. IOL INDONESIA - LABORATORIUM PAITON

JOB NO. :
STANDARD METHOD : ASTM D3682
ANALYST :
DATE :
Balance Number :
Balance Correction :

Sample ID DATA 1 Sample ID DATA 2

Weight Weight Repeatability (r)

(a) (b) (c) (d) % Element % Element (a) (b) (c) (d) % Element % Element
Element Dillution b x c x 100 Element Dillution b x c x 100
Conc.(ppm) factor Chem.factor e = (a x d) % e x 100 Conc.(ppm) factor Chem.factor e = (a x d) % e x 100
100 100 - LOI 100 100 - LOI Conct r

LOI LOI

SiO2 2.0000 2.139 4.278 SiO2 2.0000 2.139 4.278 33.14 - 57.73 0.33 + 0.04x
11.698 50.04 50.04 11.623 49.72 49.72
Al2O3 0.5000 1.889 0.945 Al2O3 0.5000 1.889 0.945 11.32 - 31.83 0.80
29.53 27.89 27.89 29.72 28.07 28.07
Fe2O3 2.0000 1.429 2.858 Fe2O3 2.0000 1.429 2.858 2.93 - 41.11 0.01 + 0.06x
3.696 10.56 10.56 3.647 10.42 10.42
CaO 2.0000 1.400 2.800 CaO 2.0000 1.400 2.800 1.46 - 22.19 0.21 + 0.04x
1.249 3.50 3.50 1.234 3.46 3.46
MgO 2.0000 1.658 3.316 MgO 2.0000 1.658 3.316 0.45 - 7.12 0.04 + 0.03
0.3725 1.24 1.24 0.3705 1.23 1.23
TiO2 0.5000 1.667 0.834 TiO2 0.5000 1.667 0.834 0.57 - 1.44 0.13
1.60 1.33 1.33 1.569 1.31 1.31
Na2O 2.0000 1.348 2.696 Na2O 2.0000 1.348 2.696 0.14 - 7.15 0.06 + 0.03x
0.179 0.48 0.48 0.1707 0.46 0.46
K 2O 2.0000 1.205 2.410 K2O 2.0000 1.205 2.410 0.45 - 2.99 0.03 + 0.03x
0.3633 0.88 0.88 0.3689 0.89 0.89
0.01 - 1 0.059
P2O5 P2O5
1 - 5.0 0.250
0.01 - 1.0 0.01
SO3 SO3
5 - 15 0.1
TOTAL
95.92 95.92 45.83

x = mean of analytical result Analyzed By : Checked by : Date :

Note : TiO2 use 3 dilation factor
in astm standard = 1
1 : 3 = 0,333
NO. DOKUMEN FLB-7.2.1.8.2
EDISI 01 ASH ANALYSIS
NO. REVISI 00
TANGGAL TERBIT 1-Feb-20 BY ATOMIC ABSORPTION SPECTROFOTOMETRIC
HALAMAN 1 Dari 1 PT. IOL INDONESIA - LABORATORIUM PAITON

JOB NO. :
STANDARD METHOD : ASTM D3682
ANALYST :
DATE :
Balance Number :
Balance Correction :

Sample ID DATA 3 Sample ID DATA 4

Weight Weight Repeatability (r)

(a) (b) (c) (d) % Element % Element (a) (b) (c) (d) % Element % Element
Element Dillution b x c x 100 Element Dillution b x c x 100
Conc.(ppm) factor Chem.factor e = (a x d) % e x 100 Conc.(ppm) factor Chem.factor e = (a x d) % e x 100
100 100 - LOI 100 100 - LOI Conct r

LOI LOI

SiO2 2.0000 2.139 4.278 SiO2 2.0000 2.139 4.278 33.14 - 57.73 0.33 + 0.04x
11.725 50.16 50.16 11.874 50.80 50.80
Al2O3 0.5000 1.889 0.945 Al2O3 0.5000 1.889 0.945 11.32 - 31.83 0.80
28.9 27.30 27.30 29.39 27.76 27.76
Fe2O3 2.0000 1.429 2.858 Fe2O3 2.0000 1.429 2.858 2.93 - 41.11 0.01 + 0.06x
3.775 10.79 10.79 3.694 10.56 10.56
CaO 2.0000 1.400 2.800 CaO 2.0000 1.400 2.800 1.46 - 22.19 0.21 + 0.04x
1.2 3.36 3.36 1.236 3.46 3.46
MgO 2.0000 1.658 3.316 MgO 2.0000 1.658 3.316 0.45 - 7.12 0.04 + 0.03
0.3748 1.24 1.24 0.3741 1.24 1.24
TiO2 0.5000 1.667 0.834 TiO2 0.5000 1.667 0.834 0.57 - 1.44 0.13
1.58 1.32 1.32 1.568 1.31 1.31
Na2O 2.0000 1.348 2.696 Na2O 2.0000 1.348 2.696 0.14 - 7.15 0.06 + 0.03x
0.1686 0.45 0.45 0.1746 0.47 0.47
K 2O 2.0000 1.205 2.410 K2O 2.0000 1.205 2.410 0.45 - 2.99 0.03 + 0.03x
0.3682 0.89 0.89 0.374 0.90 0.90
0.01 - 1 0.059
P2O5 P2O5
1 - 5.0 0.250
0.01 - 1.0 0.01
SO3 SO3
5 - 15 0.1
TOTAL
95.51 95.51 45.70

x = mean of analytical result Analyzed By : Checked by : Date :

Note : TiO2 use 3 dilation factor
in astm standard = 1
1 : 3 = 0,333
NO. DOKUMEN FLB-7.2.1.8.2
EDISI 01 ASH ANALYSIS
NO. REVISI 00
TANGGAL TERBIT 1-Feb-20 BY ATOMIC ABSORPTION SPECTROFOTOMETRIC
HALAMAN 1 Dari 1 PT. IOL INDONESIA - LABORATORIUM PAITON

JOB NO. 12
STANDARD METHOD : ASTM D3682
ANALYST :
DATE :
Balance Number :
Balance Correction :

Sample ID DATA 5 Sample ID DATA 6

Weight Weight Repeatability (r)

(a) (b) (c) (d) % Element % Element (a) (b) (c) (d) % Element % Element
Element Dillution b x c x 100 Element Dillution b x c x 100
Conc.(ppm) factor Chem.factor e = (a x d) % e x 100 Conc.(ppm) factor Chem.factor e = (a x d) % e x 100
100 100 - LOI 100 100 - LOI Conct r

LOI LOI

SiO2 2.0000 2.139 4.278 SiO2 2.0000 2.139 4.278 33.14 - 57.73 0.33 + 0.04x
8.187 35.02 35.02 11.774 50.37 50.37
Al2O3 0.5000 1.889 0.945 Al2O3 0.5000 1.889 0.945 11.32 - 31.83 0.80
12.71 12.00 12.00 29.29 27.66 27.66
Fe2O3 2.0000 1.429 2.858 Fe2O3 2.0000 1.429 2.858 2.93 - 41.11 0.01 + 0.06x
5.22 14.92 14.92 3.68 10.52 10.52
CaO 2.0000 1.400 2.800 CaO 2.0000 1.400 2.800 1.46 - 22.19 0.21 + 0.04x
1.206 3.38 3.38 1.207 3.38 3.38
MgO 2.0000 1.658 3.316 MgO 2.0000 1.658 3.316 0.45 - 7.12 0.04 + 0.03
0.3762 1.25 1.25 0.3703 1.23 1.23
TiO2 0.5000 1.667 0.834 TiO2 0.5000 1.667 0.834 0.57 - 1.44 0.13
1.59 1.32 1.32 1.5715 1.31 1.31
Na2O 2.0000 1.348 2.696 Na2O 2.0000 1.348 2.696 0.14 - 7.15 0.06 + 0.03x
0.1706 0.46 0.46 0.1725 0.47 0.47
K 2O 2.0000 1.205 2.410 K2O 2.0000 1.205 2.410 0.45 - 2.99 0.03 + 0.03x
0.3729 0.90 0.90 0.3888 0.94 0.94
0.01 - 1 0.059
P2O5 P2O5
1 - 5.0 0.250
0.01 - 1.0 0.01
SO3 SO3
5 - 15 0.1
TOTAL
69.25 69.25 45.50

x = mean of analytical result Analyzed By : Checked by : Date :

Note : TiO2 use 3 dilation factor
in astm standard = 1
1 : 3 = 0,333