Professional Documents
Culture Documents
Energy Reports: Mona N. Radwan, M.M. Morad, M.M. Ali, Kamal I. Wasfy
Energy Reports: Mona N. Radwan, M.M. Morad, M.M. Ali, Kamal I. Wasfy
Energy Reports
journal homepage: www.elsevier.com/locate/egyr
article info a b s t r a c t
Article history: A solar steam distillation system is constructed to be used for extracting volatile oils distinguished
Received 3 July 2020 of simple design and high efficiency. The solar distillation system consists of a parabolic solar dish
Received in revised form 4 October 2020 collector, boiler, extracting unit, condenser and connection hoses. The performance of the constructed
Accepted 7 November 2020
solar distillation system is studied as a function of change in boiler inlet water flow rate (1.00, 1.25 and
Available online 12 November 2020
1.50 l/h) and a batch size of the whole lavender plant (400, 600 and 800 g). Performance evaluation
Keywords: is conducted in terms of system efficiency, productivity, extraction efficiency, essential oil yield and
Parabolic solar collector final product quality.
Distillation unit Results reveal that the solar steam distillation system has been proven to be an effective way for
Lavender plant extracting high-quality lavender volatile oil with 7.3 ml system productivity, 60.25 % system efficiency,
Water flow rate
98.13% extraction efficiency and 0.785% (w/w) essential oil yield under conditions of 1.25 l/h boiler
Essential oil yield
inlet water flow rate and 800 g batch size.
Product quality
The solar system requires approximately two, three and four hours for extracting oil from batch
sizes of 400, 600 and 800 g, respectively.
© 2020 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY license
(http://creativecommons.org/licenses/by/4.0/).
https://doi.org/10.1016/j.egyr.2020.11.034
2352-4847/© 2020 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
M.N. Radwan, M.M. Morad, M.M. Ali et al. Energy Reports 6 (2020) 3080–3087
Table 1 carefully with aluminum foil to get a precise focal point. A manual
Some properties of lavender plant. tracking mechanism was provided and adjusted to follow the
Properties Values sun so that the incident beam radiation will be reflected and
Stem diameter (mm) 3.26 concentrated in the focus area. Two motions about the horizontal
Stem length (cm) 25–45
and vertical axis were necessary to fix both solar azimuth and
Plant mass (g) 8–32
Number of branches 6–26 solar altitude angles. So, two-axis truckers (full tracking) moved
Number of leaves 11–50 east to west and north to south to collect normal solar radiation
throughout the year.
■ Boiler
The used boiler was made of stainless steel with a 2 mm
receiver in combination with a hybrid biomass-based boiler was
thickness. It was 20 cm in diameter, 30 cm height and has a
developed. Results indicate that essential oils concentration was
volume of 9.42 l. The boiler size was suitable to admit most
0.59% w/w from fresh eucalyptus leaves and 0.40% w/w for pep-
of the concentrated sunlight with a limitation for radiation and
permint leaves (Afzal et al., 2017). Solar energy was used in
convection losses. It was put at the concentrator focus. The boiler
extracting essential oil. The extraction rate and yield percent
had two openings in its top. The first opening was used to feed
were determined at normal conditions. Results showed that the
cool water through a pipe (1.26 cm diameter) to keep continuous
extraction rate varied with the plant samples of oregano as the
fastest (3.4 ml/day) and rose petals as the slowest (1.8 ml/day). water flow, while the other opening was to deliver steam to
The yield percent of plant extracts varied with the kind of plant the extracting unit through another pipe (2.64 cm diameter)
samples, sambong (Conyza balsamifera Linn) having 72% as the connected with stainless steel hose of 2.94 cm diameter. The
highest percent yield and 18.5% for rose petals (Rosa damascena) boiler was fully insulated with fiberglass to reduce the heat losses,
as the lowest percent yield (Pesimo, 2017). expect the exposed part to the solar rays, which was reflected by
From the above previous literature review, it is clear that dif- the dish surface. The water supplied to the boiler was adjusted
ferent researches were conducted and published on solar systems to be with various continuous flow rates through a water tank
that were used for extracting volatile oils from the leaves of located at 2.5 m from the system base.
medicinal and aromatic plants and the most important emerging ■ Extracting unit
problems during the extraction process. However, such studies The extracting unit was manufactured to accommodate
have to be carried out to find out a simple solar system from local enough batch sizes of the lavender plant and it was completely
material to be used easily for the extraction process with a high insulated with fiberglass to reduce heat losses. The extracting
extraction efficiency of whole lavender plants. unit was cylindrical in shape with a 30 cm diameter and 50 cm
Therefore, the main purpose of the present investigation was height. The extracting unit was made of stainless steel with a
to construct a solar steam distillation system for extracting 2 mm thickness. A net with a 29 cm diameter was installed inside
volatile oil from the lavender plant. To achieve the ultimate goal, the extracting unit at a height of 7 cm from the bottom of the
the following criteria were taken into consideration: unit (based on preliminary experiments) to put the lavender plant
batch to allow the steam to extract volatile oil easily. The unit had
• Study some different operating parameters affecting the two openings; the first opening was located in the unit bottom
performance of the solar steam distillation system. to deliver steam produced from the boiler to the extracting unit
• Compare the final lavender oil quality obtained by the con- to move around and inside the plant to extract volatile oil. While
structed solar steam distillation system with the standards the second opening was located in the unit top to deliver steam
of quality guidelines. with the extracted volatile oil to the condenser to extract oil.
■ Condenser
2. Materials and methods The used condenser was a counter flow heat exchanger. The
condenser used a system of tubes exposed to constant water flow
A solar steam distillation system for extracting volatile oil was
to cool and facilitate the condensation. It was made from glass
constructed specially for this work from low cost, local material
and consisted of outer and inner tubes. The outer tube was 35 cm
and tested in Belbeis city (30◦ 25′ 17.9′′ N. 31◦ 30′ 32.6′′ E), Sharqia
length and 2.58 cm in diameter. While the inner tube was the
Governorate, Egypt. The experiments were carried out during the
shape of six bulges of 1 cm in diameter with five throats of 0.5 cm
summer season of 2019.
in diameter. The condenser consisted of four openings for steam
inlet, condensed water outlet, cooling water inlet and cooling
2.1. Experimental setup
water outlet. The condenser unit was connected with a water
tank to receive the cooling water and controlled by a hand valve.
2.1.1. The used plant
And also, it was associated with the extracting unit to receive
The used plant for extracting its volatile oil was lavender (La-
steam and oil to be cooled to produce volatile oil. The extracted
vandula angustifolia). Some properties of the experimental plant
volatile oil was collected in a funnel tube. The oil was less dense
were illustrated in Table 1.
than water so it floated up and then collected.
2.1.2. The solar steam distillation system ■ Connection hoses
A solar steam distillation system suitable for extracting volatile The connection hoses were made of rubber tubes to prevent
oil from lavender consisted of the following main parts: parabolic any heat loss through the steam flow. Additionally, they were
solar dish collector, boiler, extracting unit, condenser and connec- connected with hand valves to control any part and water flow
tion hoses as indicated in Figs. 1 and 2. rates.
■ Parabolic solar dish collector
Parabolic solar concentrated dish collector as a point-focus 2.2. Methods
collector was installed to gain heat from solar radiation and
tracked the sun in two axes for heating the water. It was made Experiments were done to assess the performance of the con-
of aluminum with a 1.7 m dish aperture diameter and 2.5 m2 structed solar steam distillation system for extracting volatile oil
surface area. Additionally, the surface was covered and assembled from the lavender plant.
3081
M.N. Radwan, M.M. Morad, M.M. Ali et al. Energy Reports 6 (2020) 3080–3087
2.2.1. Experimental conditions Solar radiation and temperatures versus time of the day were
The performance of the solar steam distillation system was recorded throughout the experiments. Dish focus temperature
studied under the following parameters: (Tfocus ) as well as both extracting unit inlet (to the extracting
unit) and outlet (from the extracting unit) steam temperatures
• Three different boiler inlet water flow rates (1.00, 1.25 and (TEi and TEo ) added to boiler outlet steam temperature (TBo ) were
1.50 l/h). measured. Temperatures were recorded by copper-constantan
• Three different batch sizes of the whole plant (400, 600 and thermocouples, T type.
800 g). ■ System efficiency
Solar extraction system efficiency (ηs , %) was estimated using
The extracting time was kept constant at four hours during the the following formula according to Munir and Hensel (2009) as:
day from 11:00 to 15:00. The whole lavender plant was placed
on trays in the extracting unit with a constant moisture content ηs = [P /(As × Gb )] × 100 (1)
of 50.7% (wb) under all experimental conditions. where: P: Power required for operating the solar extraction sys-
Each flow rate or batch volume was adjusted prior to the tem (W), As: Aperture area of the reflector (2.46 m2 in average)
start of the experiment and then maintained while studying their and Gb : Beam radiation (W/m2 ).
effect on the volatile oil extraction process. The required power (P) for operating the solar extraction
system was calculated as:
2.2.2. Measurements and determinations
The performance of the solar steam distillation system was P = (Qs + QL )/t (2)
evaluated taking into consideration the following indicators: Qs = mw Cp ∆T (3)
• Thermal performance of the solar steam distillation system
where: Qs : Sensible heat (kJ), mw : Water mass (kg), Cp : The
The thermal performance of the solar steam distillation sys-
specific heat (Cp = 4.187 kJ/kg for water) and ∆T: Temperature
tem was illustrated through recording system temperatures and
difference at a specific time (◦ K).
system efficiency as:
■ System temperatures QL = mLfg (4)
3082
M.N. Radwan, M.M. Morad, M.M. Ali et al. Energy Reports 6 (2020) 3080–3087
SP = V /t (5)
Fig. 5. Effect of batch size on system temperatures under constant boiler inlet
water flow rate of 1.25 l/h.
Fig. 4. Effect of batch size on system temperatures under constant boiler inlet
water flow rate of 1.00 l/h.
3.3. Operational performance of the solar steam distillation system
efficiency was decreased by increasing batch size from 400 to 600 Operational performance of the solar steam distillation sys-
g and it was increased by increasing batch size from 600 to 800 tem was measured by recording system productivity, extraction
efficiency and essential oil yield as follows:
g.
• Hourly and cumulative system productivity
The variation in system efficiency with the difference of both The hourly system productivity at various lavender plant batch
water flow rate and batch size was attributed to the variation sizes for different boiler inlet water flow rates versus experi-
of solar radiation during day hours throughout the experimental mental hours was shown in Fig. 8. The maximum hourly system
productivity was 3.3 ml/h at 13.0 and 14.0 pm under conditions
days. Added to that, the variation in system efficiency was also
of 1.50 l/h boiler inlet water flow rate and 800 g batch size. While
due to the difference in the amount of steam consumed for the its minimum value was 0.5 ml/h at 12.0 pm under conditions of
oil extracting operation that affects the required power and as 1.50 l/h boiler inlet water flow rate and 600 g batch size.
a result, affects system efficiency. The obtained values of the It was observed from results that, increasing the boiler inlet
constructed solar system efficiency were so far good enough and water flow rate from 1.00 to 1.50 l/h at 13.0 pm, increased the
hourly system. This may be due to the increase of the generated
in agreement with Munir and Hensel (2010), who found that
amount of steam that accelerating the steam motion inside the
the average efficiency of the solar distillation system was about extracting unit to move around and inside the plant, which al-
33.21%. lowing extraction of volatile oil easily. Regarding the use of batch
3084
M.N. Radwan, M.M. Morad, M.M. Ali et al. Energy Reports 6 (2020) 3080–3087
Fig. 6. Effect of batch size on system temperatures under constant boiler inlet Fig. 8. Effect of batch size and water flow rate on hourly system productivity.
water flow rate of 1.50 l/h.
of 1.00, 1.25 and 1.50 l/h, respectively at 13.0 pm. The extracted
volatile oil was increased by a large amount of plant batch and
so, the hourly system productivity was increased.
The cumulative system productivity as illustrated in Fig. 9
was affected by both batch size and boiler inlet water flow
rate throughout experimental hours. The maximum cumulative
system productivity was 7.4 ml at 15.0 pm under conditions of
1.50 l/h boiler inlet water flow rate and 800 g batch size. While
the minimum value was 0.5 ml at 12.0 pm under 1.50 l/h boiler
inlet water flow rate and 600 g batch size.
Obtained data explained that the cumulative system produc-
tivity was increased from 2.9 to 3.4, from 5 to 5.4 ml and from
7 to 7.4 ml by increasing the boiler inlet water flow rate from
1.00 to 1.50 l/h at 14.0 pm under batch sizes of 400, 600 and
Fig. 7. Effect of batch size and water flow rate on system efficiency.
800 g, in the same arrangement. As to the effect of batch size,
the obtained data showed that the highest cumulative system
productivity batch size was obtained under a batch size of 800
size, results explained that increasing batch size from 400 to 800 g at 14.0 pm.
g, increased hourly system productivity from 1.2 to 2.8, from 1.8 Results also noticed that the solar system required two hours
to 2.9 and from 2.6 to 3.3 ml/h under boiler inlet water flow rates for extracting oil from a batch size of 400 g. While required
3085
M.N. Radwan, M.M. Morad, M.M. Ali et al. Energy Reports 6 (2020) 3080–3087
Fig. 10. Effect of batch size and water flow rate on extraction efficiency.
Fig. 11. Effect of batch size and water flow rate on essential oil yield.
Table 2
Some chemical properties of final lavender volatile oil.
Properties Quality standards Values
Linalool (%) 25.0–38.0 37.6
Linalyl acetate (%) 25.0–45.0 18.4
Camphor (%) 0.0–0.5 7.3
Terpineol-4-ol (%) 2.0–6.0 3.3
Cymene (%) 4.0–10 5.4
3087