Quantachrome® ASiQwin™- Automated Gas Sorption Data

Acquisition and Reduction

© 1994-2012, Quantachrome Instruments
version 3.0

Analysis Report
Operator: Lab. Energi ITS Date:2020/01/15 Operator: Lab. Energi ITS Date:2020/01/16
Sample ID: EI-14 AKTIVATOR H2SO4 Filename: iq_phisy_st1_2020_01_15_13_34_16EI-14 AKTIVATOR H2SO4.qps
Sample Desc: Comment:
Sample Weight: 0.1375 g Instrument: Autosorb iQ Station 1
Approx. Outgas Time:12.7 hrs Final Outgas Temp.: 140 °C Extended info: Available
Analysis gas: Nitrogen Non-ideality: 6.58e-05 1/Torr CellType: 9mm w/o rod
Analysis Time: 3:47 hr:min Bath temp.: 77.35 K
Analysis Mode: Standard VoidVol Remeasure: off
VoidVol. Mode: He Measure Cold Zone V: 3.95662 cc Warm Zone V: 17.2389 cc
SF method : Volume
Data Reduction Parameters
Thermal Transpiration: on Eff. mol. diameter (D): 3.54 Å Eff. cell stem diam. (d): 4.0000 mm
SF method Tabulated data interval: 1
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid Density:
-24
0.808 g/cc
Avg. Diameter:0.300 nm 14
Polarizability: 1.460 (cc/molec) x 10 Magn. Suscept.: 2.000
Molec. Density6.700 (mol/cm²)x10
Adsorbent Carbon 14 -24
Atom Diameter: 0.340 nm Surf. Atom Dens.: 38.450 (mol/cm²)x10 -29Polarizability: 1.020 (cc/molec)x10
Magn. Susc.: 13.500 (cc/molec)x10

V dV

4.8000 5.7888

4.4000 5.3064

4.0000 4.8240

3.6000 4.3416
Cumlative Pore Volume (cc/g)

3.2000 3.8592

Pore Volume (cc/Å/g)

2.8000 3.3768

2.4000 2.8944

2.0000 2.4120

1.6000 1.9296

1.2000 1.4472

0.8000 0.9648

0.4000 0.4824

0.0000 0.0000
0.00 4.00 8.00 12.00 16.00 20.00 21.40

Half pore width (Å)

SF method summary
Mode : 7.844 Å
Micropore Volume : 0.319 cc/g

Quantachrome® ASiQwin™- Automated Gas Sorption Data Acquisition and Reduction © 1994-2012, Quantachrome Instruments version 3.0 Report id:{666509615:20200116 124144140} Page 1 of 1