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Hydrocyclones Simulation Using a New Modification in Plitt´s Equation

Conference Paper · August 2013


DOI: 10.3182/20130825-4-US-2038.00005

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16th IFAC Symposium on Automation in Mining, Mineral
and Metal Processing
August 25-28, 2013. San Diego, California, USA

Hydrocyclones simulation using a new modification in Plitt´s equation


André Carlos Silva* Elenice Maria Schons Silva**
Jainer Diogo Vieira Matos***

* Goiás Federal University, Catalão, GO, 75704-020


Brazil (Tel: 55(64)3441-5327; e-mail: andrecarlos@catalao.ufg.br).
** Goiás Federal University, Catalão, GO, 75704-020
Brazil (e-mail:elenice@catalao.ufg.br)
*** Goiás Federal University, Catalão, GO, 75704-020
Brazil (e-mail: jainerdiogo@gmail.com)

Abstract: Hydrocyclones are devices worldwide used in mineral processing and used for desliming,
classification, selective classification, thickening and pre-concentration. Versatile in application, the
hydrocyclone is the standard classifier used in closed circuit milling in mineral processing plants. A
hydrocyclone is composed by a cylindrical and a conical section joint together, without any moving parts
and it is capable of perform granular material separation in pulp. The pulp is feed under pressure
tangentially to the cylindrical section. The granular separation mechanism is complex and its mathematical
modelling is empirical. The most used model for hydrocyclone dimensioning was proposed by Plitt
(1976). Combining the first industrial database on cyclones generated at JKMRC with his own laboratory
data, Plitt developed an alternative general- purpose cyclone model. Over the years many revisions and
corrections to Plitt´s model were proposed. The present paper shows a modification in the Plitt´s model
constant, obtained by exponential regression of simulated data for three different hydrocyclones
geometries (Rietema, Bradley and Krebs). The proposed model validation used literature data obtained
from phosphate ore using fifteen different hydrocyclones geometries. The proposed model shows a
correlation equals to 88.2% between experimental and calculated corrected cut size, while the correlation
obtained using Plitt´s model was 11.5%.
Keywords: hydrocyclone, modelling, simulation, Plitt´s equation, mineral pulp.

model were proposed. The present paper shows a statistical


1. INTRODUCTION
analysis between Plitt´s model and five other models based in
According to Sampaio et al (2007) only after 1940 the the first one, which allowed a new model proposal. The
hydrocyclone manufacture has adopted high technology proposed model validation used literature data obtained from
material, though the existence of this equipment report to phosphate ore using fifteen different hydrocyclones
1890. In the following years, thousands of hydrocyclones geometries. The proposed model shows a correlation eight
were installed and nowadays it is considered the standard times higher than the correlation obtained using the Plitt´s
classifier for closed circuit milling and the most used model.
equipment used for fine particles classification (from 2 to 837
2. METHODOLOGY
P ,W LV D YHUVDWLOH KLJK FDSDFLW\ DQG ZLWKRXW PRYLQJ SDUWV
equipment. 2.1. Hydrocyclone empirical models
Hydrocyclones major application is granulometric
classification in closed circuit milling, but it is possible to Within the empirical models used to hydrocyclones
highlight its operation in desliming, selective classification, dimensioning the most used is the model proposed by Plitt
thickening and pre-concentration. It is possible to use (1976). This model can be used to predict the hydrocyclones
hydrocyclones for water, liquid effluents and even some types operation without additional experimental data for a wide
of bacteria filtering. range of operational conditions. According to Plitt (1976) the
experimental data used to produce the model were processed
Centrifuge sedimentation is hydrocyclone operation basic using a stepwise multiple linear regression program to
principle and its performance is influenced by its geometry, formulate the functional relationships between the measured
size, operational variables and solids and pulp physics and calculated parameters (cut size, flow split, capacity and
properties. The separation mechanisms and hydrodynamics sharpness of separation) and the design and operational
acting in hydrocyclones are very complex and hard to be hydrocyclone variables. The linear regression procedure was
theoretical modeled being common the adoption of empiric repeated using different functional forms of the variables
models based in laboratories tests to estimate hydrocyclones (linear, power, exponential) and different variable
performance. The most used model for hydrocyclone combinations. The mean sum of the residuals squared was
corrected cut size calculation was proposed by Plitt (1976) used as the main criterion as to the goodness of fit. Only
and over the years many revisions and corrections to Plitt´s

978-3-902823-42-7/2013 © IFAC 12 10.3182/20130825-4-US-2038.00005


IFAC MMM 2013
August 25-28, 2013. San Diego, USA

variables which were significant at the 99 per cent confidence ,á02 ,á2 -á.- ,á,2/×
96á89 HY H_ He c
†94a L (6)
level were added to the regression equation. Plitt´s model for ,á3- ,á/4 ,á01
Hk f U :¡q? ¡j ;,á1
corrected cut size (in µm) is given by:
,á02 ,á2 -á.- ,á,2/×
94á9 HY H_ He c
†94a L ,á3- ,á/4 ,á01
:¡i ? ¡b ;,á1
(1) 2.2 Hydrocyclones typical geometries
Hk f U

It is possible to group hydrocyclones in families according to


Where Dc is the inside diameter of a hydrocyclone measured their geometric characteristics and according to Svarovsky
at the bottom of the vortex finder [cm], Di is the inside (2000) the three main hydrocyclones families are Bradley,
diameter of a hydrocyclone inlet [cm], Do is the inside Krebs and Rietema. Table 1 summarizes the geometric
diameter of the overflow or vortex finder [cm], Du is the relations between the three families.
inside diameter of the underflow, or apex, orifice [cm], h is
the free vortex height of a cyclone, which is defined as the
distance from the bottom of the vortex finder to the top of the Table 1. Three main hydrocyclones families
underflow orifice [cm], Q is the volumetric flow rate of Family Di/Dc Do/Dc l/Dc L/Dc Œ
hydrocyclone feed [l/min], !l is the liquid phase density
Bradley 0.133 0.200 0.330 6.850 9.0°
[g/cm3], !s solid density [g/cm3] and Ë is the volumetric
Krebs 0.267 0.159 - 5.874 12.7°
percentage of solids present in the feed [%].
Rietema 0.280 0.340 0.400 5.000 15 - 20.0°
Over the years Plitt´s model has suffered many modifications
and corrections. The addition of the fluid dynamic viscosity
(expressed by µ and given in cP) to the original model was 2.3 Mathematical model proposition
proposed by Plitt et al (1980), resulting in the expression:
,á02 ,á2 -á.- ,á1 ,á,2/× Hydrocyclone operation simulations using equations 1 to 6
94á9 HY H_ He — c
†94a L (2) were realized to generate the proposed mathematical model,
Hk f,á/4 U,á01 :¡q? ¡j ;,á1
,á3-
using three hydrocyclone geometries (one for each family)
and operational conditions. The adopted pulp was composed
by iron ore (!s = 3.53 g/cm3) and water (!l = 1.00 g/cm3). Ë
Flintoff et al (1987) proposed two modifications in equation
assumed eleven different values: 0.5, 5.0, 10.0, 15.0, 20.0,
2: a calibration factor (k1) dependent on the solid fed in the
25.0, 30.0, 35.0, 40.0, 45.0 and 50.0%. Ten volumetric flow
hydrocyclone and a constant (D) dependent on the feed flow rate of hydrocyclone feed were used (from 0.5 to 5.0 m3/h
rate, given by: with increment equals to 0.5 m3/h). Table 2 shows the adopted
7=á; H,á02
,á2
-á.- ,á1 ,á,2/×
Y H_ He — c hydrocyclones dimensions for each geometry.
†94a L •5 ™i 7 ™b (3)
H,á3-
k f
,á/4 U,á01 @ A
-á2

Table 2. Hydrocyclones dimensions used in the simulations


Where k1 is a dimensionless calibration factor dependent on Dc Di Do Du
the solid. According to Valadão et al (2007) the following Family h [cm] T [°]
[cm] [cm] [cm] [cm]
equation can be used to estimate big diameter hydrocyclones Bradley 10.0 1.33 2.00 1.00 65.20 9.0
performance fed with high volumetric fraction of solids pulp. Krebs 10.0 2.67 1.59 1.00 54.74 12.7
,á02 ,á2 -á.- ,á,2/×
58á< HY H_ He c Rietema 10.0 2.80 3.40 2.50 46.00 20.0
†94a L ,á3- ,á/4 ,á01 (4)
Hk f U :¡i ?¡b ;

Altogether 330 simulations (110 simulations for each


The difference between the solid and the liquid density in the geometry) were realized and exponential regressions were
equation 4 is raised by one and not by 0.5 as in the original performed using the d50c calculated in the simulations. The
model. A model proposed using laboratory hydrocyclones fed exponential regression was chosen because the original
with pulp containing high purity silica suspensions was equation proposed by Plitt´s is an exponential equation. This
proposed by Gupta and Yan (2006), given by: operation allowed recalculating the coefficients in Plitt´s
model and therefore proposing a model which better fits to the
,á02 ,á2 -á.- ,á1 ,á,2/×
†94a L • 6
6á:<=6 HY H_ He — c
(5) simulated data. Equation 7 presents the proposed model which
,á3- ,á/4 ,á01
Hk f U :¡i ?¡b ;,á1 differs from Plitt´s model in the constant model and the
adoption of fluid dynamic viscosity in agreement with
equation proposed by Plitt et al (1980).
Where k2 is a dimensionless calibration factor (adopted as 1.0 ,á02 ,á2 -á.- ,á1 ,á,2/×
6á98 HY H_ He — c
when there is no experimental data available). Another model, †94a L (7)
H,á3- ,á/4 U,á01 :¡q? ¡j ;,á1
different from Plitt´s model only in the model constant, was k f

proposed by Luz (2005), in a work demonstrating the


convertibility between probabilistic distribution used in
hydrocyclones model, given by: Figure 1 shows a comparison between the proposed model
(represented as a red line) and the simulated data from

13
IFAC MMM 2013
August 25-28, 2013. San Diego, USA

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IFAC MMM 2013
August 25-28, 2013. San Diego, USA

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IFAC MMM 2013
August 25-28, 2013. San Diego, USA

Through the study of the models based on Plitt´s model


(1976) used to calculate the hydrocyclone corrected cut size
was possible to propose a new empirical model, very similar
to the original one. Iron ore pulps operating with three
different hydrocyclone geometries were simulated to propose
the new model and experimental data using phosphate ore
pulp in fifteen hydrocyclones different geometries were used
to validate the new model. The obtained correlation
coefficient between experimental and calculated data using
the proposed model was almost eight times higher than the
coefficient using Plitt´s model (1976). It is possible to affirm
that Plitt´s model is incapable of accurate calculate the
corrected cut size for pulps with low volumetric percentage of
solids present in the feed and this incapacity was not observed
in the proposed model.
Future works are needed to test the new model against wide
Fig. 8 Correlation between experimental and calculated d50c chances in operational variables, pulps with two or more types
using Gupta e Yan (2006) model. of ores, fluid dynamic viscosity, volumetric flow rate of
hydrocyclone feed and even pulp temperature.
5. ACKNOWLEDGEMENTS
The authors thank financial support from the Brazilian
agencies CNPq, CAPES, FAPEG and FUNAPE.
6. NOMENCLATURE
d50c corrected cut size [µm]
Dc inside diameter of a hydrocyclone measured at the bottom
of the vortex finder [cm];
Di inside diameter of a hydrocyclone inlet [cm];
Do inside diameter of the overflow or vortex finder [cm];
Du inside diameter of the underflow, or apex, orifice [cm];
h free vortex height of a cyclone, which is defined as the
distance from the bottom of the vortex finder to the top of the
Fig. 9 Correlation between experimental and calculated d50c underflow orifice [cm];
using Luz (2005) model.
k1 dimensionless calibration factor dependent on the solid;
k2 dimensionless calibration factor (adopted as 1.0 when there
is no experimental data available);
l vortex finder length [cm]
L total hydrocyclone length given by h=L-l [cm].
Q volumetric flow rate of hydrocyclone feed [l/min];
D constant dependent on the feed flow rate;
Ë volumetric percentage of solids present in the feed [%];
µ liquid phase dynamic viscosity [cP];
T conic section angle [o];
!l liquid phase density [g/cm3];
!s solid density [g/cm3].
Fig. 10 Correlation between experimental and calculated d50c
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16
IFAC MMM 2013
August 25-28, 2013. San Diego, USA

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