Instrument: Aglient GC

Injector: Split /Split Less Injector

Detector: FID

Sampler: Autosampler

Column: Stationary Phase DB-1, Methylsilicone, similar phase SE-30,

30M X 250 micron capillary, Film thickness .25mic

Carrier Gas: Helium

Data System: LMA

Project:

System Methods:

Instrument Conditions:

Oven Temp: 160C Injector Temp: 250

Initial Temp: 160C Detector Temp: 300

Initial Time: 0.00 minutes Run Time: 15.00 minutes

Rate: 12/minute
Final Temp: 275C
Final Hold Time: 4.42 minutes

Inlet system: Column flow as measured at column end by external flow meter - 30.0 mls./minute.

Detector: Range: 4

Reagents: Helium: 1-A High-Purity

Sample Preparation: Mix 1 part sample to 1 part n-Propanol, shake well. Using a Hewlett Packard
syringe , set autoinjector to inject 1.0 L of the mixture. Actual amount
injected will be 0.5 L of sample.