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sgs minerals services – T3 SGS 965 09-2013

Geochemical analysis of Iron ore


sgs geochemical SAMPLE PREPARATION Fusion by XRF
analysis for iron ore Sample preparation is the process by SGS offers unmatched XRF expertise
exploration which a sample is readied for analysis. at many of our operations. Iron ore
The right sampling method will produce a is common in many mineral forms
No matter where you are, what limits sub-sample that is representative of the (hematite, magnetite, goethite, limonite or
of detection, precision or accuracy total sample. Good sample preparation siderite) and has mineral-specific analysis
you require, SGS Minerals Services practice is essential to obtaining requirements. Borate fusion with XRF
has the technical expertise to supply meaningful and reliable analytical data. analysis is an extremely robust technique
chemical analysis for iron ore. We for major and minor elemental analysis in
have the locations, technical strength, complex mineralization and offers highly
independence, consistency and ethical precise and accurate results for iron ore
compliance you need. Our unmatched samples. This method is not suitable
network of over 100 commercial labs, for high sulphide materials >1%. The
sample preparation facilities and mine-site following package is available at select
labs are linked to form a uniform global SGS geochemical laboratories:
platform that extends into an unparalleled
XRF78S – Iron Ore Analysis of Majors and
number of countries and mining camps.
Minors by Fusion-XRF
•• Majors: Al2O3, CaO, Cr2O3, K2O,
MgO, MnO, Na2O, P2O5, Fe2O3,
SiO2, TiO2, LOI and S as SO3
SGS is committed to providing •• Minors: Ba, Cu, Ni, Ta, V, Zn, Zr
preparation procedures that are dedicated
to exploration or mining for ores at each of
Thermogravimetric analysis
our locations. This involves technologically
advanced equipment and, in most cases, SGS provides thermogravimetric analysis
physically separated sample processing at many of our geochemistry labs globally.
areas for different sample types. The Thermogravimetric analysis allows for the
crushing and pulverizing options available determination of Loss on Ignition (LOI)
are varied. Your choice can depend on from raw iron ore samples by passing
the sample type, size and/or form of the them through a number of furnaces with
element of interest within the sample progressively higher temperatures. The
matrix. Please consult with our staff for LOI is a measure of the water content
the best possible option for your samples of the ore and an important step in iron
Through our unparalleled global network,
before starting analysis. ore analysis. When ore is fed into a blast
SGS has the capabilities to provide you
furnace, the water contained in it will
with a range of services for geochemical During sample preparation, there are
evaporate. In order to characterize the
analysis for iron ore including: many critical points where sample
sample, we must determine the weight
contamination can occur. One such area
•• Sample preparation loss of the ore at specific temperatures.
arises from the type of equipment used.
•• Laboratory analysis
Unfortunately, during sample preparation,
•• Davis Tube Analysis
contamination can never be avoided. The
•• Party (settlement) and umpire
levels are dependent on sample hardness,
analysis
crushing and pulverizing time as well as
crushing / grinding media used.
sgs minerals services – T3 SGS 965 2

davis tube recovery QUALITY Assurance standards our labs adhere to. Problems
are detected and remedied promptly to
As many iron ores either are magnetite or SGS operates a quality assurance
ensure analytical accuracy.
contain magnetite, the use of Davis Tube program to ensure our data meets
Recovery (DTR) is industry standard for international quality standards. Quality
the quantitative analysis of the magnetic assurance standards are constantly
minerals in the sample. SGS experts monitored through participation in
will use DTR to determine the magnetic numerous industry and organizational
content of your iron ore. Sample material programs, as well as in our own, unique
is placed in a glass tube at a 45° angle round robin program administered through
between 2 powerful electromagnets. the Institute for Inter-laboratory Studies.
A slurry sample is poured through the Our lab uses concepts of Total Quality
tube slowly and then the tube is rinsed Management (TQM) to ensure consistent
with water so only a clean concentrate operation on a daily basis. TQM is a
of magnetic material remains. Other comprehensive and structured approach
geochemical analyses can then be used to laboratory work that seeks to improve Internal Quality Control
to further quantify the nonmagnetic the quality of analysis through ongoing
All SGS laboratories have formally
content of the ore, providing you with refinements in laboratory processes
documented QA/QC procedures and data
accurate information to forecast potential based on continuous quality feedback.
acceptance systems that are contained in
commercial recoveries.
on-site Quality and SOP manuals. Where
the laboratories are accredited or going
through the accreditation process these
documents have been audited repeatedly
by international quality authorities as part
of the ISO/IEC 17025 accreditation held
by many SGS laboratories.
© SGS Group Management SA – 2013 – All rights reserved - SGS is a registered trademark of SGS Group Management SA

Conclusion
SGS provides unmatched analytical
services to all aspects of the minerals
industry. Our Centres of Excellence are
ISO / IEC 17025 accredited for specific
registered tests and most of our major
Party (settlement) and umpire regional facilities are ISO 9001 certified.
analysis Regardless of the stage of your project,
SGS Minerals Services laboratories SGS geochemists perform quality,
have been performing control, party rapid-turnaround analyses targeting a
and umpire assays and analytical wide variety of elements in many types
SGS continually monitors analytical
determinations of pay and penalty for of sample matrices. We have firmly
processes through the application of
over 20 years. We have strong, long- committed to advanced technology, and
statistical process control (SPC). SPC
term laboratory-client relationships. this commitment ensures we can deliver
involves plotting the results of chemical
Commercial transactions are settled on on our promise to provide benchmark-
processes and using statistical methods
our results, so we know that they must setting services.
to monitor, evaluate, and predict process
be timely and accurate. Our laboratory behaviors. SPC is an effective tool that
Contact Information
uses industry-standard methods and ISO determines if process results are outside
/ IEC 17025 quality assurance and quality either the acceptable range for the Email us at minerals@sgs.com
control practices. Our laboratories are chemical process or outside the quality www.sgs.com/mining
first-rate facilities staffed by experienced
technical professionals including a team of
research chemists that have the expertise
to solve the most daunting sampling and
analytical problems.

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