Name Method of ISOcyanate (PMDI)-Desmodur 44V 20 Date Issued

Parameter Name Test Method Unit Specification Measured Value

S/L No
1 Appearance/Color In house N/A Brownish

2 Viscosity at 25 ◦C ASTM D-4878 Cps 160~240

3 NCO Content Tritometric % 30.5~32.50

4 Acidity ASTM D-974 mg/gm ≤200

5 Density In house gm/cc 1.22~1.24

Draft By Check By Approval(1) Approval(2) Walton High -Tec Industries Ltd, Chandra
Kaliakoir,Gazipur
Depart Name QC
Section Wire Harness QC, IQC &
QC Lab

Page 1 of 4 Ref No Rev No Sub Section Chemical IQC

Name Method of ISOcyanate (PMDI)-Desmodur 44V 20 Date Issued

1.0 List of machine ,Equipment or tools used

1.1 Viscosity Meter
1.2 Dropper
1.3 Beaker
1.4 Conical Flask
1.5 Burette
1.6 Burette Stand
1.7 Shringe
1.8 High precision laboratory Balance
1.9 Tissue
1.10 Volumetric Flask
1.11 Glass Funnel
1.12 Pipette 10ml & 25ml
1.13 Pipette Filler
1.14 Electromagnetic stirrer
2.0 List Of Chemical Raw material
2.1 0.5 N HCL Solution
2.2 Distilled water
2.3 Phenolpthlein Indicator
2.4 Bromofanol Blue Indicatore
2.5 0.2N N-dibutyl Amine
2.6 Sodium carbonet an-hydros Pure

Draft Check Approval(1) Approval(2)

Walton High -Tec Industries Ltd, Chandra Kaliakoir

Depart Name QC
Section Wire Harness QC, IQC & QC
Lab
Page 2 of 4 Ref No Rev No Sub Section Chemical IQC
Name Method of ISOcyanate (PMDI)-Desmodur 44V 20 Date Issued
3.0 Method of analysis
3.1 Appearance:
Take 50 ml sample in 100 ml beaker.Check visually the solution should be clear.
3.2 Viscosity :
3.3.1: At first power on the machine & Spindle are setting to the machine (According to higher & lower range of the sample)
3.3.2: Sample are taken in the beaker & spindle of the viscometer are dipped in the tested sample.
3.3.3: Select the spindle ,RPM & Time of the machine .
3.3.4: Then start the test by click the run batton
3.3.5: End of the time a fixed value show in the machine display in a specific unit as Cps .
3.3.6: Again click the run batton for continue the test.
3.3.7: Tested result are recorded .
3.3.8: After complete the test the spindle are clean within cleaning agent(Acetone then water)
3.4.0 NCO Content:
3.4.1: Test Procedure:-
3.4.1: 3.4.2: 0.5 - 0.6g PMDI (ISO)
0.5- 3.4.3: 50ml 0.2N di-butyl amine are taken in Conical Flask, being careful not splash any out of the jar.
0.60g 3.4.4: Add Teflon coated stirring bar, cap jar tightly and place on a magnetic stirrer.
m
3.4.5: Agitate sample gently until it is completely dissolved.
PMDI
(ISO) 3.4.6: Add 6 drop of bromphenol blue indicator & titrate to a yellow –green endpoint with aqueous 0.5N HCl
50ml 3.4.7: Run a blank at the same time as the sample, following the sample procedure omitting the same.
0.2N
di-
buty
amin Draft Check Approval(1) Approval(2)
are Walton High -Tec Industries Ltd, Chandra Kaliakoir
taken
in Depart Name QC
Conica
Section Wire Harness QC, IQC & QC
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,being Page 3 of 4 Ref No Rev No Sub Section Chemical IQC
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Name Method of ISOcyanate (PMDI)-Desmodur 44V 20 Date Issued

3.5.0: Calculation:
3.5.1: %NCO =4202*Conc.HCl(B-A)/Sample Wt.*1000
3.6.0: Where:-
3.6.1: B=Blank titer
3.6.2: A=Sample titer
3.6.3: Preparation 0.5N HCl & 0.2N n-di-butyl amine solution:
3.6.4: Take 42.36ml HCl in 1000ml D.I water (For Lab grade 37% HCl)
3.6.5: Add 35ml N-di-butyl amine in 1000ml tetrahydrofuran(for 0.2N di-butyl amine solution)

Draft By Check By Approval(1) Approval(2)

Walton High -Tec Industries Ltd, Chandra Kaliakoir

Swapon Kumar Shill Depart Name QC

Section Wire Harness QC, IQC & QC
Lab
Page 4 of 4 Ref No Rev No Sub Section Chemical IQC