This document provides instructions for preparing hydrochloric acid solutions between 0.02 N and 1 N and standardizing the solutions. It describes measuring concentrated hydrochloric acid and diluting it with water to make the desired normality. For standardization, a known amount of sodium carbonate is titrated with the acid solution using methyl red as an indicator. The normality of the acid solution is then calculated based on the grams of sodium carbonate used and milliliters of acid consumed. Safety precautions like controlling temperature, using personal protective equipment and understanding instructions are also outlined.
Original Description:
Original Title
OKP for the preparation of hydrochloric acid(0.02 to 1.0 N) & Its standardization.
This document provides instructions for preparing hydrochloric acid solutions between 0.02 N and 1 N and standardizing the solutions. It describes measuring concentrated hydrochloric acid and diluting it with water to make the desired normality. For standardization, a known amount of sodium carbonate is titrated with the acid solution using methyl red as an indicator. The normality of the acid solution is then calculated based on the grams of sodium carbonate used and milliliters of acid consumed. Safety precautions like controlling temperature, using personal protective equipment and understanding instructions are also outlined.
This document provides instructions for preparing hydrochloric acid solutions between 0.02 N and 1 N and standardizing the solutions. It describes measuring concentrated hydrochloric acid and diluting it with water to make the desired normality. For standardization, a known amount of sodium carbonate is titrated with the acid solution using methyl red as an indicator. The normality of the acid solution is then calculated based on the grams of sodium carbonate used and milliliters of acid consumed. Safety precautions like controlling temperature, using personal protective equipment and understanding instructions are also outlined.
Process Description Method Information. Machine TG:N/A Reference Number: Dept. Name & Rev. No. 00 OKP for the preparation of ASTM E200 Calibration Number: Section SOP Source: hydrchloric acid(0.02 to 1N) & Quality Control/IQC Its standardization Chemical
Operational Key Point
Hydrochloric acid Solution preparation: 1.To prepare a 0.1 N Solution, measure 8.3 ml of concentrated hydrochloric acid(Sp gr 1.19) into 1L Volumetric flask & dilute to the mark with water, mix well , and store in a tightly closed glass container .For the other normalities of HCl solution use the requirements given in the table-4. 2. Standardize the solution in the following Manner. Standardization Procedure: 1) Transfer 2 to 4 g of anhydrous sodium carbonate to a platinum dish or crusible, and dry at 250 degree for 4 hour . Cool in desicator. 2) To standardize a 0.1 N solution or any normality take weight accurately 0.22 ±0.01 g [From table-5 as per Normality] of the dried sodium carbonate, and transfer to 500 ml conical flask. 3) Add 50ml of water, swirl to dissolve the carbonate & add 2 drops of a 0.1% solution of methyl red in alcohol. 4)Add the acid slowly from a burette, with constant stirring , until the solution becomes faintly pink.Heat the solution to boiling,cool & continue the titration. 5) Heat again to boiling & titrate further as necessary until the faint pink color is no longer affected by continued boiling. Calculation :Calculate the molarity of HCl Solution as follows: A =B/0.053V Where, A=Normality of HCl Solution B=grams of Sodium Carbonate used V= ML of HCl Solution consumed. Stability: Restandardize Monthly.
1. Control the room temperature At 25°C .
2. Use safety Mask when chemical is Used. 3. Put on Hand Gloves when clean & chemical used in laboratory. 4. Read and understand all the instructions mentioned in the process manual before the test.