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Influence of Interpass Cooling Conditions On Microstructure WAAM TiAl
Influence of Interpass Cooling Conditions On Microstructure WAAM TiAl
https://doi.org/10.1007/s40194-020-00921-3
RESEARCH PAPER
Abstract
Wire and arc additive manufacturing (WAAM) technology is growing in interest in the last years. The technology enables the
manufacturing of real geometries by overlapping weld beads and is well suited for metallic parts with high buy-to-fly ratio.
Manufacturing costs and time are critical issues which determine the business case. Therefore, it is necessary to develop strategies
that minimise the production time while meeting quality requirements. In this regard, cooling conditions are a key factor to reduce
time and determine mechanical properties and resulting microstructure. This study aims at investigating the effect of interpass
cooling conditions on resulting mechanical properties and microstructure of Ti-6Al-4V alloy. The influence of dwell time
between successive deposition of layers is investigated both for air and forced interpass cooling. Forced cooling is done by
using water-cooled anvil under base plate. The goal is to find a minimum dwell time to maximise arc-on time and deposition rate
while avoiding wall collapse, widening, oxidation and the need to apply post building heat treatment. Obtained mechanical
properties are compared with standards for products manufactured by conventional manufacturing. Additionally, microstructure,
surface finishing and part accuracy of WAAM samples are characterised.
Keywords WAAM . Ti-6Al-4V . Microstructure . Tensile properties . Dwell time . Interpass cooling
1 Introduction Main challenges related to the technology are high part accu-
racy, robust process build-up, achieving proper mechanical
In the last years, WAAM technology has been extensively properties and high part quality. Moreover, the business case
investigated by many research teams around the world. depends greatly on the manufacturing time which is usually
optimised in different steps along the process. In a first step,
Recommended for publication by Commission I - Additive welding parameters are optimised for a specific material, i.e.
Manufacturing, Surfacing, and Thermal Cutting filler metal, by manufacturing simple walls. The next step
This article is part of the collection Additive Manufacturing – Processes, requires the application of these parameters for real parts.
Simulation and Inspection The application of parameters adds complexity due to inter-
sections, different or variable wall thicknesses, heat accumu-
* L. Vázquez lation and distortions among others [1], which reduce part
lvazquez@lortek.es accuracy and prevent stable and even build-up process. At this
point, the manufacturing time needs to be optimised without
N. Rodríguez
nrodriguez@lortek.es
compromising the part quality.
The quality of WAAM-produced Ti-6Al-4V parts is
I. Rodríguez mostly related to the part accuracy which directly affects
irodriguez@lortek.es
the buy-to-fly ratio (BTF), the achievement of even layers
E. Alberdi with constant layer height and the absence of defects to
ealberdi@lortek.es obtain the required mechanical properties. Heat accumu-
P. Álvarez lation is one of the main concerns related to part accuracy
palvarez@lortek.es and distortion [2] [3–5]. For Ti-6Al-4V, the mechanical
1
characteristics are not only linked to the resulting micro-
LORTEK, Technological Centre, Arranomendia kalea 4A, structure but also the oxidation level. Both factors are
20240 Ordizia, Spain
Weld World
Table 1 Chemical composition given by the provider of Ti-6Al-4V (grade 5) wire in wt.%
Ti C O N H Fe Al V
Ti-6Al-4V Bal. 0.050 max 0.12–0.20 0.030 max 0.015 max 0.220 max 5.5–6.75 3.5–4.5
largely affected by the thermal history. Hence, interpass The nature of additive manufacturing itself consists of the
temperature can be controlled by different methods such deposition of numerous material layers leading to a near net
as the application of specific dwell times or by the use of shape part. This introduces a very specific thermal history
forced cooling [6]. which determines the final microstructure, distortion and re-
When reactive materials are used in WAAM, such as Ti- sidual stresses in the part. During the WAAM process, the
6Al-4V which is one of the widely used materials for struc- relative cooling rate is low compared to other additive
tural parts in aerospace, oxidation has to be avoided in order to manufacturing processes such as laser-based powder bed fu-
maintain its specific properties [7]. In order to avoid oxidation, sion, as it melts a very fine layer of powdered particles at high
the exposure to oxygen-containing atmospheres must be lim- speed [11]. The amount of material melted with WAAM is
ited, especially at temperatures above 300–400 °C, as below higher which leads to higher heat preservation while obtaining
this temperature range, the oxidation rate slows down [7, 8]. In slower cooling rates [11].
this sense, different protection solutions have been developed In general, AM induces preferential grain growth along
in different WAAM studies including closed chambers and the building direction and hence anisotropic mechanical
dynamic shielding systems [9]. Closed chambers limit the size properties [12] due to columnar prior β grains aligned in
of to-be manufactured parts and the demand of protective gas the growing direction as a consequence of different heat
is very high. Alternative devices comparable to conventional dissipation conditions in different directions [13]. Prior β
trailing systems for welding have also been used for the same grains are formed during solidification from liquid melt
purpose with promising results [9]. For these dynamic pool and can be transformed afterwards due to diffusional
WAAM shielding systems, it is essential to ensure good and non-diffusional solid-state transformation. In WAAM-
shielding conditions while the deposited material is above produced Ti-6Al-4V parts, the final microstructure inside
the temperature range leading to quick oxidation kinetics both these prior β grains consists of lamellar α phase inside a β
during welding and interpass dwell time. matrix. This is generally known as a Widmanstätten struc-
Interpass temperature also influences the stability of the ture [14, 15]. These prior β grains can be observed due to a
building process: at very high interpass temperatures, the ma- surrounding α phase in the grain boundaries and the dif-
terial flow eases and increases the width of the weld bead ferent textures between grains. According to different au-
which then leads to a loss in part accuracy and finally col- thors, rapid cooling rates result in a microstructure which
lapses [10]. Effect of interpass temperature must be taken into consists on very fine α phase, and in some cases, martens-
account when calculating the BTF ratio and a balance must be ite (α′) can be found in the as-built condition in WAAM-
found between manufacturing time and finishing machining produced Ti-6Al-4V parts [15]. This entails low ductility
work. When WAAM is applied to high-value materials, the which normally is solved by the application of post build-
BTF ratio needs to be as close as possible to 1. Being a near ing heat treatments or HIP (hot isostatic pressure) [16, 11].
net shape manufacturing process requiring final machining, On one hand, these treatments also improve the fatigue
optimum BTF ratios for WAAM parts are usually in the range behaviour which is required for aerospace applications;
of 1.2–1.5. These values support the business case of many on the other hand, they add long processing times and extra
products built by WAAM [5, 10]. costs.
Besides the use of post building heat treatments in order to working forces have on the final microstructure. Despite the
optimise mechanical properties of Ti-6Al-4V parts resulting recrystallised grains being mostly equiaxed, some
manufactured by WAAM [11], some authors applied cold irregular grains are also obtained and improved interpass
work between the deposition of successive layers aiming to working methods are being currently studied. Side peening
create new finer microstructures with less residual stresses [8, has led to equiaxed grains with more regular grain size [8];
17, 18]. The resulting microstructure showed equiaxial grains, however, this method cannot be applied easily to real parts.
and hence, more isotropic mechanical properties were obtain- This work aims to study the effect of interpass cooling
ed. The drawback of this method is the additional time needed conditions on microstructure and tensile properties of Ti-
for the application of cold work after the deposition of each 6Al-4V parts produced by WAAM. Cooling conditions
layer and the extra axis required for that job which adds com- have been modified by changing the dwell time between
plexity to the WAAM equipment. Moreover, nowadays, it is the deposition of consecutive weld beads both in air cooled
not completely clear what influence the temperature and cold and forced cooled WAAM samples. Forced cooling
Table 2 Welding parameters for the manufacturing of walls of 16 L/min. Additionally, a dynamic shielding device, de-
Current Wire feed speed Voltage Travel speed Deposition rate signed by the authors, was used in order to provide protection
(A) (m/min) (V) (cm/min) (kg/h) against the oxidation in a big area (200 × 200 mm). The gas
flow of the shielding device was settled to 200 L/min. A 1.14-
140 8.5 15.8 70 2.3 mm diameter Ti-6Al-4V (grade 5) wire was employed as filler
metal. The chemical composition of the wire, given by the
provider, can be shown in Table 1.
conditions were applied by using a cooling plate beneath For the study, a plate with internal water conformal
the base plate. The assessment of the influence has been cooling connected to a chilling machine was attached un-
done by the analysis of the tensile properties in different derneath the substrate of the part in order to induce forced
directions (X, horizontal and Z, vertical) and the advanced cooling conditions. The monitoring of the temperature dur-
characterisation of the obtained microstructure. Best ing the whole manufacturing process was achieved by two
interpass cooling conditions are proposed at the end in K type thermocouples welded to the substrate. The dis-
order to meet the requirements such as low processing tance between the manufactured part and the thermocou-
time, regular growing and best balance of mechanical ples was 2 mm and the distance between the thermocouples
properties. To the best knowledge of the authors, a specific was 40 mm (Fig. 1).
standard for the WAAM process has not been developed The set-up for the manufacturing of WAAM-produced
until now, and as a consequence, standards from cast and walls can be observed in Fig. 2.
wrought materials have to be considered to check the ful- Two different types of walls were manufactured. Both
filment of the required quality. consisted of 18 mm wall thickness. Additionally, small walls
(Fig. 3a) were built by the deposition of six layers and used for
microstructural characterisation and big walls (125 × 80 mm)
(Fig. 3b) for mechanical characterisation.
2 Experimental procedures Oscillating weld beads with continuous C1001 synergic
CMT curve were deposited on approximately 10-mm-thick
Ti-6Al-4V parts produced by WAAM were built in an arc substrate plates which were clamped to the cooling plate. In
welding robotic cell. A Fronius transplus synergic (TPS) Table 2, the welding parameters are detailed.
4000 CMT R power source and a Robacta drive CMT Depositing of the layers was done according to an oscillat-
W/F++ 6.25-mm torch from Fronius International were used. ing strategy as is detailed in Fig. 4. This strategy is more
A CMT torch was attached to a 6-axis Kuka robot KR 16 KS versatile than parallel one as it allows the manufacturing of
model with a KRC2 controller. The gas shielding of the torch zones with variable thickness present in real parts. The strate-
was carried out with Argon (99.999% purity) and a gas flow gy was based on a repeated sequence of a pair of layers in
0 Without
0 With
1 With
5 Without
9 Without
Table 4 Mechanical properties achieved for the as-built in the horizon- Table 5 Interpass temperatures measured for the different cooling
tal direction conditions
Dwell t (min) Cooling plate YS (MPa) UTS (MPa) e (%) Interpass Te (°C) Dwell t (min) Cooling plate
Fig. 7 Temperature record during WAAM for the different interpass cooling conditions, including the records from two thermocouples and the use of
forced cooling (AC). The dwell times: a 0 min, b 1 min, c 3 min, d 5 min
Weld World
Table 6 Microstructure
description and measurements of Dwell t (min) Cooling plate Microstructure Wid α laths (μm) GB α (μm)
thickness of α phase
0 Without Coarse 1.41 2.85
0 With Fine 1.73 2.71
1 With Mixed 1.37 2.02
5 Without Martensitic 1.45 2.37
9 Without Mixed 1.37 1.35
9 + 920 °C Without Coarse 3.66 3.79
The estimated values of interpass temperatures are collect- and Widmanstätten α phase are found. When a dwell time of
ed from Fig. 7 and Table 5. Beyond the deposition of three 1 min is applied, martensite is broadly displayed and both α in
weld beads, the interpass temperature keeps constant during the grain boundaries and Widmanstätten α are finer.
the process, which means steady-state process condition and Some microstructures are composed of grains of differ-
assures a stable part manufacturing. ent phases (martensite, fine and coarse Widmanstätten α
Micrographs were obtained from each cross section in or- phase), which have been named as mixed microstructures.
der to get a general overview of microstructural characteristics The thickness of Widmanstätten α laths and α in the grain
for different tested interpass cooling conditions. boundaries was measured and the data is plotted in Table 6.
The microstructures created without forced cooling can be A minimum of 15 measurements were done in different
observed in Fig. 8. In the case of a dwell time of 0 min, that is, areas.
for the highest interpass temperature and lowest cooling Figure 10 represents the measured data and shows a trend
rates, traces of martensite (α′) can be found, whereas coarse to gather a thicker α phase in the grain boundary for higher
Widmanstätten α is the general phase. For a dwell time of interpass temperatures. In the case of the thickness of
5 min, extended martensite is observed, the α phase in the Widmanstätten α laths, it remains constant. As shown in
grain boundary is finer and the Widmanstätten α is very fine. Fig. 8, after the post building heat treatment, the thickness
After a dwell time of 9 min, the trend is even more distinct. On for both α types grew considerably.
the other hand, after the application of a post building heat Macrographs of cross-sections of WAAM walls with dif-
treatment at 920 °C for 5 h to these samples, the martensite ferent cooling conditions are shown in Fig. 11. In the top row,
disappears, and both α in the grain boundary and the profiles of walls manufactured without forced cooling are
Widmanstätten α become coarser. shown for different dwell times. In this case, stable growth in
Figure 8 d compares the as-built microstructure and the mi- terms of constant wall thickness is achieved at a dwell time of
crostructure after complete post building heat treatment [19]. 3 min; below this dwell time, the profile acquires a V shape
The resulting microstructure when applying forced cooling which entails a high BTF and is very likely to collapse. The
is seen in Fig. 9. For dwell time of 0 min, traces of martensite bottom row shows the profiles obtained with the use of a
Fig. 11 Profiles of WAAM-produced walls for studied cooling condition (dwell time-application of forced cooling): a 0 min-without, b 1 min-without, c
3 min-without, d 5 min-without, e 0 min-with, f 1 min-with, g 3 min-with and h 5 min-with
cooling plate. In this case, a stable growth is noticeable for a manufacturing time must be achieved while assuring the
dwell time of just 1 min. soundness of manufactured parts.
The oxygen content was measured in the centre of the The first goal was to optimise the manufacturing time.
walls. As the obtained values reveal (Table 7), no extra oxy- CMT technology has demonstrated deposition rates up to
gen was added to the chemical composition during the 2.3 kg/h for Ti-6Al-4V alloy (Table 2) [19]. The reported
manufacturing of the walls. deposition rates are theoretical and do not include the
dwell time between the deposition of the weld beads or
arc-off time. Yet, in real WAAM applications, the time As shown in Fig. 11, small walls that were built without
consumption for the manufacturing of a part should in- forced cooling and using dwell times of 0 and 1 min, start
clude the time required for all steps. Hence, maximising losing their straight shape. Instead, a V shape is obtained
the arc-on time provides the best benefits of this due to the heat accumulation. Hence, the use of forced cooling
manufacturing process. In the current study, forced helps to reduce dwell times while keeping constant wall thick-
cooling has been used to increase the interpass cooling, ness along the growth direction. In the reference [20], it is
reduce the dwell time and optimise the manufacturing remarked that the use of forced cooling at the substrate en-
time. Through the application of interpass forced cooling, hances the heat dissipation to avoid collapse. According to the
it was shown that minimum elongation requirements are results of this study, the use of forced cooling increases the
deployed for using a dwell time 1 min versus 9 min for strength and elongation at break values when increasing the
the air cooling conditions. dwell time for 1 min. However, without forced cooling, the
The second goal was to check if the application of dwell time needed to achieve similar results is 9 min. In both
suitable interpass cooling conditions could lead to sam- cases, all obtained values fulfil the standard AMS 4985C-
ples meeting the standards in terms of static mechanical 2003 for Ti-6Al-4V castings.
properties and without the need of applying any post Forced cooling and longer dwell times avoid the growth of
building heat treatment. Additional thermal treatments α phase along the grain boundaries as shown in Table 6. The
are not desirable in order to avoid the extra cost. Two samples with a thinner α phase along the grain boundaries
interpass cooling conditions with and without forced showed higher elongations at break as observed from
cooling that comply with the current casting standards Fig. 12. The coarse size and elongated shape of prior β grains
were obtained in this study. However, in order to comply which solidified initially from the melt pool and the presence
with current wrought standards, which are more demand- of α phase along their grain boundaries act as a path for dam-
ing, the application of post building heat treatment was age propagation [21]. Other authors also reported previously
required. the assisted propagation of cracks along thick α phase grain
The conditions to enable a constant wall thickness and to boundary [13]. On the other hand, the thickness of
avoid a collapse of the walls due to excessive heat accumula- Widmanstätten α laths does not have a clear influence on
tion have also been studied. For this, sound and straight wall the elongation at break.
of six layers with constant width and 25 mm total height were Fast cooling conditions also promote the formation of mar-
manufactured while maintaining flat and regular weld beads tensite in the bottom of the newly deposited weld beads due to
along the whole deposition. The manufacturing of vertical the high cooling rates. In the resulting mixed structures, mar-
walls with constant thickness is critical to reduce the final tensite is not as detrimental as a thick α phase along the grain
machining time which implies important savings of the costs boundaries. The combination of thick α phase along the prior
associated to the machining of Ti-6Al-4V. β grain boundaries and the high amount of grain boundaries in
Weld World
Fig. 13 Macrostructure of
WAAM-produced Ti-6Al-4V
parts in the a as-built condition
and b after the application of post
building heat treatment at 920 °C
Weld World
& Forced cooling is very effective in getting appropriate me- Weld World 62:1083–1096. https://doi.org/10.1007/s40194-018-
0606-6
chanical properties for Ti-6Al-4V alloy at short dwell
11. Bermingham MJ, Nicastro L, Kent D, Chen Y, Dargusch MS (Jul.
times (1 min). 2018) Optimising the mechanical properties of Ti-6Al-4V compo-
& To achieve comparable results without forced cooling, the nents produced by wire + arc additive manufacturing with post-
dwell time must be increased to 9 min in order to reduce process heat treatments. J Alloys Compd 753:247–255. https://
the interpass temperature and to avoid excessive coarsen- doi.org/10.1016/J.JALLCOM.2018.04.158
12. Ding D, Pan Z, Cuiuri D, Li H (2015) Wire-feed additive
ing of the αGB phase. manufacturing of metal components: technologies, developments
& The mechanical properties in as-built condition highly de- and future interests. Int J Adv Manuf Technol 81(1–4):465–481.
pend on the thickness of αGB and prior β grain columnar https://doi.org/10.1007/s00170-015-7077-3
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Funding information The Provincial Council of Guipuzcoa provided 14. Baufeld B, Brandl E, Van Der Biest O (2011) Wire based additive
support within the ADITARC project with number OF2018/2018, which layer manufacturing: comparison of microstructure and mechanical
has been financed by Science, Technology and Innovation support properties of Ti-6Al-4V components fabricated by laser-beam de-
program. position and shaped metal deposition. J Mater Process Technol
211(6):1146–1158. https://doi.org/10.1016/j.jmatprotec.2011.01.
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