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Gas Detection Microsystem With MEMS Gas Sensor and Integrated Circuit
Gas Detection Microsystem With MEMS Gas Sensor and Integrated Circuit
Abstract— In this paper, a gas detection microsystem which occupies a large area and leads to a high price [12], [15]–[17].
consists of a highly sensitive micro-electro mechanical sys- Although the design of the PCB is extremely simple, it is
tems (MEMS) gas sensor and a CMOS integrated circuit, necessary to design a chip which can take the place of PCB
including a read-out circuit, data processing circuit, and an
interface circuit is presented. The integrated microsystem whose for miniaturization and low price.
area is less than 3 mm2 can work with only power supply due With the development of technology in the past 20 years,
to the integration and flexibility. By packing the MEMS gas a miniaturized gas-sensing system can be realized on a
sensor with the integrated circuit using a customized package, single chip (single-chip approach) [18]–[20] or on different
the system can detect a variety of gases, including ethylene glycol, chips included in the same package [21], [22] (multi-chip
ammonia, and alcohol accurately at low concentrations (<1 ppm).
The maximum response toward the gas in the concentration approach) [6]. In the single-chip approach the whole system
of 100 ppm can reach about 8. is realized in a fabrication process optimized for integrated
circuits (IC) including the interface circuit, with a few com-
Index Terms— MEMS gas sensors, CMOS integrated circuit,
integrated microsystem. patible post-processing steps (typically etching or deposition
of materials) [10]. Essay gives a good example of an excellent
I. I NTRODUCTION designed integrated system by Afridi et al. [18] in 2002.
Although he achieved monolithic integration, the interface
W ITH the improvement of living environment require-
ments and the safety of industrial production, there
had been more and more interests and efforts in gas detection
circuits can’t meet all the needs for data processing and
communicating with the computer. Similarly, the multi-chip
systems. Particular development has been made to monitor approach the interconnections between the sensor chip and the
the environment-related gases such as VOC [1]–[5]. The new interface circuit, chip can be made with bonding wires or with
demand for portable, low-cost gas-sensing systems is growing other techniques, such as flip-chip or wafer bonding. With
every year, with a focus on safety and security issues [6]. With this approach the different chips can be fabricated with dif-
the development of micro-electro mechanical systems(MEMS) ferent technologies and optimized for the sensors and the
technology [7], [8], miniaturized resistive MEMS gas sensors circuitry [6]. Therefore, both of two approaches are more
can work at high temperature around 300-400° to achieve an useful than the design with the PCB.
acceptable sensitivity in few tens of milliseconds, consuming The single-chip gas-sensing system requires smaller area for
a small amount of power [3], [9]–[14]. the whole chip. However, this approach may increase the costs
A gas detection system has to be self-consistent and it for an advanced fabrication process and decrease the
has to work without the need of any laboratory instruments. flexibility of the system, thus making the design more
Therefore, a gas-sensing system consists of a particular gas challenging [6]. Moreover, if there is any problem in the any
sensor, a readout circuit, a data processing circuit including a one of two parts, the other parts can’t work while the multi-
high precision analog-to-digital converter (ADC) and an inter- chip approach can avoid the problem because of separate
face circuit for communication with the computer [10]. In the design. So a lot of researchers chose to design a gas sensor and
past decades, many researchers built the interface circuitry an application specific chip in multi-chips approach., in view
which can realize the independence of the system in the form of its flexibility and potentially low cost. Malcovati et al. [6]
of discrete components on a printed circuit board(PCB) which designed a CMOS integrated interface circuit which can realize
the independence of the system for metal-oxide gas sensors by
Manuscript received November 29, 2017; revised March 27, 2018; accepted the means of the multi-chip approach in 2012. Many problems
April 14, 2018. Date of publication April 24, 2018; date of current version on the accuracy and communication with computer and smart
July 24, 2018. This work was supported by the Fundamental Research
Funds for the Central Universities under Grant WK2100000005. The associate phone still exist in gas detection system. Meanwhile, the area
editor coordinating the review of this paper and approving it for publication of the chip will affect the portability of the system when it is
was Dr. Pantelis Georgiou. (Jin Wang and Jiaqi Yang are co-first authors.) larger than 10 mm2 [6].
(Corresponding author: Lei Xu.)
J. Wang, J. Yang, D. Chen, L. Jin, Y. Li, L. Xu, F. Lin, and F. Wu are with In this paper, we give a detailed description of the gas
the School of Information Science and Technology, University of Science and detection microsystem including the MEMS gas sensor [23]
Technology of China, Hefei 230027, China (e-mail: okxulei@ustc.edu.cn). and the specific chip. The chip which is fabricated in a
Y. Zhang and Y. Guo are with the School of Physics and Materials Science,
Anhui University, Hefei 230601, China. standard 0.18 um CMOS process can realize all the functions
Digital Object Identifier 10.1109/JSEN.2018.2829742 above, for instance, a variable power supply for gas sensors,
1558-1748 © 2018 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission.
See http://www.ieee.org/publications_standards/publications/rights/index.html for more information.
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6766 IEEE SENSORS JOURNAL, VOL. 18, NO. 16, AUGUST 15, 2018
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WANG et al.: GAS DETECTION MICROSYSTEM WITH MEMS GAS SENSOR AND IC 6767
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6768 IEEE SENSORS JOURNAL, VOL. 18, NO. 16, AUGUST 15, 2018
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WANG et al.: GAS DETECTION MICROSYSTEM WITH MEMS GAS SENSOR AND IC 6769
chip and gas sensor were connected with different pins of the
package by an Au wire using a bonding process. The different
functions of different pins are shown in Fig. 9(a). As shown
in Fig. 9(a), pin2 and pin6 are the ground for the chip; pin5 and
pin7 can be a power supply for the chip; pin3 and pin4 are the
communication ports which can communicate with an external
microcontroller; the output of gas sensor was connected with
pin8 for convenient verification. After the chip was connected
with package, the gas sensor can be enabled or disabled and
measured using a serial interface by a microcontroller (MCU).
The MCU can control the chip by writing data to the
register. To enable the gas sensor, the MCU sends a start signal
to each part in the chip and gas sensor. After measurement in
ADC, the data will be saved in the register and passed to the
MCU using I2 C interface through pin3 and pin4. Fig. 12. Calibration curve of the gas sensor towards H2 .
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6770 IEEE SENSORS JOURNAL, VOL. 18, NO. 16, AUGUST 15, 2018
Fig. 13. Sensor response to gases. (a) Response of the gas sensor to different concentrations of H2 , without recovery in pure air. (b) Response of the gas
sensor to different concentrations of (CH2 OH)2 . (c) Response of the gas sensor to different concentrations of NH3 . (d) Response of the gas sensor to different
concentrations of CH3 CH2 OH.
over the range from 10 ppm to 100 ppm. The response can be
defined as the following:
Rair
Resonpse = (3)
Rgas
where Rair is the measured resistance in ambient air, Rgas is
the resistance when the sensor is exposed to target gases. The
sensitivity is directly proportional to the change in resistance.
The Rair can be expressed through the voltage of gas sensor
by Ohm’s law [36]:
V outair
Rair = Rl (4)
V r e f − V outair
the response value can be expressed by voltage:
(V r e f − V outgas) V outair
Response = (5) Fig. 14. Gas response to different concentration of H2 , NH3 , CH3 CH2 OH,
V outgas (V r e f − V outair ) (CH2 OH)2 .
where Voutair is the measured voltage in ambient air, Voutgas
is the voltage when the sensor is exposed to target gases. gas sensor are also presented as shown in the Fig. 14, which
The response to H2 can reach about 6.6. Apart from H2 , the shows different linear increment in the response change to
response of the gas sensor to other gas has been measured. the increment in concentration of gas over different ranges.
As shown in Fig. 13, the gas sensor can distinguish different Among the target gases, the response to alcohol and ethylene
concentrations of ammonia (NH3 ), alcohol (CH3 CH2 OH) and glycol ((CH2 OH)2 ) are over 6, and fast response time is
ethylene glycol (CH2 OH)2 . Those experiments are static tests within 10 s. It has been observed that when the concentration
with a sealed chamber (volume 19L) at room temperature. of gas reaches a high level, the response will be slower
After the voltage of the gas sensor stabilizing in the air, the with the increase in gas concentration. The possible reason
concentrations of gas in the chamber can be increased by for the nearly saturated response to higher concentration is
injecting gas into the chamber. Fig. 13 shows a representative that the rate of absorption at the surface of structures is
response to different concentrations of ammonia ranging from close to saturation [37]. The response to ethylene glycol
1ppm to 100 ppm. As shown in the Fig. 13, the 1 ppm can reach about 8. So the gas sensor is a multiplexing gas
ammonia was clearly detectable. Calibration curves of the detector. However, the response to ethylene glycol can reach an
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WANG et al.: GAS DETECTION MICROSYSTEM WITH MEMS GAS SENSOR AND IC 6771
especially higher value than other gases when the concentra- [6] P. Malcovati, M. Grassi, and A. Baschirotto, “Towards high-dynamic
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6772 IEEE SENSORS JOURNAL, VOL. 18, NO. 16, AUGUST 15, 2018
[31] K. Choe, O. D. Bernal, D. Nuttman, and M. Je, “A precision relaxation Lei Xu received the B.S. degree in electronic and information engineering
oscillator with a self-clocked offset-cancellation scheme for implantable from Anhui Normal University, Wuhu, China, in 2007, and the Ph.D. degree
biomedical SoCs,” in IEEE Int. Solid-State Circuits Conf. (ISSCC) Dig. from the Shanghai Institute of Microsystem and Information Technology,
Tech. Papers, Feb. 2009, pp. 402–403. Chinese Academy of Sciences, Shanghai, China, in 2012. Then, he joined the
[32] Y. Tokunaga, S. Sakiyama, A. Matsumoto, and S. Dosho, “An on-chip No. 38 Research Institute, China Electronics Technology Group Corporation,
CMOS relaxation oscillator with voltage averaging feedback,” IEEE Hefei, China, where he was an Engineer in 2012 and a Senior Engineer
J. Solid-State Circuits, vol. 45, no. 6, pp. 1150–1158, Jun. 2010. in 2015. He was a Visiting Scholar with the California Institute of Technology,
[33] I. Lee, G. Kim, and W. Kim, “Exponential curvature-compensated Pasadena, CA, USA, from 2014 to 2015. In 2016, he joined the University of
BiCMOS bandgap references,” IEEE J. Solid-State Circuits, vol. 29, Science and Technology of China, Hefei, where he is currently a Professor
no. 11, pp. 1396–1403, Nov. 1994. with the School of Information Science and Technology and the School of
[34] C. M. Andreou, S. Koudounas, and J. Georgiou, “A novel wide- Microelectronics. His research interests include MEMS gas sensors, MEMS
temperature-range, 3.9 ppm/°C CMOS bandgap reference circuit,” IEEE bio/medical sensors, odor identification, and neural signal detection.
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[37] B. Behera and S. Chandra, “An innovative gas sensor incorporating
ZnO–CuO nanoflakes in planar MEMS technology,” Sens. Actuators B, Youmin Guo received the Ph.D. degree in chemical engineering from the
Chem., vol. 229, pp. 414–424, Jun. 2016. Nanjing University of Technology in 2011. She held a post-doctoral position
with the Institute of Researches on Catalysis and Environment in Lyon,
(IRCELYON-CNRS), France, from 2011 to 2014. In 2014, she joined the
School of Physics and Materials Science, Anhui University. Her research
interests include fuel cells, energy conversion device, and gas sensors.
Jin Wang received the B.S. degree in electronic science and technology from
the Huazhong University of Science and Technology, Wuhan, China, in 2017.
He is currently pursuing the M.Sc. degree with the University of Science and
Technology of China. His research includes the integration of MEMS gas
sensors and CMOS circuits.
Fujiang Lin (M’93–SM’99) received the B.S. and M.S. degrees in electrical
Jiaqi Yang received the B.S. degree in electronic engineering from the engineering from the University of Science and Technology of China (USTC),
Nanjing University of Science and Technology, Nanjing, China, in 2012. Hefei, China, in 1982 and 1984, respectively, and the Dr.Ing. degree in elec-
She is currently pursuing the Ph.D. degree with the Micro-/Nano-Electronic trical engineering from the University of Kassel, Kassel, Germany, in 1993.
System Integration R&D Center, Department of Electronic Science and He was a Research Scientist with the National University of Singapore, Singa-
Technology, University of Science and Technology of China, Hefei, China. pore. In 1995, he was transferred to the Institute of Microelectronics (IME),
Her current research interests include data converters and sensor interface. Singapore, as a Member of Technical Staff, where he pioneered practical
RF modeling for MMIC/RFIC development. In 1999, he joined HP EEsof,
as the Technical Director, where he established the Singapore Microelectronics
Modeling Center, providing accurate state-of-the-art device and package
characterization and modeling solution service worldwide. From 2001 to 2002,
Dongliang Chen received the B.S. degree in communication engineering from he started up and headed Transilica Singapore Pte. Ltd., the Research And
Anhui University, Hefei, China, in 2013, and the M.Sc. degree from the Micro- Development Design Center, Transilica Inc., a Bluetooth and IEEE 802.11 a/b
/Nano-Electronic System Integration R&D Center, Department of Electronic wireless system-on-chip (SoC) company. The company was acquired by
Science and Technology, University of Science and Technology of China, Microtune Inc. After the close down of Transilica Singapore in 2002, he joined
Hefei, in 2016. His research includes the digital integrated circuit. Chartered Semiconductor Manufacturing Ltd. (now GlobalFoundries, second
largest foundry) as the Director, where he led the SPICE Modeling Team in
support of company business. In 2003, he rejoined IME as a Senior Member
of Technical Staff, where he focused on upstream research and development
Lele Jin received the B.S. degree in electronic engineering from the Hefei initiatives and leadership toward next waves. His current research interests
University of Technology, Hefei, China, in 2013, and the M.Sc. degree from include the development of CMOS as a cost-effective technology platform for
the Micro-/Nano-Electronic System Integration R&D Center, Department of 60-GHz band millimeter-wave SoC and millimeter wave therapy for healthcare
Electronic Science and Technology, University of Science and Technology of applications. As an Adjunct Associate Professor with the National University
China, Hefei, in 2016. His research includes the data converters. of Singapore and an Adjunct Professor with USTC, he is actively involved
in educating and training post-graduate students. In 2010, he returned back
USTC as a Full Professor under the Chinese 1000 Talents Program, where he
is currently the Head of the Department Electronic Science and Technology.
He is also the Executive Director of the Micro-/Nano-Electronic System
Yu Li received the B.S. degree in electronic science and technology Integration R&D Center, which is jointly established by USTC and IME.CAS.
from the University of Science and Technology of China, Hefei, China, He has authored or co-authored over 120 scientific papers. He holds seven
in 2013, where he is currently pursuing the Ph.D. degree with the Micro-/ patents. His current research interests include modeling cum IC validation of
Nano-Electronic System Integration R&D Center, Department of Electronic next-generation technology devices, such as GaN and FinFET. Dr. Lin has
Science and Technology. His current research interests include digital inte- been involved in the IEEE activities in different functions since 1995,
grated circuit and digital communication system. including the Chair of the IEEE Singapore MTT/AP Chapter, Committee
Member of the Singapore Section, Reviewer Board Member for a few of
transactions or journals, and a Technical Program Committee Member of
numerous conferences, such as RFIC and ESSCIRC. He is the initiator and
the co-organizer of international workshops and short courses at APMC99,
Yidan Zhang received the bachelor’s degree from the School of Physics and SPIE00, ISAP06, and IMS07. In 1995, he and his team initiated and
Materials Science, Anhui University, China, where she is currently pursuing organized the IEEE International Symposium on Radio-Frequency Integration
the master’s degree. Her current research is focused on the rational design Technology, Singapore, and now becomes the MTT-S fully sponsored flagship
and efficient synthesis of perovskite oxides as electrochemical sensor’s solid conference in Asia. He was a recipient of the 1998 Innovator Award presented
electrolyte and oxygen reduction reaction for the metal-air batteries. by the EDN Asia Magazine.
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WANG et al.: GAS DETECTION MICROSYSTEM WITH MEMS GAS SENSOR AND IC 6773
Feng Wu (M’99–SM’06–F’13) received the B.S. degree in electrical engi- international video coding standards. His current research interests include
neering from Xidian University, Xi’an, China, in 1992, and the M.S. and image and video compression, media communication, and media analysis and
Ph.D. degrees in computer science from the Harbin Institute of Technol- synthesis. He received the IEEE Circuits and Systems Society 2012 Best
ogy, Harbin, China, in 1996 and 1999, respectively. He was a Principle Associate Editor Award. As a co-author, he received the Best Paper Award
Researcher and Research Manager with Microsoft Research Asia, Beijing, at the IEEE T-CSVT 2009, PCM 2008, and SPIE VCIP 2007. He was
China. He is currently a Professor with University of Science and Technology also the TPC Chair in MMSP 2011, VCIP 2010, and PCM 2009, and the
of China, Hefei, China. He has authored or co-authored over 200 high- Special Sessions Chair at ICME 2010 and ISCAS 2013. He was an Associate
quality papers (including several dozens of the IEEE T RANSACTIONS papers) Editor of the IEEE T RANSACTIONS ON C IRCUITS AND S YSTEM FOR V IDEO
and top conference papers on MOBICOM, SIGIR, CVPR, and ACM MM. T ECHNOLOGY, the IEEE T RANSACTIONS ON M ULTIMEDIA, and several
He holds 77 granted U.S. patents. His 15 techniques have been adopted into other international journals.
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