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BGMEA University of Fashion & Technology

(BUFT)

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Lab Report

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Course Code: TEX1202

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Course Title: Dyeing, Printing & Finishing Lab.
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Experiment No.: 03
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Experiment Name: Study on Stock Solution Preparation and Recipe Calculation for
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Dyeing Lab.
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Date of Experiment: 25th October, 2020

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Date of Submission: 1st November, 2020

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Submitted By: Submitted To:

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Rownak Jahan Sraboni Rozina Aktar

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ID: 201-008-111 Lecturer,

Batch: 201 (AMM) Department of AMM
Section: 1 (A) BUFT

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INTRODUCTION

Calculation of dyeing recipe is done by the dyeing master. The whole work processes are done
in lap dip. Lab dip is a process by which buyers supplied swatch is matched with the varying
dyes percentage in the laboratory. Lab dip plays an important role in shade matching & and
detaching the characteristics of the dyes and chemicals are to be used in the large scale of
production. So this is an important task before bulk production.

OBJECTIVE

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1. To calculate the recipe for sample dyeing.
2. To find out the accurate quantity of solution for sample dyeing.

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3. To calculate revise recipe for sample dyeing.
4. To compare dyed sample with swatch by Light Box or Spectrophotometer.

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RAW MATERIALS
• Dye.
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•
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Sodium Hydroxide.
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• Soda Ash.
• Wetting Agent.
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Water.
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• Fabric.
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NECESSARY EQUIPMENTS
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2.
➢ Pipette.
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➢ Digital Balance Machine.

➢ Heat Oven.
➢ Measuring Cylinder.
➢ Metal Container.

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➢ Mug.
➢ Beakers.
➢ Glass Rod.

DIFFERENT PROCESS / METHOD

3.
❖ Required Recipe:
▪ Direct Dye → 2%

▪ Wetting Agent → 1-2 g/l

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▪ Sequestering Agent → 1-2 g/1

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▪ Leveling Agent → 0.5-1 g/1

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▪ rs e
Lubricant → 1-3 g/1
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▪ Soda Ash → 1-5 g/1

▪
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Glubar Salt → 5-20 g/l

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▪ Temperature → 95-100º C
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▪ Time → 30-50 min

▪ M:L → 1:20
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❖ Recipe Calculation:
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▪ Fabric Weight = 3.92gm

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❖ Stock Solutions:

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Dye 1%

▪ Salt 20%

▪ Soda 10%

▪ Others 5%

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We know that,
𝑭𝒂𝒃𝒓𝒊𝒄 𝑾𝒆𝒊𝒈𝒉𝒕 ×𝑺𝒉𝒂𝒅𝒆(%)
Dyestuff Calculation = 𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 (%)

Total Liquor = 𝐹𝑎𝑏𝑟𝑖𝑐 𝑤𝑒𝑖𝑔ℎ𝑡 × 𝐿

𝑇𝑜𝑡𝑎𝑙 𝐿𝑖𝑞𝑢𝑜𝑟 ×𝑅𝑒𝑐𝑖𝑝𝑒 𝐴𝑚𝑜𝑢𝑛𝑡
Chemical Calculation = 𝑆𝑡𝑜𝑐𝑘 𝑆𝑜𝑙𝑢𝑡𝑖𝑜𝑛 ×1000

Required Water = Total Liquor – (All liquid chemical)

𝑭𝒂𝒃𝒓𝒊𝒄 𝑾𝒆𝒊𝒈𝒉𝒕 ×𝑺𝒉𝒂𝒅𝒆(%)
A. Dyestuff Calculation =
𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 (%)

3.92 ×2%
=
1%

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= 7.84 gm.

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B. Total Liquor = 𝑭𝒂𝒃𝒓𝒊𝒄 𝒘𝒆𝒊𝒈𝒉𝒕 × 𝑳

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= 78.4 ml.
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B.1 Chemical Calculation:

aC s

𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

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• Wetting Agent =
𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎
78.4 ×1
=
0.01×1000
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= 7.84 ml.

𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

• Sequestering Agent =
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𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎

78.4 ×1
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=
0.05 ×1000

= 1.568 ml.
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𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

• Levelling Agent =
𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎
78.4 ×.5
=
0.05 ×1000
= 0.784 ml.

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𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

• Lubricant =
𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎
78.4 ×2
=
0.05 ×1000

= 3.136 ml.

𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

• Soda Ash =
𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎
78.4 ×3
=
0.10×1000

= 2.352ml.

𝑻𝒐𝒕𝒂𝒍 𝑳𝒊𝒒𝒖𝒐𝒓 ×𝑹𝒆𝒄𝒊𝒑𝒆 𝑨𝒎𝒐𝒖𝒏𝒕

• Glubar Salt =

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𝑺𝒕𝒐𝒄𝒌 𝑺𝒐𝒍𝒖𝒕𝒊𝒐𝒏 ×𝟏𝟎𝟎𝟎

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78.4 ×8

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=

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0.20×1000

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= 3.136ml.
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C. Required Water = Total Liquor – (All liquid chemical)

= 78.4 - (7.84+1.568+0.784+3.136+2.352+3.136)
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= 78.4 – 18.816
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= 59.584 ml.

= 3200 ml.
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WORKING PROCEDURE
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✓ A metal container was used to remove dyes & impurities.

✓ 3200ml water transferred to the container.
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✓ Added 400ml Dye in it.

✓ Also added 120ml soda ash, 200ml sodium hydroxide & 80ml wetting agent with it.
✓ Then stirred the solution for some time.
✓ After that, a cotton fabric added to the container n put the lid on it.

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✓ Then the container was kept in to a heat oven machine.

✓ The temperature was set in to 100o Celsius and time was set to 60 minutes.
✓ After the set time as over the container was removed from the oven.
✓ The fabric was removed and rinsed with cold water.
✓ Lastly, the fabric was dried.

RESULT & DISCUSION

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We will be able to know of all chemicals and the perfect calculation of wet processing. How the
chemical reacts when it mixed up with materials and how they work we can figure them out.

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PRECAUTION

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• Pure water should be used in all process.
• Necessary equipments should be handled properly.
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• Amount of chemicals should be balanced and as per written in the recipe and
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chemical calculation.
• While removing the container from the oven must use the gloves.
• Time and temperature should be maintained according to the recipe.
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• We must not touch anything without permission.

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• We must be careful with the chemicals and apparatus.

• We must use gloves and masks.
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• We must wear lab coat.

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CONCLUSION
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7.
Dyeing recipe calculation is not a tough task that we have normally seemed. The person who is
engaged in textile dyeing industry has to know the dyeing recipe calculation method to dye the
fabric perfectly. Wet textile manufacturing requires several phases leading to finished goods,
each passing through a variety of complicated conditions that rely on well-trained personnel

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instead of modern machines and technologies. Developments, though, are taking place at a fast
rate that will satisfy consumers with higher content and relatively lower costs. The secret to
progress in textile wet processing technologies would be the systemic indicator of a well
qualified workforce at advantageous salaries.

REFERENCE
8.
→ BUFT Dyeing, Printing & Finishing Lab.

→ Lab Book.

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Internet.

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→ Chemical Chart.

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THE END

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