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Nuclear Engineering and Technology: Gyo-Geun Youn, Yun-Jae Kim, Yasufumi Miura
Nuclear Engineering and Technology: Gyo-Geun Youn, Yun-Jae Kim, Yasufumi Miura
Nuclear Engineering and Technology: Gyo-Geun Youn, Yun-Jae Kim, Yasufumi Miura
Original Article
a r t i c l e i n f o a b s t r a c t
Article history: This paper presents thermal aging effect on fracture toughness properties of GTAW (gas tungsten arc
Received 11 May 2020 welding) and SMAW (shielded metal arc welding) of 316L stainless steels, and investigates the appli-
Received in revised form cability of the existing three thermal aging models for CASS (cast stainless steels). Thermal aging was
9 October 2020
carried out at 350 C for up to 15,000h and at 400 C up to 8,000h. After aging, tensile and fracture
Accepted 11 October 2020
Available online 15 October 2020
toughness tests using 0.5T C(T) specimens were carried out at room temperature and at 288 C.
Comparing with the predictions using three (ANL, French and H3T) thermal aging models for CASS show
that the predictions can be very non-conservative at operating temperature, and thus that the existing
Keywords:
Thermal aging effect on fracture toughness
thermal aging models for CASS cannot be applied to the welded stainless steels.
GTAW 316L stainless Steel © 2020 Korean Nuclear Society, Published by Elsevier Korea LLC. This is an open access article under the
SMAW 316 CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Applicability of thermal aging models
https://doi.org/10.1016/j.net.2020.10.007
1738-5733/© 2020 Korean Nuclear Society, Published by Elsevier Korea LLC. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/
licenses/by-nc-nd/4.0/).
G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 1. (a) Cross sectional and (b) upper view of SMAW of 316L stainless steel plate and (c) cross sectional and (d) upper view of GTAW of 316L stainless steel plate [29].
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Table 1
Chemical composition of the test materials [29].
Material C Si Mn P S Ni Cr Mo N Fe
SMAW (ES316L-16) 0.014 0.42 1.63 0.015 0.003 11.76 19.50 2.25 0.066 Bal
GTAW (YS316L) 0.016 0.44 1.46 0.010 0.015 11.83 19.96 2.80 0.048 Bal
Table 2
Summary of test conditions.
Test Material Aging Temperature (oC) Aging Time (hours) Test Temperature (oC)
proof stress. To obtain both 0.2% proof stress and tensile strength
from a single specimen, stress-rate control test was conducted at 1
εf ðuniÞ ¼ ln (1)
the rate of 10 MPa/s up to 0.2% proof stress, and then strain-rate 1 R:A
control one at the rate of 0.3/min (which is the mean value sug- The results show that the effect of aging time and temperature
gested in JIS Z2241). At 288 C, JIS G0567 suggests only strain-rate at room temperature is similar to that at 288 C. The effect of the
control test and thus the tests were performed at the rate of 0.003/ aging temperature on strengths is more important than that of the
min until 0.2% proof stress, and then at the rate of 0.1/min (which is aging time, particularly on the tensile strength. It is also true for
the mean value suggested in G0567). For the fracture toughness uni-axial fracture strain that the effect of the aging temperature is
tests, experiments were performed twice for each aging condition more important.
and tests were conducted according to ASTM E1820-15 [32]. The Corresponding results for un-aged and aged SMAW of 316L
load was applied so that the crack opening displacement had the stainless steel are shown in Figs. 7 to 9. Overall trends are similar to
speed of 0.005 mm/s and the crack extension was measured by the those for GTAW of 316L stainless steel. In engineering stress-strain
unloading compliance method. curve, yield and tensile strength are higher in the 400 C 5,000h
than in the 350 C 15,000h, as shown in Fig. 7. The strength values
3. Experimental results are higher at 400 C than 350 C for all aging conditions as shown in
Fig. 8. As shown in Fig. 9, the uni-axial fracture strain value de-
3.1. Tensile test results creases with thermal aging time and its decreasing rate is faster at
400 C.
Selected engineering stress-strain curves for un-aged and aged
GTAW of 316L stainless steels are shown in Fig. 4. As expected,
3.2. Fracture toughness test results
strengths tend to increase with aging but ductility decreases. It can
be seen that the aging temperature is more important than time.
Fig. 10(a) and (b) show the effect of aging on fracture toughness
For instance, the aging time at 350 C for 15,000h is three times
test results for un-aged and aged GTAW of 316L stainless steel at
longer than that at 400 C for 5,000h. However, the yield and
room temperature. The results show that the fracture toughness
tensile strength at 400 C for 5,000h are higher than those at 350 C
gradually decrease with the aging time. It can be also seen that the
for 15,000h.
aging conditions of 350 C for 15,000h and 400 C for 8,000h have
For all GTAW test data, the effect of aging time and temperature
almost the same fracture toughness. The J-R curves for both aging
on the yield and tensile strengths are shown in Fig. 5 and on the
conditions are decreased by almost half, compared to those for the
uni-axial fracture strain in Fig. 6. The uni-axial fracture strain
un-aged condition. Fig. 10(c) and (d) are corresponding results at
(εf(uni)) was calculated from the reduction of area (R.A) using the
288 C. The J-R curves at 288 C are generally lower than those at
following equation
room temperature, but the effect of aging time and temperature on
fracture toughness is almost the same as that at room temperature.
The present experimental results are consistent to the results
presented in Ref. [33].
Fig. 11 shows fracture toughness test results for un-aged and aged
SMAW of 316L stainless steel. As for the aged GTAW of 316L stainless
steel, fracture toughness tends to decrease with thermal aging.
However, since the ferrite content in SMAW is 9% which is smaller
than that in GTAW (15%), the effect of thermal aging is less significant
in SMAW than in GTAW. On the other hand, although the ferrite
content in SMAW is lower than that in GTAW, fracture toughness
values of SMAW are overall smaller than those of GTAW, possibly due
to the welding process [29]. Despite its lower cost and better
weldability than other welding techniques [34e36], SMAW is known
Fig. 2. Schematic diagram for 0.5T C(T) specimen extraction locations in 316L stainless to have low welding quality, since the high thermal input alloying
steel plate weld joints [29]. elements are applied during welding. It causes dendritic or hard
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 3. Dimensions of the test specimens: (a) smooth bar tensile specimen and (b) 0.5T C(T) specimen. (unit: degree and mm).
phases result in the reduction of ductility and brittleness [36,37]. On developed based on enormous fracture toughness test data of base
the other hand, GTAW is known to have high welding quality due to materials. Relevant equations are given to predict fracture tough-
its low heat input process [38]. It has been reported in Ref. [38] that ness with high accuracy when the chemical composition and aging
SMAW has more uneven micro-hardness and less homogeneous conditions are known. As these models have been developed based
strain fields than GTAW. Thus the lower welding quality might be the on huge amount of toughness test database, it would be valuable to
main reason for its lower fracture toughness than GTAW. see whether these models can be also applied to the present GTAW/
SMAW of 316L stainless steel, which is the topic of this section.
4. Validation for the applicability of assessment rules to
welded stainless steels 4.1. Application of the ANL (Argonne National Laboratory) model
Currently there is no model to evaluate the thermal aging effect The ANL model [16] provides an estimation of the thermal aging
on fracture toughness of stainless steel welds. However, several effect on fracture toughness for CF3, CF8 and CF8M materials. For
models are currently available to evaluate the thermal aging effect GTAW and SMAW in the present work, the molybdenum (Mo)
on fracture toughness of CASS [14,16,17]. These models have been contents were 2.25 wt% and 2.80 wt%, the estimation equations of
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 4. Selected engineering stress-strain curves for GTAW of 316L stainless steel aged at 350 C for 15,000h and 400 C for 5,000h: (a) room temperature and (b) 288 C.
Fig. 5. Variations of true yield and tensile strengths of GTAW of 316L stainless steel: (a) room temperature and (b) 288 C.
Fig. 6. Variations of uni-axial fracture strain of GTAW of 316L stainless steel: (a) room temperature (b) 288 C.
Fig. 7. Selected engineering stress-strain curves for SMAW of 316L stainless steel aged at 350 C for 15,000h and 400 C for 5,000h: (a) tested at room temperature and (b) 288 C.
Fig. 8. Variations of true yield and tensile strengths of SMAW of 316L stainless steel: (a) room temperature and (b) 288 C.
Fig. 9. Variations of uni-axial fracture strain of SMAW 316L stainless steel: (a) room temperature (b) 288 C.
Fig. 10. Selected fracture toughness test results for aged GTAW of 316L stainless steel tested: (a)-(b) at room temperature and (c)-(d) at 288 C.
the value of CVint is not known, the suggested value of 200 J/cm2 can 4.3. Application of the H3T model
be used [16]. The ferrite content is recommended to use the value
obtained from the estimation methods such as the Hull’s equivalent The H3T model [14] developed by MHI can provide predictions
factor [39] or ASTM A800 method [40]. It should be noted that, for only for the fracture toughness of aged CF8 and CF8M materials
GTAW and SMAW, the estimated ferrite contents from the Hull’s using the same prediction equations. Furthermore, it provides the
equivalent factor were 11.1% and 6.5%, respectively. However, the fracture toughness prediction equation only at operating tempera-
actual measured ferrite contents were 15% and 9%, respectively. In ture so the data at 288 C can be analyzed. Contrary to the previous
this study, predictions of fracture toughness using the ANL model two models providing fracture toughness estimation from the
were performed not only using the estimated ferrite content but Charpy impact energy, this model gives fracture toughness estima-
also using the measured ferrite content for comparison. tion directly from the chemical composition, ferrite content and
aging conditions. The estimated fracture toughness values are
resistance J values corresponding to the 0.2 mm offset line [32], J0.2/
4.2. Application of the French model BL, and to the crack extension of Da ¼ 6.0 mm, J6.0 (see Fig. 12 for the
definitions). For constructing the blunting line, 2sf was used, where
The French model [17] developed by EdF only provides fracture sf denotes the flow strength (the average of the yield and tensile
toughness estimation of the aged CF8M CASS. As for the ANL model strength). In the present experiments, the crack extension was
[16], the French model [17] provides the Charpy impact energy value measured only up to 4 mm. Thus, comparison will be made only for
of the U-notch specimen CU at 20 C and V-notch specimen CV at J0.2/BL values from the H3T model.
320 C from the chemical composition and equivalent aging time at For this work, the chemical composition and aging conditions are
the aging temperature of 400 C. To obtain equivalent aging time, the given in Section 2. For the ferrite contents, the actual values esti-
following activation energy Q (kJ/mol) is used mated from ASTM A800 method [40] were used; 9.8% for GTAW and
5.8% for SMAW. In addition, the suggested value of Q ¼ 100 kJ/mol
Q ¼ 193:1 þ 13:66ðCr þ Mo þ SiÞ (5) [14] was used to calculate the activation energy and initiation acti-
vation energy for conservative estimations.
The fracture toughness can then be predicted using the equations
relating the Charpy impact energy, CV, and fracture toughness. The 4.4. Comparison results
provided equations are for predicting resistance J values at the crack
extension of Da ¼ 0.2, 1.0 and 3.0 mm, J0.2, J1.0 and J3.0, respectively Fig. 13 compares predicted J-resistance curves of aged GTAW and
(see Fig. 12 for the definitions). SMAW using the ANL model with experimental data for selected
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 11. Selected fracture toughness test results for aged SMAW of 316L stainless steel tested: (a)-(b) at room temperature and (c)-(d) at 288 C.
cases. For predictions, two curves are given; one using the ferrite prediction using the predicted ferrite content is higher (more non-
content measured in experiment (15%) and the other using the conservative).
ferrite content predicted by the Hull’s equivalent factor [39] (11%). For the case of SMAW, predicted J-R curves are much higher
For the case of aged GTAW tested at room temperature (Fig. 13a), (non-conservative) than experimental data, regardless of the ferrite
the predicted J-R curve using the predicted ferrite content is slightly content and temperature. The use of the measured ferrite content
lower (conservative) than the test data. However, when the pre- moves the curves closer to the experimental data, but the pre-
diction is made using the actual measured ferrite content, the dictions are still much higher (more than twice). This implies that
predicted J-R curve is further lower, suggesting that all predictions the use of the ANL model [16] to SMAW always gives highly non-
are conservative. However, for the case of aged GTAW tested at conservative prediction in fracture toughness.
288 C (Fig. 13b), the predicted J-R curve are higher (non-conser- Fig. 14 shows the ratios of the predicted fracture toughness (J0.2,
vative) than the experimental data. Now the prediction using the J1.0 and J3.0) using the French model [17] and experimental one for
measured ferrite content is closer to the experimental data. The aged GTAW and SMAW at aging temperature of 350 C. As the ratio
of the predicted and experimental value is given, the ratio less than
unity implies the prediction is conservative. The ratio greater than
unity means the prediction is non-conservative. For the case of
aged GTAW tested at room temperature (Fig. 14(a)), the ratios are
less than unity (ranging from ~0.3 to ~0.7). They increase with
increasing aging time. For the case of aged GTAW tested at 288 C
(Fig. 14(b)), the ratios are greater than unity (ranging from ~2 to ~4).
Thus, the fracture toughness predictions of aged GTAW using the
French model are very conservative at room temperature but are
non-conservative at 288 C.
For the case of aged SMAW tested at room temperature
(Fig. 14(c)), the ratios are greater than unity (ranging from ~1.1 to
~1.9) and they tend to increase with aging time. For the case of aged
SMAW tested at 288 C (Fig. 14(d)), the ratios are much greater than
unity (ranging from ~5 to ~12). Thus, the fracture toughness pre-
Fig. 12. Various definitions of resistance J. dictions of aged SMAW using the French model [17] are
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 13. Comparison of experimental and predicted J-R curves using the ANL model: (a)-(b) GTAW and (c)-(d) SMAW.
nonconservative both at room temperature and at 288 C, but the fractional (or similar) changes in fracture toughness due to thermal
degree of non-conservatism is much larger at 288 C. aging in the existing model can be applied to ASSW, then the
Fig. 15 shows the ratios of the predicted fracture toughness (J0.2/ reduction factor due to thermal aging should be the same for both
BL) using the H3T model [14] and experimental one for aged GTAW CASS and welded stainless steels
and SMAW at aging temperature of 350 C and tested at 288 C.
! !
Since, the H3T model is only applicable to operating temperature Jaged Jaged
conditions, the experimental J0.2/BL values tested at 288 C are ¼ RðTs ; tÞ ¼ (6)
Junaged Junaged
compared with the prediction results. The blunting lines to deter- CASS ASSW
mine the experimental J0.2/BL values are shown in Figs. 10 and 11.
Similar to the results in Fig. 14, the ratio of the predicted and where R is the reduction factor being a function of aging temper-
experimental value is given. For the case of aged GTAW (Fig. 15(a)), ature and time, and the subscript ASSW stands for austenitic
the ratios are much larger than unity (ranging from ~7.6 to ~8.8). stainless steel welds. Rearranging Eq. (6) leads to
For the case of aged SMAW (Fig. 15(b)), the ratios are even larger
(ranging from ~19 to ~32). Thus, the fracture toughness predictions Junaged Jaged
of aged GTAW and SMAW using the H3T model are non- CASS
¼ CASS ¼ constant (7)
conservative. Junaged Jaged
ASSW ASSW
Fracture toughness estimation results for all test data are sum-
marized in Table 3. The present results show that it is inappropriate As the fracture toughness ratio of unaged ASSW and CASS
to apply the existing assessment rules to aged GTAW and SMAW should be constant, that of aged ASSW and CASS should also be
stainless steels. constant and be independent of the aging time and temperature.
Note that fracture toughness values of unaged GTAW and SMAW Note that (Jaged)CASS in Eq. (7) is indeed the predicted J value for
can be lower than those of unaged CASS. Thus inaccurate prediction aged GTAW or SMAW, shown in Fig. 14 for instance as J(Pred). On the
of aged GTAW and SMAW might be caused by different initial other hand, (Jaged)ASSW is the experimentally measured toughness
(unaged) fracture toughness between austenitic stainless steel value of aged GTAW or SMAW, shown in Fig. 14 for instance as J(Test).
welds (ASSW) and CASS, rather than thermal aging models them- The results in Fig. 14 as well as those in Figs. 13 and 15 suggest that
selves. Thus it would be worth checking whether the fractional (or the values of J(Pred)/J(Test) are not constant and depend strongly on
similar) changes in fracture toughness due to thermal aging in the the aging time and temperature. Therefore the existing thermal
existing model can be applied to ASSW. Assuming that the aging models for CASS cannot be used to welded stainless steels
and the thermal aging models based on experimental data of
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Fig. 14. Comparison of experimental and predicted J values using the French model: (a)-(b) GTAW and (c)-(d) SMAW.
Fig. 15. Comparison of experimental and predicted J0.2/BL values using the H3T model: (a) GTAW and (b) SMAW.
welded stainless steels are required to properly predict the fracture and fracture toughness tests using 0.5T C(T) specimens were car-
toughness of aged GTAW and SMAW. ried out at room temperature and at 288 C.
Test data show that, with thermal aging, ductility and fracture
5. Conclusions toughness decrease but the strengths (yield and tensile) increase.
The aging temperature has a greater effect than the aging time.
This paper firstly presents experimental tensile and fracture To check the applicability of the existing thermal aging models,
toughness test results of un-aged and aged GTAW and SMAW of predicted fracture toughness values using three (ANL, French and
316L stainless steels. The thermal aging was carried out at 350 C H3T) models are compared with experimental data of aged GTAW
for up to 15,000h and at 400 C up to 8,000h. After aging, tensile and SMAW. The predicted J-R curves using the ANL model are
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G.-G. Youn, Y.-J. Kim and Y. Miura Nuclear Engineering and Technology 53 (2021) 1357e1368
Table 3
Summary of fracture toughness estimation results.
slightly conservative for aged GTAW tested at room temperature. [12] O.K. Chopra, W.J. Shack, Mechanical Properties of Thermally Aged Cast
Stainless Steels from Shippingport Reactor Components, U.S.NRC, NUREG/CR-
However, they are non-conservative for all other cases. In the case
6275, ANL-94/37, 1995.
of the French model, the model provides very conservative [13] P.L. Delliou, S. Saillet, Large EDF Tests on Aged Cast Duplex Stainless Steel
toughness only for aged GTAW tested at room temperature, but Components e Part I: Reduced Scale Tests, ASME 2015 PVP Conference, 2015.
very nonconservative predictions in all other cases. Finally, the H3T PVP2015-45960.
[14] S. Kawaguchi, T. Nagasaki, K. Koyama, Prediction Method of Tensile Properties
model also provides non-conservative predictions for aged GTAW and Fracture Toughness of Thermally Aged Cast Duplex Stainless Steel Piping,
and SMAW tested at 288 C. The degrees of conservatism and non- ASME 2005 PVP Conference, 2005. PVP2005-71528.
conservatism are summarized in Table 3. Thus, it is shown that the [15] N. Ligneau, C. Pages, M. Akamatsu, C. Pokor, V. Calonne-Chatelee, Integrity and
Life Assessment of Cast Duplex Stainless Steel Elbows Used in the Primary
existing thermal aging models for CASS cannot be applied to the Loops of PWRs, ASME 2009 PVP Conference, 2009. PVP2009-77731.
welded stainless steels. [16] O.K. Chopra, Estimation of Fracture Toughness of Cast Stainless Steels during
Thermal Aging in LWR Systems, U.S.NRC, NUREG/CR-4513, ANL-15/08, 2016.
[17] C. Faidy, Ageing Management of Cast Stainless Steel Components in French
Declaration of competing interest PWRs, ASME 2012 PVP Conference, 2012. PVP2012-78843.
[18] J.Y. Jeon, Y.J. Kim, J.W. Kim, S.Y. Lee, Effect of thermal ageing of CF8M on multi-
The authors declare that they have no known competing axial ductility and application to fracture toughness prediction, Fatigue Fract.
Eng. Mat. 38 (2015) 1466e1477.
financial interests or personal relationships that could have [19] G.G. Youn, H.S. Nam, Y.J. Kim, J.W. Kim, Numerical prediction of thermal aging
appeared to influence the work reported in this paper. and cyclic loading effects on fracture toughness of cast stainless steels CF8A:
experimental and numerical study, Int. J. Mech. Sci. 163 (2019) 105e120.
[20] S. Bonnet, J. Bourgoin, J. Champredonde, D. Guttman, M. Guttman, Relation-
Acknowledgement ship between Evolution of mechanical properties of various cast duplex
stainless steels and metallurgical and aging parameters: outline of current
This research was funded by National Research Foundation of EDF programmes, Mat. Sci. Tech. 6 (1990) 221e229.
[21] Y. Miura, M. Yamamoto, Effect of Aging Temperature on Fracture Toughness of
Korea (NRF) supported by Ministry of Science and ICT (NRF-
Cast Austenitic Stainless Steel, ASME 2015 PVP Conference, 2015. PVP2015-
2018M2A8A4084016, NRF-2019M2D2A2048296). 45434.
[22] Y. Miura, T. Sawabe, K. Betsuyaku, T. Arai, Thermal Aging Behavior of Grade
CF3M Austenitic Stainless Steels, ASME 2017 PVP Conference, 2017. PVP2017-
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