CHM025.

2 Analytical Chemistry for Engineering and Applied Sciences 1 Laboratory

Name: Francisco, Justin Mark Rating, % =

Solidum, Joseph Cyron Deduction, % =
Course No. & Section CHM025.2- W58
Semester: 1 SY 2020-2021 Net Rating, % =

Activity No. 4

Standardization of NaOH against KHP and

Determination of Concentration of HCl by Titration with Standardized NaOH

DATA AND RESULTS:

A. Standardization of NaOH
Example I II III
Weight of KHP, g 0.2500 0.2425 0.2505 0.2481

Final reading, mL NaOH 12.15 11.85 24.15 36.10

Initial Reading, mL NaOH 0.00 0.30 11.85 24.15
Volume, mL NaOH 12.15 11.55 12.30 11.95

Molar concentration of NaOH 0.1007 0.1028 0.09973 0.1017

Normal Concentration of NaOH 0.1007 0.1028 0.09973 0.1017

B. Determination of Concentration of HCl

Example I II III
Volume of HCl used, mL 25.00 25.00 25.00 25.00

Final reading, mL NaOH 37.00 25.85 25.70 24.55

Initial Reading, mL NaOH 12.15 1.00 0.60 0.20
Volume of NaOH, mL NaOH 24.85 24.85 25.10 24.35

Molar concentration of HCl 0.1001 0.1022 0.1001 0.09902

Normal Concentration of HCl 0.1001 0.1022 0.1001 0.09902

STATISTICAL EVALUATION OF VRESULTS

Molarity, NaOH:
Mean, Molarity NaOH 0.1014
Median, Molarity NaOH 0.1017
Cl for μ .1014 ± .0039
Reported value, M NaOH 0.1017

Molarity HCl:
Mean, M HCl 0.1004
Median M HCl 0.1001
Cl for μ .1004 ± .0040
Reported value, M HCl 0.1001

Reference:
Capangpangan, Mario B., Quantitative Inorganic Analysis Laboratory Manual, Iligan City, Philippines,
(2004), pp. 9-10.