Formulation Guide Personal Care and Cosmetics EN

You might also like

Download as pdf or txt
Download as pdf or txt
You are on page 1of 44

PERSONAL CARE

Formulation Guide
CONTENT

PRODUCT CATEGORY PAGES

BODY TREATMENT

Liquid Hand Soaps 04 - 11

Shower Gels 12 - 21

Shower Oils & Body Wash Emulsion 22 - 27

Intimate Hygiene Products 28 - 37

Skin Care Products 38 - 43

FACE TREATMENT

Face Care Products 44 - 55

Make up removers & micellar fluids 56 - 63

Shaving products 64 - 67

HAIR TREATMENT

Shampoos 68 - 73

OTHER

Products dedicated to babies 74 - 85


Body Treatment

LIQUID
HAND SOAPS
Liquid hand soap is a product formulated to wash and clean hands.
It belongs to the group of common dirt removers in commercial and
industrial cleaning processes. Liquid hand soaps are the most widely
used products in cleaning sector.

Liquid hand soaps can be characterized by different features which are


dependent on their components. There are plenty of various products
available on the market such as liquid hand soaps for babies, mechanical
workers, traditional or economic products.

Liquid hand soaps have to be effective general-purpose cleaners, easy


to apply and use and their suppose to be capable of removing different
types of dirt such as vegetable and animal oils, fat, wax deposits, dust
and many others.

According to WHO, 70% cases of


gastrointestinal intoxication, skin
infections and conjunctivitis are
caused by the germs transmitted
to hands.

On one square centimeter of the skin there are plenty of various bac-
teria. All these germs are transferred every day from human to human
when shaking hands, holding on to the handles in public transport, to-
uching coins and banknotes that come into contact with hundred of
hands a day.

Only proper hand hygiene will protect us against dangerous germs and
bugs. That is the reason why hands should be oftently washed with the
usage of an appropriate designed formulations.

4 Liqide Hand Soaps Personal Care - Formulation Guide 5


LIQUID HAND SOAP [RD-01] TRADITIONAL LIQUID SOAP [MP-01]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua up to 100 solvent

Sodium Benzoate, Benzophenone-4 0.05 UV absorber


0.50 preservative
Potassium Sorbate

Sodium Laureth Sulfate SULFOROKAnol L227/1 30.00 surfactant


MEA Lauryl Sulfate ROSULfan M 12.00 surfactant

Sodium Lauroyl Sarcosinate ROKAtend LS 5.00 surfactant


Sodium Laureth Sulfate SULFOROKAnol L227/1 10.00 surfactant

Citric Acid 0.25 pH modifier


Cocamide DEA ROKAmid KAD 1.00 surfactant
Sodium Benzoate,
0.60 preservative
Potassium Sorbate
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 re-oiling agent

B Parfum 0.30 fragrance B Parfum 0.50 fragrance

Cocamidopropyl Betaine ROKAmina K30 7.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 re-oiling agent

Sodium Chloride 0.80 viscosity modifier CI 19140 q.s. colorant

C Citric Acid q.s. pH modifier Cocamidopropyl Betaine ROKAmina K30 7.00 surfactant

C Sodium Chloride 2.20 viscosity modifier

APPEARANCE visual method clear, homogenous liquid APPEARANCE visual method bright-yellow gel

pH 4.8 – 5.5 pH 4.8 – 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2500 – 5000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Add ingredients from phase A to warm water (50-55°C). 4. If necessary, add Sodium Chloride to adjust the viscosity. 1. Add ingredients from phase A to the warm water (45- 5. Add Sodium Chloride to adjust the viscosity. NOTE.
Mix until homogenous solution is obtained. NOTE: it is very important to equilibrate a sample at 50°C). Mix until uniform. Add salt (not in one go) – after addition of each portion
25°C for at least one hour to get an accurate viscosity mix well.
2. Cool the batch down to at least 35°C. 2. Cool the batch down to at least 35°C.
measurement.
6. Control the pH range – if necessary, add citric acid. Mix
3. Add parfum and Cocamidopropyl Betaine during 3. Add fragrance, PEG-7 Glyceryl Cocoate and colorant
5. If necessary, adjust pH by Citric Acid to 4.8 – 5.5. well after adjustment.
mixing. Mix until homogenous solution is obtained. during mixing. Mix until uniform.
7. Control viscosity if necessary, add Sodium Chloride.
4. Add slowly Cocamidopropyl Betaine during mixing.
Mix until uniform.

6 Liqide Hand Soaps Personal Care - Formulation Guide 7


LIQUID BLACK SOAP FOR MEN [MP-02] MILD YELLOW HAND SOAP [MP-03]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua 46.55 solvent

Acrylates/C10-30 Alkyl Potassium Oleate 8.00 surfactant


1.00 viscosity modifier
Acrylate Crosspolymer

Sodium Lauroyl Glycinate ROKAtend GL 25.00 surfactant


B Aqua 16.00 solvent

Decyl Glucoside 7.00 surfactant


Sodium Lauroyl Glycinate ROKAtend GL 5.00 surfactant

B Citric Acid 0.20 pH modifier


Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant
C Parfum 0.50 fragrance
Cocamidopropyl Betaine ROKAmina K30 7.00 surfactant
Benzy Alcohol,
Ethylhexyglycerin,Tocopherol 1.00 preservative
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 re-oiling agent

Cocamidopropyl Betaine ROKAmina K30 10.00 surfactant


C Parfum 0.50 fragrance

Sodium Chloride 1.75 viscosity modifier


Activated Charcoal 0.02 black color additive

Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol

Sodium Hydroxide
D q.s pH modifier
(30% solution)

APPEARANCE visual method black, viscous gel APPEARANCE visual method yellow liquid

pH 5.5 – 6.5 pH 8.5 - 9.0

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 20°C 15000 – 20000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 5000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Pour the warm deionized water (40-50°C) into the main 3. Add phase B to phase A. Mix until homogenous 1. Into the large vessel (big enough to provide adequate 4. Adjust pH to 8.5 – 9.0 by using Citric Acid. Mix well
vessel and add the Acrylates/C10-30 Alkyl Acrylate solution is obtained. Cool the batch down to 30°C. mixing while preparing batch) pour deionized water. after adjustment.
Crosspolymer. Start mixing when the agent is completely When the batch is around 30°C, add preservative,
2. Add ingredients from phase A to the vessel while mixing. 5. Add fragrance, preservative and Cocamidopropyl
wetted. Mix until the homogenous solution is obtained. Activated Charcoal and fragrance. Mix for 20 – 30
Heat up to 70 – 75°C. Mix until homogenous solution Betaine. Mix until homogenous solution is obtained.
minutes with slow agitation. If necessery, homogenise
2. Combine ingredients from phase B in a separate vessel. is obtained.
for 1-2 minutes. 6. If necessary, add Sodium Chloride to adjust the viscosity.
Heat up to 60°C with gentle agitation. Mix until
4. Readjust the final pH to 5.5 – 6.5 with additional 3. Cool the batch down to at least 35°C. NOTE: it is very important to equilibrate a sample at
homogenous solution is obtained.
Sodium Hydroxide (30%) if necessary. 25°C for at least one hour to get an accurate viscosity
measurement.

8 Liqide Hand Soaps Personal Care - Formulation Guide 9


MILD LIQUID HAND SOAP [MP-04] ECONOMIC LIQUID HAND SOAP [KD-103]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 74.50 solvent A Aqua up to 100 solvent

Sodium Laureth Sulfate,


Potassium Oleate 4.00 surfactant
Cocamidopropyl Betaine, EXOcare PC60 8.00 surfactant
Coco-Glucoside
MIPA Laureth Sulfate
SULFOROKAnol L390/1M 10.00 surfactant
and Propylene Glycol Sodium Benzoate,
Potassium Sorbate 0.50 preservative

Cocamide DEA ROKAmid KAD 1.50 surfactant


Betaine 0.50 active

Parfum 0.50 fragrance


Lactic Acid 0.15 pH adjuster

Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol Cocamide DEA ROKAmid KAD 0.50 surfactant

Cocamidopropyl Betaine ROKAmina K30K 7.00 surfactant B Parfum 0.50 fragrance

Sodium Chloride 1.50 viscosity modifier CI 42090 q.s. colorant

CI 19140 q.s. colorant

C Sodium Chloride 2.50 thickener

APPEARANCE visual method clear yellowish gel APPEARANCE visual method light-green, viscous gel

pH 8.5 - 9.0 pH 4.8 – 5.3

VISCOSITY [cP] Brookfield LV, spindle 34, speed 4.0 RPM, T: 25°C 3000 – 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 2000 - 5000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Heat up the water to (40-50°C) and add the ingredients 3. Add Sodium Chloride to adjust the viscosity. NOTE. 1. Combine ingredients from phase A. Mix until uniform. 3. Add Sodium Chloride while mixing. Mix until uniform.
one after another in the order from the table above. Add salt (not in one go) – after addition of each
2. Add phase B ingredients. Mix until uniform. 4. Control viscosity and pH.
portion mix well.
2. Before adding a parfum cool the mixture down to room
temperature and add the rest of ingredients.

10 Liqide Hand Soaps Personal Care - Formulation Guide 11


Body Treatment

SHOWER
GELS
Shower gels are designed to remove dirt, tallow and impurities of the
epidermis, as well as prevent its drying. Products of this type should also
adequately moisturize and nourish the skin.

There are plenty of different shower gels available on the market such as:
• pearly / transparent / coloured products,
• traditional / mild products,
• designed for babies / people with sensitive skin,
• moisturising products.
and many others, although there are general requirements for this type
of cosmetics.

The choice of products which con-


tain an appropriate components,
provides feeling of smoothness
and softness to the skin.

In general, shower gels should be characterized by:


• good foaming properties (should quickly create high-volume, stable
foam),
• good wettability of dirt and fat on the skin,
• not causing the skin dryness and be safe for the environment,
• ability to disperse emulsified dirt particles in the bath,
• good performance in the presence of hard water,
• improving skin condition after bathing,
• not irritating efect to the eyes, mucous membranes and skin.

12 Shower Gels Personal Care - Formulation Guide 13


SHOWER GEL WITH PEARLY EFFECT [ZP-01] CLASSIC SHOWER GEL [ZP-02]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 46.12 solvent A Aqua 49.15 solvent

Citric Acid 0.15 pH modifier Citric acid 0.20 pH modifier

Polyquaternium 10 0.06 conditioning agent Lauryl Glucoside 5.00 surfactant

Disodium Laureth Sodium Laureth Sulfate SULFOROKAnol L227/1 15.00 surfactant


EXOsoft L3/40 2.50 surfactant
Sulfosuccinate

Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant


Sodium Laureth Sulfate SULFOROKAnol L227/1 20.00 surfactant

Sodium Benzoate,
0.60 preservative
Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant Potassium Sorbate

Sodium Benzoate, PEG-120 Methyl


0.50 preservative B 0.70 thickening agent
Potassium Sorbate Glucose Dioleate

PEG-120 Methyl PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.50 re-oiling agent
B 0.50 thickening agent
Glucose Dioleate

C Parfum 0.50 fragrance


C Coco Betaine ROKAmina K30B 5.50 surfactant

Cocamidopropyl Betaine ROKAmina K30 5.00 surfactant


Parfum 0.50 fragrance

D Citric acid 0.20 pH modifier


Sodium Laureth Sulfate,
D Cocamide DEA, EXOpearl N 2.00 pearling agent
Glycol Distearate Sodium Chloride 2.15 viscosity modifier

E Sodium Chloride 2.00 viscosity modifier

Citric Acid 0.17 pH modifier

APPEARANCE visual method viscosus, pearl gel APPEARANCE visual method clear, viscosus gel

pH 5.0 – 5.5 pH 5.0 – 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 – 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 – 6000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Add ingredients from phase A to the hot water (70-75°C). 5. Add pearling agent. Mix until uniform. 1. Add ingredients from phase A to the warm water (55-60°C). 5. Add Sodium Chloride to adjust the viscosity. NOTE.
While mixing add ingredients one after another in the Mix until uniform. Add salt (not in one go) – after addition of each portion
6. Add Sodium Chloride to adjust the viscosity. NOTE.
order from the table above. Mix until uniform. mix well.
Add salt (not in one go) – after addition of each portion 2. Cool the batch down to at least 50°C.
2. Cool the batch down to at least 50°C. mix well. 6. Control the pH range – if necessary, add Citric Acid.
3. Add PEG-120 Methyl Glucose Dioleate and PEG-7
Mix well after adjustment.
3. Add PEG-120 Methyl Glucose Dioleate during mixing. 7. Control the pH range – if necessary, add Citric Acid. Glyceryl Cocoate during mixing. Mix until uniform.
Mix until uniform. Cool the batch down to at least 35°C. Mix well after adjustment. Cool the batch down to at least 35°C.
4. Add fragrance and Coco Betaine during mixing. Mix 8. Control the viscosity, if necessary add Sodium Chloride. 4. Add fragrance and Cocamidopropyl Betaine during
until uniform. mixing. Mix until uniform.

14 Shower Gels Personal Care - Formulation Guide 15


WHITE SHOWER GEL [ZP-03]
BLACK-GOLD SHOWER GEL FOR MEN [ZP-04]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent


A Aqua 67.09 solvent
Acrylates/C10-30 Alkyl
0.40 viscosity modifier
Acrylate Crosspolymer Xanthan Gum 0.90 viscosity modifier

Sodium Hydroxide q.s pH modifier Glycerin 2.50 moisturising agent

B Aqua 20.00 solvent Sodium Benzoate,


0.30 preservative
Potassium Sorbate

Xanthan Gum 0.45 viscosity modifier


Polyquaternium-7 0.01 conditioning agent
Glycerin 2.00 moisturising agent
B Ammonium Laureth Sulfate SULFOROKAnol A325/1 24.00 surfactant
Polyquaternium 10 0.01 conditioning agent
CI 77000, CI 77491, Silica 0.03 pigment
C Aqua 10.00 solvent
Activated Charcoal 0.02 pigment
Talc 2.00 skin conditioner
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 re-oiling agent
Mica, Titanium dioxide 0.02 pearling agent
Cocamidopropyl Betaine ROKAmina K30K 3.40 surfactant
Sodium Lauroyl Glycinate ROKAtend GL 10.00 surfactant
Parfum 0.30 fragrance
Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant
Sodium Benzoate,
0.30 preservative
Potassium Sorbate
D Parfum 0.50 fragrance

Citric acid 0.15 pH modifier


Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol

APPEARANCE visual method white viscous gel APPEARANCE visual method black-gold gel

pH 6.0 – 7.5 pH 4.8 - 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 6000 – 9000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 8000 – 15000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Pour the warm deionized water (40-50°C) into the 4. Add phase B to main vessel. Mix until homogenous 1. In a main vessel combine ingredients from phase A 3. Combine ingredients from the phase B and mix until
main vessel and add the Acrylates/C10-30 Alkyl Acrylate solution is obtained. If needed, homogenise for 2-3 by adding Xanthan Gum to Glycerin and mixing until uniform. Control the pH range – if necessary, add
Crosspolymer. Start mixing when the agent is completely minutes. homogenous solution is obtained. Then, take 2.5 g of Citric Acid.
wetted. Mix until the homogenous solution is obtained. water from phase A to a separate beaker add Polyqu-
5. Combine ingredients from phase C in a separate vessel. 4. Add phase B to phase A and mix well. Cool the batch
2. Add Sodium Hydroxide. Mix until homogenous solution Heat up to 40°C with gentle agitation. Mix until aternium-7 and mix them well.
down to 30°C and homogenise for 2-3 minutes.
is obtained. homogenous solution is obtained. 2. Add the rest of warm water (50-55°C) from phase A
3. Combine ingredients from phase B in a separate vessel. 6. Add phase C to the main vessel. Mix until homogenous to the main vessel and homogenise for 1-2 minutes.
Add Xanthan Gum to Glycerin – mix until homogenous solution is obtained. Cool the batch down to 30°C. At the and of preparation, mix the solutions, add
solution is obtained. Add warm water (40-50°C) and preservative and homogenise for 2-3 minutes.
7. Add fragrance and preservative. Mix gently until
Polyquaternium-10. Mix until homogenous solution is
homogenous solution is obtained.
obtained. If necessery, homogenise for 2-3 minutes.

16 Shower Gels Personal Care - Formulation Guide 17


BLACK SHOWER GEL FOR MEN [ZP-05] MILD SHOWER GEL [ZP-10]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 56.58 solvent A Aqua 65.76 solvent

Xanthan Gum 0.90 viscosity modifier Xanthan Gum 0.90 viscosity modifier

Glycerin 2.50 moisturising agent Glycerin 2.50 moisturising agent

Sodium Benzoate, Sodium Benzoate,


0.30 preservative 1.00 preservative
Potassium Sorbate Potassium Sorbate

Polyquaternium-7 0.01 conditioning agent B Aqua 1.95 solvent

B Aqua 1.24 solvent Magnesium Laureth Sulfate EXOsoft MG 23.10 surfactant

Ammonium Laureth Sulfate SULFOROKAnol A325/1 24.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant

Sodium Lauroyl Sarcosinate ROKAtend LS 10.00 surfactant Parfum 0.30 fragrance

Activated Charcoal 0.01 pigment Cocamidopropyl Betaine ROKAmina K30K 3.40 surfactant

Parfum 0.50 fragrance Citric Acid 0.09 pH modifier

Sodium Benzoate,
0.30 preservative
Potassium Sorbate

Cocamidopropyl Betaine ROKAmina K30K 3.40 surfactant

Citric Acid 0.26 pH modifier

APPEARANCE visual method black clear gel APPEARANCE visual method colorless clear gel

pH 4.8 – 5.5 pH 4.8 - 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 6000 – 15000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 7000 – 15000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from phase A 3. Combine ingredients from the phase B and mix until 1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A and mix well. Cool the batch
by adding Xanthan Gum to Glycerin and mixing until uniform. Control the pH range – if necessary, add Add Xanthan Gum to glycerin – mix until homogenous down to 30°C and homogenise for 2-3 minutes.
homogenous solution is obtained. Then, take 2.5 g of Citric Acid. solution is obtained. Then, pour warm water (50-55°C)
water from phase A to a separate beaker add from phase A to the main vessel and mix. Add
4. Add phase B to phase A and mix well. Cool the batch
Polyquaternium-7 and mix them well. preservative. Homogenise for 2-3 minutes.
down to 30°C and homogenise for 2-3 minutes.
2. Add the rest of warm water (50-55°C) from phase A to 2. Combine ingredients from the phase B and mix until
the main vessel and homogenise for 1-2 minutes. At uniform. Control the pH range – if necessary, add Citric
the and of preparation, mix the solutions, add Acid.
preservative and homogenise for 2-3 minutes.

18 Shower Gels Personal Care - Formulation Guide 19


LIQUID SHOWER GEL FOR WOMEN [ZP-11] MOISTURIZING BODY WASH GEL [KD-104]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 66.53 solvent A Aqua 81.25 solvent

Xanthan Gum 0.90 viscosity modifier Sodium Laureth Sulfate,


Cocamidopropyl Betaine, EXOcare PC60 15.00 surfactant
Coco-Glucoside
Glycerin 2.50 moisturising agent
Sodium Benzoate,
0.50 preservative
Potassium Sorbate
Sodium Benzoate,
0.30 preservative
Potassium Sorbate
Allantoin 0.10 active

B Aqua 8.30 solvent


Lactic Acid 0.15 pH adjuster

MIPA Laureth Sulfate


SULFOROKAnol L390/1M 7.00 surfactant
and Propylene Glycol PEG-120 Methyl
B 0.50 thickener
Glucose Dioleate

Sodium Lauroyl Sarcosinate ROKAtend LS 10.00 surfactant


Parfum 0.50 fragrance

CI 77000,
0.02 pigment
Acrylates Crosspolymer Urea 0.50 active

Parfum 0.50 fragrance C Sodium Chloride 1.50 thickener

Sodium Benzoate,
0.30 preservative
Potassium Sorbate

Cocamidopropyl Betaine ROKAmina K30K 3.40 surfactant

Citric Acid 0.25 pH modifier

APPEARANCE visual method gold scintillating gel APPEARANCE visual method transparent, viscous gel

pH 4.8 – 5.5 pH 4.8 - 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 7000 – 15000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 2000 - 7000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A and mix well. Cool the batch 1. Combine ingredients from phase A. Mix until uniform. 3. Add Sodium Chloride while mixing. Mix until uniform.
Add Xanthan Gum to glycerin – mix until homogenous down to 30°C and homogenise for 2-3 minutes.
2. Add ingredients from phase B while mixing. Mix until
solution is obtained. Then, pour warm water (50-55°C)
uniform.
from phase A to the main vessel and mix. Add
preservative. Homogenise for 2-3 minutes.
2. Combine ingredients from the phase B and mix until
uniform. Control the pH range – if necessary, add
Citric Acid.

20 Shower Gels Personal Care - Formulation Guide 21


Body Treatment

SHOWER OILS
& BODY WASH
EMULSION
Shower oils and body wash emulsions are suitable for dry and very dry
skin. They gently cleanse and at the same time renew the lipid layer of
the skin.

Beautiful fragrance, pleasant consistency, cleansing and moisturizing


properties - these are the features of an ideal shower product. Usually
consumers choose gels or lotions, although shower oils have recently
become very popular on the market.

Shower oils turn into foam when exposed to water what brings a pleasant
feeling to the skin.

Shower oils and body wash emul-


sions are recommended for sen-
sitive skin. They improve elasticity
and strengthens the lipid layer of
the epidermis. The shower oil gen-
tly oils and nourishes the skin.

They are oftently recommended for washing sensitive, dry skin, but in
winter shower oils will be useful for any skin. They grease it well, rebu-
ild protective film strained by winter conditions, prevent moisture loss,
smooth, soften, nourish and strengthen. They are very delicate, so using
them brings a real pleasure.

After bathing, the skin is lightly dry by a towel with no need to lubricate
it with a moisturizer, because it is slightly oily.

22 Shower oils & body wash emulsion Personal Care - Formulation Guide 23
SHOWER AND BATH OIL [KD-115] MILD BODY WASH EMULSION [KD-80]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

MIPA Laureth Sulfate A Aqua 72.55 solvent


A SULFOROKAnol L390/1M 15.00 surfactant
and Propylene Glycol

Betaine 1.00 active


Glycine Soja Oil 27.00 emollient

B Xanthan Gum 0.50 rheology modifier


Helianthus Annuus Seed Oil 26.00 emollient

Glycerin 2.00 solvent


Tocopheryl Acetate 1.00 active

C Cetearyl Alcohol EXOalc 1618 flakes 3.00 emulsion stabilizer


B Laureth-2 30.00 surfactant

Ceteareth-25 ROKAnol T25 2.00 emulsifier


Parfum 1.00 fragrance

Helianthus Annuus Seed Oil 10.00 emollient

Stearic Acid 1.00 rheology modifier

Phenoxyethanol, Methylparaben,
D 0.80 preservative
Ethylparaben, Propylparaben

MIPA Laureth Sulfate


SULFOROKAnol L390/1M 2.00 surfactant
and Propylene Glycol

E Sodium Lauroyl Sarcosinate ROKAtend LS 5.00 surfactant

Lactic Acid 0.15 pH adjuster

slightly yellowish viscous APPEARANCE visual method white emulsion


APPEARANCE visual method
liquid
pH 4.8 – 6.0
VISCOSITY [cP] Brookfield LV, spindle 18, speed 10 RPM, T: 25°C 70-120
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 8000 - 15000
STABILITY 1 month at 5°C, RT, 40°C confirmed
STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from phase A 3. Add ingredients from phase B to phase A while mixing. 1. In a main vessel combine ingredients from the phase A. 6. Add C into A, stir well with hand stirring, keep A/B at
and mix until uniform. Mix until uniform. 75-80°C. Homogenize with 2000-3000 RPM, 90 sec.
2. Add Xanthan Gum to Glycerin - mix until homogenous
2. Combine ingredients from phase B in a separate vessel solution is obtained. 7. Cool the batch down to 50°C. Add phase D ingredients
and mix until uniform. while mixing. Homogenize with 2500-3500 RPM, 90 sec.
3. Add the phase B components to phase A while mixing.
Mix until uniform. 8. Cool the batch down to 25°C. Add phase E ingredients
while mixing. Homogenize with 2500-3500 RPM, 30 sec.
4. In a separate vesselI combine ingredients from the
phase C.
5. Heat phase A and C to 75-80°C.

24 Shower oils & body wash emulsion Personal Care - Formulation Guide 25
BODY EMULSION [KD-81]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Cetearyl Alcohol EXOalc 1618 flakes 2.50 emulsion, stabilizer

Ceteareth-25 ROKAnol T25 1.50 emulsifier

Petrolatum 1.00 emollient

Helianthus Annuus Seed Oil 3.00 emollient

PPG-15 Stearyl Ether ROKAnol SP15L 4.00 emollient

Phenoxyethanol, Methylparaben,
B 0.80 preservative
Ethylparaben, Propylparaben

PEG-7/PPG-2
ROKAnol GA7LAW 1.00 emollient
Propylheptyl ether

Betaine 1.00 active

Glycerin 2.00 solvent

Aqua 80.41 solvent

C Carbomer 0.25 rheology modifier

PPG-15 Stearyl Ether ROKAnol SP15L 2.00 emollient

D Sodium Hydroxide 0.14 pH adjuster

Parfum 0.40 fragrance

APPEARANCE visual method white emulsion

pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
1. In a separate vesselIs combine ingredients from phase 5. Cool the batch down to 25°C. Add phase D ingredients
A, B and C. while mixing. Homogenize with 2500-3500 RPM,
120 sec.
2. Heat phase A and B to 75-80°C.
3. Add B into A, stir well with hand stirring, keep A/B at
75-80°C. Homogenize with 2000-3000 RPM, 120 sec.
4. Cool the batch down to 50°C while mixing. Add phase C
ingredients while mixing. Homogenize with 2500-
3500 RPM, 120 sec.

26 Shower oils & body wash emulsion Personal Care - Formulation Guide 27
Body Treatment

INTIMATE
HYGIENE
The intimate woman place is a unique ecosystem which is inhabited
by over 100 species of microorganisms. Among them are the bacteria,
whose metabolic product like lactic acid protects the vaginal environment
from pathogens. Because of that the pH of intimate area is below 4.5.

A number of factors, can disrupt the balance of the vaginal microbiota


and compromise women’s health. Therefore, the proper care for the
most delicate part of the body should be taken very seriously.

Formulations presented below com-


bine an approriate and well-thought
components of the final formula which
restores the natural pH balance.

Intimate hygiene products provide a gentle care for places requiring


special protecion. The main function which suppose to be fulfiled by
Intimate Hygiene Products are:

• provide a feeling of well-being,


• provide protection from infection,
• be suitable for daily use,
• prevent skin dryness,
• destroy the lipid mantle of the skin,
• neutral and natural composition,
• be without potential ingredients that cause allergies and irritations,
• provide care and regeneration.

28 Intimate Hygiene Personal Care - Formulation Guide 29


GEL FOR INTIMATE HYGIENE [PHI-01] GEL FOR INTIMATE HYGIENE [KD-01]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 67.95 solvent A Aqua 68.00 solvent

Sodium Benzoate, Sodium Benzoate,


0.50 preservative 0.50 preservative
Potassium Sorbate Potassium Sorbate

Betaine 1.00 active Betaine 1.00 active

Glycerin 2.00 moisturising agent Glycerin 2.00 moisturising agent

Lactic Acid 0.55 pH adjuster Lactic Acid 0.50 pH adjuster

B Sodium Laureth Sulfate SULFOROKAnol L227/1 18.00 surfactant B Sodium Laureth Sulfate SULFOROKAnol L227/1 18.00 surfactant

PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant

C Parfum 0.25 fragrance C Parfum 0.25 fragrance

D Coco Betaine ROKAmina K30B 8.75 surfactant D Coco Betaine ROKAmina K30B 8.75 surfactant

APPEARANCE visual method bright-yellow gel APPEARANCE visual method light-yellow gel

pH 4.0 – 4.5 pH 4.0- 4.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 - 7000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 4. Add slowly Coco Betaine while mixing. Mix until uniform. 1. In a main vessel combine ingredients from phase A. 4. Add slowly Coco Betaine while mixing. Mix until uniform.
Mix until uniform. Mix until uniform.
5. If nesesery, adjust pH by Lactic Acid to 4.0 – 4.5. 5. If nessesery, adjust pH by Lactic Acid to 4.0 – 4.5.
2. Add ingredients from phase B. Mix until uniform. 2. Add ingredients from phase B. Mix until uniform.
3. Add parfum while mixing. Mix until uniform. 3. Add parfum while mixing. Mix until uniform.

30 Intimate Hygiene Personal Care - Formulation Guide 31


GEL FOR INTIMATE HYGIENE [KD-02] GEL FOR INTIMATE HYGIENE [KD-03]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua 70.65 solvent

Sodium Benzoate, Sodium Laureth Sulfate SULFOROKAnol L227/1 18.00 surfactant


0.50 preservative
Potassium Sorbate

Sodium Lauroyl Sarcosinate ROKAtend LS 3.00 surfactant


Betaine 1.00 active

Betaine 0.50 active


Glycerin 1.00 moisturising agent

Glycerin 1.00 moisturising agent


Lactic Acid q.s pH adjuster

Coco-Glucoside,
B 0.50 surfactant
Sodium Laureth Sulfate SULFOROKAnol L227/1 12.00 surfactant Glyceryl Oleate

PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant Sodium Benzoate,


0.50 preservative
Potassium Sorbate

Magnesium Laureth Sulfate EXOsoft MG / EXOsoft MGB 6.00 surfactant


Lactic Acid 0.60 pH adjuster

C Parfum 0.25 fragrance


B Parfum 0.25 fragrance

D Coco Betaine ROKAmina K30B 9.00 surfactant


C Coco Betaine ROKAmina K30B 5.00 surfactant

APPEARANCE visual method transparent gel APPEARANCE visual method transparent gel

pH 4.0 – 4.5 pH 4.0 – 4.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6 RPM, T: 25°C 2000 – 7000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 3. Add Parfum while mixing. Mix until uniform. 1. Combine ingredients from phase A. Add ingredients 3. Add Coco Betaine while mixing. Mix until uniform.
Add ingredients from phase A to warm water (40-45°C). from phase A to warm water (40-45°C). Mix until
4. Add slowly Coco Betaine while mixing. Mix until uniform. 4. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5.
Mix until uniform. homogenous solution is obtained. Cool the batch
5. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5. down to at least 30°C.
2. Add ingredients from phase B. Mix until uniform. Cool
the batch down to at least 30°C. 2. Add parfum while mixing.

32 Intimate Hygiene Personal Care - Formulation Guide 33


GEL FOR INTIMATE HYGIENE [KD-04] GEL FOR INTIMATE HYGIENE [KD-05]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua up to 100 solvent

MEA Lauryl Sulfate ROSULfan M 18.00 surfactant Magnesium Laureth Sulfate EXOsoft MGB 25.00 surfactant

Magnesium Laureth Betaine 2.00 active


EXOsoft MG / EXOsoft MGB 4.00 surfactant
Sulfate

Glycerin 2.00 moisturising agent


Glycerin 1.00 moisturising agent
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant
Sodium Benzoate,
0.50 preservative
Decyl Glucoside 0.50 surfactant Potassium Sorbate

Sodium Benzoate, Coco-Glucoside,


0.50 preservative 0.50 surfactant
Potassium Sorbate Glyceryl Oleate

B Coco Betaine ROKAmina K30B 6.00 surfactant Lactic Acid q.s. pH adjuster

Parfum 0.25 fragrance B Parfum 0.20 fragrance

C Lactic Acid q.s pH adjuster Coco Betaine ROKAmina K30B 8.00 surfactant

APPEARANCE visual method bright-yellow gel APPEARANCE visual method transparent gel

pH 4.0 – 4.5 pH 4.0 – 4.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 6 RPM, T: 25°C 2000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.0 RPM, T: 25°C 1000 - 4000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5. 1. Combine ingredients from phase A. Add ingredients 3. Add slowly Coco Betaine and parfum while mixing. Mix
from phase A to water (25-30°C). Mix until homogenous from phase A to water and heat to 50°C. Mix until until uniform.
solution is obtained. homogenous solution is obtained.
2. Add slowly Coco Betaine and parfum while mixing. 2. Cool the batch down to at least 30°C.
Mix until uniform.

34 Intimate Hygiene Personal Care - Formulation Guide 35


GEL FOR INTIMATE HYGIENE [KD-06] FOAM FOR INTIMATE HYGIENE [KD-07]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua up to 100 solvent

Sodium Benzoate, Glycerin 4.00 moisturising agent


0.50 preservative
Potassium Sorbate

Magnesium Laureth Sulfate EXOsoft MG / EXOsoft MGB 4.00 surfactant


Betaine 0.50 active

Disodium Laureth
Glycerin 1.00 moisturising agent EXOsoft L3/40 4.00 surfactant
Sulfosuccinate

Lactic Acid q.s. pH adjuster Betaine 0.50 active

B Magnesium Laureth Sulfate EXOsoft MGB 24.00 surfactant Sodium Benzoate,


0.50 preservative
Potassium Sorbate
PEG-120 Methyl
0.25 thickener
Glucose Dioleate Lactic Acid q.s pH adjuster

PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant B Panthenol 0.10 active

C Coco Betaine ROKAmina K30B 8.00 surfactant PEG-120 Methyl


0.25 thickener
Glucose Dioleate
Sodium Laureth Sulfate,
D Cocamide DEA, EXOpearl N 1.50 surfactant
C Cocamidopropyl Betaine ROKAmina K30 2.00 surfactant
Glycol Distearate

Parfum 0.20 fragrance

APPEARANCE visual method pearly gel APPEARANCE visual method bright-yellow liquid

pH 4.0 – 4.5 pH 4.0 – 4.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 8000 STABILITY 1 month at 5°C, RT, 40°C confirmed

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
Procedure: 1. In a main vessel combine ingredients from phase A. 3. Add Cocamidopropyl Betaine and parfum during
Add ingredients from phase A to warm water (40-45°C). mixing. Mix until uniform.
1. In a main vessel combine ingredients from phase A. 3. Add ingredients from phase C and D during mixing. Mix until uniform.
Add ingredients from phase A to warm water (40-45°C). Mix until uniform. 4. If nessesery, adjust pH by Lactic Acid to 4.0 – 4.5.
Mix until uniform. 2. Add PEG-120 Methyl Glucose Dioleate and Panthenol.
Mix until uniform. Cool the batch down to at least 30°C.
2. Add ingredients from phase B. Mix until uniform. Cool
the batch down to at least 30°C.

36 Intimate Hygiene Personal Care - Formulation Guide 37


Body Treatment

SKIN CARE
PRODUCTS
Skin Care Products are a big group of cosmetics which are available in
many different categories. Generally each skin care product like balm,
moisturiser or lotion should provide to the skin sufficient nourishment
as well as protection.

In the beauty market there are plenty of brands and products to choose
from. Selection of the suitable product should be connnected with the
skin type and it’s compatibility.

In terms of oily skin, light weight lotion are recommended. In case of dry,
mature skin, moisturiser with a thicker consisitency should be chosen.
Night creams will generally be thicker than a day cream.

Skin Care Products are designed


for the body to help keep the
smooth of skin.

Cosmetic companies are coming up with plenty of creative products to


market what is increasing the range of them. Technically, beside of their
different consistency and various names, skin care products like treat-
ment balms, nourishing hand creams, intensive moisturisers and body
lotions have one common goal: to hydrate, treat and repair the dry skin.
Some may have anti-aging effects, others may include skin regenerating
ingredients, but in general they work to protect our skin making it more
supple and smooth.

38 Skin care products Personal Care - Formulation Guide 39


BODY LOTION [KD-82] HAND CREAM [KD-83]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 2.50 emulsion stabilizer A Cetearyl Alcohol EXOalc 1618 flakes 4.00 emulsion stabilizer

Ceteareth-12 ROKAnol T12 1.00 emulsifier Glyceryl Stearate,


2.00 emulsifier
PEG-100 Stearate

Petrolatum 2.00 emollient


Ceteareth-12 ROKAnol T12 1.50 emulsifier

Helianthus Annuus Seed Oil 1.00 emollient


Helianthus Annuus Seed Oil 1.00 emollient

PPG-15 Stearyl Ether ROKAnol SP15L 6.00 emollient


Petrolatum 0.50 emollient

Glyceryl Stearate,
1.50 emulsifier
PEG-100 Stearate Stearic Acid 1.50 rheology modifier

B Aqua 78.35 solvent PPG-15 Stearyl Ether ROKAnol SP15L 8.00 emollient

PEG-7/PPG-2 B Aqua 58.00 solvent


ROKAnol GA7LAW 1.00 emollient
Propylheptyl ether

Betaine 2.00 active


Betaine 2.00 active

Glycerin 20.00 solvent


Glycerin 2.00 moisturising agent

Phenoxyethanol, Methylparaben,
C 1.00 preservative
C Carbomer 0.30 rheology modifier Ethylparaben, Propylparaben

PPG-15 Stearyl Ether ROKAnol SP15L 1.00 emollient D Parfum 0.50 fragrance

Phenoxyethanol, Methylparaben,
D 1.00 preservative
Ethylparaben, Propylparaben

E Sodium Hydroxide 0.05 pH adjuster

Parfum 0.30 fragrance

APPEARANCE visual method white emulsion APPEARANCE visual method white emulsion

pH 5.0 – 7.0 pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a separate vessel combine ingredients from phase 3. Cool the batch down to 50°C while mixing. Add 1. In a separate vesselI combine ingredients from phase 4. Cool the batch down to 50°C while mixing. Add phase C
A, B and C. Heat the phase A and B to 75-80°C. ingredients from phase C and D while mixing. A and B. ingredients while mixing. Homogenise with 2500-3500
Homogenise with 2500-3500 RPM, 120 sec. RPM, 90 sec.
2. Add A into B, stir well with hand stirring, keep A/B at 2. Heat phase A and B to 75-80°C.
75-80°C. Homogenize with 2000-3000 RPM, 120 sec. 4. Cool the batch down to 25°C. Add phase E while 5. Cool the batch down to 25°C. Add phase D ingredients
3. Add A into B while mixing, keep A/B at 75-80°C.
mixing. Homogenize with 2500-3500 RPM, 120 sec. while mixing. Homogenise with 2500-3500 RPM, 30 sec.
Homogenise with 2000-3000 RPM, 120 sec.

40 Skin care products Personal Care - Formulation Guide 41


NIGHT FACE CREAM [KD-84]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

Glyceryl Stearate,
A 2.50 emulsifier
PEG-100 Stearate

Ceteareth-12 ROKAnol T12 1.00 emulsifier

Cetearyl Alcohol EXOalc 1618 flakes 2.00 emulsion stabilizer

PPG-15 Stearyl Ether ROKAnol SP15L 4.00 emollient

Caprylic/Capric Triglyceride 5.00 emollient

Stearic Acid 1.00 rheology modifier

Helianthus Annuus Seed Oil 2.00 emollient

Butyrospermum Parkii Butter 1.00 emollient

B Aqua 73.10 solvent

Betaine 5.00 active

C Glycerin 2.00 solvent

Xanthan Gum 0.10 rheology modifier

Acrylates/C10-30 Alkyl
D 0.20 rheology modifier
Acrylate Crosspolymer

Phenoxyethanol, Methylparaben,
E 0.80 preservative
Ethylparaben, Propylparaben

Sodium Hydroxide 0.05 pH adjuster

F Parfum 0.25 fragrance

APPEARANCE visual method white emulsion

pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
1. In a separate vesselI combine ingredients from phase 4. Heat phase A and B to 75-80°C.
A and B. 5. Add A into B while mixing, keep A/B at 75-80°C.
2. Add slowly phase D ingredients to phase B while mixing. Homogenise with 2000-3000 RPM, 120 sec.
Mix until uniform. 6. Cool the batch down to 50°C while mixing. Add phase E
3. In a separate vesselI combine ingredients from phase C. ingredients while mixing. Homogenise with 2500-3500
Mix until uniform. Add slowly phase C ingredients to RPM, 90 sec.
phase B while mixing. Homogenise with 2000-3000 7. Cool the batch down to 25°C. Add phase F ingredients
RPM, 90 sec. while mixing. Homogenise with 2500-3500 RPM, 120 sec.

42 Skin care products Personal Care - Formulation Guide 43


Face Treatment

FACE CARE
PRODUCTS
Face Care Products are basic care cosmetics for every woman. Facial
skin is our business card, that is why we should take care of it as best as
possible. Today’s Face Care Cosmetics are multi-tasking, but they also
meet the needs of skin living under strong oxidative stress, which can
lead to loss of collagen and elastin. There are many types of Face Care
products, so it’s worth knowing their purpose and application.

Selecting the best quality ingre-


dients provides gentle, moisturi-
zing, anti-wrinkle properties de-
livered to the skin.

Face Care products should first and foremost be chosen according to


the needs of the skin and age. Currently, the use of multifunctional face
care cosmetics which are suitable for day and night use is moving away.

During the day, our skin has different needs than at night, hence the
need to use a different day and night care products. The face care pro-
ducts for the day have a protective function against harmful external
factors. The consistency of the day cosmetic is much lighter than the
night one. Many day cosmteics also have a small UV filter that protects
from sunlight. The night cosmetic is designed to regenerate and nourish
the face. The skin regenerates quickly at night, which is why the cosme-
tic applied during the evening care ritual should contain many nutrients.

44 Face care products Personal Care - Formulation Guide 45


DEEPLY CLEANSING GEL FOR SKIN FACE [ST-02] MILD EMULSION FOR SKIN FACE [ST-03]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 49.00 solvent A Paraffinum Liquidum 1.50 emollient

Acrylates/C10-30 Alkyl Butyrospermum Parkii


1.00 viscosity modifier 0.50 emollient
Acrylate Crosspolymer (Shea Butter)

B Aqua 14.00 solvent Caprylic/Capric Triglyceride 1.00 emollient

Sodium Lauroyl Glycinate ROKAtend GL 10.00 surfactant Glyceryl Stearate,


3.00 emulsifier
PEG-100 Stearate

Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant


Cetearyl Alcohol 2.50 co-emulsifier

Cocamidopropyl Betaine ROKAmina K30 3.40 surfactant


B Aqua 25.30 solvent

C Parfum 0.40 fragrance


C Xanthan Gum 0.40 viscosity modifier

Propylene Glycol 1.00 solvent


Glycerin 1.30 moisturising agent

Benzyl Alcohol,
Ethylhexylglycerin, 1.00 preservative Aqua 50.20 solvent
Tocopherol

D Sodium Hydroxide 0.20 pH modifier D Citric Acid 0.10 pH modifier

Sodium Lauroyl Glycinate ROKAtend GL 5.00 surfactant

Sodium Lauroyl Sarcosinate ROKAtend LS 7.70 surfactant

Parfum 0.50 fragrance

Ethylparaben, Methylparaben,
1.00 preservative
Phenoxyethanol,Propylparaben

clear, viscous gel with APPEARANCE visual method white emulsion


APPEARANCE visual method suspended air bubbles
pH 6.5 - 7.5
pH 5.5 - 6.5
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 5000 - 10000
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 15000 - 20000
STABILITY 1 month at 5°C, RT, 40°C confirmed
STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
Procedure:
1. In a main vessel heat all ingredients to 75-80°C and Gum, Glycerin and warm water (50°C). To obtain
1. Pour the warm deionized water (40-50°C) in to the 3. Add phase B to phase A. Mix until homogenous solution do the same with phase B. homogenous solution, homogenize for 1 min.
main vessel and add the Acrylates/C10-30 Alkyl Acrylate is obtained. Cool the batch down to 30°C.
Crosspolymer. Start mixing when the polymer is com- 2. Pour the hot water form phase B into phase A, mix 4. Combine ingredients from the phase D and mix until
4. When the batch temperature is around 30°C, add pre- well (avoid cooling) and homogenise for 5 minutes. uniform. If necessary, add Citric Acid.
pletely wetted. Mix until the homogenous solution is
servative, Propylene Glycol and fragrance. Then, start cooling the formulation and repeat homo-
obtained. 5. Add phase D and B to main vessel (phase A) and mix
5. Readjust the final pH to 5.5 - 6.5 with addition of genization at 60°C. Do the same at 40°C.
2. Combine ingredients from phase B in a separate vessel. for 5 min, then homogonise for 1 min.
Sodium Hydroxide (30%) if necessary. 3. At the same time, prepare phase C by mixing Xanthan
Heat up to 60°C with gentle agitation. Mix until homo-
genous solution is obtained.

46 Face care products Personal Care - Formulation Guide 47


FOAMING FACE WASH [ST-04] TWO PHASE FOAMING FACE WASH [ST-05]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 48.20 solvent A Aqua 38.40 solvent

PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.50 re-oiling agent Sodium Lauroyl Glycinate ROKAtend GL 10.00 surfactant

Glycerin 1.00 moisturising agent Sodium Lauroyl Sarcosinate ROKAtend LS 30.00 surfactant

Sodium Lauroyl Sarcosinate ROKAtend LS 34.70 surfactant Propylene Glycol 3.00 solvent

Cocamidopropyl Betaine ROKAmina K30K 9.70 surfactant Parfum 0.60 fragrance

Parfum 0.50 fragrance Ehylhexyl Glycerine,


1.00 preservative
Phenoxyethanol

Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.60 re-oiling agent

Propylene Glycol 2.50 solvent Mineral Oil 15.00 emollient

Cocamide DEA ROKAmid KAD 0.50 surfactant Citric acid 0.40 pH modifier

Citric acid 0.40 pH modifier

APPEARANCE visual method clear, colorless liquid clear colorless liquid


APPEARANCE visual method
(water phase)

pH 6.0 - 7.5
pH 6.0 - 7.5 (water phase)

STABILITY 1 month st 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Add ingredients from phase A to the warm water (40-5°C). 3. Control the pH range – if necessary, add Citric Acid. 1. Add ingredients from phase A to the warm water 3. Control the pH range – if necessary, add Citric Acid.
Mix until uniform. Mix well after adjustment. (40-50°C). Mix until uniform. Mix well after adjustment.
2. Then, cool the mixture down to room temperature 2. Then, cool the mixture down to room temperature 4. Add Sodium Chloride to adjust the viscosity. NOTE.
before adding a preservative and add the rest of before adding a preservative and add the rest of Add salt (not in one go) – after addition of each portion
ingredients. ingredients. mix well.

48 Face care products Personal Care - Formulation Guide 49


MILD PEARLING GEL FOR SKIN FACE [ST-06] MILD GEL TO SKIN FACE WASHING [KD-61]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua 50.00 solvent

Xanthan Gum 0.65 viscosity modifier Acrylates/C10-30 Alkyl


0.85 rheology modifier
Acrylate Crosspolymer

Glycerin 2.00 moisturising agent


B Aqua up to 100 solvent

Sodium Benzoate,
0.60 preservative
Potassium Sorbate Disodium Laureth
EXOsoft L3/40 5.00 surfactant
Sulfosuccinate

B Aqua 15.70 solvent


Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant
Magnesium Laureth Sulfate EXOsoft MGB 20.00 surfactant
Betaine 1.00 active

Sodium Lauroyl Sarcosinate ROKAtend LS 10.00 surfactant


Glycerin 1.00 moisturising agent

Cocamidopropyl Betaine ROKAmina K30 3.40 surfactant


PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant

C Citric Acid q.s pH modifier


CI 42090 q.s. colorant
Sodium Laureth Sulfate,
Cocamide DEA, EXOpearl N 1.00 pearling agent Benzophenone-4 0.05 UV filter
Glycol Distearate

Parfum 0.50 fragrance Phenoxyethanol,


C 1.00 preservative
Ethylhexylglycerin

Parfum 0.30 fragrance

Sodium Hydroxide 0.50 pH adjuster

APPEARANCE visual method viscous pearling gel clear, blue viscous gel with
APPEARANCE visual method
suspended air bubbles
pH 4.8 – 5.5
pH 5.0 – 6.0
VISCOSITY [cP] Brookfield LV, spindle 34, speed 4.0 RPM, T: 25°C 6000 - 9000
STABILITY 1 month at 5°C, RT, 40°C confirmed
STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
Procedure:
1. Pour the warm deionized water (40-50°C) in to the 3. Add phase B to phase A. Mix until homogenous solution
1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A. Mix until homogenous solution main vessel and add the Acrylates/C10-30 Alkyl Acrylate is obtained. Cool the batch down to 30°C.
Add Xanthan Gum to Glycerin - mix until homogenous is obtained. Cool the batch down to 30°C. Crosspolymer. Start mixing when the polymer is
4. When the batch temperature is 30°C, add preservative,
solution is obtained. Add warm water (40-50°C) and completely wetted. Mix until the homogenous solution
4. Adjust pH to 4.8 – 5.5 by using Citric Acid. Mix well fragrance and Sodium Hydroxide. Mix for 20 minutes
preservative. Mix until homogenous solution is obtained. is obtained.
after adjustment. with slow agitation.
Homogenise for 2-3 minutes.
5. Add ingredients from phase C. Mix until homogenous 2. Combine ingredients from phase B in a separate vessel.
5. Readjust the final pH to 5.0 - 6.0 with addition of
2. Combine ingredients from phase B. Add ingredients Heat up to 30°C with gentle agitation. Mix until homo-
solution is obtained. Sodium Hydroxide (30%) if necessary.
from phase B to warm water (40-45°C). Mix until genous solution is obtained.
homogenous solution is obtained.

50 Face care products Personal Care - Formulation Guide 51


GEL FOR WASHING SKIN FACE [KD-62] CREAMY FACE SCRUB [KD-91]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

Acrylates/C10-30 Alkyl A Ceteareth-12 ROKAnol T12 1.50 emulsifier


A 0.90 rheology modifier
Acrylate Crosspolymer

Ceteareth-25 ROKAnol T25 0.50 emulsifier


Aqua 40.00 solvent

Cetearyl Alcohol EXOalc 1618 flakes 3.00 emulsion stabilizer


B Aqua up to 100 solvent

PPG-15 Stearyl Ether ROKAnol SP15L 6.00 emollient


Sodium Laureth Sulfate SULFOROKAnol L270/1 7.00 surfactant

Caprylic/Capric Triglyceride 1.00 emollient


Magnesium Laureth Sulfate EXOsoft MG / EXOsoft MGB 4.00 surfactant

Helianthus Annuus
Betaine 2.00 active 5.00 emollient
Seed Oil

PEG-75 Lanolin ROKAnol LN75/50 1.00 surfactant Butyrospermum


0.50 emollient
Parkii Butter
Glycerin 1.00 moisturising agent
Tocopheryl Acetate 0.20 active
CI 17200 q.s. colorant
B Aqua 73.68 solvent
Benzophenone-4 0.05 UV filter
Betaine 1.00 active
Phenoxyethanol,
C 1.00 preservative
Ethylhexylglycerin
Glycerin 4.00 solvent

Parfum 0.30 fragrance Pentylene Glycol 2.00 solvent

Cocamidopropyl Betaine ROKAmina K30 3.00 surfactant Magnesium Aluminum Silicate 0.10 rheology modifier

D Sodium Hydroxide q.s pH adjuster Acrylates/C10-30 Alkyl


C 0.27 rheology modifier
Acrylate Crosspolymer

Phenoxyethanol, Methylparaben,
D 0.50 preservative
Ethylparaben, Propylparaben
APPEARANCE visual method pink gel

pH 5.0 – 6.0 Sodium Hydroxide 0.10 pH adjuster

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 18000 - 22000
E Parfum 0.30 fragrance
STABILITY 1 month at 5°C, RT, 40°C confirmed
Cellulose acetate 0.35 abrasive

Procedure:
1. Pour the deionized water (25-30°C) into the main 3. Add slowly phase B to phase A while mixing. Mix until emulsion with scrub
APPEARANCE visual method
vessel and add the Acrylates/C10-30 Alkyl Acrylate uniform. particles
Crosspolymer. Start mixing when the polymer is
4. Add Preservative, Cocamidopropyl Betaine and parfum pH 5.0 – 7.0
completely wetted. Mix until the homogenous solution
while mixing. Mix until uniform.
is obtained. Homogenise for 1-2 minutes. STABILITY 1 month at 5°C, RT, 40°C confirmed

2. Combine ingredients from phase B in a separate vessel.


Heat up to 40-45°C with gentle agitation. Mix until
homogenous solution is obtained.

52 Face care products Personal Care - Formulation Guide 53


Procedure: FACE MASK [KD-120]
1. In a main vessel combine ingredients from the phase B. 4. Heat phase A and B to 75-80°C.
Add Pentylene Glycol, Glycerin, Betaine to the water. PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
5. Add A into B, while mixing, keep A/B at 75-80°C.
Add Magnesium Aluminum Silicate while mixing. Mix
Homogenise with 2000-3000 RPM, 120 sec.
for 10 min - 150-200 RPM. Homogenise with 2000-
A Ceteareth-12 ROKAnol T12 2.00 emulsifier
3000 RPM, 5-6 min. 6. Cool the batch down to 50°C while mixing. Add phase
D ingredients while mixing. Homogenise with 2500-
2. Add Acrylates/C10-30 Alkyl Acrylate Crosspolymer
3000 RPM, 120 sec. Ceteareth-25 ROKAnol T25 0.50 emulsifier
while mixing. Mix for 10 min - 100-150 RPM. Homogenise
with 700-1000 RPM, 60-90 sec. 7. Cool the batch down to 25°C while mixing.
Cetearyl Alcohol EXOalc 1618 flakes 3.00 emulsion stabilizer
3. In a separate vessel combine ingredients from phase A. 8. Add Parfum and abrasive while mixing. Mix until uniform.

PPG-15 Stearyl Ether ROKAnol SP15L 5.00 emollient

Caprylic/Capric Triglyceride 5.00 emollient

Glycine Soja Oil 2.50 emollient

Stearic Acid 1.00 rheology modifier

Tocopheryl Acetate 0.50 active

Butyrospermum Parkii Butter 1.00 emollient

B Aqua 71.50 solvent

Pentylene Glycol 2.50 solvent

Betaine 1.00 active

Magnesium Aluminum Silicate 1.00 rheology modifier

C Kaolin 3.00 absorbent

Phenoxyethanol, Methylparaben,
0.50 preservative
Ethylparaben, Propylparaben

APPEARANCE visual method slightly gray emulsion

pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
1. In a main vessel combine ingredients from the phase B. 4. Add A into B, while mixing, keep A/B at 75-80°C.
Add Pentylene Glycol, Betaine to the water. Add Homogenise with 2000-3000 RPM, 120 sec.
Magnesium Aluminum Silicate while mixing. Homogenise
5. Cool the batch down to 50°C while mixing. Add phase C
with 2000-3000 RPM, 5-6 min.
ingredients while mixing. Homogenise with 2500-
2. In a separate vessel combine ingredients from the pha- 3500 RPM, 120 sec.
se A.
6. Cool the batch down to 25°C.
3. Heat phase A and B to 75-80°C.

54 Face care products Personal Care - Formulation Guide 55


Face Treatment

MAKE UP
REMOVERS &
MICELLAR FLUIDS
Eye Make-up Remover and micellar fluid products are intended to help
easily remove make-up that has been applied. They help to remove the
applied color and to make sure it easily wipes off using a tissue.

Ideally, we should remove our


make-up not only before going
to bed but refresh it after wake
up. In the morning, it helps to get
rid of perspiration and sebum ac-
cumulated on the skin overnight.

Makeup removal should be part of our daily skin care ritual because it is
healthy for skin.

The specific benefits of make-up removers are:

• washes away cosmetics, impurities and dirt from the surface of our
skin, which could lead to irritation or cause our skin to age more rapidly
• reduces the risk of developing pimples, redness, blackheads and other
types of blemishes
• promotes cellular renewal by eliminating dead skin
• stimulates skin’s microcirculation due to the massage action
• lets our skin breathe

56 Make up removers & micellar fluids Personal Care - Formulation Guide 57


MICELLAR CLEANSING FLUID [DEM-01] MAKE-UP REMOVING LIQUID [KD-70]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 85.46 solvent A Aqua 92.85 solvent

PEG-7/PPG-2 Betaine 0.10 active


ROKAnol GA7LAW 3.00 surfactant
Propylheptyl Ether

Glycerin 3.00 moisturising agent


PEG-40 Hydrogenated surfactant
ROKAcet HR40 4.00
Castor Oil
Citric Acid 0.05 pH adjuster

Glycerin 1.00 moisturising agent


Sodium Lauroyl Sarcosinate ROKAtend LS 2.00 surfactant

Propylene Glycol 6.00 solvent


Phenoxyethanol,
B 1.00 preservative
Ethylhexylglycerin
Parfum 0.50 fragrance
Propylene Glycol 1.00 solvent
Sodium Benzoate,
0.50 preservative
Potassium Sorbate

Citric Acid 0.04 pH modifier

APPEARANCE visual method clear colorless liquid APPEARANCE visual method transparent liquid

pH 4.8 – 5.5 pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
Procedure:
1. Heat up the water to 40-50°C and add the ingredients
one after another in order from the table above. 1. In a main vessel combine ingredients from phase A 4. Add phase B to phase A and mix well.
and heat up to 65-70°C.
2. Before adding a parfum cool down the mixture to room 5. Cool the batch down to at least 30°C while mixing.
temperature and add the rest of ingredients. 2. Combine ingredients from phase B in a separate vessel
and mix until uniform.
3. Add Citric Acid if necessary.
3. Cool the batch down to at least 50°C while mixing.

58 Make up removers & micellar fluids Personal Care - Formulation Guide 59


MAKE-UP REMOVING LIQUID [KD-71] MAKE-UP REMOVING LIQUID [KD-72]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 92.94 solvent A Aqua 87.55 solvent

Betaine 0.25 active Pentylene Glycol 4.00 solvent

B Glycerin 1.00 moisturising agent Methylparaben 0.15 preservative

Xanthan Gum 0.05 rheology modifier Ethylparaben 0.15 preservative

C Sodium Lauroyl Sarcosinate ROKAtend LS 4.00 surfactant Betaine 0.10 active

D Polysorbate 20 ROKwinol 20 0.20 surfactant Glycerin 4.00 moisturising agent

Phenoxyethanol, B Sodium Lauroyl Sarcosinate ROKAtend LS 4.00 surfactant


1.00 preservative
Ethylhexylglycerin

C Citric Acid 0.05 pH adjuster


Propylene Glycol 0.50 solvent

E Citric Acid 0.06 pH adjuster

APPEARANCE visual method transparent liquid APPEARANCE visual method transparent liquid

pH 5.0 – 6.5 pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
Procedure:
1. In a main vessel combine ingredients from phase A and 4. Combine ingredients from phase D in a separate vessel
heat up to 65-70°C. and mix until uniform. 1. Combine ingredients from phase A. Add ingredients 2. Add Sodium Lauroyl Sarcosinate. Mix until uniform.
from phase A to hot water (75-80°C). Mix until homo- Cool the batch down to at least 30°C.
2. Add Xanthan Gum to Glycerin - mix until uniform. Add 5. Add ingredients from phase C, D and E to phase A
genous solution is obtained. Cool the batch down to
phase B to phase A while mixing. Mix until uniform. while mixing. Mix until uniform. 3. If necessary, adjust pH by Citric Acid to 5.0 – 7.0.
at least 50°C.
3. Cool the batch down to at least 50°C.

60 Make up removers & micellar fluids Personal Care - Formulation Guide 61


MAKE-UP REMOVING LIQUID [KD-73] MAKE-UP REMOVING MILK [KD-85]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 87.85 solvent A Ceteareth-12 ROKAnol T12 1.00 emulsifier

Betaine 0.10 active Ceteareth-25 ROKAnol T25 1.00 emulsifier

Glycerin 5.00 moisturising agent Cetearyl Alcohol 2.00 emulsion stabiliser

Phenoxyethanol, PPG-15 Stearyl Ether ROKAnol SP15L 5.00 emollient


B 1.00 preservative
Ethylhexylglycerin

Helianthus Annuus Seed Oil 1.00 emollient


PEG-7 Glyceryl Cocoate ROKAcet KO300G 2.00 surfactant

Caprylic/Capric Triglyceride 2.00 emollient


Sodium Lauroyl Sarcosinate ROKAtend LS 4.00 surfactant

B Aqua 83.35 solvent


E Citric Acid 0.05 pH adjuster

Betaine 0.50 active

C Glycerin 1.00 moisturising agent

Xanthan Gum 0.05 rheology modifier

D Carbomer 0.25 rheology modifier

E Sodium Hydroxide 0.05 pH adjuster

Phenoxyethanol, Methylparaben,
0.80 preservative
Ethylparaben, Propylparaben

PEG-7/PPG-2
F ROKAnol GA7LAW 2.00 emollient
Propylheptyl ether

APPEARANCE visual method transparent liquid APPEARANCE visual method white emulsion

pH 5.0 – 7.0 pH 5.0 – 7.0

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 2. Add ingredients from phase B. Mix until uniform. Cool 1. In a separate vesselI combine ingredients from phase 5. Add A into B, stir well with hand stirring, keep A/B at
from phase A to hot water (75-80°C). Mix until homo- the batch down to at least 30°C. A, B and C. 75-80°C. Homogenise with 2000-3000 RPM, 120 sec.
genous solution is obtained. Cool the batch down to
3. If necessary, adjust pH by Citric Acid to 5.0 – 7.0. 2. Add slowly phase D ingredients to phase B while mixing. 6. Cool the batch down to 50°C while mixing. Add phase E
at least 50°C.
Mix until uniform. ingredients while mixing. Homogenise with 2500-
3500 RPM, 90 sec.
3. Add slowly phase C ingredients to phase B while mixing.
Homogenise with 2000-3000 RPM, 90 sec. 7. Cool the batch down to 25°C. Add phase F ingredients
while mixing. Homogenise with 2500-3500 RPM, 90 sec.
4. Heat phase A and B to 75-80°C.

62 Make up removers & micellar fluids Personal Care - Formulation Guide 63


Face Treatment

SHAVING
PRODUCTS
Shaving products are intended to be used to assist in the removal of
unwanted body hair. Those products have to guarantee the ease and
effective shaving for both women and men. Cosmetic category called
“shaving products” beside of typical shaving product include cosme-
tics such as shaving soaps and creams as well as pre- and after shaving
lotions.

Shaving products are oftenly dispensed as an aerosol foam or gel that


produces a lather when rubbed on the skin. Shaving Creams typical-
ly contain ingredients that help lubricate the skin so that the razor can
work effectively.

In every shaving cream formulation,


each ingredient plays a role, howe-
ver some ingredients are essential,
others only have a minor effect.

The performance of the cream serves as the ultimate test for the formu-
lation and indicates whether the correct blend of ingredients and con-
centrations has been used. In addition, shaving creams often contain
ingredients including: botanicals, essential oil derivatives, chelators, pre-
servatives and other chemicals. Besides modulating performance, these
ingredients can add antiseptic qualities, serve as skin toners, increase
shelf life, etc. but more importantly, they make each formulation unique.

64 Shaving products Personal Care - Formulation Guide 65


AFTER SHAVING MOISTURIZING GEL [KD-101]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent

Acrylates/C10-30 Alkyl
0.40 rheology modifier
Acrylate Crosspolymer

Betaine 2.00 active

CI 42090 q.s. colorant

B Sodium Hydroxide 0.15 pH adjuster

C Parfum 0.30 fragrance

PPG-15 Stearyl Ether ROKAnol SP15L 3.00 emollient

Caprylic/Capric Triglyceride 2.00 fragrance

Starch Hydroxypropyltrimonium
0.10 conditioner
Chloride

Phenoxyethanol,
0.80 preservative
Ethylhexylglycerin

APPEARANCE visual method blue opaque gel

pH 4.5 – 5.5

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
1. In a separate vessel combine ingredients from phase A. 2. Homogenise with 2000-3000 RPM, 90-120 sec.
Add slowly Acrylates/C10-30 Alkyl Acrylate Crosspolymer
3. Add phase C ingredients while mixing. Homogenise
to water while mixing. Mix until uniform. Add other
with 2000-3000 RPM, 90-120 sec.
phase A components.

66 Shaving products Personal Care - Formulation Guide 67


Face Treatment

SHAMPOOS
Shampoo is a basic hair care product representing the largest segment
of hair care cosmetics. Typically, hair products are in the form of a visco-
us liquid, that is used for cleaning hair with some exception of waterless
solid form such as bar.

Shampoo is used by applying it to wet hair, massaging the product into


the hair, and then rinsing it out. Some consumers may follow a shampo-
oing with the use of products called 2 in 1. Conditioning shampoos, were
introduced to global markets in the late 1980s. A conditioning shampoo
is designed to deposit conditioning actives on hair while washing off dirt
at the same time.

The typical reason of using shampoo is to cleansing scalp, environmen-


tal dust, residues of hair care products and to remove the unwanted
build-up of sebum in the hair. Most of the dirt including sebum are water
insoluble and cannot be effectively removed by water alone. Therefore,
a shampoo contain a combination of surfactants. The content of surfac-
tants in a shampoo is typically between 10% - 20%.

Formulated shampoos are designed


to target every hair & lifestyle need
by nourishing, strengthening and
repairing hair with a variety of ingre-
dients from natural to synthetic.

Specialty shampoos are design to people with dandruff, color-treated


hair, gluten or wheat allergies, an interest in using an organic product,
and infants and young children.

68 Shampoos Personal Care - Formulation Guide 69


CLASSIC SHAMPOO [SZ-01] PEARL SHAMPOO [SZ-02]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 39.89 solvent


A Aqua 37.95 solvent

Citric Acid 0.06 pH modifier


PEG-7 Glyceryl Cocoate ROKAcet KO300G 2.00 re-oiling agent

Polyquaternium 10 0.15 conditioning agent


Polyquaternium 7 2.50 conditioning agent

Disodium Laureth
Disodium Laureth EXOsoft L3/40 2.50 surfactant
EXOsoft L3/40 4.00 surfactant Sulfosuccinate
Sulfosuccinate

Sodium Laureth Sulfate SULFOROKAnol L227/1 30.00 surfactant


Sodium Laureth Sulfate SULFOROKAnol L227/1 30.00 surfactant

Sodium Lauroyl Sarcosinate ROKAtend LS 15.00 surfactant


Sodium Lauroyl
ROKAtend LS 15.00 surfactant
Sarcosinate
B PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.50 re-oiling agent
B Citric Acid 0.05 pH modifier
PEG-120 Methyl
1.00 thickening agent
Glucose Dioleate
PEG-120 Methyl
C 1.00 thickening agent
Glucose Dioleate
C Parfum 0.50 fragrance
D Parfum 0.50 fragrance
Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol
Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol
Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant
Cocamidopropyl Betaine ROKAmina K30 4.50 surfactant
Sodium Laureth Sulfate,
D Cocamide DEA, EXOpearl N 1.00 pearling agent
E Sodium Chloride 1.50 viscosity modifier Glycol Distearate

E Sodium Chloride 1.40 viscosity modifier

APPEARANCE visual method turbid gel APPEARANCE visual method viscous, pearl gel

pH 5.0 – 7.0 pH 5.0 – 7.0

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1500 - 5000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 6000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Add ingredients from phase A to the hot water (70-75°C). 4. Add fragrance, Cocamidopropyl Betaine and preservative
1. Add ingredients from phase A to the hot water (70-75°C). 5. Add PEG-120 Methyl Glucose Dioleate during mixing.
While mixing add ingredients one after another in the during mixing. Mix until uniform.
Mix until uniform. Cool the batch down to at least 35°C.
2. While mixing add ingredients one after another in the order from the table above. Mix until uniform. NOTE.
5. Add pearling agent. Mix until uniform.
order from the table above. Mix until uniform. 6. Add fragrance, preservative and Cocamidopropyl Betaine Add Polyquaternium-10 and mix untill homogenous
during mixing. Mix until uniform. liquid is obtained. Add the rest of the phase A components. 6. Add NaCl to adjust the viscosity. NOTE. Add salt (not
3. Cool the batch down to at least 50°C.
in one go) – after addition of each portion mix well.
2. Cool the batch down to at least 50°C.
4. Control pH range. If necessary, adjust pH by Citric Acid
7. Control the pH range – if necessary, add Citric Acid.
to 5.0 – 7.0. 3. Add PEG-120 Methyl Glucose Dioleate and PEG-7
Mix well after adjustment.
Glyceryl Cocoate during mixing. Mix until uniform.
Cool the batch down to at least 35°C. 8. Control the viscosity if necessary, add Sodium Chloride.

70 Shampoos Personal Care - Formulation Guide 71


SHAMPOO FOR DAMAGED AND FRAGILE HAIR [SZ-03] MILD BRIGHT-GREEN SHAMPOO [SZ-05]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 46.62 solvent A Aqua up to 100 solvent

Xanthan Gum 0.75 viscosity modifier Benzophenone-4 0.05 UV absorber

Glycerin 2.00 moisturising agent CI 19140 q.s. colorant

Microcrystalline Cellulose 0.50 viscosity modifier CI 42090 q.s. colorant

B Aqua 13.00 solvent Ammonium Laureth Sulfate SULFOROKAnol A325/1 35.00 surfactant

Citric Acid 0.20 pH modifier Ammonium Lauryl Sulfate ROSULfan A 15.00 surfactant

Polyquaternium 10 0.03 conditioning agent Sodium Benzoate,


0.60 preservative
Potassium Sorbate
PEG-7 Glyceryl Cocoate ROKAcet KO300G 2.00 re-oiling agent
Citric Acid q.s. pH modifier

Ammonium Lauryl Sulfate ROSULfan A 10.00 surfactant


B Aqua 1.50 solvent

Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant


Citric Acid 0.01 pH modifier

Cocamidopropyl Betaine ROKAmina K30 3.50 surfactant


Polyquaternium 10 0.02 conditioning agent

C Parfum 0.40 fragrance


C Parfum 0.50 fragrance

Ehylhexyl glycerine,
1.00 preservative Cocamidopropyl Betaine ROKAmina K30 5.00 surfactant
Phenoxyethanol

Sodium Chloride 1.80 viscosity modifier

APPEARANCE visual method viscosus milky gel APPEARANCE visual method bright-green clear liquid

pH 5.0 – 7.0 pH 4.7 – 5.5

VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 9000 - 11000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2000 - 5000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. In a main vessel combine ingredients from the phase A. Add the rest of the phase B components. Mix until uni- 1. During mixing add Citric Acid and polyquaternium-10 4. Add parfum and Cocamidopropyl Betaine during mixing.
Add Xanthan Gum to Glycerin - mix until homogenous form. to warm water (40-45°C). Mix until homogenous solution Mix until homogenous solution is obtained.
solution is obtained. Add warm water (50-55°C) and is obtained.
3. Add phase B to phase A. Mix until homogenous solution 5. If necessary, add Sodium Chloride to adjust the viscosity.
Microcrystalline Cellulose. Mix until homogenous solution
is obtained. Cool the batch down to 30°C. 2. Add ingredients from phase A to warm water (40-45°C).
is obtained. Homogenise for 2-3 minutes. 6. Control pH range – if necessary, add Citric Acid. Mix well
While mixing add ingredients one after another in the
4. When the batch temperature is 30°C, add parfum and after adjustment.
2. Combine ingredients from the phase B. During mixing order from the table above. Mix until uniform.
preservative. Mix until uniform.
add Citric Acid and Polyquaternium-10 to warm water
3. Add phase B to phase A. Mix until homogenous solution is
(50-60°C). Mix until homogenous solution is obtained.
obtained. Cool the batch down to 35°C.

72 Shampoos Personal Care - Formulation Guide 73


Other

PRODUCTS
DEDICATED
TO BABIES
The skin of infants, babies and children require special treatment. Each
product form this category has to be developed in a way to support
the natural functions of the skin. Carefully selected ingredients work to-
gether and strengthen each other, making cosmetics very effective in
contact with even the most delicate, sensitive and problematic skin.

Babies, just like grown-ups, are expo-


sed to many chemicals via personal care
products throughout the day including
sunscreens, ointments, oils, shampoos
and soaps. Many of these products are
easily absorbed through the skin into
the blood stream, and babies are at least
ten times more vulnerable to the chemi-
cals in these products than adults.

Cosmetic products dedicated to babies must be safe for the health of in-
fants and should only contain ingredients that are non-toxic; potent aller-
gens or substances with endocrine disrupting activity should not be present
and preservatives should be used at their lowest effective concentrations.
Detailed recommendations for baby creams and lotions were agreed by
experts in the field to provide guidance to manufacturers and safety asses-
sors.

74 Other Personal Care - Formulation Guide 75


MILD BABY SHAMPOO WITHOUT SALT WASHING & BATHING LIQUD [2 in 1] FOR
ADDITION [SZ-06] INFANTS [KD-21]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua up to 100 solvent A Aqua 79.90 solvent

Sodium Benzoate, Xanthan Gum 0.80 rheology modifier


0.60 preservative
Potassium Sorbate

Glycerin 3.00 moisturising agent


Magnesium Laureth Sulfate EXOsoft MGB 17.70 surfactant

B Lactic Acid 0.30 pH adjuster


PEG-75 Lanolin ROKAnol LN75/50 1.00 moisturising agent
Sodium Benzoate,
0.50 preservative
Potassium Sorbate
MEA Lauryl Sulfate ROSULfan M 10.00 surfactant

Betaine 2.00 active


PEG-120 Methyl
B 1.50 thickening agent
Glucose Dioleate
Sodium Lauroyl Sarcosinate ROKAtend LS 5.00 surfactant
C Cocamidopropyl Betaine ROKAmina K30 6.50 surfactant
Panthenol 0.50 active
Parfum 0.30 fragrance
C Cocamidopropyl Betaine ROKAmina K30K 8.00 surfactant
Citric acid q.s. pH modifier

APPEARANCE visual method clear, light-yellow gel APPEARANCE visual method transparent, viscous gel

pH 5.0 – 5.5 pH 4.8 – 5.3

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1500 - 5000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 9000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add parfum and Cocamidopropyl Betaine during 1. In a main vessel combine ingredients from the phase A. 3. When the batch temperature is 35°C, add Cocami-
from phase A to warm water (55-60°C). Mix until mixing. Mix until uniform. Add Xanthan Gum to Glycerin - mix until homogenous dopropyl Betaine during mixing. Mix until uniform.
homogenous solution is obtained. solution is obtained. Add warm water (50-55°C). Mix
5. If necessary, adjust pH by Citric Acid to 5.0 – 5.5. 4. Control the pH range – if necessary, add Lactic Acid.
until homogenous solution is obtained. Homogenise
2. Add PEG-120 Methyl Glucose Dioleate during mixing. Mix well after adjustment.
for 2-3 minutes.
Mix until uniform.
2. Add the phase B components. Mix until uniform. Cool
3. Cool the batch down to 35°C.
the batch down to 35°C.

76 Other Personal Care - Formulation Guide 77


WASHING & BATHING LIQUD [2 in 1] FOR WASHING & BATHING GEL FOR INFANTS [KD-23]
INFANTS [KD-22]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION


A Aqua 84.20 solvent

A Aqua 82.25 solvent


Lauryl Glucoside 4.00 surfactant

Lauryl Glucoside 2.00 surfactant


Sodium Benzoate,
0.50 preservative
Potassium Sorbate
Betaine 1.00 active
Glycerin 2.00 moisturising agent
Glycerin 4.00 moisturising agent
Lactic Acid 0.30 pH adjuster
Lactic Acid 0.50 pH adjuster

Disodium Laureth
B EXOsoft L3/40 2.00 surfactant
Sodium Benzoate, Sulfosuccinate
0.50 preservative
Potassium Sorbate

Coco-Glucoside,
0.50 surfactant
B Sodium Lauroyl Sarcosinate ROKAtend LS 4.00 surfactant Glyceryl Oleate

Panthenol 0.25 active PEG-120 Methyl


C 0.50 thickener
Glucose Dioleate

PEG-120 Methyl
C 0.50 thickener D Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant
Glucose Dioleate

D Cocamidopropyl Betaine ROKAmina K30 5.00 surfactant

APPEARANCE visual method hazy, viscosus gel APPEARANCE visual method bright-yellow, viscous gel

pH 4.8 – 5.3 pH 4.8 – 5.3

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 9000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2000 - 8000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. Add PEG-120 Methyl Glucose Dioleate while mixing. 1. Combine ingredients from phase A. Add ingredients 4. Add Cocamidopropyl Betaine during mixing. Mix until
from phase A to warm water (55-60°C). Mix until Mix until uniform. Cool the batch down to at least 30°C. from phase A to warm water (55-60°C). Mix until uniform.
homogenous solution is obtained. Cool the batch homogenous solution is obtained. Cool the batch
4. Add Cocoamidopropyl Betaine while mixing. Mix until 5. If necessary, adjust pH by Lactic Acid to 4.8 – 5.3.
down to at least 50°C. down to at least 50°C.
uniform.
2. Add ingredients from phase B durin mixing. Mix until 2. Add ingredients from phase B. Mix until uniform.
uniform.
3. Add PEG-120 Methyl Glucose Dioleate during mixing.
Mix until uniform. Cool the batch down to at least 30°C.

78 Other Personal Care - Formulation Guide 79


HAIR & BODY WASHING FOAM FOR CHILDREN [KD-25] BATHING LIQUID FOR INFANTS [KD-26]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 89.10 solvent A Aqua up to 100 solvent

Sodium Benzoate, Lauryl Glucoside 2.00 surfactant


0.50 preservative
Potassium Sorbate

Glycerin 2.00 moisturising agent


Betaine 0.50 active

Betaine 0.50 active


Glycerin 2.00 moisturising agent

Sodium Benzoate,
0.50 preservative
Disodium Laureth Potassium Sorbate
B EXOsoft L3/40 5.50 surfactant
Sulfosuccinate

Lactic Acid q.s pH adjuster


PEG-120 Methyl
C 0.25 thickener
Glucose Dioleate
B Magnesium Laureth Sulfate EXOsoft MG / EXOsoft MGB 12.00 surfactant

D Lactic Acid 0.15 pH adjuster


PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant

Cocamidopropyl Betaine ROKAmina K30 2.00 surfactant


PEG-120 Methyl
0.80 thickener
Glucose Dioleate

D Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant

APPEARANCE visual method transparent liquid APPEARANCE visual method light-yellow liquid

pH 5.0 – 5.5 pH 4.8 – 5.3

STABILITY 1 month at 5°C, RT, 40°C confirmed VISCOSITY [cP] Brookfield LV, spindle 34, speed 10 RPM, T: 25°C 1000 - 3000

STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add Cocamidopropyl Betaine during mixing. Mix until Procedure:
from phase A to warm water (45-50°C). Mix until uniform.
homogenous solution is obtained. 1. Combine ingredients from phase A. Add ingredients 3. Add Cocoamidopropyl Betaine during mixing. Mix
5. Readjust the final pH to 5.0 - 6.5 with additional Lactic
from phase A to warm water (50-55°C). Mix until until uniform.
2. Add Disodium Laureth Sulfosuccinate during mixing. Acid.
homogenous solution is obtained. Cool the batch
Mix until uniform.
down to at least 50°C.
3. Add PEG-120 Methyl Glucose Dioleate during mixing.
2. Add ingredients from phase B while mixing. Mix until
Mix until uniform. Cool the batch down to at least 30°C.
uniform. Cool the batch down to at least 30°C.

80 Other Personal Care - Formulation Guide 81


BATHING & WASHING LIQUID FOR INFANTS [KD-27] BATHING & WASHING LIQUID FOR CHILDREN FROM
3 YEARS OLD [KD-33]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

A Aqua 71.35 solvent PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

Sodium Benzoate, A Aqua 76.90 solvent


0.50 preservative
Potassium Sorbate
Sodium Benzoate,
0.50 preservative
Glycerin 2.00 moisturising agent Potassium Sorbate

Lactic Acid 0.35 pH adjuster Betaine 0.50 active

B Ammonium Laureth Sulfate SULFOROKAnol A325/1 15.00 surfactant Glycerin 2.00 moisturising agent

Decyl Glucoside 1.00 surfactant


Sodium Lauroyl Sarcosinate ROKAtend LS 3.00 surfactant

B MEA Lauryl Sulfate ROSULfan M 10.00 surfactant


Coco-Glucoside,
C 1.00 surfactant
Glyceryl Oleate
PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant
PEG-120 Methyl
0.80 thickener
Glucose Dioleate
C Polysorbate 20 ROKwinol 20 0.30 surfactant

D Coco Betaine ROKAmina K30B 6.00 surfactant


Parfum 0.30 fragrance

D Cocamidopropyl Betaine ROKAmina K30 8.00 surfactant

APPEARANCE visual method light-yellow liquid APPEARANCE visual method light-yellow gel

pH 4.8 – 5.3 pH 4.8 – 5.2

VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1000 - 3000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1000 - 4000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. Add PEG-120 Methyl Glucose Dioleate and Coco- 1. Combine ingredients from phase A. Add ingredients 4. Add phase C to the main vessel while mixing. Mix until
from phase A to warm water (50-55°C). Mix until Glucoside, Glyceryl Oleate during mixing. Mix until from phase A to water (30-35°C). Mix until homogenous uniform.
homogenous solution is obtained. uniform. Cool the batch down to at least 30°C. solution is obtained. Cool the batch down to at least 30°C.
5. Add Cocoamidopropyl Betaine while mixing. Mix until
2. Add ingredients from phase B durin mixing. Mix until 4. Add slowly Coco Betaine during mixing. Mix until 2. Add ingredients from phase B. Mix until uniform. uniform.
uniform. uniform.
3. Combine ingredients from phase C in a separate vessel. 6. If necessary, adjust pH by Lactic Acid to 4.8 – 5.2.
Add Parfum to Polysorbate 20 - mix until uniform.

82 Other Personal Care - Formulation Guide 83


BATHING LIQUID FOR CHILDREN FROM 3 YEARS SHAMPOO FOR CHILDREN FROM 3 YEARS OLD [KD-37]
OLD [KD-35]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION

PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION A Aqua up to 100 solvent

A Aqua 71.85 solvent Sodium Benzoate,


0.50 preservative
Potassium Sorbate
Sodium Laureth Sulfate SULFOROKAnol L227/1 13.00 surfactant
Betaine 1.00 active

Sodium Lauroyl Sarcosinate ROKAtend LS 3.00 surfactant


Lactic Acid 0.25 pH adjuster

Sodium Benzoate,
0.50 preservative
Potassium Sorbate Benzophenone-4 0.05 UV filter

Glycerin 3.00 moisturising agent CI 42090 q.s. colorant

PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant B Ammonium Laureth Sulfate SULFOROKAnol A325/1 30.00 surfactant

Lactic Acid 0.25 pH adjuster C Polyquaternium-7 0.25 conditioner

PEG-120 Methyl PEG-120 Methyl


B 0.50 thickener 0.50 thickener
Glucose Dioleate Glucose Dioleate

C Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant

Parfum 0.50 fragrance D Cocamidopropyl Betaine ROKAmina K30K 6.00 surfactant

D Sodium Chloride 0.90 thickener E Parfum 0.30 fragrance

Sodium Laureth Sulfate,


Cocamide DEA, EXOpearl N 1.00 surfactant
Glycol Distearate

F Sodium Chloride 1.80 thickener

APPEARANCE visual method transparent liquid APPEARANCE visual method pearl, light-blue gel

pH 4.8 – 5.3 pH 4.8 – 5.3

VISCOSITY [cP] Brookfield LV, spindle 34, speed 12 RPM, T: 25°C 1000 - 4000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 8000

STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed

Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add Sodium Chloride during mixing (Add small 1. In a main vessel combine ingredients from phase A. 4. Add slowly Cocoamidopropyl Betaine while mixing.
from phase A to water (55-60°C). Mix until uniform. portions and dissolve). Heat up to 55-60°C. Mix until uniform. Mix until uniform.
Cool the batch down to at least 50°C.
5. If necessary, adjust pH by Lactic Acid to 4.8 – 5.3. 2. Add Ammonium Laureth Sulfate. Mix until uniform. 5. Add ingredients from phase E. Mix until uniform.
2. Add PEG-120 Methyl Glucose Dioleate during mixing.
3. Add ingredients from phase C. Mix until uniform. Cool 6. Add Sodium Chloride while mixing (Add small portions
Mix until uniform. Cool the batch down to at least 30°C.
the batch down to 30°C. and dissolve).
3. Add Cocamidopropyl Betaine and Parfum during
mixing. Mix until uniform.

84 Other Personal Care - Formulation Guide 85


www.products.pcc.eu

You might also like