ICP-OES Plasma Troubleshooting Guide

Agilent 700 Series
ICP Optical Emission

Spectrometers
Plasma
Troublshooting Guide
Agilent Restricted
ICP-OES Plasma Troubleshooting Guide
Contents
Introduction ...............................................................................................................................................................4
First steps ...................................................................................................................................................................4
1. Check the reported error message ................................................................................................................4
RF Error list .................................................................................................................................................................5
RF RAM Failure .......................................................................................................................................................5
RF ROM Checksum Failure .....................................................................................................................................5
HV Supply Failure ...................................................................................................................................................6
Plasma Has Gone Out.............................................................................................................................................6
Plasma compartment door is open or emergency RF-off button is depressed .....................................................6
Insufficient Water Flow ..........................................................................................................................................6
RF Power Tube Air Flow Failure .............................................................................................................................6
RF Power Tube Voltage Failure ..............................................................................................................................7
Power Unattainable ...............................................................................................................................................7
Maximum power timeout failure...........................................................................................................................7
Over current failure ...............................................................................................................................................7
RF failure ................................................................................................................................................................7
Troubleshooting procedures......................................................................................................................................8
A. Plasma does not light .................................................................................................................................8
B. Plasma lights and then goes out ................................................................................................................9
RF Interface board .............................................................................................................................................. 10
Filament Power Supply ....................................................................................................................................... 11
High Voltage Power Supply (HVPS) Checks ......................................................................................................... 12
The HVPS module is activated. ....................................................................................................................... 12
The HVPS module is delivering the requested voltage and current. .............................................................. 14
RF Generator Assembly....................................................................................................................................... 16
1. Fibre Optic Looker ................................................................................................................................... 16
2. RF Power Tube ........................................................................................................................................ 17
3. Current Sensor ........................................................................................................................................ 17
4. Grid Circuit .............................................................................................................................................. 18
5. Anode Circuit........................................................................................................................................... 20
Appendix ................................................................................................................................................................. 21
RF Interface board details ................................................................................................................................... 21
Issued: May 2013 – SPSD Product Support Copyright ã 2013 Agilent Technologies Agilent Restricted Page 2 of 40
Typical RF test point voltages ............................................................................................................................. 23

Tables for recording RF voltages ......................................................................................................................... 24
Work Coil adjustment ..................................................................................................................................... 25
Checking torch installation.............................................................................................................................. 27
HVPS Status LED’s and connections ................................................................................................................ 28
RF System Circuit Diagram .................................................................................................................................. 29
Plasma System Illustrated parts breakdown ...................................................................................................... 30
Instrument front ............................................................................................................................................. 30
Instrument right hand side ............................................................................................................................. 31
Anode compartment ....................................................................................................................................... 32
Grid compartment .......................................................................................................................................... 33
Filter Assembly ................................................................................................................................................ 34
Current Sensor - Axial ..................................................................................................................................... 35
Current Sensor - Radial ................................................................................................................................... 36
Igniter compartment ....................................................................................................................................... 37
Torch Compartment - Radial ........................................................................................................................... 39
Cables .............................................................................................................................................................. 40
Introduction
Problems with the 700 Series ICP-OES plasma RF can sometimes be difficult to troubleshoot. The aim of this
troubleshooting guide is to guide service personnel to efficient fault resolution.
Prior to commencement of work on the RF plasma system please read and understand the following warning:
WARNING RF Radiation – Electric Shock – Hot Surfaces

The RF power Generator contains components operating at high voltages
(7kVDC), high RF power levels (1.8 kW, 40 MHz) and high temperatures.
To prevent death or injury from contact with hazardous components or

radiation, never operate the instrument unless all safety panels are secured
in their correct position and all the safety interlocks are satisfactory and
working.
The High Voltage Power Supply contains no serviceable parts, do not attempt
to disassemble.
Never compromise original safety standards by modifying or altering wiring

looms, circuit boards, or circuit connections.
First steps
1. Check the reported error message
The first step to begin troubleshooting is to identify the error message that is reported at the time of the plasma failure.
This may be the software error number and message reported by the customer or found by viewing the contents of the
Error and Debug log files:
The Error and Debug log files can be found in the following locations:
ICP Expert, ICP Expert II v1.x.x, ICP Expert II v2.x.x -Windows XP:
C:\Program Files\Varian\ICP Expert II 7xx-ES\Run\log
ICP Expert II v2.x.x - Windows 7:
C:\Users\Public documents\Varian\ICP Expert II\Log
For RF issues it is possible to receive multiple error messages at the same time. For example if the plasma goes out
suddenly to a hardware fault it is common to receive “Plasma has gone out” along with other RF error messages. In this
case the “Plasma has gone out” message is because of the hardware fault causing the plasma to fail. The attention should
be placed on other messages aside from the “Plasma has gone out” message.
If the only message received is “Plasma has gone out” then the cause may well be something other than the RF system.
Once the error messages are obtained review the RF error list on page 5 for the suggested action.
Other symptoms can be of significant importance too and need to be considered when determining troubleshooting
actions. The types of other symptoms are often noises such as a pop, loud bang or crackling which indicates an electrical
discharge.
RF Error list
Table 1 lists the Software error number the message along with the corresponding firmware error number and message.
Once the error message for the plasma fault has been determined refer to table 1 to determine the next actions to take.
Table 1 Plasma Error Messages
Software error Software message Firmware Firmware Refer to page

Error Message
1240 RF RAM failure 1 RAM Failure 5
1241 RF ROM checksum failure 2 ROM Checksum 5
Failure
1243 High voltage supply failure 4 HV Supply Failure 6
1245 Plasma has gone out 6 Plasma Has Gone Out 6
1244, 1246 Plasma compartment door 7 HV Cabinet Open 6
is open or emergency RF-
off button is depressed
1248 Insufficient water flow 9 Water Flow Failure 6
1250 RF power tube air flow 11 Filament Air Flow 6
failure Failure
1251 RF power tube voltage 12 Filament Voltage 7
failure Failure
1252 Power Unattainable 13 ALC Failure 7
1253 Maximum power timeout 14 Max Power Timeout 7
failure Failure
1254 Over current failure 15 Current Overload 7
Failure
60304 The Torch ignition has 16 Grid Bias Failure 7
failed
1255 RF Failure 16 Grid Bias Failure 7
1256 Plasma compartment door 17 HV Interlock open 6
is open or emergency RF-
off button is depressed
RF RAM Failure
Cause Fault detected with RF Interface board RAM
Actions Replace RF Interface board
RF ROM Checksum Failure

Cause Checksum failure when reading ROM contents
Actions
1. Check seating of PROM in socket, IC 7 on RF interface board
2. Replace RF Interface board
HV Supply Failure
Cause The High Voltage Power Supply has reported an error.
Actions
1. Check that the circuit breaker on rear of the instrument is switched on.
2. Verify all interlocks are enabled to allow the HVPS to energise. These include Air, water,
switch Interlocks and filament voltage
3. Verify if the HVPS is being energised; refer to troubleshooting checks to see if the HVPS is
being energised on page 12
4. Test the HVPS in isolation, if it fails to provide voltage then replace. Refer to page 15 for the
procedure.
5. Possible short on high voltage supply line in RF Generator. Follow troubleshooting for the
Anode circuit on page 20.
Plasma Has Gone Out

Cause The plasma has gone out unexpectedly or the plasma has failed to form during ignition.
Actions
1. Plasma has gone out will often be reported along with other plasma error messages as the
result of some other fault. If there are other errors reported at the same time follow the
troubleshooting for these items first.
2. If plasma does not light then check troubleshooting Plasma does not light on page 8.
3. If plasma lights and then goes out some time later check troubleshooting for Plasma lights
and then goes out on page 9.
Plasma compartment door is open or emergency RF-off button is depressed

Cause Plasma compartment door is not closed or RF off button is depressed.
Actions
1. Check RF-off button is not depressed.
2. Check plasma compartment door is closing correctly and switches are correctly adjusted.
3. Check door switches are not faulty.
4. Check RF Generator interlocks on top cover and filter compartment
Insufficient Water Flow

Cause Cooling water flow is below the required 1.1 l/min
Actions
1. Check water chiller is operating correctly and supply pressure is between 55-310kPa (8-
45psi)
2. Verify water level in water chiller reservoir is OK
3. Check instruments rear water filter for blockage, clean if needed.
4. Check water flow direction is correct through the instrument
5. Replace water flow sensor.
6. Replace Peristaltic pump driver board.
RF Power Tube Air Flow Failure

Cause No air flow detected to RF tube.
Actions
1. Check fan is operating. If not ensure mains voltage is applied to the motor.
2. Inspect for dust accumulation; dust can often accumulate on the honeycomb filter below
the RF tube socket, the fan intake grill and fan blades.
3. If fan is operating and the air system is free from dust replace the air sensor switch.
RF Power Tube Voltage Failure

Cause Filament voltage for the RF power tube is not able to be supplied correctly
Actions
1. Measure voltage from TP8 to ground. ~5vdc indicates filament voltage is OK if LED 8
(filament voltage OK) is off replace RF interface board.
2. Check filament transformer supply connections are clean and tight.
3. Check water and air flow interlocks are reporting OK.
4. Follow troubleshooting for Filament power supply on page 11.
Power Unattainable
Cause The requested power level by software is not able to be achieved by the RF system.
Actions
1. The RF tube has reached the end of its life and needs to be replaced. If a lower power level
can still be delivered without error this verifies the RF tube has reached the end of its life.
2. Current transformer faulty, follow troubleshooting to check the current sensor circuit on
page 18.
Anode circuit page 20.
Maximum power timeout failure

Cause RF Interface PCA has not received a run power setting after 4 seconds of plasma ignition.
Actions
1. Failure of the RF interface PCA
2. Failure of the Instrument control board
3. Communications failure with PC
Over current failure

Cause High voltage power supply has reached maximum current output.
Actions
1. Fault of RF tube. The RF tube efficiency has dropped to the point where the excessive
current is needed to deliver the requested power. Try a lower power setting, if this is
successful then the tube has reached the end of its life.
Anode circuit on page 20.
3. Fault in grid bias circuit, refer to troubleshooting the grid circuit on page 18
RF failure
Cause The RF Generator failed to oscillate (no grid current detected)
Actions
1. The RF tube has failed, test with new RF tube.
2. Fault in grid bias circuit, refer to troubleshooting the grid circuit on page 18
Troubleshooting procedures
A. Plasma does not light
If no plasma is formed at all then the following items should be checked.
1. Argon purity.
If the argon is not the required 99.996% purity or is contaminated the plasma may not form. Check the grade of
argon being used. If using cylinders try another cylinder, if possible try a cylinder from another batch or supplier.
Check the argon supply and regulator for leaks.
Long lengths of plastic tubing should not be used for the argon as plastic is air permeable.
Issues with liquid argon supplies are extremely rare and are normally not suspected.
2. Air in torch or spray chamber.

This in effect is the same as argon purity issues where the argon is being contaminated by air. If the torch has just
been cleaned, ensure it is dry before lighting the plasma.
Connections:
Check all connections of the sample introduction system for cracks, missing or damaged items. This includes the
torch, torch connection gas lines, transfer tube, spray chamber, o-rings, nebuliser, drain and sample tubing.
Purge:
The torch may fail to light at the first attempt if the air in the torch and spraychamber has not been fully purged.
Repeat the torch light procedure. You may wish to increase the purge time in the Instrument setup Ignition tab if
this occurs regularly. Also, the nebulizer flow must be allowed to drop to zero before ignition. This is particularly
important for axial instruments. This may require a longer Delay time, especially if you have an Argon Saturator
Accessory fitted.
3. Incorrect torch gas connections.

Check that the plasma and auxiliary gas lines are connected to the torch correctly and free from kinks.
It is possible to reverse these fittings inadvertently or route the lines so they kink and close over.
4. Organics samples.
After running organic samples, the torch area and spraychamber may fill up with organic vapors. Use a
higher power and longer purge time for the ignition. If this is unsuccessful, clean the spraychamber before
attempting to light the plasma again.
A higher power level is required to ignite and maintain the plasma when running low boiling point organic samples
such as methanol. Ignition parameters can be set on the Ignition tab of the Instrument Setup screen.
5. Torch alignment.
Check that the torch is correctly positioned in the work coil. Refer to checking torch installation on page 27 also
check the torch is set to the correct depth in the torch stand as shown below:
Figure 1 Radial Torch positioning Figure 2 Axial Torch positioning
The top of the torch intermediate tube should The intermediate tube of the torch should be
sit at least 2 mm below the induction coil. approximately 3 mm to the left of the induction coil
6. Torch condition and cleanliness (including bonnet).

If the torch is deformed (melted), cracked, blocked or dirty the gas flows may be affected which can cause plasma
problems as well as analytical performance issues.
7. Work coil shape and position

The shape and the position of the work coil can affect the amount of RF energy entering the plasma. Verify the
correct work coil shape and position. Incorrectly positioned work coils can also cause melting of torches. Refer
the Appendix for Work coil Adjustment on page 25
8. Incorrect gas flows for Plasma, Auxiliary and Nebuliser flows. Verify correct gas flows for these gasses. Refer to
700 series Service Manual chapter 10 for details on how to check these flows.
9. No seeding spark.
Check that the seeding spark is reaching the torch during the ignite phase. The ignitor may have failed or the
spark is discharging to some other point due to contamination.
10. Check that there is communications with the PC.

On the Instrument Setup, Status tab ensure that the instrument is Online.
Check communications to the RF interface board by observing periodic blinking of the RF activity LED on the
Instrument setup screen or by watching LED D5 on the RF interface board.
B. Plasma lights and then goes out

If the plasma lights and goes out in a few seconds of ignition then check the following.
1. Check the Fiber Optic Looker refer to page 16

2. Verify ignition parameters.
The ignition parameters are loaded after successful ignition of the plasma. If the values are inappropriate the
plasma may shut off. Refer to the default ignition parameters below:
Figure 3 Instrument default ignition settings
3. Check spray chamber is draining correctly and there are no droplets of liquid in the torch.
If the plasma stays lit and then goes out some time after check the following:
1. The spray chamber is not draining.
If the spray chamber is not draining correctly then it may fill up and allow liquid to enter the torch putting out
the plasma.
2. A droplet of liquid enters the torch.

If the spray chamber or transfer tube is dirty, droplets may form on the surface and eventually these may
enter the torch extinguishing the plasma. Clean spray chamber if droplets are forming on the surface.
3. An RF component has overheated.

Verify the exhaust ducting is providing sufficient extraction and the extraction hood is correctly positioned.
Inspect the honeycomb filter beneath the RF power tube, if this is blocked clean with a brush and vacuum
cleaner.
Verify both cooling fans are operating correctly and are not blocked on the front of the HVPS. If a fan has
failed then replace the HVPS unit.
Replace the HVPS as excessive dust may have accumulated within the power supply.
RF Interface board
The RF interface board controls and monitors the plasma generating system. These functions include:
• Cooling fan air flow monitoring
• Cooling water flow
• Safety interlocks
• Filament supply status
• High voltage supply status
• Power oscillator grid current
• Plasma ON
• RF power level control (ALC)
Below are some important points to aware of;
1. The following interlocks must be satisfied before the HVDC power supply is turned on
• RF Door and RF cabinet interlock bi-stable switches closed
• Water On
• Fan On
• Filament On
You can visually check the status of these interlocks by looking at either the Software indicators in the
Diagnostics software or the LED state indicators on the RF interface board.
LED state indicators on the RF interface board
D7 ON = Water Flow OK (green)
D8 ON = Cooling Fan OK (green)
D9 ON = Filament Supply OK (green)
D13 ON = Plasma/HV interlock OK (green)
Refer to the RF Interface board details on page 21 for the location of the LED’s
For details on the Diagnostics software, refer to Section 7 of the 700-ES series Service Manual.
2. During the Plasma Ignition sequence, some of the monitors in the plasma generating system are ignored until the
start of the Run phase. These include;
• Plasma ON
• RF power level control (ALC)
If there is a fault with any of these, the plasma may ignite for a short time and then go out when the Plasma
Ignition sequence starts the Run phase.
You can visually check the status of these interlocks by looking at the LED state indicators on the RF interface board.
LED state indicators on the RF interface board
D6 ON = Plasma ON (yellow)
D14 ON = ALC fail (red)
The “ALC fail” LED state indicator will be on momentarily when the plasma first
NOTE ignites - this is normal.
If a fault with the ‘Plasma ON’ monitoring is suspected, then the Fibre Optics checks should be carried out, refer
page 16.
If a fault with the ‘ALC fail’ monitoring is suspected, then the Current Sensor checks should be carried out, refer
page 17.
Filament Power Supply

The purpose of the filament power supply is to provide low voltage at high current to the RF tube filament. It is
supplied by a transformer located at the left-rear side of the instrument. Control for the filament power supply is
provided by the Instrument Power board.
The filament supply enters the RF power Generator assembly through four low pass filters mounted on the outer wall
of the filter compartment. The input voltage is further filtered by inductors L6, L7 and capacitors C1, C9, C10, C16, C17,
and C18. The filament supply passes into the grid compartment and is terminated at pins 1 and 5 on the RF tube
socket.
The filament draws ~22A at 6.61 VRMS +/- 5% measured at the filament transformer during the first 200 hours and
reduces to 6.17VRMS thereafter. All voltages measured at the filament transformer terminals.
There are four main areas to check for correct filament supply operation:
1. The Filament power supply is activated.
This can be tested by simply observing if LED indicator “D9” on the RF interface board is ON.
If LED indicator “D9” is OFF, ensure that the Filament supply is activated in the instrument software.
Figure 4 Setting supply

If the Filament filament (Stage 1) On
is activated, but the LED indicator “D9” is OFF. This may indicate;
If the filament supply is activated, but the LED indicator ‘D9’ is off, this may indicate:
• Failed Solid State Relay (SSR)
• Failed Instrument Power Control board.
2. The filament voltage and current.

This can be tested by simple measurement using a True RMS meter. An Agilent U1193A True RMS clamp meter has
been used to take the measurements below.
Figure 6 Measuring the filament voltage Figure 5 Measuring the filament current
If the measured voltage and current are not as expected, then possible causes are;
• Failed filament transformer,
• Failed filament Solid State Relay (SSR)
• Failed instrument power board
3. The electrical resistance of the filament wires from the transformer terminals to the RF tube socket.
This can be tested by measurement to ensure good electrical contact is made at all electrical connections and
terminations. There should be little (if any) electrical resistance from the filament transformer terminals to the RF
tube socket. Note: Circuit resistance is less than multimeter lead resistance.
4. The RF Tube Filament

The RF tube contains a filament that can fail open circuit. Refer to the picture below for the RF tube filament pins to
the continuity of the filament. The filament resistance is less that the resistance of the multimeter leads.
Figure 7 Checking continuity of RF tube filament
High Voltage Power Supply (HVPS) Checks

The purpose of the HVPS is to provide high voltage to the anode of the RF tube. Control for the HVPS is
provided by the RF Interface board.
The high voltage passes into the RF Generator through the filter compartment (capacitors C13, C14, and C15
with RF chokes RFC4 and RFC5) into the anode compartment (through RFC1 and tank coil L1), and is terminated
at the anode of the RF tube.
There are two main areas to check on the HVPS module:
The HVPS module is activated.

There are three visual indicators that can be used to determine if the HVPS is activated and ready to deliver the
requested output voltage and current.
• LED 2 (Green) on the HVPS
• Rotation of the internal fans on the HVPS
• LED (Red) inside the HVPS is on (this LED can be seen on the bottom circuit board through the air-intake
grate of the internal fan on the right side of the HVPS). Refer Figure 28 HVPS Energised LED
If the LED 2 (Green) is ON, both internal fans are rotating and LED energised is ON, the HVPS is activated.
If the LED 2 (Green) is OFF and the internal fans are not rotating, ensure that the HVPS (HV (Stage 2)) is enabled in
the instrument software.
Figure 8 Setting HV (Stage 2) on

Filament (Stage 1) MUST be enabled and active first before HV (Stage 2) will be
NOTE enabled.
If the HVPS is enabled in the software, but the LED 2 (Green) on the HVPS and/or the Red LED inside the HVPS are
OFF, this indicates that the contactor (internal to the HVPS) has not been energised.
There are two methods to check if the contactor is ‘energised’.

1. Using a voltmeter, Measure the voltage between pin 1 & 2 of 2PL1 (this is the 2 pin connector on the
HVPS.). The voltmeter reading should be 24vdc (~30vdc typical).
Figure 9 Checking HVPS contactor energize voltage
2. Disconnecting and reconnecting 2PL1 on the HVPS. As you disconnect and reconnect 2PL1, you should
hear the contactor clicking as the contacts open and close.
If the contactor is not ‘energised’,

• Check on the RF interface board that D13 (Plasma/HV interlock OK (green)) is ON
• Check all the safety interlocks (all RF box interlock switches, plasma compartment door and the Plasma off
button) for correct operation, high resistance contacts/connections or short circuits to chassis.
• Replace RF interface board
NOTE The power supply to the contactor is routed through all the safety interlocks.
If the contactor is ‘energised’,

• Using a voltmeter, measure between the mains terminals of the HVPS.
The voltmeter reading should be reading the site mains voltage (between 187-264vac depending on local supply)
If not then,
• Check if the circuit breaker at the rear of the instrument is ON and working correctly.
• Check the associated mains filter components.
• Replace HVPS
The HVPS module is delivering the requested voltage and current.

This can be tested by simple measurement of the test points on the RF Interface board using a voltmeter.
Refer to RF interface board details on 21 for test point locations and refer to the table of RF test point voltages on
page 23 for typical values for a range of RF power settings.
Figure 10 Applying an RF Power of 1.0kW
Filament (Stage 1) and HV (Stage 2) MUST be enabled first before the RF power will
NOTE be applied.
Select an RF power level of 1.0kW.

At a power level setting of 1.0kW,
• The request output voltage (mod voltage) between (TP21) and ground, TP 18 should be ~ 5.5Vdc
• The HVPS output voltage signal (TP19) and ground (TP18) should be ~ 3.8Vdc
Measure the output voltage signals using a voltmeter.

• If the output voltage signals are as expected, then the HVPS is OK.
• If the output voltage signals are not as expected, then follow the procedure below;
a) View the contents of the Error and Debug log files and check for any reported RF system faults.
b) If there are faults such as Grid Bias Failure, the RF Interface board will shut down the RF system and you will not
be able to measure the output voltage signals.
You can over-ride this error and force the HVPS to remain on by:
1. Connect a ‘clip lead’ from TP1 (+5v) to the anode of D17 on the RF Interface board. Refer to Figure 11 Clip
lead from TP1 +5V to the anode of D17
2. Move ALC test link to LK1 to the test position. Refer to RF Interface board details on page 21 for the location
of the ALC test link
3. Apply an RF power of 1.0kW
4. Measure the HVPS output voltage signals (TP19) using a voltmeter. If the output voltage signals are as
expected ~3.8Vdc, then the HVPS is OK.
If the HVPS checks out OK then the cause of the Grid Bias error is a failure of the RF Generator to oscillate. The
RF Generator assembly needs to be inspected for a cause.
D17 Anode
TP1 +5v
Figure 11 Clip lead from TP1 +5V to the anode of D17
A suitable clip lead would be p/n 8184000200 12IN Test Clip-BLK or Pomona 3781
NOTE Minigrabber® Test Clip Patch Cord.
c) If the output voltage signals are not as expected and there are no error messages displayed.
Then using a voltmeter, check that;
• PL4 pin 14 (Enable) on the HVPS is > +2.4vdc.
• PL4 pin 1 (Cntrl) on the HVPS is ~ +5.7vdc.
If these voltages are as expected, then the HVPS is faulty.

If the output voltage signals are not as expected, then the RF interface board or cabling is faulty.
d) If the output voltage signals are not as expected and a “Current Overload Failure” or “ALC Failure” is recorded,
then an overcurrent or overvoltage has been reported by the HVPS. At the time the error is reported the
overcurrent orange LED on the HVPS will momentarily light for an overcurrent fault and the red overvoltage
LED for an ALC failure. The RF interface board will then shut down the HVPS and you will not be able to
measure the HVPS output voltage signals. In this case it is necessary to test the HVPS in isolation from the RF
Generator assembly. Please follow the procedure testing the HVPS in isolation on page 15 to determine if the
HVPS or RF Generator is at fault.
Refer to Figure 27 for the location of the overcurrent and overvoltage LED’s.
Testing the HVPS in isolation

1. Turn off the instrument power.
2. Disconnect the red HV wire at the HVPS right hand side.
3. Connect a ‘clip lead’ from TP1 (+5v) to the anode of D17 on the RF Interface board. Refer to Figure 11
Clip lead from TP1 +5V to the anode of D17
4. Move ALC test link LK1 to the test position. Refer to RF Interface board details on page 21 for the
location of the ALC test link.
5. Power on the instrument
6. Turn on Filament (Stage 1) and HV (Stage 2) and ensure they are on.
7. Apply an RF power of 1.0kW
8. Measure the HVPS output voltage signals (TP19) using a voltmeter. If the output voltage signals are as
expected ~3.8Vdc, then the HVPS is OK. If there is no voltage then the HVPS is not being enabled or
has failed.
RF Generator Assembly
There are several areas inside the RF box that can be checked, these include;
1. Fibre Optic Looker
2. RF Tube
3. Current sensor
4. Grid circuit
5. Anode circuit
1. Fibre Optic Looker

An optical fibre in the torch compartment is positioned to look at the plasma. When the plasma is on, light
from the plasma is monitored by the RF Interface board.
There is an LED on the RF interface board to indicate its status:

LED D6 (Plasma ON (yellow))
If LED D6 is OFF and the plasma is on, light is not being detected from the fibre optic looker. The RF system will
be shut down the RF, firmware error [6] and the following error will be displayed PC. “Plasma has gone out”.
Typically if the above error is the only error written in the error log file, this indicates that the fibre optical
looker failed to see the light from the plasma.
To confirm a fault with the Fibre optic looker, the monitoring of the fibre optic looker can be over-ridden by
placing LK2 on the RF Interface board into the “Test” position. Refer to RF interface Board details on page 21
for the location of LK2.
With LK2 in the test position, the LED D6 will be ON and the plasma ON button in the
software will not be active. Therefore to ignite the plasma, place LK2 in the ‘Run’
NOTE
position and press the Plasma ON button, as the ignition sequence enters the ignite
phase move LK2 to the ‘Test’ position.
If the plasma ignites and runs normally with LK2 in the ‘Test’ position and goes out when LK2 is returned to the ‘Run’
position. This indicates one of the following conditions
a) The optical fibre is faulty.
If this is the case, check if the tip of the optical fibre is damaged.
If it is damaged, you can cut off the damaged section and strip the outer sheath as detailed below, then
reposition the fibre in the direction of the plasma.
Remove 2.5mm
of outer sheath
Figure 12 Repairing the fibre end Figure 13 Fibre optic position in torch box
b) Check the fibre optic is secured correctly on the RF interface board.
c) The plasma is below the intensity necessary to be detected. With certain types of samples (particularly
organics) and low plasma power settings the plasma may not be sensed even though it is on. In this case try
increasing the plasma power 0.1 to 0.2kW.
2. RF Power Tube
The RF tube has a finite life and as the RF tube ages, it will require more anode current to deliver the requested
RF power level. Eventually the RF tube will require more anode current than the HVPS can deliver (470mA) and
the HVPS will then go into current limit (LED 1 (Orange) on the HVPS is ON). In this case the RF Interface board
will shut down the RF system, the RF firmware error [15] is written in the error log and the following error will be
displayed on the PC “Over current failure”
Typically the average life of an RF tube in an instrument is around 5500 Filament on hours.
If the ‘Filament On’ hours reported in the DETAILS page of the Diagnostics software is greater than this, the RF
tube should be suspected and replaced.
If the RF Tube is known to be good, then the HVPS checks on page 12 should be carried out.
If the RF Tube and HVPS are known to be good, then the Current Sensor checks on page 17 should be carried out.
3. Current Sensor
The RF current in the induction coil is monitored by a current sense circuit located between the return lead of
the induction coil and ground. The RF current level is then fed back to the Automatic Level Control circuit on
the RF Interface board where it is compared to the required power level as set by the instrument software.
The requested output voltage signal to the HVPS is then adjusted so that the RF current in the induction coil
matches the requested power level in the instrument software.
If the RF Interface board is unable to match the measured RF current in the induction coil to the requested RF
power level in the instrument software, there are several error messages that may be displayed.
“Power unattainable”
This indicates that the requested output voltage signal to the HVPS (TP21) has exceeded 10V.
A failed RF Tube should be suspected.
If the RF Tube is known to be good, then a failed HVPS should be suspected,
“ALC Failure”
This indicates that the delivered output voltage signal from the HVPS (TP19) has exceeded 7kV and the RF
Interface board has been unable to match the measured RF current in the induction coil to the requested RF
power level in the instrument software.
The status of the ALC can be observed on the LED indicator “D14” on the RF interface board.
If this LED is ON, a failed ALC circuit on the RF Interface board or a failed current sensor circuit should be
suspected.
NOTE Power unattainable and ALC Failure are related.
“Over current failure”

This indicates that in order to maintain the requested power level, the current required by the RF tube has
exceeded 470mA an aged or failed RF Tube should be suspected.
If the RF Tube is known to be good, then a failed HVPS should be suspected.
If the RF tube and HVPS are known to be good, then a failed HV Filter Component should be suspected.
Checking the current sensor circuit

Monitoring of the RF current in the induction coil can be over-ridden by placing LK1 on the RF Interface
board into the “Test” position and ignite a plasma.
With LK1 in the test position the plasma will appear a little weaker than
NOTE when LK1 is in the 'Run' position.
CAUTION If LK1 is removed from the RF Interface board while the plasma is ON, the plasma will
run at full RF power (2kW). If the AUX and PLASMA gas flow settings are not
appropriate for this power setting, the torch may melt.
Now you can measure the voltages by setting a power level of 1.2kW,
- The delivered output voltage signal (TP19) should be ~ 5Vdc
- The delivered output current signal (TP20) should be ~ 3.3Vdc
To confirm that the Current sensor board is OK and that the fault is with the ALC circuit on the RF Interface
board, measure the feedback voltage from the current sensor circuit (TP14 on the RF Interface board) while
LK1 is in the test position. The voltage at TP14 should read ~ 4.3 Volts.
4. Grid Circuit
Grid current is monitored on the RF interface board to determine if the RF power Generator is oscillating. If the
grid current fails to flow, the ‘RF Failure’ error message will be displayed on the PC. This fault condition will
inhibit plasma ignition and cause the plasma to shut down if detected during plasma operation.
There are several electronic components inside the RF box that may fail. Below are some checks that can be to
done.
Without a plasma and the RF power set to 2KW

the anode current should be about 55mA, which can be measured as 0.55V at TP20.
the grid current should be at least 55mA which can be measured as -5.5V at TP16.
If your measurements are much different from this, then you have an RF fault.
at 1.2KW
The anode voltage should be ~5kV, which can be measured as 5V at TP19 on the RF interface board.
The grid current should be 300mA, which can be measured as 3v at TP20
The 'Grid bias' voltage should be > 55mA, which can be measured as > -5.5v at TP16.
A low value for the Grid Bias voltage usually indicates that the tube is near the end of its life
It is also possibly cause by:

· Corroded connections or coils.
· Distorted L3 or work coil.
· Anode & Grid coil (L1 and L2) are positioned too far apart.
The grid inductor should be vertical and not leaning away from the anode coil. The bottom of the grid
inductor and the bottom of the Anode coil should be about 20mm apart.
Figure 14 verifying the 20mm gap between L1 and L2
If all the inductors in the RF box visibly look ok, not distorted or burnt, including the induction coil, check the
grid circuit capacitors C2, C3, C4, C5 and C19 for a possible short circuit. Check resistors R1, R3 and R4 for
open circuit along with RFC2. D1 inside the Filter compartment may also be short circuit; this can be verified
by measuring the resistance from TP16 on the RF interface board to ground. IF D1 is good the resistance is
~100 ohms. Ensure the RF is not energised when measuring the resistance of D1.
If C5 (25pF 5KV capacitor connected from the grid inductor to ground) is open
circuit the RF efficiency will be poor. If it is open it will look damaged or cracked
NOTE
or may not be soldered properly.
You should be able to check the capacitors for a short circuit by removing the RF tube and measuring the
resistance between the grid pins on the RF Tube socket and chassis with a multimeter. If all is well, you
should measure about 7.0K ohms. You can also do this by measuring the resistance from L2 to ground,
which should also be 7.0K ohms.
Figure 15 Checking resistance from L2 to ground
This is not a 100% reliable test as the capacitor(s) may break down only when
NOTE voltage is applied.
It is also possible that C19 may have failed, in which case the Generator may partly function since part of the
grid bias resistance R1 (2.2K) will be in circuit. Any of these components failing would show a grid bias failure
error.
5. Anode Circuit
The HV filter capacitors C13, C14 & C15 can fail either externally, leaving a visible track mark across the external
surface of the capacitor(s), or internally, which is unfortunately invisible. Typically, this type of failure will force
the HVPS into current limit, which is indicated by the yellow LED on the HVPS and an “over current” error
message. A noise may also be heard when HV is being applied, this may indicate some discharge across some
components in the RF Generator, typically this is the filter capacitors.
There are two methods to check the High Voltage filter capacitors;
· You can test whether the capacitors are breaking down by testing the HVPS in isolation, Refer to page 15. If
you see no yellow “overcurrent” LED activity with the red wire removed, this is a strong indication (but not
proof) that the capacitors are the root cause, though it may still be the RF tube.
· You can remove both filament wires from the filament transformer, and try and apply some RF power in no
plasma mode. With the filament wires disconnected, there is should be no anode current flowing. If there is
anode current measured (any voltage measured at TP20 on the RF interface board), replace the HV filter
capacitors C13, C14 & C15.
The anode circuit also includes capacitors C6, C7 and C8. If one of these have failed it will give the same symptoms
as the filter capacitors, however experience has shown these capacitors to be very reliable.
A remote possibility is either RFC4 or RFC5 and the insulated feedthroughs in the HV filter compartment
breaking down to chassis, but there may be visible signs of such a failure.
Appendix
RF Interface board details
D6 Plasma on
D7 Water Flow OK D5 Communications Activity
D8 Fan Air Flow OK
D9 Filament Voltage OK
D13 Interlocks OK
D14 ALC Fail
TP17
TP16
TP18
TP19
TP20
Plasma Test Jumper (LK2)
D17 Anode
Adjust RV1
Axial -5.715V
TP5 -15V
Radial -5.302V TP2
Sig Earth
ALC Test Jumper (LK1)
TP3 +15V
TP6 +12V
TP1 +5V
Sig Earth
TP10
TP11
TP15
TP13
TP14
TP21
TP4
TP8
TP9
Figure 16 RF interface details
RF Interface test points
Test Point Function

TP 1 +5 volts power supply monitor point
TP 2 Signal earth
TP 4 Ground
TP 5 -15 volts power supply monitor point
TP 8 Filament control
TP 9 Filament sense
TP 10 Watch dog timer for microprocessor
TP 11 HVPS Enable.
TP 13 Calibration point. Adjust RF interface board RV1 to: -5.302VDC Radial -5.715VDC Axial at 1.8kW
TP 14 ALC Det +
TP 15 Grid Bias failure test point. +5V indicates system in Grid Bias Failure (no oscillation)
TP 16 Grid Current monitor, 1VDC = 10mA
TP 17 RF Oscillator Ground. Use as a ground point for TP 16
TP 18 HVPS Ground. Use as a ground point for TP 19 and 20
TP 19 Anode voltage monitor, 1VDC = 1000V. Note this signal is supplied from the HVPS as a low voltage
TP 20 Anode current monitor, 10VDC = 1A
TP 21 Modulation voltage. Monitors requested Anode voltage from the RF interface board. 10VDC = 7KVDC
Typical RF test point voltages
Table 2 Plasma On test point voltages

Power Level Anode Voltage Anode Current Grid Current Mod Voltage Calibration Point
TP19 TP20 TP 16 TP21 TP13 to TP2(sig gnd)
(kW) 1VDC = 1000V 10VDC = 1A 1VDC=10mA 0 to 10V Adjust at 1.8kW
0.6 3.6 2.5 -3.2 5.2 -3.260 -3.518 A
0.8 4.1 2.7 -3.9 5.8 -3.687 -3.980 A
1.0 4.5 3.0 -4.3 6.4 -4.083 -4.407 A
1.2 4.8 3.3 -4.8 7.0 -4.445 -4.794 A
1.4 5.1 3.6 -5.2 7.4 -4.741 -5.112 A
1.5 5.3 3.7 -5.4 7.7 -4.906 -5.292 A
1.7 5.6 4.0 -5.7 8.2 -5.202 -5.612 A
1.8 5.7 4.1 -5.9 8.3 Adjust RF interface
board RV1 to:
-5.302VDC Radial
-5.715VDC Axial
2.0 6.1 4.3 -6.2 8.8 -5.597 -6.037 A
Table 3 Plasma Off test point voltages

Power Level Anode Voltage Anode Current Grid Current Mod Voltage Calibration Point
TP19 TP20 TP 16 TP21 TP13 to TP2(sig gnd)
(kW) 1VDC = 1000V 10VDC = 1A 1VDC=10mA 0 to 10V Adjust at 1.8kW
0.6 3.0 0.35 -3.7 4.3 -3.261 R` -3.518 A
0.8 3.4 0.40 -4.2 4.9 -3.687 R -3.980 A
1.0 3.8 0.44 -4.7 5.5 -4.083 R -4.407 A
1.2 4.2 0.47 -5.2 6.0 -4.445 R -4.794 A
1.4 4.5 0.50 -5.6 6.5 -4.740 R -5.113 A
1.5 4.6 0.52 -5.7 6.7 -4.906 R -5.291 A
1.7 4.9 0.55 -6.1 7.1 -5.202 R -5.612 A
1.8 5.0 0.57 -6.2 7.3 Adjust RF interface
board RV1 to:
-5.302VDC Radial
-5.715VDC Axial
2.0 5.4 0.60 -6.5 7.7 -5.597 R -6.037 A
The numbers given in the tables above are typical values to be used as a guide
NOTE only. They do not form part of any specification.
The plasma may extinguish at the limits of plasma power (0.6kW and 2.0kW).
This is normal for some systems and does not represent a fault. The method
NOTE
allows up to 1.5kW for a radial and 1.7kW for an Axial system.
CAUTION When setting RF power of 1.5kW and above, be sure to increase the AUX gas flow to
2.25l/min and PLASMA gas flow to 18 l/min, otherwise the torch may melt.
Tables for recording RF voltages

Use these tables for recording voltages when troubleshooting The RF system. They are a useful record to pass onto other
support resources when seeking further assistance.
Plasma off
Power Level Anode Voltage Anode Current Grid current Mod voltage Calibration point
1VDC=1000 10VDC=1amp 1VDC=10mA 0 to 10VDC 5.302VDC Radial
5.715VDC Axial @
1.8kW
TP19 TP20 TP16 TP21 TP13
0.6
0.8
1.0
1.2
1.4
1.5
1.7
1.8
2.0
Plasma on
Power Level Anode Voltage Anode Current Grid current Mod voltage Calibration point
1VDC=1000 10VDC=1amp 1VDC=10mA 0 to 10VDC 5.302VDC Radial
5.715VDC Axial @
1.8kW
TP 18 (Gnd) TP19 TP20 TP16 TP21 TP13 -TP2 (sig gnd)
0.6
0.8
1.0
1.2
1.4
1.5
1.7
1.8
2.0
CAUTION When setting RF power of 1.5kW and above, be sure to increase the AUX gas flow to
2.25l/min and PLASMA gas flow to 18 l/min, otherwise the torch may melt.
Work Coil adjustment
Radial
The radial work coil can be aligned using the Pre optics torch align tool 7210021100. The work should also be
centered vertically about the mounting posts. Also ensure there is approximately 9.4mm between the top and
bottom turns of the work coil and the middle turn is centered.
9.4mm
Figure 17 Using the pre optics align tool to

center the work coil to the torch stand Figure 18 Radial coil spacing
Axial
The axial work coil can be aligned using the axial alignment tool Mk III p/n 9910104400. The kit consists of an
interface alignment disk, coil alignment nut and a coil alignment shaft. The following instructions give details on
using the alignment tool:
Remove cone Fit alignment disk to interface
Figure 19 Remove cone from the interface Figure 20 Fit Interface alignment disk to the
interface. Note: this will only fit in one orientation.
Center within work coil Tighten torch clamp on shaft
Ensure tool shaft and

nut edge are touching
Figure 21 Install the coil alignment nut into Figure 22 Insert coil alignment shaft through work
the work coil and center within the work coil. coil and tighten into the interface disk
Also check the work coil for correct orientation as shown below and that there is 7.5mm between work coil
spacing’s.
Install work coil with sharp

bend at top towards cone
Figure 24 Work coil orientation
7.5mm
Figure 23 Work coil spacing
Checking torch installation

To avoid melting the torch it is important the torch is centered within the work coil. If it is to touch at any point
the torch will overheat at that point and soon melt. There are 2 methods to check the centering of the torch one
is to use an inspection mirror and view the gap around the torch, the other is to insert a piece of card and rotate
this around the torch, it should move smoothly around and not get stuck at any point. A business card cut to the
right size and then curved makes a good tool for this.
If you find the coil is too close at any point remove the torch and bend the coil gently by hand, refit the torch and
check again.
Figure 25 Using an inspection mirror to check torch is centered in the work coil
and not touching at any point.
Figure 26 Using a piece of card to check torch position
HVPS Status LED’s and connections
LED 1 LED 10
Mains connection
LED 10 LED 11 HVPS energize 2PL1
Figure 27 HVPS
LED 1 Orange Status LED's and connections
Overload
LED 1 Orange Overcurrent

If this is ON, it indicates the high voltage output is in current limit. (470mA)
LED 2 Green V_Mode
If this is ON, it indicates that power to the unit is applied and it is not in current limit.
LED 10 Red Overvoltage
If this is ON, it indicates that the high voltage output is disabled as the output voltage has exceeded 8kV.
This fault condition is cleared only when power is removed from the power supply and then reapplied.
LED 11 Red HV disabled
If this is ON, it indicates that the high voltage output is disabled.
HVPS energised LED
Figure 28 HVPS Energised LED
RF System Circuit Diagram
Plasma System Illustrated parts breakdown
Instrument front
2 3 5
4
6
7
9 10 11 12
Item Description Part Number Remark

1 Assy RF Amp 7X5 Series (Radial) 210204890 Complete RF oscillator assembly for a Radial system
1 Assy RF Amp 7X0 Series (Axial) 210204990 Complete RF oscillator assembly for a Axial system
2 Switch, Pressure 9371D0-XS-00003 4810037300
3 Screen Mesh Honeycomb Dia 107mm 4310043400
4 Tube Nalgene 0.12 IDX0.062INTK 3710024600 Supplied per meter (0.32m required for fan switch)
5 Assy Fanblower Series II- Tested 110588690 Includes start capacitor (not available separately)
6 Resistor 0E1 10pct20WWW 3910107500
7 Elbow rubber 1610114300 Cut square end off for round to round tube connection
8 Cushion connector Mackay M6 810099500 Rubber fan assembly mounts. 3 required
9 Switch Pushbutton Illuminated LED 4810038690
10 Switch Rocker DPDT 0I HOR 250V 16(4)A 4810034800
11 Indicator 230V Neon Green 6.3 QC-TABS 3510006700
12 Assy high voltage power supply spare 210173990
Instrument right hand side
1
2
3 4
5
4
7
6
8

1 Gas control board 210159590
2 RF interface board ICP-OES Series II Tested 210149890
3 Relay solid-state 280VAC 18A 4810038900 Top for filament transformer – Bottom for poly heater
4 Switch Supply Mains 110W512-1224V 7910020900
5 Resistor 3K3 5pct0.5W100PPMMF 3910009100 1R2
6 Transformer Filament 5310019800
7 Transformer Power ICP-OES 5310021000
8 MP254 Bridge Rectifier P254 25A 40V 1410106100
Anode compartment
1
4
5
2
8
3 6

1 Assy Choke 110596900 RFC1
2 Hose Clamp 95.2571.44 810127100
3 Vacuum tube 3CX1500D3 5610132700
4 Assy Choke RF Grid 110597000 RFC2
5 Capacitor CR 75pF 5pct 15KV 510040600 C3. C4
6 Insulator Pad 2110016800 Air flow Shield, Requires assembly with paper staples.
7 Contact Clip on twist strip .406MT 1210109800 RF Shield supplied in 0.406M lengths
8 Capacitor CR 200pF 10pct 15KV 510040500 C6. C7, C8
9 Assy Transmission Coil Axial 110857590 For Axial. Includes, L1, L3, C6, C7, C8 Anode Clamp
9 Assy Transmission Coil Radial 110857690 For Radial Includes, L1, L3, C6, C7, C8 Anode Clamp
Grid compartment
5
1

1 Assy RF Socket spare 110690490 Complete grid assy.
2 Socket Valve EIMAC SK-410 4410008300
3 Capacitor CT 25PF5pct5KVNPO 510039300 C2, C5
4 Kit, Grid Resistor Network 9910103400 Consists of R1, R4, C5, C19
5 Assy Choke RF Grid 110597000 RFC2
6 Capacitor MI IN0 500V P0602050394 510036300 Filament filter capacitor
Filter Assembly
1
2 4
3
5 7
6
8

1 CAPC CT 1NO 7K5 HIGH ENERGY CO 510032700 Quantity 3 required C13, C14 and C15. required
2 Choke 1.8UH OHMITE Z-144 5310009700 RFC3, RFC4 and RFC5
3 Insulator Pad PTFE 2110017300
4 Insulator Bush 6ID 2110016700 Use 6910019800 o-ring to hold bush in place
5 CAPC MI IN0 500V P0602050394 510036300 C11, C12 plus filament supply filter capacitors
6 Resistor 100R 1p/0W5/50PPM/MF No part number R2, R3
7 EMI Filter Feed-Thru 10A Murata-Erie 1210079400 Grid bias voltage feed through
8 6631474000 Diode Zener IN4740A 1418016500 D1
9 EMI Filter Feed-Thru 25A Murata-Erie 1210079500 Quantity 4. Used for filament supply
Not shown Ferrite Bead 3.2 OD 1.3 ID 3.0 L FC540 7410004700 Quantity 13. Used on RFC4 and RFC5 leads
Current Sensor - Axial
2 4 5
6 7
9 10 11 12

1 Cnctr Union 1/8 Bsp X 1/4 Tube 1610097700
2 Cnctr MLRUNTSlock 400-3TMT 1610042400 Use to on thread to fit item 1
3 Tubing PFA 0.125 id x 0.060 wall 3710047500 Supplied quantity is per meter
4 Cnctr MLE 14 Tube X 18 BSPT 1610026900
5 Assy current sensor Axial 110698900
6 Kit Coil Resonant 9910111100 Includes coil and support mounting bracket
7 Spare Cooled Cone Interface 110665990 Includes 2 x water fittings
8 Plate PTFE work coil mtg Axial 910190100
9 Mount RF Coil Live Swagelok Plated 810188600
10 Mount RF Coil Grounded Swagelok Plated 810188400
11 Assy loom current sense - 6 pin 110766000
12 Elbow Male Brass 18 BSP 14 Tube 1610027000 Included with current sensor assy
Not Shown Loctite 569 8210028200 Used on water fitting for sealing
Current Sensor - Radial
2 3 4
1 5
8 9

1 Assy current sensor Radial 110700900
2 Mount RF Coil Grounded Swagelok Plated 810188400
3 Mount RF Coil Live Swagelok Plated 810188600
4 Plate PTFE work coil mounting Radial 910100100
5 Cnctr MLE 14 Tube X 18 BSPT 1610026900
6 Assy loom current sense radial 110781000
7 Elbow Male Brass 18 BSP 14 Tube 1610027000 Included with current sensor assy
8 Tubing PFA 0.125 id x 0.060 wall 3710047500 Supplied quantity is per meter
9 Cnctr Union Bhead B-400-61 SLOK 1610098000
Not Shown Loctite 569 50ml 8210028200 Used on water fitting for sealing
Igniter compartment
1 2 3 4 5 6 7
9 10
tem Description Part Number Remark

1 Ignitor Assembly 110649690
2 EMI Filter Feed-Thru 10A Murata-Erie 1210079400
3 Capacitor EL 100U 35V 510012800
4 Diode IN4007 1410001600
5 Resistor 27E5pct5W 3910128600
6 Terminal block 4 Way 10A 5110010300
7 Barb argon igniter 1610133600
8 Igniter Gas 1.5VDC 7910028700
9 Barb Male Nylon 18 BSP 14 Hose 1610079300
10 Nut M16 - nylon 1510261200
Torch Compartment - Axial
1 2 3 4 5 6 7
10
11

1 Assy Torch Clamp Universal 110775200
2 Kit, work coil AX – 710 720 730-ES 9910127900 Includes Swagelok fittings and coil alignment nut
3 Pre-optics cone-Vista/700-ES axial ICPOES 3610007300
4 Finger nut-cone 1510220200
5 Spare Cooled Cone Interface 110665990 Includes 2 x water fittings
6 Insulator Spacer Axial 2110021500 Uses 3 x 1510220900 Screw Insulating for mounting
7 Housing -Pre Optics AX Poly 810137900
8 Strip Contact 406mm 1210109600
9 Gazfit fitting for ICP torch, 6mm, 4/pk 9910107100
10 Transfer tube FEP fm s/chamber axial ICP 7910051590 Suitable for cyclone and Sturman-Masters spray chambers
Tubing s/chamber-torch 1/4 in id 3710033400 Qty per meter. Use for semi and fully demountable torches
11 Silicon tubg,3/16 in.IDx5/16 in.OD/m 2410023800 Quantity per meter
Torch Compartment - Radial
1 2 3
5
6
7

1 Torch bonnet, quartz, radial ICP, 1/p 2010070790
2 Kit, work coil RAD – 715 725 735-ES 9910128000 Includes Swagelok fittings
3 Snout - ICP-OES, Radial 110652690
4 Assy Torch Clamp Universal 110775200
5 Gazfit fitting for ICP torch, 6mm, 4/pk 9910107100
6 Silicon tubg,3/16 in.IDx5/16 in.OD/m 2410023800 Quantity per meter
7 Transfer tube FEP cycl s/c on radial ICP 7910051290 For use with cyclonic spray chamber
7 Transfer tube inert SM s/c on radial ICP 7910051490 For use with Sturman Masters spray chamber
7 Tubing s/chamber-torch 1/4 in id 3710033400 Qty per meter. Use for semi and fully demountable torches
Cables
Description Part Number Remark

Assy loom door interlock 110601400 Includes 2 door switches, wiring and feed-thru’s
Assy loom current sensor 110600800 Includes Plasma looker fibre optic and ALC cable from RF oscillator
feed-thru’s to RF interface board PL6
Cable Fibre Optic 2.5mm OD 5910049500 Ordered per meter, requires 1.83 meters and ends stripped 2.5mm.
Recommended to order 110600800 Assy loom current sensor as it
includes fibre optic of correct length
Assy loom current sense - 6 pin Axial 110766000 For axial. Cable located in current sense compartment
Assy loom current sense radial 110781000 For radial. Cable located in current sense compartment
Assy loom ICP Simul Power PWBS 110644100 From instrument power board to RF interface board PL2
Assy loom ICP Simul Coms PWBS 110644600 Serial Comms cable to Gasbox and 386 Board to RF interface board
PL1
HVPS control 110781200 From HVPS PL1 and PL2 to RF interface board PL4 and PL5. Also
includes connections to interlock switches
Assy loom with peri pump PWB 110796400 Connects to air flow Switch, igniter, peri pump board PL10 and RF
interface board PL3
Assy loom ICP Simul – Filament 110645300 Blue filament supply wires from filament transformer to RF oscillator
Assy loom ICP Simul – Filament Resistors 110645900 Resistor mounted on outside of filter compartment. 2 required.
Assy Loom ICP RF Interlock 110651200 Loom including filter and anode compartment interlock switches
Assy Cable HV 110601300 Red HV wire from HVPS to Filter compartment

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Agilent 700 Series

ICP Optical Emission

Typical RF test point voltages ............................................................................................................................. 23

WARNING RF Radiation – Electric Shock – Hot Surfaces

To prevent death or injury from contact with hazardous components or

Never compromise original safety standards by modifying or altering wiring

Table 1 Plasma Error Messages

Software error Software message Firmware Firmware Refer to page

Actions Replace RF Interface board

RF ROM Checksum Failure

Plasma Has Gone Out

Plasma compartment door is open or emergency RF-off button is depressed

Insufficient Water Flow

RF Power Tube Air Flow Failure

RF Power Tube Voltage Failure

Maximum power timeout failure

Over current failure

2. Air in torch or spray chamber.

3. Incorrect torch gas connections.

Figure 1 Radial Torch positioning Figure 2 Axial Torch positioning

6. Torch condition and cleanliness (including bonnet).

7. Work coil shape and position

10. Check that there is communications with the PC.

B. Plasma lights and then goes out

1. Check the Fiber Optic Looker refer to page 16

Figure 3 Instrument default ignition settings

2. A droplet of liquid enters the torch.

3. An RF component has overheated.

Below are some important points to aware of;

Filament Power Supply

Figure 4 Setting supply

2. The filament voltage and current.

4. The RF Tube Filament

Figure 7 Checking continuity of RF tube filament

High Voltage Power Supply (HVPS) Checks

There are two main areas to check on the HVPS module:

The HVPS module is activated.

Figure 8 Setting HV (Stage 2) on

There are two methods to check if the contactor is ‘energised’.

Figure 9 Checking HVPS contactor energize voltage

If the contactor is not ‘energised’,

If the contactor is ‘energised’,

The HVPS module is delivering the requested voltage and current.

Figure 10 Applying an RF Power of 1.0kW

Select an RF power level of 1.0kW.

Measure the output voltage signals using a voltmeter.

Figure 11 Clip lead from TP1 +5V to the anode of D17

If these voltages are as expected, then the HVPS is faulty.

Testing the HVPS in isolation

1. Fibre Optic Looker

There is an LED on the RF interface board to indicate its status:

b) Check the fibre optic is secured correctly on the RF interface board.

If the RF Tube is known to be good, then a failed HVPS should be suspected,

NOTE Power unattainable and ALC Failure are related.

“Over current failure”

If the RF Tube is known to be good, then a failed HVPS should be suspected.

Checking the current sensor circuit

Without a plasma and the RF power set to 2KW

It is also possibly cause by: