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Zaim 2021 Desgaste Cerámicas
Zaim 2021 Desgaste Cerámicas
Supported by Karadeniz Technical University Coordination Unit of Scientific Research Project No. 2019-8358.
a
Research Assistant, Department of Restorative Dentistry, Faculty of Dentistry, Karadeniz Technical University, Trabzon, Turkey.
b
Assistant Professor, Department of Restorative Dentistry, Faculty of Dentistry, Karadeniz Technical University, Trabzon, Turkey.
c
Professor, Department of Mechanical Engineering, Karadeniz Technical University, Trabzon, Turkey.
Table 2. Two-way analysis of variance for surface roughness, coefficient Table 3. Mean values and standard deviations for surface roughness (Ra)
of friction, maximum depth, and mean maximum depth Antagonist
Type III After Wear Test
CAD-CAM
Sum of Mean
Material Before Wear Test Composite Enamel Porcelain
Parameter Source Squares df Square F P
Brilliant Crios 0.10 ±0.01Aa 0.28 ±0.05Aa 1.19 ±0.28Ab 1.42 ±0.28Ac
Surface CAD-CAM 6.694 3 2.231 48.196 <.001
roughness Lava Ultimate 0.09 ±0.03Aa 0.39 ±0.02ABb 1.13 ±0.41Ac 1.43 ±0.43Ad
Antagonists 34.847 3 11.616 250.884 <.001
Vita Enamic 0.17 ±0.02Aa 0.54 ±0.11Bb 1.09 ±0.25Ac 1.69 ±0.33Bd
CAD- 4.684 9 0.520 11.241 <.001
CAM×Antagonists Vita Suprinity 0.04 ±0.02Aa 0.31 ±0.03Ab 0.37 ±0.08Bb 0.62 ±0.13Cc
Error 6.667 144 0.046 - - CAD-CAM, computer-aided design and computer-aided manufacturing. Different
Total 127.542 160 - - - uppercase superscript letters indicate statistically significant difference between CAD-
CAM materials (P<.05). Different lowercase superscript letters indicate statistically
Coefficient CAD-CAM 2.264 3 0.755 226.287 <.001
significant difference between antagonist type (P<.05).
of friction Antagonists 1.086 2 0.543 162.759 <.001
CAD- 0.249 6 0.041 12.435 <.001
CAM×Antagonists
Error 0.360 108 0.003 - - are shown in Table 2. The 2-way ANOVA showed that
Total 35.993 120 - - - the factors CAD-CAM materials and antagonists signif-
Maximum depth CAD-CAM 10896.870 3 3632.290 34.421 <.001 icantly affected the Ra, CoF, maximum depth, and mean
Antagonists 49497.734 2 24748.867 234.527 <.001
maximum wear depth (P<.001). The mean Ra values and
CAD- 7262.123 6 1210.354 11.470 <.001
CAM×Antagonists standard deviation before and after the wear test for all
Error 11396.900 108 105.527 - - tested materials are shown in Table 3. No significant
Total 269376.506 120 - - - difference was found between the initial Ra values of the
Mean maximum CAD-CAM 8424.385 3 2808.128 27.141 <.001 CAD-CAM materials (P>.05). All CAD-CAM materials
depth Antagonists 38528.194 2 19264.097 186.190 <.001 exhibited the highest Ra values after wear against por-
CAD- 7378.439 6 1229.740 11.886 <.001 celain (P<.05). Vita Enamic generally showed the highest
CAM×Antagonists
Ra values, while Vita Suprinity generally had the lowest
Error 11174.207 108 103.465 - -
Ra values.
Total 218680.879 120 - - -
The 1-way ANOVA showed a significant difference in
CAD-CAM, computer-aided design and computer-aided manufacturing.
the microhardness values between the CAD-CAM ma-
terials (df=3, F=855.466, P<.001). Vita Suprinity displayed
10; Mahr) after the tests. The transverse length was set as
the highest microhardness value (P<.05), while Brilliant
1.5 mm during this scan. Five measurements were per-
Crios showed the lowest value. No significant difference
formed for each specimen. The maximum depth and
was found between Brilliant Crios and Lava Ultimate
mean maximum depth wear values were calculated by
(P=.478). The microhardness, CoF, maximum depth, and
using wear profiles.34
mean maximum depth values and standard deviations
Surface characterization and wear pattern were eval-
for all materials are shown in Table 4.
uated by scanning electron microscopy (SEM) (EVO
All CAD-CAM materials showed the highest CoF
LS10; Zeiss) and a 3D noncontact optical profilometer
value against porcelain and the lowest CoF value against
(mscan; Nanofocus). One specimen from each group was
composite resin (P<.05). Brilliant Crios and Lava Ultimate
selected for SEM surface analysis. The specimens were
exhibited no significant difference in the CoF values
gold sputter-coated (SPI-Module Sputter Coater; Struc-
during wear against composite resin (P=.124) and the
ture Probe Inc), and then their surfaces were examined
enamel (P=.396). Furthermore, no significant difference
by using the secondary electron mode. Additionally, the
was found between Vita Enamic and Vita Suprinity
topography of the wear surfaces and wear tracks was
against the same antagonists (P=.375; P=.060).
evaluated with the 3D noncontact profilometer.
All CAD-CAM materials exhibited the lowest
Statistical analysis was performed with a statistical
maximum depth and mean maximum depth values after
software program (SPSS Statistics for Windows, v17.0;
wear against composite resin. No significant difference
SPSS Inc). The normality of the data was evaluated with
was found between the maximum depth values after the
the Shapiro-Wilk test. Maximum wear depth, mean
wear test against enamel and feldspathic porcelain in
maximum wear depth, CoF, and Ra values were analyzed
Brilliant Crios (P=.721).
by using 2-way ANOVA and Bonferroni correction, and
SEM images of the CAD-CAM materials before and
microhardness values were also analyzed by using 1-way
after the wear test are shown in Figure 1, and the SEM
ANOVA and Tukey post hoc tests (a=.05).
images of the antagonists after the wear test are shown in
Figure 2. From these micrographs, Brilliant Crios, Lava
RESULTS
Ultimate, and Vita Enamic were observed to have minor
From the analysis of variance, the CAD-CAM materials, pitting after wear against composite resin but generally
antagonists, and the interaction between these 2 factors smooth surfaces (Fig. 1B, 1F, 1J). The composite resin
Table 4. Mean values and standard deviations for maximum depth, mean maximum depth, coefficient of friction, and microhardness
Material Antagonists Maximum Depth (mm) Mean Maximum Depth (mm) Coefficient of Friction (CoF) Microhardness (Hv)
Brilliant Crios Composite 9.43 ±1.64Aa 8.13 ±1.73Aa 0.26 ±0.03Aa 76.73 ±4.14*
Ab Ab
Enamel 61.89 ±15.48 59.93 ±16.33 0.42 ±0.06Ab
Porcelain 63.53 ±13.71Ab 52.28 ±11.60Ab 0.45 ±0.04Ab
Lava Ultimate Composite 13.22 ±2.04ABa 11.72 ±2.05Aa 0.22 ±0.01Aa 92.68 ±2.76*
Enamel 42.74 ±12.45Bb 39.77 ±11.32Bb 0.39 ±0.08Ab
Porcelain 71.22 ±20.34ABc 63.37 ±19.98Bc 0.51 ±0.05Bc
Vita Enamic Composite 19.15 ±3.41 Ba
16.64 ±3.49 Aa
0.56 ±0.02Ba 154.36 ±12.88†
Bb Bb Ba
Enamel 47.14 ±9.17 42.53 ±10.79 0.57 ±0.06
Porcelain 78.39 ±11.04Bc 69.79 ±10.57Bc 0.86 ±0.06Cb
Vita Suprinity Composite 11.50 ±2.01ABa 10.56 ±2.24Aa 0.58 ±0.04Ba 558.05 ±47.22§
Enamel 22.10 ±5.19Cb 20.01 ±6.05Cb 0.62 ±0.09Ba
Porcelain 37.53 ±3.69Cc 33.94 ±4.77Cc 0.72 ±0.04Db
CAD-CAM, computer-aided design and computer-aided manufacturing. Different uppercase superscript letters indicate statistically significant difference between different CAD-CAM materials-
same antagonist pair. Different lowercase superscript letters indicate statistically significant difference between same CAD-CAM materials-different antagonist. Different symbols (*, †, §)
indicate a statistically significant difference between microhardness values.
smeared onto the surface of the Vita Suprinity after wear configuration, reciprocation (linear forward and back-
is shown in Figure 1N. Brilliant Crios, Lava Ultimate, and ward) sliding motion was chosen to simulate the motion
Vita Enamic exhibited microcracking, microploughing, and sliding during mastication.3,33 Surface friction and
and delamination after wear against enamel (Fig. 1C, 1G, wear from tooth-to-tooth or tooth-to-restoration contact
1K). Vita Suprinity showed thin grooves in the sliding has generally been considered 2-body friction and
direction after wear against enamel (Fig. 1O). All CAD- wear.1,6 In the clinical situation, debris from materials
CAM materials exhibited parallel scratches and/or and the food bolus can act as a third body in the sys-
grooves in the direction of sliding contact after wear tem,10 contributing to small oscillations in the friction
against porcelain (Fig. 1D, 1H, 1L, 1P). However, thinner coefficient.31
grooves were observed on worn surfaces of the Vita Microstructural parameters can affect the mechanical
Suprinity specimens (Fig. 1P). and tribological properties of materials.12 Consistent with
Antagonist composite resins exhibited a relatively a previous study,35 Brilliant Crios and Lava Ultimate
smooth surface (Fig. 2A, 2D, 2G, 2J). The enamel against exhibited similar Ra and CoF values after wear tests,
Brilliant Crios showed few grooves and had the which may be because of their similar microstructural
smoothest surface among the antagonist enamels features.20 Larger particles embedded into the matrix
(Fig. 2B). In contrast, the enamel against Vita Suprinity along with a porous structure13,21,22 may be the reason
showed cracks, delamination, and concave areas that the Vita Enamic exhibited relatively greater rough-
(Fig. 2K). Grooves were seen in the porcelains against ness and CoF values during the friction and wear tests
Brilliant Crios, Lava Ultimate, and Vita Enamic (Fig. 2C, (Tables 3 and 4).
2F, 2I). Cracks, delamination, and material loss were Consistent with the present study, Vita Suprinity has
observed in the porcelain against Vita Suprinity (Fig. 2L). been reported to show generally lower Ra than the other
The 3D profilometer images of CAD-CAM materials CAD-CAM materials because of its relatively smaller
against various antagonists are shown in Figure 3. The crystal size.24 Its relatively higher CoF value may be
wear pattern and depth distributions in the worn areas related to the addition of zirconia particles, which may
were observed and found to be consistent with the wear influence friction behavior, especially in the running-in
profiles obtained from the surface and SEM analysis. period, as such particles can act as load-carrying parti-
cles inside the matrix of the ceramic.9,36 During the
subsequent sliding or running period, these particles
DISCUSSION
begin to migrate to the interface with an increasing
The 2-body wear behavior of Brilliant Crios, Lava Ulti- friction force.9
mate, Vita Enamic, and Vita Suprinity was evaluated The Ra and CoF values of materials differed according
against different types of antagonists with a pin-on-disk to the antagonist type. The higher values and increased
test for friction and wear tests.1,5-9 The null hypothesis wear depth associated with the porcelain antagonist can
that no difference would be found between the wear be attributed to its greater hardness and porous
behavior of CAD-CAM materials was rejected. structure.11,14,15
Tooth enamel, composite resin, and feldspathic por- This study demonstrated that the maximum wear
celain were used as antagonist alternatives to simulate depth values of Lava Ultimate and Brilliant Crios against
the oral cavity.2,4,8,18 For the pin-on-disk test porcelain were similar to and slightly lower than that of
Figure 1. Scanning electron microscope images of CAD-CAM materials. Original magnification ×2000. A, Brilliant Crios surface before wear. B, Brilliant
Crios against composite resin. C, Brilliant Crios against enamel. D, Brilliant Crios against porcelain. E, Lava Ultimate surface before wear. F, Lava Ultimate
against composite resin. G, Lava Ultimate against enamel. H, Lava Ultimate against porcelain. I, Vita Enamic surface before wear. J, Vita Enamic against
composite resin. K, Vita Enamic against enamel. L, Vita Enamic against porcelain.
Vita Enamic. Santos et al37 studied the wear mechanisms microhardness and filling ratio among the materials. The
of Vita Enamic and reported that Vita Enamic showed a higher loss in nanofill composite resins might be because
high wear rate because of degradation of its organic the nanosized filler particles are too small to provide
binder phase, likely from fatigue. The study by Santos preferential load support and the small particles might be
et al37 was consistent with previous studies that reported swept away by the asperities on the antagonist.38
similar wear depth values for Lava Ultimate and Vita Vita Suprinity had the highest microhardness values
Enamic against enamel.5,28 Brilliant Crios exhibited the among the CAD-CAM materials and exhibited the
greatest maximum depth and mean maximum depth lowest maximum depth and the mean maximum depth
values against enamel, possibly because it had the lowest values after wear against enamel and feldspathic
Figure 1. (Continued). M, Vita Suprinity surface before wear. N, Vita Suprinity against composite resin. O, Vita Suprinity against enamel. P, Vita Suprinity
against porcelain. CAD-CAM, computer-aided design and computer-aided manufacturing.
porcelain. Consistent with the present study, Matzinger loading on the material surface. Because the crystalline
et al,20 evaluating the wear behavior of CAD-CAM blocks structure in Vita Suprinity is very fine, tracks and grooves
against ceramic antagonists, reported that the lowest are also thinner than those of other materials (Fig. 1P).
maximum wear depth was also observed in Vita Consistent with the present study, Silva et al31 reported
Suprinity. The microstructure of Vita Suprinity consists of the highest wear resistance for Vita Suprinity and the
a relatively homogeneous fine crystalline structure that absence of a debris layer on its surface during sliding
increases flexural strength and exhibits improved me- compared with Vita Enamic. In the SEM evaluation, tri-
chanical and tribological properties after bolayers were noticed on the CAD-CAM materials except
crystallization.25,26 for Vita Suprinity, which may be the result of debris
The surfaces of the specimens were analyzed by SEM, adhesion through reciprocating sliding wear movement,
and the wear mechanisms were determined for all ma- which contributes to the removal of material.32
terials. Because the composite resin had a lower hardness In the present study, more surface damage was
than Vita Suprinity, its wear mechanisms were associated observed on the antagonists against Vita Suprinity that
with plastic deformation on its surface and material can be attributed to the high fracture toughness of Vita
transference as smearing layers.32,38 Wear occurs as as- Suprinity.16 Ludovichetti et al36 reported similar results
perities on the surface of the antagonist and material, for the wear behavior of different CAD-CAM materials
causing reciprocal abrasive tracks. The ploughing, against bovine enamel. Consistent with the results of the
grooves, cracks, ridges, and particles observed on the present study, Yin et al40 reported that Vita Enamic
CAD-CAM materials represent abrasive and adhesive caused greater wear damage to the antagonist tooth than
wear.39 In addition, fatigue wear occurred from repeated Lava Ultimate. Lawson et al27 reported that composite
Figure 2. Scanning electron microscope images of antagonists. Original magnification ×500. A, Composite resin antagonist against Brilliant Crios.
B, Enamel antagonist against Brilliant Crios. C, Porcelain antagonist against Brilliant Crios. D, Composite resin antagonist against Lava Ultimate.
E, Enamel antagonist against Lava Ultimate. F, Porcelain antagonist against Lava Ultimate. G, Composite resin antagonist against Vita Enamic. H, Enamel
antagonist against Vita Enamic. I, Porcelain antagonist against Vita Enamic. J, Composite resin antagonist against Vita Suprinity. K, Enamel antagonist
against Vita Suprinity. L, Porcelain antagonist against Vita Suprinity.
resins caused less antagonist enamel wear than infil- lacking. In addition, it was performed under in vitro
trated ceramic and glass ceramics. Additionally, com- conditions, and it remains unclear to what extent clini-
posite resins containing quartz or zirconium silicate fillers cally observed wear may differ. Future studies should
were reported to cause higher enamel wear than micro- include clinical evaluation of the wear properties of these
filled composite resins or those containing barium silicate materials.
fillers.41 Surface deformation can occur in all materials.
Limitations of this study included that quantitative Therefore, intraoral repairability and the ability to
information about the wear depth of the antagonists was repolish the roughened surface are important for
Figure 3. Three-dimensional profilometer images of CAD-CAM materials against antagonists. A, Brilliant Crios against composite resin. B, Brilliant Crios
against enamel. C, Brilliant Crios against porcelain. D, Lava Ultimate against composite resin. E, Lava Ultimate against enamel. F, Lava Ultimate against
porcelain.
Figure 3. (Continued). G, Vita Enamic against composite resin. H, Vita Enamic against enamel. I, Vita Enamic against porcelain. J, Vita Suprinity against
composite resin. K, Vita Suprinity against enamel. L, Vita Suprinity against porcelain. CAD-CAM, computer-aided design and computer-aided
manufacturing.
restoration survival.42 Excessive wear of restorative ma- 11. Heintze SD, Zellweger G, Zappini G. The relationship between physical
parameters and wear of dental composites. Wear 2007;263:1138-46.
terials can lead to functional and esthetic prob- 12. Amer R, Kürklü D, Johnston W. Effect of simulated mastication on the
lems.4,5,17,34 Additionally, there is some concern that surface roughness of three ceramic systems. J Prosthet Dent 2015;114:
260-5.
microsized and nanosized wear particles of restorative 13. Heintze SD, Reichl FX, Hickel R. Wear of dental materials: clinical signifi-
materials can be swallowed or inhaled and then accu- cance and laboratory wear simulation methods -a review. Dent Mater J
2019;38:343-53.
mulate in tissues.13 Further studies are needed to eval- 14. Jung YS, Lee JW, Choi YJ, Ahn JS, Shin SW, Huh JB. A study on the in-vitro
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acteristics of dental ceramic CAD-CAM materials opposing various dental
Based on the findings of this in vitro study, the following composite resins. Materials (Basel) 2019;12:1-16.
18. Shimane T, Endo K, Zheng JH, Yanagi T, Ohno H. Wear of opposing teeth by
conclusions were drawn: posterior composite resins -evaluation of newly developed wear test
methods. Dent Mater J 2010;29:713-20.
1. The microstructural and mechanical properties of 19. Wendler M, Kaizer MR, Belli R, Lohbauer U, Zhang Y. Sliding contact wear
and subsurface damage of CAD-CAM materials against zirconia. Dent Mater
the materials and antagonists are effective in con- 2020;36:387-401.
trolling the wear behavior of CAD-CAM materials. 20. Matzinger M, Hahnel S, Preis V, Rosentritt M. Polishing effects and wear
performance of chairside CAD-CAM materials. Clin Oral Investig 2019;23:
2. Brilliant Crios and Lava Ultimate exhibited similar 725-37.
Ra and CoF values after friction and wear tests. In 21. Awada A, Nathanson D. Mechanical properties of resin-ceramic CAD-CAM
restorative materials. J Prosthet Dent 2015;114:587-93.
addition, Brilliant Crios caused less damage to the 22. Hampe R, Theelke B, Lümkemann N, Eichberger M, Stawarczyk B. Fracture
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42. Ruse ND, Sadoun MJ. Resin-composite blocks for dental CAD-CAM appli- Beyza Zaim: Conceptualization, Methodology, Validation, Investigation,
cations. J Dent Res 2014;93:1232-4. Writing e original draft, Visualization. Tugba Serin Kalay: Conceptualization,
Methodology, Writing e review & editing, Visualization, Project administration,
Corresponding author: Resources. Gencaga Purcek: Software, Methodology, Resources, Data curation,
Dr Tugba Serin Kalay Validation, Writing e review & editing.
Department of Restorative Dentistry
Faculty of Dentistry Copyright © 2021 by the Editorial Council for The Journal of Prosthetic Dentistry.
Karadeniz Technical University https://doi.org/10.1016/j.prosdent.2021.09.024