Doted

nerimna

Aug20018 Quanlitative Analysis

C0peniment
bxperiment s l
y u n 0dum
dn ddonuit wBungt h s
a u o d u d wdh M/.
Cobgnah 0tuton you ho bur o ehuimunt -0thumunt ngth of he gupa
huonidd wth M20
ADdum caubenau Aolh ow aL
hydochloue ocid 0tn
Na. C0, + 2HCI Naa +o,+ H20
Chumcal0u NacL +CD, t H20
Chomieal cauaten- Na,co t 2HOL
n buu tu yoechlosic Aad
aecduu
Unsh m u and he buUiL unth quun HC

Caxcb onal
0 Rndt the 4puptL uith the Qmun ADduum
Alh,
(3)Ppettrout R0 mi 0 Naz COa 1ol a clian ubaen
laAR
(U Acc -3 duoha of muthye 0uanoL Andicoto te th
ibaton ioLk. Ihi aolh un yuloo
5) Not dh iniol uodurg o the buwwtte ondlatost
SNG Corcou Oclduing He daohuuit nto the tibraton lo4k tll
Rucdurys ocabe hod donk the colou chang4om yuulous te lght penk. dhis
Vol
00 50 10-50
the Lnd point.
50 23 00
50 10 50 Nob the ral uoci o dhe buubte
25 30 G)Ruhat th cpuumurd to ObTaun huL ConcOudont
35-50 10-50
uacung
Lalalalhen Caleulatng molauty o Na 2C0 wOP

0Signaure
 enmai
OlCul ot Calculatng molaity oNa 2 C03 Col
fAomtha balonces chmco eaolon Can
MNa,C0 VALastO3 that 1molL ol Naz C03 octh with moty o H
MHU Xx Vu
M Na C0s X VNaz03 0ichiomtuc coy ofNlaCO3
Mx 10 MHL x V HCc 1oichiomsuc oHCL
20X 50

MNa, t0, J0
shi MNa 0 the molary o Na CO 4oln= ?
V2o x 10 50 V Na,c03 t h volum op tgCO 0l = 10.0 m
MHC ubhe molaiy q HC selh M/20
050 VHc uth volume e H Aoln VmL
06 M NazCO> x b
cs110150ME O02 6 25 M 20 x V

Jodsbu V M
400
010
0 D 6 25 X106 Calculatnq alungh o Na 0 olh
27564 o Sonoh molauty nmollculok mau

R h x 106
urg th 9ener ofC20duuum 400
Ocbono 15 6 4/ 3 V 41At
2

Ruult- hu Auno th o gmen Cocum Caxbomlu

u
00

0Sinatur
 Dated DA 18
nd artstt n etima product

Expeniment 3
0 M 4ol o o t auum
tuua
Aunr
Prufartoppior
andanctat AUng M20 Aum:ebae aphnorimatly 0:1M Aoln o botauurn
and
pmanganatuand atondaudui i ALng M/20 sol
Abwnarganau

o Dcau ad

Chemucal taalLO coO H20 Chemucal ouaon-

5.2H,0 K2S04 t
2 MnS0 + 1R
O+3H,SO, + CO0H
2 KMn COOH o
K2S04t 3MnS04 +
KMnON t 3H2SO t 5 /2H20
uIrdicaln.
KMnact a a
0OH 18 H20
ncicnto M
nd Poun:Colowlus tefurk
Sncucato-_ KMnON och as a Alundica toe

nd Pount -Colorle te Aunk (KMnD un buwntu)

bANotor
Lcl O Cach uUahon= 20ml PAgcduww-
Volum o ecau
Molasuty of ocaue acud etn = M/20 Prubaatuer o uaphnorumatuy 0:1 M KMnOy AOluton-
eLanaeuatily vclhon ond cluy watch Qta
SNo riual burutu Fiunal Buuuttu Vglumt Concndont
Votum
Pocur Riaguna KMn0y LoLdu
iustLght_ecactly3:45 go knely hQurduud KMnly en
13 10 Lth useighid untch Qau

19 30 90 12 50 2 50n ( namsr th KMnO cstalA to a 250 ml beaku Ond

about l0D mL o diutilld wat to t
3610 1 12 50
du aale KMnD ky guntly eung wlh a gla 0d

Acad pni u tutube ( 20m) ul o dil H2S04

te i
OSinaue
 enmd es Otsa
x !0

MHu X12. 50
i at thr sdntuon te 60-+0 Ð thot it 4ust unbeamab

Mu vNot the initial vuadng ok thu ouut

2x 10

2 50 viitRuwndeun KMnD_Aot Ldachu inla thitbadon

ok uikh. Conutant shakig t l a ighi hink cotou
O16 M

t 9 n HAI h) : _ix Not hL unal Ladimgs o te bwu.

O:16M
xMakL thaulCAmceidant adungs

Calulatuonn
fo molariy og KMnD
h thamital mat ivolu o 2molu o KMnD» @nd
5 melu cauic aud
MKMnD X VkMnOy N9.mo o KMn0M
Mocalic ocid X Vsali nid NJg-moly g orayc

MKMnOXV- 2
5
V20 X20

MKMD 2 M
5V

malanitomKMnd A M
Obimatt RaAult
 Dated 6 8
erma y
To und cut trpeniment-
melauly a d
dl nqiu o th qwn
KMnOy e by uuaung l
agaunil M/50 ahe
Aum-1e kd put molaiky OndL Atunqth o tha
LQun KMnOy 0lh by taatung t 0ginst M[50
CO0H
2KMnO + 3H2$0 t 5| 2H20 Lhemical auaton,
CDDH
KSD+2 MnSO4 + 18 H20 +10o COOH

KHnO t 3H2Soy t 5,2H0 KSO4 t2Mn304 t18 Ha0

CO0H +J0CO2
KMn O oct uas
Al ncucoato
buwatuoru
nsucato
Molatty ocoluc acid ouon: M/50
Volur o caue acid Aolutom takin t04 ath tihaten _( Uash ith whols ashanatuu thoneuLQhly uuh wat

>20mL (Rn anc 4 tha buutto uh tha QMn KMn

SNo ndal uutu Furnat buuutt Vob ncodont|
PLadun4S RLarung KMn0 UAd NOlun
Rnd th puput uu ealic 0cud Asln and uhtu
Ih3 20.9 9.6
:
Dut 20 mt ofiku dha tubalon nuk
20.9 30 3 q.4 &cld
CYN).
30.4
)Notu e miial eatung 0 the buutt
| at dhenins uto 60-+0c ad un, h
KMnO ACln duohuui unlo haLen {Ra4t l a
OSignature
 erima podudt

Catcul aiuon MKMnDy 04pMa

Amannt funk_dingu
buute
6.043 mot/ t adn thu
Nctu the n a l Uadang
concodont
Lehmint te e t shui
Reprat th
bengh K MnOu CO
Callaiuonn :
0 4 3 A58
Calculaiin
molanuty Mn 01 01h
6 79 q/ ka clua
ua_Chamical iajua ton,t
Ph th balan
KMn O T a t t 5 nmoles o
that 2 meus
O
MOlas 093 mol/u Oraui Qcuc.

btn ath
M KMnOX VKMnO
MoralucX Voxale
oKMnO del"=_
ughu KMn0 ui the molau
Leln _ Vml
VKmn Ou the vouume _L KMnOy mL
More alui the Volumi oß ocalue
th vOlume O cauë M/50
Mocaui
M KMn Oy xV

20

20
Mrm 50
50 25 V

Odignatu
 erma Adut

aleulaturg atungb o KMoDy plutn

Aangth Mplaut x Mocular Has

5 6.71 g
25 V

Rulk Thu atunglh un KMnO wion

Signature
 Dated 2 2 38
Epcrimenl8
2715
Crperiment :8
Lud
4m- you a ud ub a Al o hydatud
ntHz0 6:3 whn au dutlnd
(ODH
huch u cue Osa O/1alii
calue i d nHa0 63g
COOH tha valuw of'n h Ottam CoOH Mlumitukolly tha 0ku n
b a . tumuru
voluni ucay Vo au ponidd uh N1D Kmn0i Aol
uclud uih N/10 KMnD c0(
yo ovu s Chemueal 4quakion
2 KMnD t 3H2904t 5H20,Oy nH20 K2S0 t 2Mn80y
t 10C0s (5n +8H
2KMnOyt 31,50y +51,C, 0, nH,0 K2 304 t 2Mn o
+lDC02 +(5n+8) mdcao KMnD u a AlLncuio tu
H20

Pecedusr
wash dhe akhaahw wth uwat nrl and ul
Punk.
ord Pouni -(olwlus to manurt uaht the bLtiL th, tha gyun KMn0ALuten

olswatu enk ( Runae t hibebt wtth Bealuc acio aslutn amd

Volu o oralc ocud Ol VLkn loarh
iputi ot 20 ml o n it the tuhaton losk
iuato
()Addne tut ubr uu d i HaSD4 N).
- e i i a l bwette Funal 8uutile Voo KMnO, oncondant
RLadirng )Not the nutial uadurigs ol the buet.
1-30 08S0 5 ml
KMnOy
95m
6 Hrat thi conientu ubte 60- 70 C Omol un thu
10 S0 A0 30
5n Aon dhohunii vnte tubalanRasR tu eumannt

20 30 296
6)Not h unal ladung o wuttb
0Signature
 N,V, Na V
dculateu
(oxalut) erima

N, X10Lx95 Calculatin
V205n 10
Noumal caue octd
N 9.5
N2 100 XIO NV NV
N: N
(caleacia) KMnD).
N: 0 095 N Nx

ug Ma& a u t ACUa Ctungh 6:3

0 095 6-3
N x 100
N
Nelnm

.8 0 098
Moleula mau opdlut Acud: 44 Maus x Ba 00
M 63 x2
Calcula hg he ne o_uain moltelu ooyatalliotuer
126 uo

Ng molecul M 90 + 18x Eouivalunt mau o oealuéacel dungth faj

1Snl8610d u Noumal
18n 6 O d 6/3
V/200

6-3 2 128-57
Judn3hbA 0D98
NG mb utulu pwatt ol oLyataluatutn
Molou la mass o otaluc acd =g may bauciky
6 x2 M
V/200

olual mocular mass calc acd

CDO H
nH0 90+18V
C0OH

0Sigmaut
 pemy0 Dated 213 D8
23 Crima oe
txperiment:9
ty puu KaGa.0.
A nd out ocntgepuM Ra0a02
A m eknd out þucntag pity o umhuu lius
Snples35g o ohuth ho bun
diuoluid pu

ncuato N-phenylcuuthuue aid

d rountpunte oal-2d

K H,S0, +CSD4) tH03/ e.ecluu uth wi

2F$0. H.)Soge1,SCo)Fe (0) +2/N),$0 8 6 OAh the usholu Aphanatus hoeughiy KzCiz
the buutts uh nen
KGD 6feS0(NHa 6H0 r 7Ha$D K2 50, +60 iRim Qnd u
ADluTLo
uLuen and
3Fe504 +NH)S 4 1 9311:0 RinaL uthe þihe tr usith Mohns alt
OLon unls tha
Dbit u 20 ml ok Mohu 40 N- Pheny
tihatr Loak ALcdte it 8-10 cop8 o tube ol Hz280,
Tere Euien anth0uie ond nducato Cind
enu bet
+HT66- 2C+7H0 Netzthe inuio ALcung oRLTE
Fe3 colow chong
c Rn clow K2 Ct2 Dp ioluton tulu
0 H+ie 20 7H,0+ 6fe
Not keral uiadung o buuit
h
Colculalens viRurod thu vcbownentto
qut v u emcoudant riadug4
SNG bot foadurg tonal fearung Vot uucd Cprcede
3 &3in Caleulaluens
265 Calulating motasaudy o K20, O daluen
:2 nc 2n MK2CO x VC0
MMeháatt X msahun dalt
2 m

Sigmatun
 Dated
imoo t
MOlaruly c K2beDg 401
MKCuaO1
L0 0 01 M /20 X 20
M x
Mk2n O
6
burgth o K, Gr207 el"
X 2941 2-94 Col tulatun aungth K l Of 4o
0 Ol

Stunoth molaity x ourula mau

Pwuy o

211x
35
100
Caucuulater o_eAuntoge puüy o 9uar ample
3-002

Pw Pucauh.on
d NeMv piptto out H2S0 by uckung
Mplorily Ka OtOq selh OIM
ai any acidd Apla4hus
enHou boclg, wauh tt
and aBbeg eenm Ountmint

6) puio 0 Lo 817

Qiynatn
 orma Dated 2 8 8

29 8 18
p e r i m c n t : 1 0

hperimtnt : 10
omolutuul of won oL
ne m- Odumun oumebucoy thu uumbuu d moluouu
Aun ttvmunt velumaucally
4 Capl
oMohs sat atu ok ustalnouon n a Compu Meh
ul
utatluauen
Poeded My100 K2 Crz0 4el Cclt. Fe 504 NH, SO nH0 Phoidd M/100 K2 D
n H20
Fe SO4NHLS02. Apubbon
Jbwwtu, tpelt, funnel, beoke
Tutn aten tauk,
Abbaratus
A-haatuu ibatorauk, bwut, bipult unnk
Chemica CQuauP
MoLCa OLLA Poudu
3 (D)
K SO+($D,) + 1lH,0 + wash the whol bhaatw with won
KD 1H,SO,
t

S04+[o]felS0),2(NH4) 3o ete_out 10 me e Mhá Saet nto tbahen Lask

- Fe S0u[N,) S04 H0+ Ha
+n
fi
+ (2n+I)H,0 K3 8-10 daohu o_N- PherlyonUhauibo a4 ndicatier
ome one tst ube ol1Dmb) cllud He SO4
Gra 0a + 6FeSO,[NH D nHa0 +7H,SQ, KS04 +Ot0, Noi the unvia mading buule
+3FeSO)6/NH),SOt6n+7) Run dlousr Kz & O4 Col Jaem HCL buulduop.wue
Ha0
eith Cenutant hokury til h coou uchangu grUn

Aot the uÄal wadung o he bwuti

4Ht - 6c- 2o3 + tH20
(vRALat dhi cbtument Qet the concoiclant atadungs

Calulatuonu-
H+6e S23t+ 6fg31+ 7 H20 O t Ael
CoLcubatng molosity K
MKaCtrXVKn0
MMOha &aL X VMehdat

Mxa0a Da x
20 X 20
Signatnun
 Dated ILL
Calculaluend
arvd
ebtN atens
MkaCr04
Fin al feaceng/wol.
uibcorcuclont
Vs
S No l u a l feadung 83 8 3m
8 2 ml
265 Calculturg Albungth o Kala Ot "
183
26-5 3 4.2
8 2 ml 2mu
20 28-2
82ml ungth Mglaribyx MoiuDudas mius
X 294
6T
at e
Molarity ok Moh
-

100x 2
N
MX10
Pescenton purity kaaDa 100
82
6 100
ucautions
Ma 2 x6 O049 2 M d NN pibet out HSCbu auckung
o00 any eid ablasheu on you boy wouh d
thououghly ahd 04bly domu Ontmant
Me ulan mau Mohus Sad Ssh
MM 196 400M.

HOD284+18n
6

Rsul nD of meuculu ol ar k Cupatallisaluon =6

0Sigmatune