Jsa Jis R 1701-4

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JAPANESE

INDUSTRIAL
STANDARD
Translated and Published by
Japanese Standards Association

JIS R 1701-4: 2016

(JFCAI AIST IJSA)


Fine ceramics (advanced ceramics,
advanced technical ceramics)-
Test method for air purification
performance of photocatalytic
materials-Part 4: Removal of
formaldehyde --``,,`,,,`,`,,`,`,```,`,,``-`-`,,`,,`,`,,`---

ICS 81.060.30
Reference number: JIS R 1701-4 : 2016 (E)

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R 1701-4 : 2016

Date of Establishment: 2008-10-20


Date of Revision: 2016-07-20
Date of Public Notice in Official Gazette: 2016-07-20
Investigated by: Japanese Industrial Standards Committee
Standards Board for ISO area
Technical Committee on Metal and Inorganic
Materials

JIS R 1701-4:2016, First English edition published in 2016-12

Translated and published by: Japanese Standards Association


Mita MT Building, 3-13-12, Mita, Minato-ku, Tokyo, 108-0073 JAPAN

In the event of any doubts arising as to the contents,


the original JIS is to be the final authority.

© JSA 2016
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or
utilized in any form or by any means, electronic or mechanical, including photocopying and
microfilm, without permission in writing from the publisher.

Printed in Japan
HT/AT

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R 1701-4 : 2016

Contents

Page

Introduction·········································· ...................................................... ·························1


1 Scope················································· ...................................................... ·····················1
2 Normative references ................................................................................................ 1
3 Terms and definitions ............................................................................................... 2

4 Test equipment ...................................................... ····················································2

5 Test piece···················································································································· 3
6 Test methods·············································································································· 3
6.1 General··············································· ...................................................... ···················3
6.2 Pretreatment of test piece························································································3
6.3 Preparation for measurement······················································· ···························4
--``,,`,,,`,`,,`,`,```,`,,``-`-`,,`,,`,`,,`---

6.4 Pretest ............................................................................................................ ·············4


6.5 Formaldehyde removal test ...................................................... ·······························4
7 Calculation of test results ...................................................... ··································5
8 Test method for test pieces with lower performance ........................................... 6

9 Test report·················································································································· 6
Annex JA (informative) Comparison table between JIS and corresponding
International Standard ...................................................... ···8

(i)

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R 1701-4 : 2016

Foreword
This translation has been made based on the original Japanese Industrial Standard
revised by the Minister of Economy, Trade and Industry through deliberations at the
Japanese Industrial Standards Committee as the result of proposal for revision of
Japanese Industrial Standard submitted by Japan Fine Ceramics Association (JFCA)!
National Institute of Advanced Industrial Science and Technology (AIST)!Japanese
Standards Association (JSA) with the draft being attached, based on the provision of
Article 12 Clause 1 of the Industrial Standardization Law applicable to the case of
revision by the provision of Article 14.
Consequently JIS R 1701-4: 2008 is replaced with this Standard.
This JIS document is protected by the Copyright Law.
Attention is drawn to the possibility that some parts of this Standard may conflict with
patent rights, applications for a patent after opening to the public or utility model rights.
The relevant Minister and the Japanese Industrial Standards Committee are not
responsible for identifying any of such patent rights, applications for a patent after
opening to the public or utility model rights.
JIS R 1701 series consists of the following five parts under the general title "Fine
ceramics (advanced ceramics, advanced technical ceramics)-Test method for air
purification performance of photocatalytic materials":
Part 1: Removal of nitric oxide
Part 2: Removal of acetaldehyde
Part 3: Removal of toluene
Part 4: Removal of formaldehyde
Part 5: Removal of methyl mercaptan

(ii)
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JAPANESE INDUSTRIAL STANDARD JIS R 1701-4 : 2016

Fine ceramics (advanced ceramics,


advanced technical ceramics)-
Test method for air purification
performance of photocatalytic materials-
Part 4: Removal of formaldehyde

Introduction
This Japanese Industrial Standard has been prepared based on the first edition of
ISO 22197-4 published in 2013, by modifying some of the technical contents to ensure
consistency among JIS R 1701-1 to JIS R 1701-5 and JIS R 1751-1 to JIS R 1751-5
which have been established after the publication of ISO 22197-4.
Sidelines and dotted underlines represent the parts modified from the correspond-
ing International Standard. A list of modifications with the explanations is given in
AnnexJA.

1 Scope
This Standard specifies the method to test the removal performance of formaldehyde
(HeHO), among air purification performances, of the photocatalytic materials supported
on the surface of building materials and other products.
This Standard is mainly intended for photocatalysts which are effective in ultravio-
let (UV) region within a wavelength range of 300 nm to 380 nm, under solar radiation.
To the testing of formaldehyde removal performance under visible light, the method
given in JIS R 1751-4 shall be applied instead of the method specified in this Standard.
NOTE: The International Standard corresponding to this Standard and the sym-
bol of degree of correspondence are as follows.
ISO 22197-4: 2013 Fine ceramics (advanced ceramics, advanced technical
ceramics)-Test method for air-purification performance of semiconduct-
ing photocatalytic materials-Part 4: Removal of formaldehyde (MOD)
In addition, symbols which denote the degree of correspondence in the
contents between the relevant International Standard and JIS are IDT
(identical), MOD (modified), and NEQ (not equivalent) according to ISO/
lEe Guide 21-1.

2 Normative references
The following standards contain provisions which, through reference in this text, con-
stitute provisions of this Standard. The most recent editions of the standards (includ-
ing amendments) indicated below shall be applied.

:-!_~~ __~__ ~~~~ ___ !!~~~~'!!:~_~C!~~_?-'!__ ?ftC?~'!':~_~cJf!0)'_0f!_~!1:_C!_f!~0_~~_~~r:_'??_r!Y~_~?]!!l!l!~-,!_cJ~_~!1:__~,!0_C?~~


~~_r:__~'!~__ ~f!~_~_~/!~-'!!_~f!r:__C!~~=~_~t_~~~__ ~_~,!!:p/_~l}:~__'!!:f!~0_?_c!
:-!_~~ __~__ ~~~~ ____(;H?_~~f!:~~_l!(_~f!r:_'!!~__ ~~/_~~~_'!~_t_?_f~_~~__ ~_~~~'!1:_~~_~_

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R 1701-4 : 2016

JIS R 1701-1 Fine ceramics (advanced ceramics, advanced technical ceramics)-


------------------------------------------------------------------------------------------------------------------------------------------------------

'!~_~~__ '!!~~!!_?_~ _f?_r:__C!~'::}? _l1:_r:_ift~l'!!~C! ~_ p~!IC!!'!!_C!~~~__?f p~C!~C!~l'!~_C!~~~_(q__~l'!!~_-_


rials-Part 1: Removal of nitric oxide
JIS R 1709 Fine ceramics (advanced ceramics, advanced technical ceramics)-Light
------------------------------------------------------------------------------------------------------------------------------------------------------
source for test of photocatalytic materials used under ultraviolet
JIS R 1751-4 Fine ceramics (advanced ceramics, advanced technical ceramics)-
------------------------------------------------------------------------------------------------------------------------------------------------------

'!~_~~__ '!!~~!!_?_~_f?_r:__C!~'::I!_l1:_r:_ift~l'!!~C!~_p~!fC!!'!!_C!~~~__ C!fp~C!~C!~l'!~_C!~~~_i_q__~l'!!~_-_


'::~l'!!_~ __~~rJ~!: _
t-'l'f!:c!c!':: _!t~~~t-'!~ _~'!:_vJr:_C!!':_'!!f!'!~=!!_'!~~ _~:·_li~'!!_C!_l!~_~ _C?l fC!,:_'!!'!}-_
de hyde
-------------

~_~~ __~_~_4g_~_____g_~~lj_~ __~f!_~!!_~__ ':_C!_l1:_'!lj_('!~ __C!r~_l1:_~~~':_~_


JIS Z 8806 Humidity-Measurement methods

3 Terms and definitions


For the purpose of this Standard, the terms and definitions given in JIS R 1600 and
JIS R 1701-1 apply.

4 Test equipment

4.1 Construction of equipment The test equipment shall have a construction

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specified in 4.1 of JIS R 1701-1. Since low concentrations of formaldehyde are to be
tested, the equipment shall be constructed with materials of low adsorption so that there
is minimum loss due to adsorption that may influence the measurement.

4.2 Test gas supply The test gas supply shall be in accordance with 4.2 of JIS R
1701-1. The test gas supply provides air polluted with formaldehyde at a predetermined
concentration, temperature and water-vapour concentration by using formaldehyde
mixed standard gas contained in a gas cylinder, and supplies it continuously to the
photoreactor. It consists of a mass-flow controller, a humidifier, gas mixers, etc.
Instead of standard gas in a gas cylinder, formaldehyde gas generated by a suitable
method may be used. In this case, however, it shall have been confirmed beforehand
that the method is capable of supplying a constant concentration of formaldehyde gas
during the test, and that impurities (e.g. methanol) are not contained in the generated
gas in such an amount as may influence the test results.

4.3 Photoreactor The photoreactor shall be in accordance with 4.3 of JIS R 1701-1.

4.4 Light source The light source shall be in accordance with 4.4 of JIS R 1701-1.
The distance between the light source and the photoreactor shall be adjusted so that the
UV irradiance at the test piece surface is 10.0 W/m 2 ± 0.5 W/m2 • A calibrated UV irra-
diance meter specified in JIS R 1709 shall be used for measurement of UV irradiance.

4.5 Pollutant concentration measuring equipment The concentration of pollut-


ant (formaldehyde) shall be determined by DNPH-derivatized solid-phase adsorption/
solvent extraction-high-performance liquid chromatography (DNPH-HPLC method),
using reagents, instruments and apparatus specified in JIS A 1962.

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R 1701-4 : 2016

5 Test piece
The test piece shall be a flat or filter-type photocatalytic material ~~_._9__~~_~}~~__Il?:~
wide and ---------------------------------
99.0 mm ± 1.0 mm long. If there is a play inside the photo reactor, e.g. between
-----------------------------------------------------------------------------------------------

the test piece and the auxiliary plate, the test piece shall be moved toward the upstream
------------------------------------------------------------------------------------------------------------------------------------------------------------
~~~_~? __~_~~_~_~J~~~~~})X_~~~!?:~__?r~_~~~~~~_?_~__~!?_~J~~~_~~_~~q~~?:~~:_ If flat test pieces are to
be tested, the thickness of the test piece shall ideally be less than 5 mm, in order to
minimise the photocatalytic contribution from the side faces and to facilitate the collec-
tion of washings. Thicker materials can be tested, provided that these test conditions
are satisfied. Test pieces with a thickness 5 mm or greater can be tested by a
photoreactor with a sufficient depth, in which case, however, the side faces of the test
piece shall be sealed before testing to avoid possible adsorption thereon. In the case of
filter-type test pieces, the test piece thickness shall be 20 mm or under.
-----------------------------

6 Test methods

6.1 General
The test for formaldehyde removal shall be carried out by following procedures given
in 6.2 to 6.5 and the quantity removed under light irradiation shall be measured. Fig-
ure 1 shows a typical trace of formaldehyde concentration in this process. In the case
where the formaldehyde removal quantity is excessively small and a more certain result
is demanded, the test conditions may be altered as described in clause 8.

S0- 1.2
Irradiation Irradiation
0-
~ / start V stop
.S 1.0
t;
ell
• 0 •
~
S 0.8
0
;j
"0
~ 0.6
~
.S
-.i-J

~ 0.4 0 0
0 0 0
~
<ll
U
~ o Outlet
8 0.2
o • Inlet
::c:
~ 0.0
-60 o 60 120 180 240 300 360
Time (min)

Figure 1 Typical trace of formaldehyde concentration during the test


operation

6.2 Pretreatment of test piece


In order to completely remove the adhering or adsorbing organic matter on the test
piece, the following pretreatment procedures shall be performed. If the test pieces are
not to be tested immediately after the pretreatment, they shall be kept in an airtight
container stored in a dark place.
a) Washing with water Immerse the test piece in purified water for 2 h or more,
remove from the water, and air-dry at room temperature.

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R 1701-4 : 2016

The test piece may be dried by heating within a temperature range, at a maxi-
mum of 120°C, that does not cause physical and chemical changes to the test piece.
In either case, dryness is confirmed when a constant mass is reached. Record any
observations, such as the presence of sediment, and method used for drying.
b) Removal of organic matter Irradiate the test piece with UV lamp for 12 h or
longer but shorter than 24 h. The UV irradiance at the catalyst surface shall be
10 W/m 2 to 20 W/m 2 • The test piece shall be irradiated in zero-calibration gas or in
a clean airtight container. If contamination due to lipophilic property is expected,
the procedure in b) may be performed first, and then followed by the procedure in
a). If washing is expected to have adverse effect on the characteristics of the test
piece, the washing procedure in a) may be omitted.

6.3 Preparation for measurement


The preparation for measurement shall be as follows.
a) Adjust the test gas supply beforehand so that it can stably supply the test gas con-
taining (1.0 ± 0.1) volume fraction ppm of formaldehyde and (1.56 ± 0.16) volume
fraction % of water vapour at 25.0 °C ± 2.5 °C. Set the mass-flow controller so that
the flow rate is 3.00 L/min ------------
± 0.15 L/min (under the standard state of 0 °C, 101.3 kPa)
------------------------------------------------------------------------------
at the inlet of the photoreactor. This water-vapour concentration is equivalent to a
relative humidity of (50 ± 5) % at 25°C. For measurement of humidity, JIS Z 8806
shall apply. Also, measure and record the UV irradiance on the top surface of the
test piece from the light source.
b) Place the test piece in the central position of the gas flow channel in the photo-
reactor and attach the glass window after adjusting the space between the test piece
and the window to 5.0 mm ± 0.5 mm, and place, if necessary, auxiliary plates so that
the difference in level between the test piece and gas channel before and after the
test piece can be within 1 mm. Check that the reactor is completely sealed.

6.4 Pretest
If the concentration of formaldehyde cannot be obtained instantaneously, the time
of the adsorption of formaldehyde reaching saturation in a dark condition cannot be con-
firmed during the test. For this reason, the following pretest shall be carried out. If
the concentration can be determined immediately, there is no need for the pretest.
After pretreatment of the test piece in 6.2 and preparation for the test in 6.3, intro-
duce the test gas into the photoreactor. Measure the formaldehyde concentration under
the dark condition for 90 min at the intervals of 15 min. The time of the dark condition
shall be the time when the concentration exceeds 90 % of the supply concentration for
the first time, and the concentration of the dark condition shall be the concentration at
that time. When the concentration of formaldehyde is still less than 90 % of the supply
concentration after 90 min, then this test method shall not apply.

6.5 Formaldehyde removal test


The formaldehyde removal test shall be carried out as follows.

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R 1701-4 : 2016

a) Place the pretreated test piece according to 6.3 b).


When the test piece used during pretesting is reused, the pretreatment described
in 6.2 shall be carried out again.
b) If the pretest has been done, supply the test gas into the photoreactor until the time
of the dark condition which has been checked beforehand (if the time is less than
30 min, supply for 30 min). If the pretest has not been done, proceed as follows.
Supply the test gas to the photoreactor under the dark condition, and measure the
concentration of formaldehyde. The time of the dark condition shall be the time
when the concentration exceeds 90 % of the supply concentration for the first time,
and the concentration of the dark condition shall be the concentration at that time.
When the concentration of formaldehyde is still less than 90 % of the supply con-
centration after 90 min, then this test method shall not apply.
c) Commence irradiation of the test piece. For the light source that requires warm-
ing up, turn the power on well before the measurement of irradiance. In this case,
use the shutter appropriately to avoid unnecessary irradiation to the photoreactor,
and remove it when commencing irradiation. Record the concentration of formal-
dehyde under photoirradiation for 3 h continuously. When photocatalytic decompo-
sition of formaldehyde occurs, the formaldehyde concentration lowers as shown in
Figure 1 and becomes stable in time. The formaldehyde concentration shall be
measured at more than one point in 1 h. In the last 1 h (for 120 min to 180 min
after photoirradiation), measurement shall be made at more than 3 points. The
concentration of formaldehyde (Cp ) at the reactor exit to be used for calculation of
the removed quantity is the average of the concentration measured (at more than 3
points) during the last 1 h.
d) Stop the gas supply to the reactor and take the test piece out of the reactor.

7 Calculation of test results


If the formaldehyde concentration, Cp , at the reactor exit does not satisfy Equation
(1), the test shall be deemed invalid, in which case calculations given below need not be
performed. The percentage of toluene, R F , removed by photocatalyst is calculated by
Equation (2). The calculated value shall be rounded to one decimal place according to
JIS Z 8401. When this value is either below 5.0 % or more than 95.0 %, the removal
percentage shall be expressed as "below 5.0 %" or "more than 95.0 %", respectively.
Then, the formaldehyde removed quantity, Qp, in the last 1 h shall be calculated accord-
--``,,`,,,`,`,,`,`,```,`,,``-`-`,,`,,`,`,,`---

ing to Equation (3). The calculated value shall be rounded to two decimal places accord-
ing to JIS Z 8401.
The observed concentration of formaldehyde before water vapour correction shall be
used for calculation. For test gas flow rate J, the actually measured value converted to
the standard state of 0 °C and 101.3 kPa shall be used. When the removal percentage,
RF , is either below 5.0 % or more than 95.0 %, the removal percentage is calculated by
assigning 5.0 or 95.0 for R p , respectively, and expressed by attaching "below" or "more
than" to the obtained value.
For the test piece of removal percentage, R F , of below 5.0 %, the test conditions may
be altered in accordance with clause 8.

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R 1701-4 : 2016

C F ::; CF,d -CF,o xO.05 ............................................................. (1)

RF =
c -c
F,O F xl 00 ................................................................ (2)
CF,o

C Fo xf x 60
QF = RF X 100x 22.4 ............................................................. (3)

where, CF : concentration of formaldehyde at the reactor exit


(vol ume fraction ppm)
CF,d: concentration of formaldehyde under dark condition
(vol ume fraction ppm)
CF,o: supply concentration of formaldehyde (volume frac-
tion ppm)
RF : percentage of formaldehyde removed by the test
piece (%)
QF: quantity of formaldehyde removed by the test piece
during the last 1 h (!-tmollh)
f: test gas flow rate (L/min) converted to standard
------------------------------------------

_~g_ ~_ ~ ~ _~}~~~)_
~~_~_~~ _\9__ ~9 ~ _

8 Test method for test pieces with lower performance


In the case where the removal percentage, R F , is below 5.0 % in the measurement of
a flat test piece and a more certain result is demanded, the number of test pieces and
the flow rate of test gas may be altered at the same time, as shown in Table 1. In this
case, gas flow channel of 100 mm or more shall be provided before the test piece.
When the test conditions are altered, the reported value of the removed quantity of
formaldehyde shall be half the value obtained from Equation (3). In addition, it is re-
quired to confirm the time of adsorption (dark condition) under the altered test condi-
tions.

Table 1 Alternative test conditions

Alterable test condition Val ue after change


Test gas flow rate 1.500 L/min ----------_.
± 0.075 L/min
Number of test pieces Two

9 Test report
The test report shall include the following information.
a) General matters
1) Number of this Standard
2) Test date

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R 1701-4 : 2016

b) Testing establishment
1) Name and address of the testing establishment
2) N arne of the person in charge of the testing
c) Information on the test piece
1) Type, serial number, etc.
2) Material, shape and size
3) Process of selecting the test piece (e.g. sampling method)
4) Date of arrival of material at the testing establishment, date and time of removal
of material from the packaging, and date and time of preparation of test piece
d) Test results
1) Quantity of formaldehyde removed by the test piece during the last 1 h
2) Removal percentage of formaldehyde (optional)
e) Test conditions
1) Method of supplying formaldehyde
2) Supply concentration of formaldehyde, test gas flow rate, water-vapour concen-
tration, temperature
3) Whether the test method in clause 8 (alteration of test gas flow rate and number
--------------------------------------------------------------------------------------------------------------------------------------------------------

~~ _~~~~_ J!~~~~~) _~_~_~ __~~~_1! _~J?)!~~_~~_


4) Photoirradiation conditions (type of light source, UV irradiance)
5) Pretreatment conditions (conditions for washing with water and drying, UV irra-
--------------------------------------------------------------------------------------------------------------------------------------------------------
diance and irradiation time)
f) Testing equipment
1) Type and specification
2) Type of formaldehyde concentration analyzer, gas sampling method, irradiance
meter, UV irradiance meter, etc. used.
g) Any other matters of special importance
Matters to be noted concerning the conditions of test and test pieces after test
--``,,`,,,`,`,,`,`,```,`,,``-`-`,,`,,`,`,,`---

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Annex J A (informa ti ve) :;:000
I--'-
Comparison table between JIS and corresponding International Standard -:]
o
I--'-
~
JIS R 1701-4: 2016 Fine ceramics (advanced ceramics, advanced technical ceramics)- ISO 22197-4: 2013 Fine ceramics (advanced ceramics, advanced l'V
Test method for air purification performance of photocatalytic materials-Part 4: technical ceramics)-Test method for air-purification performance o
I--'-
Removal of formaldehyde of semiconducting photocatalytic materials-Part 4: Removal of m
formaldehyde

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(1) Requirements in JIS (II) Inter- (III) Requirements in Interna- (IV) Classification and details of (V) Justification for the
national tional Standard technical deviation between JIS and technical deviation and
Standard the International Standard by clause future measures
number
No. and title Content No. of Content Classifi- Detail of technical
"'0
~ of clause clause cation by deviation
o~ clause
M
(1 1 Scope 1 Identical
~
M 2 Normative
U
references
t:d
~
3 Terms and 3 Identical
(1
definitions
o
~ - - 4 A list of symbols used Deletion Delete the list of sym- Change of the definition of
~ for calculation. Gas boIs. flow rate j will be sug-
S flow ratejis given on gested at the time of revi-
::r: Delete the provision of
~ dry-gas basis. dry-gas basis for flow sion of ISO. See 6.3 for
ratej(see 6.3). justification.

- - 5 Descri ption of the pur- Deletion Delete the description The description need not
pose and principle of of test purpose and be provided in the main
the test principle. text of the standard.
4.2 Test gas Test gas supply in ac- 6.2 The gas flow rate con- Alteration Delete the provision of Modification regarding
supply cordance with JIS R verted to standard state dry-gas basis (see 6.3). this matter will be sug-
1701-1. (0 °C, 101.3 kPa, and gested at the time of revi-
dry-gas basis). sion of ISO (see 6.3).

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(D Requirements in JIS (II) Inter- (III) Requirements in Interna- (IV) Classification and details of (V) Justification for the
national tional Standard technical deviation between JIS and technical deviation and
Standard the International Standard by clause future measures
number
No. and title Content No. of Content Classifi- Detail of technical
of clause clause cation by deviation
clause
4.3 Photo- Photoreactor in accor- 6.3 Approximately identical Addition No technical deviation Addition to facilitate
reactor dance with JIS R 1701- with JIS R 1701-1, because an equivalent users' understanding.
1. except that it does not cross-sectional view is Suggestion for including
specify turbulence- given in ISO. this addition in ISO
inducing construction or 22197-1 (which will then
provision of at least be cited in ISO 22197-4)
"'d 100 mm gas flow chan- will be made.
~ nel before the test piece.
o
~
t:rj 5 Test piece Tolerance on test piece 7 Tolerance on test piece Alteration Widen the tolerance ISO dimensional tolerance
o
~ dimension ± 1.0 mm dimension ± 0.5 mm range for test piece is stricter in comparison to
t:rj
t::J dimensions. tolerances on other test
condi tions. Modification
OJ
~ regarding this matter will
o be suggested at the time of
o revision of ISO.
~ 6.2 Pretreat- Washing with water 8.2 Removal of organic mat- Selection Add description regard- Modification to ensure
~
Q ment of test and drying, followed by ter by UV irradiation at ing washing. Specify a consistency with JIS R
::r: piece removal of organic mat- strong irradiance of broader irradiance and 1751-1 to -5 and increase
~
ter by UV irradiation at 15 W/m 2 or higher for at time ranges. flexibility of the test pro-
strong irradiance of least 16 h (up to 24 h). cedures.
10 W/m 2 to 20 W/m 2 for Modifications regarding
12 h or longer but these matters will be sug-
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shorter than 24 h. The gested at the time of revi-


order of the procedures sion of ISO.
may be reversed, and
washing procedure may ~
be omitted. I--'-
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o
I--'-
~
~
o
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:;:tjf-L
(1) Requirements in JIS (II) Inter- (III) Requirements in Interna- (IV) Classification and details of (V) Justification for the o
f-L
national tional Standard technical deviation between JIS and technical deviation and -:]
o
Standard the International Standard by clause future measures f-L

number ~
No. and title Content No. of Content Classifi- Detail of technical
l'V
of clause clause cation by deviation o
f-L
clause m
6.3 Prepara- The mass-flow control- 8.3 The mass-flow control- Alteration Add tolerance of Add tolerance of 5 %,
tion for mea- ler is set so that the ler is set so that the ± 0.15 L/min to the flow which is considered neces-
surement flow rate is 3.00 L/min flow rate is 3.0 L/min rate specification. Both sary. This results in the
±0.15 L/min (under the (under the standard JIS and ISO proce- difference of 1.6 % in
standard state of 0 °C, state of 0 °C, 101.3 kPa dures use flow rate water-vapour concentra-
101.3 kPa) and dry-gas basis) converted to standard tion, but since its influ-
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"'0 state, but JIS proce- ence is minor compared to


~ other influences, dry-gas
o~ dure uses flow rate that
considers moisture basis is deleted in JIS for
M
(1 (wet-gas basis), while the purpose of simplicity.
~
M ISO uses one that does This addition will be sug-
U not (dry-gas basis). gested at the time of revi-
t:d sion of ISO.
~
(1
6.4 Pretest Measurement of the 8.4 Measurement of the Deletion Delete the procedure for Deletion will be suggested
o formaldehyde concen- formaldehyde concen- the case where adsorp- at the time of revision of
~ tration under the dark tration under the dark tion reaches saturation ISO.
~ condition for 90 min at condition for 90 min at within 30 min. This
S the intervals of 15 min. the intervals of 15 min. procedure is intended
::r: When the concentration for cases where judge-
~
becomes the same as ment cannot be made,
the supply gas concen- and deletion of it does
tration within 30 min, not lead to any techni-
then that time may be cal deviation from ISO.
the time of the dark
condition.

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(D Requirements in JIS (II) Inter- (III) Requirements in Interna- (IV) Classification and details of (V) Justification for the
national tional Standard technical deviation between JIS and technical deviation and
Standard the International Standard by clause future measures
number
No. and title Content No. of Content Classifi- Detail of technical
of clause clause cation by deviation
clause
7 Calcula- If the formaldehyde 9 Flow rate j: the value Alteration Add Equation (1) for Equation (1) is added so
tion of test concentration does not normalized for 0 °C, judgement of the test that adsorption action is
results satisfy Equation (1), the 101.3 kPa and dry gas validity. Delete the not evaluated as photo-
test shall be deemed basis, and then multi- provision of dry-gas catalytic action. This ad-
invalid. Flow rate j: plied by a factor of basis (see 6.3) in flow dition will be suggested at
actually measured 1.016 for water-vapour rate calculation. the time of revision of
"'d value converted to the correction. ISO.
~ standard state of 0 °C
o
~ and 101.3 kPa.
t:rj
o 8 Test Flow rate after change: 10 Flow rate after change: Addition Add tolerance. Add tolerance of 5 %,
~
t:rj
t::J method for 1.500 L/min 1.5 L/min which is considered neces-
test pieces ± 0.075 L/min sary. Addition of this
OJ
~ with lower specification will be sug-
o performance gested to ISO.
o 9 Test report I terns not included in 11 Items not included in Alteration Add the test piece pre- Addition is made to reflect
~ the ISO list: the name the JIS list: signatory treatment conditions. the increased significance
~
Q of the person respon- and a unique identifica- of the pretreatment condi-
::r: sible for the test and tion of each page. tions in the tests specified
~
test piece pretreatment in JIS R 1701-1 to -5 and
conditions. also to establish consis-
tency with other parts of
the JIS R 1701 series.
This addition will be sug-
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gested at the time of revi-


sion of ISO.
~
I--'-
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I--'-
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:;:tjf-L
Overall degree of correspondence between JIS and International Standard (ISO 22197-4: 2013): MOD f-L •
~
-:]
NOTE 1 Symbols in sub-columns of classification by clause in the above table indicate as follows: o
f-L
Identical: Identical in technical contents. ~
Deletion: Deletes the specification item(s) or content(s) of International Standard. ~
o
Addition: Adds the specification item(s) or content(s) which are not included in International Standard. f-L
m
Alteration: Alters the specification content(s) which are included in International Standard.
Selection: Provides an alternative choice by adding the specification contents of equal status, which may be used in place of that given in
the original International Standard.
NOTE 2 Symbol in column of overall degree of correspondence between JIS and International Standard in the above table indicates as follows:
- MOD: Modifies International Standard.
"'0
~
o
~
M
(1
~
M
U
t:d
~
(1
o
~
~
S
::r:
~
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Copyright Japanese Standards Association


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No reproduction or networking permitted without license from IHS Not for Resale, 02/02/2017 11:01:35 MST
--``,,`,,,`,`,,`,`,```,`,,``-`-`,,`,,`,`,,`---

Errata for JIS (English edition) are printed in Standardization and Quality Conti'oJ, published
monthly by the Japanese Standards Association, and also provided to subscribers of JIS
(English edition) in Monthly InfOl'mation.

Errata will be provided upon request, please contact:


Publishing Group, Japanese Standards Association
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TEL. 03-4231-8550 FAX. 03-4231-8665

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