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  • Analytical Techniques: Analytical Techniques Light Source Detectors Reference Standard Type of Sample Graph

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    SAURABH PRAJAPATI
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    This document discusses various analytical techniques used in chemistry. It provides details on the light sources, detectors, reference standards, and types of samples used for techniques like UV spectroscopy, IR spectroscopy, NMR, mass spectrometry, and others. It also describes sample windows or cells used for different spectroscopic techniques and basic principles of electroanalytical methods like conductometry, potentiometry, and amperometry. Finally, it lists various derivatizing agents used to analyze different compound classes by thin layer chromatography.

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    This document discusses various analytical techniques used in chemistry. It provides details on the light sources, detectors, reference standards, and types of samples used for techniques like UV spectroscopy, IR spectroscopy, NMR, mass spectrometry, and others. It also describes sample windows or cells used for different spectroscopic techniques and basic principles of electroanalytical methods like conductometry, potentiometry, and amperometry. Finally, it lists various derivatizing agents used to analyze different compound classes by thin layer chromatography.

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    12 views4 pages

    Analytical Techniques: Analytical Techniques Light Source Detectors Reference Standard Type of Sample Graph

    Uploaded by

    SAURABH PRAJAPATI
    This document discusses various analytical techniques used in chemistry. It provides details on the light sources, detectors, reference standards, and types of samples used for techniques like UV spectroscopy, IR spectroscopy, NMR, mass spectrometry, and others. It also describes sample windows or cells used for different spectroscopic techniques and basic principles of electroanalytical methods like conductometry, potentiometry, and amperometry. Finally, it lists various derivatizing agents used to analyze different compound classes by thin layer chromatography.

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    of 4

    ANALYTICAL TECHNIQUES

    Analytical Light source Detectors Reference Type Graph


    techniques standard of
    sample
    Ultraviolet Xenon arc Barrier layer cell Potassium Liquids Absorbance
    spectroscopy Hydrogen (photovoltaic cell) chromate Vs
    (UV) Tungsten Photomultiplier concentratio
    filament tube (PMT) n
    Deuterium Photocell
    Mercury arc
    Infrared Incandescent Thermal detector Polystyrene Solid %
    Spectroscopy lamp (Thermocouple film liquid Transmittanc
    (IR) Nernst Bolometer gases e
    glower Thermistor Golay Vs
    Globar source cell) Wave
    Mercury arc Photon Number
    Tungsten (semiconductor
    filament Pyroelectric FT-IR
    Nuclear Radio Tetramethy Solvent Radio
    Magnetic Frequency FT-NMR lSilane frequency
    resonance generator (for organic absorption
    (NMR) solution ) Vs
    Silapentane Field
    (for Strength
    aqueous
    solution )

    Page 1 of 4
    Mass Ionization of Quadrapole Perfluoroke Abundance
    spectrometry electrons Mass Analyser rosene Vs m/e ratio
    (MS) Time of flight (TOF)
    Electron spin Klystron Silicon DPPH(1,1di Liquids Intensity
    resonance Oscillator crystal phenylpicry (Signal) Vs
    (ESR) lhydrazyl) Magnetic
    field (Field
    Strength)
    Flame Burners Photomultiplier Sodium Liquid Relative
    Photometry (Mecker Tube (PMT) Potassium Emission
    Total Lithium Intensity
    consumption Magnesium Vs
    Lundergraph Wave
    Burner ) Number
    Atomic Hollow Photomultiplier Sodium Solid
    Absorption Cathode Lamp Tube (PMT) Potassium Liquid _
    Spectroscopy Electrodeless Calcium Gas
    (AAS) Discharge Magnesium
    lamp
    Nephelometr White light, Photomultiplier Suspens
    y/ Mono Tube (PMT) _ ions Absorbance
    Turbidometr chromatic (Most Vs
    y Radiation Sensitiv Volume
    Tungsten e for
    lamp dilute
    suspens
    ions
    100mg/
    l

    Page 2 of 4
    Spectroscopy Sample Window or Sample cell
    UV Quartz or Fused Silica
    Visible Glass or plastic
    IR Metal halide salts e.g.Nacl,kBr,CsBr
    (for non aqueous samples)
    LiF,CaF2 (For aqueous samples)
    NMR Cylindrical glass tube

    Electro-analytical Basic principle


    methods
    Conductometry Conductance Vs Volume of Titrant Added
    Potentiometry Potential Vs Volume of Titrant Added
    (No Current flow i.e I=0)
    Amperometry Current Vs Volume of Titrant Added
    (V=constant)
    Polarography Current Vs Applied Potential

    Derivatization in TLC
    Compound Class Derivatizing Agent
    General Iodine vapor,
    Sulphuric acid (50%)
    Acids Bromo cresol green
    Aldehydes and Ketones 2,4-dinitro phenyl hydrazine
    Amines and Amino acids Ninhydrin
    Alkaloids Mercuric Nitrate

    Page 3 of 4
    Barbiturates Diphenylcarbazone
    Lipids Bromo thymol blue
    Steroids Antimony trichloride
    Carbohydrate Aniline Phthalate

    Prepared by- SAGAR CHAUDHARI


    PRADIP WAGH
    (Pharmanotes Admins)

    Page 4 of 4

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