5. -Mortarconstituents 5.4.3. .Standardsand th the particle size distribution and moisture oe id determined as in 5. 1.2. During production these determinations shall be ca atleast once. clay. These requirements 5.4.4 General are insufficient to ensure that the Standard: sand is equivalent to the Reference sand. Standard sands, which are produced in various countries, shall b used to determine the stength of cementin accordance with this standard. Standard sand, shal conform tothe requirements state in 5.1.3. The conformity shal be attested by the national standardization organization within whose area of jurisdiction the Standard sand, was produced Standard sand may be delivered in seperate fractions or premixed in plastics bags with a content of (1350 + 8) g: the type of material used for the bags The national standardization organization shall ensure that the Standard shall have no effect onthe vesults ofthe strength testing, sand, during its subsequent production is continuously monitored in ~ = sera a nag ET In view of the diffcuties of spectying Standard sand com unambiguously itis necessary during cerifcaton and aly contol teeang than 24 n between sampling hall be stored n completely filed and airtight containers made ‘ostandardize thesand against clause 5.1.2 from a material which does not react with cement. valence shall be maintained by a certification testing programme ing comparison of t dard sand with the Reference sand. This programme and the associated calculation are described in 11.6. 5.1.2 Reference sand 5.3. Water The Reference sand shall be a natural, sliceous sand consisting preferably Distilled water shall be used for reference testing. Forothertests, of rounded particles and has asilica content of at leaf 98%, drinking water may be used. 's defined in table 3. 6. Preparation of mortar Its particle size distribution shall he wi 61 Composition of the mortar Table 3. Particle size distribution of the ‘The proportions by mass shall be one part of the cement (5.2), three parts of Roference sand Standard sand (5:1), and one half part of water (5.3) (waterloement ratio 0,50). ‘Square mesh size ‘Gumutative sieve residue Each batch for three test specimens shall consist of (456 + 2) g of cement, (mm) % (1350 #5)g ofsand and (225: 1)g of water, 2.00 3 6.2 Batching of mortar 4,60 7 4 5 1,00 330+ 5 The cement, sand, water and apparatus shall be at the laboratory aca ao temperature (4.1). Carry out weighing by means ofa balanee accurate 0,16 By + 5 #19 0.08 os 4 NOTE. —_fwaterisadded from automatic 225 mi pipettes they have Tobe accurateto+ 1 mi 8 7be made for centring the auxiliary plates with respecttto the axis of the loading system with an accuracy of +05 mm, Where there is no spherical seating in the testing machine or where the spherical seating is blocked, or where the diameter of the spherical seating is, NOTE. The testing machine may be provided with to or more loadranges. The highest value ofthe lower range shouldbe approximately 150f the highest value ofthe next higherrange, tis considered advisable forthe machine tobe ‘equipment or recording the results. NOTES. The spherical seating ofthe machine may be lubricated to faciltate ‘agjustmenton. the platen cannot take place under load during the test. Lubricants which are effective under high pressure are not suitable. NOTES. The terms Vertical, tower and upper referto conventional testing machines. Howe yen, machines whase axis not vertical are ‘also permited provided that they satisty an acceptance testing Procedure analogous to that in 11.7 and thatthe other ‘requirementsof 4 8 are fultilled, 4.9 Jigforcompressivestrength testing machine When 4.8 requires the use ofa jig (see Figure 6) it shall be placed between the platens of the machine to transmit the load of the machine to the ‘compression surfaces of the mortar specimen. ‘A lower plate shall be used in ths jig and it can be incorporated Platen, The upper platen receives the load from the upper ‘machine through an intermediate spherical seating. 16 ‘Spread the layer uniformly using the larger spreader (see Figure 3). held vertic its shoulders in co forwards and backwards once compact the first mortar layer using 60 jolts. Introduce the secon: mortar. level with the smaller spreader (see figure 3) and compact the layer with a further 60 jolts Lift the mould gently from the jolting table and remove the hopper. Imme a transverse sawing and moved slowly, wi th the surface of the each direction, Si ightedge held almos specimens using the same st Label ormark the moulds to identify the specimen and their position relative to ‘8 Conditioning of test specimens 8.1 Handling and storage before demoulding Wipe off the mortar lft on the perimeter of he mould as a result ofthe striking- off Place a 210 mm x 185 mm plate glass sheet of mm thickness on the mould Aplate of stee! or other impermeable material of similar size may be used. NOTE. In the interest of safety, ensure that glass plates used have ground edges. ied, without delay on a horizontal (see 4.1). The moist air shall have 1e mould, Moulds sk Place each covered mould, base in the moi access to 'S appropriate lime for demoulding. 8.2 Demoulding of specimens Carry out demoulding with due precautions, Carry out clemoulding, for 24 h tests, not more than 20 mm before the specimens are tested. Carry out demoulding, for tests at ages greater than 24 h, between 20 h and 24 h after ‘moulding, NOTE. — Demoulding maybe dby 24h ifthe mortarhas notacquired sufficient that 24 h to be handled without risk ‘ofdamage. Mention delayed demoulding in the test report 2Figure 4. Typical jolting apparatus 1 Lug '2. Cam 3. Stop 4. Cam follower Dimensions in millimetres NOTE. Moulds and jotting tables from different manufacturers ‘may have unrelated external dimensions and masses, so their compatibility needs to be ensured by the purchaser. 9. Testing the specimens 9.1 Testing procedures Use the centre - point loading method to determine the flexural strength by ‘means of the equipment specified in 4.7 When the flexural strength value ‘The compressive strength tests shi the prism broken by harmful stresses. required. this test may be omitted ne carried out on the two halves of }donot subject the prism halves to 9.2 Flexural strength the supports. Apply. to the opposite side face of ly at the rate of (50+ 10) N/s until fracture. ly by means the prism and increase it smo« Kees ism halves damp until tested in compression. Calculate the flexural strength Rf in Nimm2 from: 1 SKFF XL REE be Where: Rf isthe flexural strength, in Newtons per square milimetre ‘b? isthe side ofthe square section of the prism, in mil tres; Ff isthe load applied to the middle ofthe prism at fracture, in Newtons: 1 isthedistance between the supports. 8.3 Compressive strength Test the prism halves in compression on the side faces by means of the ‘equipment specified in4.8 and'4.9 Centre the mm, an platens or auxi ism halves laterally to the platens of the machine within + 0,5, nally such 1@ and face of the prism overhangs the ry plates by about 10 mm. Increase the load smoothly at the rate of (2400200) Nis over the entire load application unti fracture, 24.8 Jolting apparatus The jolting apparatus (a typical design is shown in figure 4) shall Comply with the following requirements, The apparatus consists essentially of a rectangular table rigidly connected by two light arms toa pivot at 800 mm from the centre ofthe table, The table shallincorporate atthe centre ofits lower face a projecting lug with a rounded face. Beneath the projecting lug shall be a small stop with a plane upper surface. In the rest position, the common normal through the point of contact ‘ofthe lug and the stop shall be vertical When the projecting lug rests on the stop, the top face of the table shall be horizontal so that the level of any of the fo a ETHESTTEVETDY More Man’ T Omni, The table shall have dimensions equal toorgreater than those of the mould baseplate, anda plane machined upper surface. Clamps shall be provided for firm attachment of the mould to the table, The combined mass of the table, including arms, empty mould, hopper and clamps shall be (20,00,5)kg, The arms connecting the table assembly to the pivot shall be rigid and Constructed of round tubing with an outside diameter lying in the range 17 mm.to 22 mm selected from tube sizes given in ISO 4200. The total mass of the twoarms, including any cross bracing, shall be (2,25 +025) kg. The pivot, bearings shall be of the ball or roller type and protected from ingress of grit or dust, The horizontal displacement of the centre of the table as caused by the Play of the pivot shalinot exceed 1,0mm, The lug and the stop shall be made of through-hardened steel of at least HV 500 Vickers hardness value (see ISO 409-1), The curvature of the hug shall be about 0.01 mm. {n operation, the table is raised by a cam and allowed to fall freely from a height of (150 + 0,3) mm before the lug strikes the stop, 2 ‘The precision of the method is measured by its repeatability (see 11.5) andits reproducibility (see 10.6). The precision of the test method for conformity testing is measured b its reproduci The precision of the test methed for acceptance testing and for production control purposes is measured by itsrepeatabil 10.6 Reproducibility The reproducibility of the method of compressive strength determination is a quantitative expression of the error asso n corey eet ST - 5 "working mm different laboratories, at different times, using standard sands of different origin and different sets ofequipment. For the 28-day compressive strength the reproducibility under these conditions between well-experienced laboratories, expressed as the Coefficient of variation, may be expectedto be less than 6%. This implies that the difference between two corresponding test results obtained in different laboratories may be expected (probability 95 %) to be less than about 15 %. 11. Acceptance testing of sand and of alternative equipment 11.1 General As indicated in clause 3, the testing of a cement in accordance with this, standard cannot be based on the use of a single, universally available, test sand: consequently itis necessary that several test sands, to be identified as Standard sands, are available. Similarly, but for a different reason, the standard does not require the test laboratory to use one specific type of compaction equipment. The term alternative materials and equipment has therefore been introduced. Clearly this freedom of choice, linked with the inevitable requirements of a European Standard, has to lead to certain limitations in respect of the alternatives. Consequently, one of the principal features of this standard is that the alternatives have to be subjected to a testing programme to ensure that the strength results obtained in conformity testing are not significantly influenced. by the use of alternatives in place of the specified Reference materials or ‘equipment. 25In assembling the cleaned mould ready for use, a suitable sealing mat shall be used to coat the outer joints of the mould. f moul shall be applied to the internal faces of the mould. itting metal hopper with vertical led. When viewed in plan, the the mould by not more than 1 The outer walls of the hopper shall be provided with a means of location to ensure correct positioning over the mould. For spreading and striking off the mortar two spreaders and a metal straightedge of the type shown in figure 3 shall be provided. YI Striking off direction with sawing motion 10 The certification testing shall be based on compressive strength testing at the age of 28 clays and shall be undertaken by testing laboratories ‘approved for this purpose by the appropriate body, ‘The approved testing laboratories shall collaborate internationally and take Part in co-operative testing schemess) to ensur the properties of Standard sands from producers in different countries are comparable with regard to the international acceptance criteria. 11.6.2 Verification testing of sand icate, comprises an annual test of a rand: Hesing Oy aM Tony the sand producers records of his quailty control tests. ‘The programme for verification testing is based on the same principles as those for certification testing and is described in 11.6.4 ‘The sand producer's quality control tests shall be carried out regularly by the Producers laboratory or by a service laboratory (monthly in the case of continuous production). The records of the resul for at least three years shall be avail inspection as part of the verification procedure 11.6.3 Method of certification testing of Standard sand 11.6.3.1 General During the Production period of at least three months three independent samples of the sand, for which certification as a Standard sand has been requested, shall be taken for certification testing by the certification agency, Acomparative test with the Reference sand shall be carried out with each of these three samples using a different one of three cements selected for this Purpose by the certification agency,4.5Moulds 11.636 Requirementfor acceptance ‘The mould shall consist of three horizontal compartments so that three prismatic specimens 40 mm x 40 mm in cross section and 160 mm in length canbe prepared simultaneously. A typical design is shown in Figure 1. 11.6.4 Method of verification testing of Standard sand 11.6.4.1 Annualtest by the certification agency 220 — A single random sample of the sand shall be taken by the certifi | {mia agency in accordance with, 11.6.2 and shall be tested in accordance: Ee oneral procedure described in 116° using one cement selected fr ths a oo =purpese by he cer eater age ey procedure de: 11.6.4.2 Monthly test by the sand producer ‘Amonthiy test shalll be carried out by the sand producer, in the same way as the verification test described in 1164.1, but making at least ten comparisons, by comparing a random sample of the sand produced di wi ‘wi 4 i cerification t 1163 11.7 Acceptance testing of alternative compaction equipment atleast 10 mm thick. The surface oe a salle aa mal side face shall be at least HV 200 (see ISO W171 General 11.7.2 Testing of alternative equipment NOTE 1. A minimum Vickers hardness value of HV 400/s recommended, indard is based on an acceptance criterion such that equipment making use of a method of compaction, which in the long run wot day compressive strength differing by about 5 from that obt method descabed in tis standard has a probably of at least 95% rejected.4.3 Testsieves Wire cloth test sieves conforming to the requirements of ISO 2591-1 and ISO 33 10-1 shallbe of the sizes from ISO 565 given in table | When each of these three tests leads to acceptance of the altemative equipment, the proposed compaction equipment is considered as an acceptable alternative. (series R20) 11.7.2.3_ Evaluation of each comparative test Table 1. Ap ieves erture oftests| Caleulate the following parameters: a) _ themean compressive strength (y) overall 20 batches prepared with tM diliD the standard equipment, 2,00 b) _ themean compressive strenath (x) overall20 batches prepared with 1.60 The proposed alternative compaction equipment. 20: 9.50 Evaluate D= 100(x- 0.16 Y tothe nearest0, 1, ignoring sign 0.08, 11.7.2.4 Treatmentofoutliers See11.6.3.5. 4.4Mixer ‘The mixer shall consist essentially of: a) _astainless steel. bow! with a capacity of about Slitres and of the general shape and size shown in figure 1, and provided with means by ‘which itcan be fixed securely to the mixer frame during mixing and by which the height of the bowl in relation to the blade and, to some extent, the gap between blade and bow! can be finely adjusted and fixed: b) __astainless steel blade of the general shape, size and tolerances shown in figure 1, revolving aboutits own axis as tis driven ina planetary movement around the axis ofthe bow by an electric motor at controlled speeds. The two directions of rotation shall be opposite and the ratio between the two speeds shall not be a whole number. Where more than one mixer is used, blades and bowis shall form sets which are always used together. ‘The gap between blade and bow! shown in figure 1 shall be checked every month. The gap of (3 + 1) mm refers to the situation when the blade in the empty bow! is brought as close as possible to the wall, Simpie tolerance gauges (feeler gauges) are useful where direct measurements difficult 6 11.7.2.5 Requirement for acceptance of the proposed alternative equipment ‘The alternative equipment shall be considered acceptable when each of the three values of D, calculated in accordance with 11.7.2.3, is less than 50. In such a case the technical description of the equipment shall be deemed to be an annex to 4.6, and the description of the compaction procedure shal be deemedto be an annex to 7.2 Where one or more of the calculated values of D is equal to, or greater than, 5,0the alternative equipmentis not acceptable. auvarious sources and countries may be used provided thet they have been shown to give cement strength results which do not differ significantly from those obtained using the standard sand (see clause 11) ‘The mortar is prepared by mechanical mixing and is compacted in a mould using a standard jolting apparatus. Alternative compaction equipment and techniques may be used provided that they have been shown to give cement ‘strength results which do not differ significantly from those obtained using the standard jolting apparatus (see clause 11), The specimens in the mould are stored in a moist atmosphere for 24 h and then the demoulded specimens are stored under water until strength testing, ‘Atthe required age, the specimens are taken from their wet storage, broken inflexure into two halves and each half tested for: 'S0 1302: 1992 Technical drawings - Method of indicating surface texture Laboratory and equipment 4.1 Laboratory The laboratory where preparation of specimens takes place shall be maintained at a temperature of (20 + 2) °C and a relative humidity of not less than 50% The moist air room or the large cabinet for storage of the specimens in the ‘mould shall be continuously maintained ata temperature of(20 + 1) °C anda relative humidity of notless than 90% The temperature of the waterin the storage containers shall be maintained at (2041) 8c. vibration is (55.5 + 0 95) Hz and the operating vertical acceleration is (4.5 + 0.25)g when measured on the base of the mould at the centre of the middle ‘compartment, The maximum acceleration in any horizontal direction is 0.5.g NA.3 Compaction procedure with the vibrating table Set the vibrating table top horizonal arid clean it, Prepare and assemble the mould in accordance with 4.5, Ensure that the lower surface of the mould base plate’is flat and clean. Cl&mp the mould and filing hopper firmly to the vibrating table and set the acceleration of the vibrating table to be (4.5 +.0.25) gims. Mould the specimens immediately after the preparation of the mortar Switch the vibrator on and fill the compartments of the mould with mortar immediately, completing tne operation within at most 45 sas follows Fill the compartments of the mould using a suitable scoop within 15 s up to about half the depth. Without switching the vibrator off, and after a pause of 15 s, add the second layer within the next 15 s, in the same sequence. The mould should be just slightly overtiled, After a total period of (120 + 1) s ‘Switch off the vibrator either manually or automatically ‘Then follow the procedures in paragraphs 2 and 3 of 7.2 NA.4 Acceptance inspection testing of cement For the purpose of testing cement for acceptance inspection at delivery. in accordance with clause 1.1 of the 1991 edition of each of the following, B 5 12, BS 146, ES 4027, BS 4246, ES 6588 and BS 6610, and clause 12 of BS. 7583 1992, unless otherwise agreed between the purchaser and the manufacturer, use the compaction procedure in use by the cement manufacturer at tne time when the cement was originally tested during operation of the manufacturers autocontrol scheme, 33FOREWORD 7 This Nigerian Industrial Standard was prepared by the Technical Committee on Gement for use in determining the compressive strength of cement using conerete prisms. ‘The method prescribes in this standard specifies the use of mortar prism of, 40 mm square cross section area cast from a 1:3 mortar and broken in flexure after 28 days curing. The two halves are then tested for compressive strength. ‘This Standard also specifies the reference procedure for the preparation and testing of mortar prisms made with Standard sands from various sources and compacted by a standard jolting apparatus but permits the use of alternati compaction equipment and procedures in well defined cases, national annexes NA_NB_and NC give the requitements for purposes for Standard “Sand, Tor the alternative compaction procemure are tor th rorroFt hen mass requirements for the jolting table, respectively ‘The contribution of local manufacturer, professionals and consumers in the formulation of the test method are hereby gratefully acknowledged National annex ND (informative) Recommendation for carrying out the test procedure In the UK NC. 4 Laboratory (see 4.1) ‘The high humidity required in moist air curing rooms is normally produced by ‘spraying water as @ fine aerosol. The bacterium Legionella pneumophila is widespread in nature and is present in the water systems of many buildings Scale in pipework and chemical nutrients in the waiter supply may encourage growth of this organism which multiplies between 25 °C and about 45°C. Tan TE SSS SS is therefore advisable to maintain cold water supplies below 20°C where possible and to store hot water above 60 °C. Cold water supplies may be disinfected by chlorination to at least S mgil free chlorine, Regular periodic checking for the presence of Legionella species in industrial water supplies isa sensible precaution NB.2 Mixing of mortar (see 6.3) ‘When cement is mixed with water, alkali is released. Take precautions to avoid dry cement entering the eyes, mouth and nose when mixing mortar. Prevent skin contact with wet cement or mortar by wearing suitable protective clothing, If cement or mortar enters the eye, immediately wash it out thoroughly with clean water and seek medical treatment without delay. Wash wet mortar off the skin immediately. 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