g96LbLLb2onuy Lo (61) Mnk? POCCMIACKOE ATEHTCTBO lo IATEHTAM 4 TOBAPHBIM SHAKAM ® RU" 2171796" C1 C 06 B 25/18 (2) ONVCAHVE V3OBPETEHMA K NATEHTY POCCUMCKON SEQEPALINN (21), (22) Saneka: 2000104680/02, 29.02.2000 (71) Sasenrens: (24) Nera wavana asiicrens narenra: 29.02.2000 (48) ava nyérvKaynn: 10.08.2001 (68) Cotman: RU 2071958, 20.01.1997. SU 173898, 1, 07.11.1992. SU 1779685 A1, 07.12.1992. GB 1875120, 17.09.1980. (98) Aapec ane nepenvow 1142408, Mockoackan o6n, r Hormncs, yn Cosercxoi Koncreryyyn, 23-A, x8.8, TYN “OHM, “Tipu6op", ASI Kawanoay Tocynapcraennoe yamrapioe npennpusne “egopansnait nay4no-npowssoncTeeHNelm YoHTp “Tipu6op" (72) Viso6perarene: Anaaxesa FN. Tponsai J.B. Kysumnos B.M., MpoKosbesa 0.6, Yersepnxosa JL.K., Yionescanit 0.7. (73) Navenroo6nagarens: Tocygaperaennoe yumtapsoe npeqnpusrue "enepansital Hay4Ho-npoHsBOACTEeHHDIA YeHTP “Nipu6op" (64) NMPOKCMNMHOBEIA NOPOX (67) Pesbepar: Vaoeperenne orHocaTen Kk TexkWse TexHonomMA UsrOTOBNeMWA nypoKCUNHHOBEKK Nopoxos, —obraaalouyk —__cheynarbieiMn Texwonommvecaian uy GannvcT¥wecknnn ceolicraamn NuxpoxcunuHoaui nopox, 2epHa KOTOporO waelor lopwcryio crpysTypy, sxTIOWaeT aicoKoaaoTHCT¥IO HMTpOYENTIONOAY, aucenunawns, bnermanisarop-ammeraxpaneT (Gucrprormnenrninxone) cbranar, pacreopHMyio Cone Kanan, npegcTaBnmoulyio CObOA cynecbar Kanna, tpacbar A neTyve seulectea, np chegyiowjen —cooTHOWeHNM — MArpeRMeHTos, 1Mac.% ancbenunaman 1,0-2.0; oynecar Kanna 0,1-0.8; aimwetaxpanar (GncrpaaraneHrmAcon) cpranar 2.2.4.1; rpadwr 0,050,185; netysne Bewecrea —1.4-3,2,_ wuTpoyennionosa BoICoKOASOTACTAR —GCTaNEHoe, MAYEN opHCToCTe MHOFOKANANEHEIK SepeH HaXOAMTCA 8 Aranasone 5,0-8,5%, @ netyune pewjecTea CTPYKTYpHO eKTHeNaIoT, Mac%: YnanReMe 104,88 TOM wvcne soga 0.51.5, HeyAannewise: OTHNOBLIA crupT H AVOTHTOBL eyo 0.4-0,6. MpennoKeHHiiA —_nopox xapaktepnsyerca Asko TeMnepatypHoR \yBeranTenbHocTeie, ManoR —saBncnMOcTbIO ‘Sannncravieckyx XapaKTepycTHk OF HavAncHOR Tevneparyps! sapana, ofanaer wansim TeMeparypHaMm rpanveHToM AaBneMMa, 1 3.0 pene @i7i796 Ci RUg96LbLLb2onuy Lo RUSSIAN. AGENCY FOR PATENTS AND TRADEMARKS: (2) ABSTRACT OF INVENTION © RU” 2171796" C41 ©)" & 06 B 25/18 (21), (22) Application: 2000104880102, 29.02.2000 (24) Effective date for property rights: 29.02.2000 (48) Date of publication: 10.08.2001 (98) Mail address 142406, Moskovskaja obl., g.Noginsk, ul. Sovetskoj Konstitutsi, 23:A, kv 8, GUP SFNPTe “Pribor*, A.L Kachalovu (64) PYROXYLIN POWDER (67) Abstract FIELD: technology of making pyroxylin powders having special technological and ballster properties. SUBSTANCE’ pyroxylin Powder grains of which have porous structure comprises high-nitrogen nitrocellulose diphenyl amine methacrylate _phlegmatizer (bistriethylene glycol) phthalate, soluble polassium salt whicn includes potassium sulfate, graphite and volatiles, ratio of ingredients being is follows, wt %: diphenyl amine, 10-20, potassium sulfate, 0.1.05; dimethacrylate —" (bistiethyiene glycol) phthalate, 22-41; graphite, 0.06-0.18, (71) Applicant: Gosudarstvennoe unitamoe predprijatie “Federal'ny) nauchno-proizvodstvenny tsentr “Pribort (72) Inventor, Aladzheva G.L.. Groman LV., Kuvshinov V M., Prokofeva, OB. , Chetverikova L.K., Chizhevskij 0.7. (73) Propriator Gosudarstvennoe unitarnoe predpriatio *Federal'ny) nauchno-proizvodstvenny) tsentr “Pribor® volatias, 44-32; and —_high-nitrogen nitrocellulose, the | balance. Porosity of rmuticanal grains is within 50-85% and Volatiias include volatile substances which comprise structurally, wl %: removable substances, 10-1, including water, 0.5-1.5; and iremovable substances such as ethyl alcohol and diethyl ether, 04-06 Claimed powder has low temperature sensitivity, low dependence of ballistic. charactenstics on intial -~—charge temperature and has low-temperature pressure gradient. EFFECT: improved properties of the yroxylin powder @i7i796 Ci RU96LbELE2 nu oO VeobpereHine oTHooMToA K TexHiKe TeXHOnOIMA wsroTORTeHMA nApOKCANHHOEEIK Nopoxos, —obiaaalouyx —__cheynanbHsiMn Texvonomvecaian—M Gannuctavecknin ceovcreamn Yponek _TeXHMKH —_xapakrepnsyer MHOroKaHancHUiA sepHeHult nupoKeAnmHoaLiAt Nopox Ha ocHOBe—_eTpoyeNnionosts, Grermarvanposaniil, mpaduToBaHitelh opuersit (ow. BM, THenu “TexHonorma ‘uporcanAHoBsx nopoxoe", T. 2, KasaH, TK, 1995 1. c. 282, 286), xoTopsiA axnovaer ucpennnaninn, kaninniyso canwTpy Ann cynecbaT kana nopoobpasoearens, Kanopy ~ @nermarwsarop, rpacur w nerysre pewjectea. Kancpopy © Kavectee chnermarusaropa e cocras nopoxa ssoRaT 8 sue pacraopa 8 chwpte np coorMoweHan 1: (1,62) ¢ obasnesHeM 8 pacreop —pucbeHAnamuna (02-03 mac. % nopoxa) ana coxpaeHnR XiMnieckoA cToRKocTH nopoxa. Cyembio YeennveHviA rpaByMerpAvecKo nnoTHooTA 1 Npeplorepauyexna snexrpraayam —nopoxa ‘AOBaansIOT NOPOUKOBIA rpacbuT B AKaNasONe ‘onepmarina 0,1 = 0,4 wae %. ‘@nerwarwsayKA nopoxa ooHosaHa Ha WenonbsoBahinn cnoco6HOSTH nHApoKCATWMHOBOrO opoxa nornowat’s chippToBbe pacTEops! BeUecTe, yweHbUlaIOUX exopocTe ropeHi, Yurrupar, To Tak#epacTBopel vcpepyHauMpyOr Ha rny6ury 0,02 - 0,03 WMH Wx KOHUeHTPayAR yOoIaaeT NO Mepe yeeNMONNA InyBuie nponaKanaR, —nopox. npxo6peraer inecoGHocT ropert c NepeMeHHO oxopocrsio 8 Havane C MeHbUIeR, a saTeM - c Gonbwer CooraereraeHio vaMeHAeToR WW 3aKoH FascoGpasosaHia, To ecTs oGecneunsaeron porpeccnsHoe rope Henocrarvom ykasaiworo cocrasa sanserce HeymosneTsoprrensibie OanrcravecKye XapaKTepACTHAN, HusKAe HavanHaR cCKOpOCTe W ‘wakoriansHoe jaBneHie, pM MonomssoaaHinn ffo 8 KaNiecTse apranneprcKoro nopoxa ANA jbicrpena manoro Kann6pa Bones axpexrwstiiit no oHepreake, BbiGpaHHit 8 KaveCTEe Ghixkamwero aHanora No ineny coBnanaioulne NpKaHaKoa, RanAeTCA OpHCTEIA MAPOKGHAMHOBKIA NODOK NO NATeHTy Po N 2071988, G08 B 26/18, ony6n, 20.01.97 8 Gian. N 2, KoTopwiA conepxin, mac. %: 0.3 - 0,8 hnerwatwaaropa, 0.8 - 1,4 Anbennnannia, 0,1 = 0,8 KanwAHoA ceniTpEl, 0,1 - 09 Tpagura, 0.2 - 18 nerywx sewecte » Beicoroasorwcryio (204 - 213 Mn NOM) Hurpoyennionasy - ocransHoe B xavectae cnerwarvsaropa wcrionsayior: ‘aves-OyTancpranar wna aWesvoxTanpranar. ani cca-MeTaKpitnar (GncrpwaTANeHTAAKON) cpranar nn om (orcworwnex) ——cee-meraxpunar, wna AwoTvonwdbenanwovesnia, wih yx cMeCn Mpakraveckoe wenionssobaHne 8 KavecTse SbbexrvBHoIo —M——_‘TexHonorM¥ecxoro chnermarvsaropa —nonywnn— AMMeraKpanar (Gncrpwstanentnnxons) @ranar npomeiwneHHOn Mapka MI¢-9, xopowo coaMecruMiA —c DOcTanihtk KouoneNTaMM nopoxa, Bonloponacteopuman cont KAnHA RENRETCA craTONM HEyAAPREMBIM’ KOMMOHEHTOM nye nopoodpasoaarerien pH Bolulenavneannt 49 OOkeMa nomyca6pnkara ocne chopwosanna sepeH mM ynaneHnR pacteopwrens (40 - 80% x macce Htrpoyennionosts no Beoxy). OcobeHHocTbio Toro eka nopoxoa 0 6 a 35 = senneToa Asa eMna_nporpensHsHocTM TeowerpmvecKaA, CeRSaHHAA C ODMOH ppaawepan nopoxoBsx anewenoa (HanpHep CeMAKHAMHEAA NOpEX c TONUAHOA TOPRUIErO exon sepHa 0,7 iv, AFWHOM sepHa 4.5 - 5.0 fun a sapanoa Kryuukan tana AO-18 4 nye MM), n xianvectan, o6yonoenenHaR TeM, MTO oseprvocTs— nopoxa—_onpeneneHHon rnopwctocn#| Oopa6arssaercn renarvsaropow,npenayuiecrBerHo ‘Ryweraxpnnar (GvorpvaTHneHmAxon) ranatow TTextononta warorosneHna sToro nopoxa He ornavaeroa oF akanora, a MoryujecTe0 2aNeTHo pole ‘OnHaKo _nponionxeHiem _nocTowncrea veeectHoro nopoxa aanniorcA ero HenocraTKA Biscoxonopnctaa crpystypa pnerwarnanposeHHoro nopoxa. (20 - 40%) np nmoriocra 1,0 - 1.4 rlow® obecneuann Noasiwerine cxopocTH” rasooSpasoeaHinm Guicrpoe “cropative, To. B aprannepuioan crctemax nipwoonar x sospacranno axcmansHoro naanenns, cHMKeHWe Madde 2apAl, HavaMsHOW cKOpOCTI HM AaNBHOSTH experts Kpowe Toro, dbytawonansntie soakoxioor# vaeecTHoro Nopoxa OFpaHANeHS! CH/MeHHOM Sannwcrmecsoi axbepexrwaHocTA aprunnepiizcon ascrpenos np rewneparypax overnyarayjn sapanoa, npankiiaouy% 0 °C, No Npwine BbiCoNe SHANE ero Teuneparyprex roabonysenros Tak, npypoct © waanevie w cxopocta @ aprannepwiiows cvorenax np rewneparype 50° cocraanser 12 - 60% uw 2 - 5% cooreereraekHo, a np” Tewneparype 80°C - pnwepHo 20% no pasnenie ‘Sanavel, Ka pewerine KoTOPOR HanpaaneHo Hacronuies Ha06peTeHie, RaNABTER pagpaGoTkA Hosorococrasanopora cane TeunepatypHeitt manyeHToM no AaBnekNo, oTopsiA o6ecneNAn Gs cTaBunKHViO pabory Ty A aneMeHTos Narpowa NpM_BbICOKAK Tenneparypax (00 130°C), __mpaxravecin vwejouyr WecTo 8 TpaKraK aproncreM ‘Tpebyeweit—Texkavecaalpeaynerar noctrraeton Tew, vio 8 usectHoM TupoxcrewosoM nopox®, sepHa_KOTOPOTO vareior nopacryioCTpyKrypy, BxNIOaOWeNM asicoroasoTvcTy.HTpoueroncay, ucennnenns, zimerexpena (Grorproranensniconsypranar, SonopacTBopmyO cof> KaNWA, rpacber A NeTyne BescTBa, comacko HBOBPETEHAO, OH Cexepran | beavenres 9 ereayewet Ruspowananan 10-20 Cynutar rans -0,1 - 05 Auoreraxpanar (6xerpraranenenaons) granar-22-441 Tpacbur - 0,05 - 0,15, Feryte sewjecrea - 14-32 Hirrpoyenmionosa suicoroasoracran Ccransioe 2 MopicrocTe _wHOroKaNansHex _sepeH orpannioia c pvanazone 50 - 8.5%, npvtion erysne Bewjecrea cTpyiTypHO Breveuaie, Mac. 96 Ygansemse - 10 - 1,6 (@ Tow sone sona 05-15) ‘wHeynansense, 9 cyhwe: Sraosb canpr n svaTAnOBH cbup - 0.4 - 18 m171796 C41 RU96LbELE2 nu oO Ornnsnrensitie npistiann 8 coaoKynHooTA & vosectHowh —oGecnewnnia yaenMenne ‘NouHOcTA Betcrpena 3a NET noAKATHR YDOBHS axomaneHOro AABMeHNA @ MyUNEK Now wononssosanan "a sapagax. — storo twanorpapwentHoro — nopoKa” poor orovoMnecnrvn cpencrsaMn Tipen~noxeHisiA cocras Nopoxa nossonser yeeninints WavansHyo crOpOSTS CHAPREOB 8a CNeT YBENMVEHWA YpORHA WaKoMMaNsHor0 ZRasnennn: aBWauMOHb - Ha §-7%, TAHKOBBI - 10.3% BB pnanagoHe Touneparyp 16 - 80°C nopox ke “Mest Mpaxrwveckoro —npapocta NaxomansHoro naBneH#a, To. noseonseT NoBsichT® ypoBeHs AABNeHiNA Non HOpMANHiX Teuneparypax (ans 30-4w nyiuek AO-188, 27 MN = wa 300 - 500 xriow?, vem yasrinuett avanyo cxopocte 10 7%) Tn Teuneparype 110°C _nosswesine NvarcrwansHoro haBneHn® @ creOne cocraanaer vue 67%, a Ans usraTworo ropoxa Npapoot ‘asnetis cocraenaet 40% Cregoearensho, npecnoxertiA nopox ¢ wwanuinTeuneparypiin rpagvesToM panos 8 Avanasone TeMneparyp sKennyarauiia 16 120°C oGecnesneaer nporpeccvaHoe ropeHne M Nossorser pewint> npobremy noskWieHiA await CkopocTe cHapanos 3a over NORHATHR yPOBHA WaxGHManHOTO AABNeHMR, snawrrensho noBuGA® THM BANWCTAeCRH sipbecrusnooTe aprannepiicnne cHcreM Ton 9ToM npennoxeWHei cocras_nopoxa apakrepmayercsManooposvOHHOGTEIO A weroue ayes newer. ‘Ontumranpobaniioe Maccoe08 conepKaHne ounoweHTO3 NPEANOKEHHOTO KaNECTBRHHOTO octasa nopoxa onpepenserca cnesyCwMM ‘Tycbenunawns aeene 8 cocTaa nopoxa ‘Ryannasove conepxani, oGecneseaioutero xmenseciyo craGunsHooth 8 TeNeHMe Fapatraioro cpoxa xpavennn (15 - 20 ner). Cotarouios conepxanine (0.1 ~ 0.5 mac %) eynepara xan ot conepxaninn no eeoay (3-5 twac. %) oGecnewusaer nopucrocre sneweHTo® nopoxa 6,0 ~ 8,5% rpm miorHocta 1,60 - 1.65 sTow®. Ypanurs ccrarousist nopooBpascearans twee 0.1 wa % sarpyannreneHo TexNECO Hiooraa rpakiya conepxanink ocrarosworo cymedpara’ xanwa 0,1 ac % obyenoanesa MEOBIOAAMOCTENO ALOMAR AyNHOTO NAMEN 8 pw efo conepxaHM 8 ‘cocTaBe BENE 0.5 mac% 8 cteone o6pasyeron¥arap, Orpmyarensio gelcrayouiAA va aBToMaTiKy nyu Boones —rpacbura orpaninuevio no umnnnynyy conepKanins ve Bsiule 0,15 wac.% 13 cooSpaKehiih coxpanenns —yonoBiit Sennawoiinewocrs, ysTaoan, “TO erwocuTensko rpynwsie sopHa aprunnepwcxoro TT-rawameworo “NOpOxA MEHSWe NODBEpKON! anexrpusauyn Tipa conepxanen rpadara wewee 0,05 wwac% We cOecnesmBReTCN pasHowepvocrs| Roxpuirna sepen, a peaynetare yxyalaoren cumnyvecrs, @ maevoe, nopox sspeisoonaceN ZansievOl TexHOROr#seGKOH NEpepaGOTRE NO chapmveniio Goenprinacca Dyanasow conepxanun nery4ix seuecre onpenenen cnenviouy. Conepaanne neryn Sauecta wewoe 1,4 wac% npwsoayt ROBBEN WaKCHMANLHOr® AAeNAR a awane ctbona i CHAKEHNO GANnncTANeCKOA ebibexrwenocts apranneputfoune cre Tov conepAAHINA & cosTaBe nOpOXA NeysiK 0 6 a 35 “+ seuscrs Gones 32 mac% — nagaer MaKonMansHoe agree Mm HavansHaR copocr> chape/ics Hike TpeOyewsK no yonoausm TTT Ha aprannepworne Soenprnacs!. Obeem ons! onpenenen ‘rpocKoriHocréie, yPOBHEM pasHOMepHOrO ‘ocToRKMA ANA aTOro Twa Nopoxoa pm gaeneHun stunoacro cnupra_ wor anoB0ro arMpA MeHe® 0.4 wad.% 8 CyMME Nopox xapakrepayerch — nossiuleHHeM MakorMansHoro AaaneHvR W cHMKeHHEM Sannvotayecain XapaKrepHcraK, MpennoKenreil cpnerwarysarop ‘uweraxproar (GvcTpHaTAneuTusons) cbranar Yynyswiaer ovepreraxy. a np ero conepxaninn & Bwenasove 2,2 - 4,1 Mac% 8 coveraHan ¢ opucroctino SneMenroe 6,0 - 8.5% nossiuaeT porpeccaHocr ropeHie nopoxa, yBenmuWaaA asonpoxoa, He MaBHos, ckmKaeTcr uyyactenTensHocts GannwcriNeckin, xapaktepcrux oF TeMiepatyob sapatia nom BbIeTpene, TO ects Nopox oTnwvaerca anorpaaveHTHocTee 0 Aaanexino, To Yyeeninuwaaer farisHocrs W TosHooT® cTp=nsOb! pA ucronssosaran HATpo\eNnIonds-¢ ‘onepmarnen asora 208.6 - 210 ma NOIr YeeHbulene Benes nopvcTooTH sepieHvoro nopoxa HAxe 5,0% 4 KonmvecTBa nermarwsaropa znMerexpmnar (Gucrprorunenrnisone) cpranara HWKe 2,2 ‘Mac.% nplBoaMT x YMeHbWeHMO ynnoTHeHMA Nopoxoasix sneweHTos ipa eucrpene M, egosarensio, K sospacranino MaKcMMansHoro ABNER NA NOBLILEHHEK TeMnepaTypax sapaiia, TO ecTe NORBNAeTCA rpanMeHT sasnenis Yeenmvenne nopvorocT Gone 8.5% konnMecraa anmeraxpanar (Gucrprormnenrnuxons) cbranara Gonee 4,1 Mac. % —npwBonvT _& —nepeynnoTHeHMio NopoxOasiX sneMEHTOR NPM CTperb6e, TO B 8010 ONepeRb, —NpHBONT x GHIMKEHHNO BeNMWHe! MaNCHMANSHOrO AaBNeHWA Ha OBLIWEHHEX TeMNepaTypax sKcNnyaTAYINM, BHAMUTENEMO WAKE YPOBKA MaKcHMANEHOTO ‘asneHia Nipn HODMANLHOA TeKMNeparype, TO ecTb K oTpriarenbHoMy rpagnenry nasneHnn Kpowe Toro, noproTaR cTpykTypa nopoxa npn ConepxaHnu cnerMaTisaTOpA BLE BepxHE Fpalysi —onTaMiayposaHHoro _avanasowa NpwBonT —« — cHMKEHWIO GannacTHYecKiK Roxasareneh —nopoxa np HOpManLHo Tenneparype, Baenenne He meHee 0,1 wac.% Nopoospasosarens K 280, 8 coctas nopoxa pn warun —cperwarwsatopa— MFro-9 (OGecneuneaer aprannepyiicKowy nopoxy Hosoe ‘ononHiTensHoe KavecTEO - nnaMaraWeHVe 8 ‘Ontwmvsiposanisi — KavecTBeHHM KOnMMecTReHHLIA — cOcTAB —-NPEAAOKEHHOTO. opoxa nosaonner cuMarTe TewnepaTypa FOpeHMA & nepBOHAVAHKA MOMeNT, TO voanaet Gores AMOK pasrap M, Kak cnagerane, yuebwaer apoano creona. ‘ChenoaaTerisHo, KaXnbih cyUleCTBeHHE pwaHak —HeOGKOMM, a MK COBOKVMHOCTE sanseTcA jOCTATOWKOR Ans pOCTIKEHMR Hoauskt: Kavecraa, HOBO coepxachebeKTa Kak Sbeborta cymes, a He CYMM oxbepeKToR, enpicyujero npwawaxanen @ Wx pasoSiulenHocTA TipennonenHoe TexHiiecioe —pewen#e lunniocrpipyeTcA npwmepoM wsroToneHuA SepHeHHOTO mMpoKcAMAHOBOTO | T-KaHaMsHOrO opoxa mapKn 6/7 T-5 61 chn, sHepreTMuecKy0 m171796 C41 RU96LbELE2 nu oO ‘ccHogy KoToporo cocTaanser 80,05 - 95,25 twac.% esicoroaaorncron (208.6 - 210 wn NO!) 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