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Expt. No. Page No.

Analysiu

ualtalese Quoritlpe

kurclional_ Volmlric baramebiss

rlsisgap anolis analss
salt anaksis
he_delicion ef_acidi and bosi 2odiala
Lopourd: helasi of wlaiz
qalaltue paramelers a4alled qualilalae anals
ualale

ka salt analgis
Qelermunalien ql aien _ besè nadiial gsoyp2
2eaceni

noupwagenl

Na OH
dl HCL
dl ACI++ Na,S 2ol"/HSca)
3rd
1-2 drepA cohc: HNO, + NH,C
+ NH,OH
NHOH+S aoHS
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NH OH + NHCI+ (NH4)> CO
NagHPO
basi Radicalk
t
NH
gHP*2
sond (A Pb, Cu Sh S*
(8) Cd B As
3t

hod A*C 2
Fe3
Co N N,*,2,*
2t
Ba Sa C
Mg
Preciptlalton of basic nadical
Jast chlouds leg AaC,PbC ade)
Srcond -klphudes lcuS, caS) whi te
Thad dydrodles (AlloH) fe Cot),
Foth&lphide NS, CaS 2S , NnS
flesh off
Hh -LanbonaluihdeMack light

&iocth-Phosphateubts
Hcd radicals 2
DilsQideradicals- CO3 CH,CooNO
Concanbatd audic adeals- a , B,T NO
2
Maullaneous addic nadicak -

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im de dabmine he lrasi and addie radiil

preAntn he qien tw inorganio alt
Basi Radical
SNO ponimont Obawolsn nane
Add sodun hydroide Ne neackon
(NOH) 2 he gienzolt as absant

2 Papare oniginal aelh while ppi

o Hhe gue aali Add m pesent nay
thdrochloic be Pa )
acid la

9acteha ppt inn

LLL8ambunt
Cwao_Qnd diide
A inle 3 pat
) Jo pot add lo pt fom
palosiuwn chmonale
Jo _pant 2 add
plaam odid
2t
7)o pot 3 add Al ppl ormt Pbcenfimid
dd H, So4

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Aidi Radicol
S No apunari BlsuaLon inprang
Add d HCL o heNe ncion did addi group
alsant

Add ur draps of ha durnie fumsconcaidi

conc H, SO to he wR_pungent gouppruuent
8alt &mell Lmay le CI)
3 Add dHNQ and while pp Jormd Prasana oC
Ag NO to he salti whucha aoldde coirmd.

Ralt-dn hi quen inoraani jalt llowing

aude and bosii hadiials a'prue
PreLerdZ
i)Adidi nadicol-hloide Ccr)
i) Base radical ead Pba*)_

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im 3- Ja delrmine tha Lasi and ocidic adiik

Presert a tha gven rgoni salt
Physiial agpearana - Blnt eystak
Basi Radiosl
S-No xpeinent Osrwaiordrperene
Prapae ginal so Ne aeacion negap
qiven oll and add NaOH olsont

2 Adddl: HCI k he No ruaclion OuP

uginalael". alkant

3 dn the alue ael"add Biach pplkmhd grep

Hgoa ladd Ne,Saoh phesunt (may be u")

4Dsselue tha ept: in ss

amaut q dle HO and
duide t'inta tive pots Dap iak lu cennds
a) potteacess ef MOH lcosn forns
bpant2t amall ameunt _choelat lacn Culcofmed
dl acaieacid+pw Pel ma
dropa potassuum
noanide so

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Acd Radical
S Na apument 9lspunlion Snane
Add dlde H ko ha No naacsn
aalt olRant

2Add dd 4,O to ha |Whilepp tou8c8u' cucdu

éolt

3 Add kushly prupoud Aon ning Conco G a p

wmos alphai to ha konmá whanhwe pserl [O,

aat Add -2 daopa hoo lipidksconinud)
o cncH, acid weh lsmbinttoqehe
hulpd mbuh of he
fest tube

Result Jhe_acice and Basic nadical prezent

in the qen l t are -
i)Aida nadcal NO
) Baic nadical - *2

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in Je delermine thu basie ard acidic nadials n

he qiuez inorganic alt

Basi Radkal
S-N perinmurt
S-N
bsvwalisr nfrnre
Add aOH o ha giver No ruaclio o"qrep
kalt soluliorz alisrt

2 Prupare oiginl soer NePpt

artd snatl_arretei rmed abaurt
o salt and add ddo
HCI

3 he ahoue sollion No ppt ftemude grep

add snall amowriof | alsert
NaS on pass HS gos

4Roil ot he above sel" Red broun ppi:3

t l all Hhe HS ges a foms presri Cmay e
not wolecl. her add )
-2 drops oCornco HNo3,|
NH, CI NH,OH

s ioe h ppt ie les

amount ef dit HCLacid
and diide inlaa
2 pols
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DTe parit ladd t-2 brops |Prusibn bla Baune f

CthcoOH acid ard fuw Pp forrad |eorfrind
drop ot polossiure foro
cyoride
T part 2, odd polossiurr ed Llood usppu
Hhio eyorolh colour ppl orprrrd
forvns

hadi kadid
SNo peuinert Obvwallon Anferan
Rdd dil. HCL fo he soll No uoion dl ocidz

2 Mdd orc HS0, arid o he | Ho rwochor ent-oide

4olt Yopprusurl

3 dd 1-2 drop4 H nd whle ppt &pcila gop

Cada o he sol pruirt l s )
4 d d _cont HNO lo p t Ppt inatuble Prusera of
orrnd

RLslt n he gwer inorgonik soll pllowng orida ond

bosin rodical onl prsrd
() Aidi rodicol- So (tulpbal)
(i) Bori rodivol- fe" (inon )
Tocseher's ignaturm
u ure :-Jo deltrmine ihe basic and adidic nadile
presenl che give nogoni. sall

Besi Radie
S-N xperinent tsarulior nfenan
dd NaON f qier dall No
solulior ec chor albsand

2 e x e ruqiral soluline No ppt

ohe 9o salt 1dded oblainud abser
dild Hce lo it

3Ar alovc soleuiorr add No ppl

small amournl of Nass oblauwd alase,

4| Boil oft the above siolerloluhile gela- |39noyp

l l all t e HS gas is nol hanous ppt \presurl ng
woled Therr aeid add foucd. be m)
-2 drop4 ronc WNOz,
NHCI and excuss ofNH;OW

5 issolue hiu ppt ir small Haait wtile Vuseie f

amerurnt odil Hc and ylalenonaá
her add NaOli buop CorkOecl
wse ( d.

e l e ' ifedn
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Rcidie Radzele
xperirent Obsoualior| Afotance
d d dlle H l Hhe No ruaclion |Dluli ocidic
solt 9noyp olsent

2 Ald pur_dreps fcans Noreaclion |lonanbrald

HSC a he gisen sall acdii rop
absert
3 Add small amount While hiik spccie gtop
p s:prusent lmay
he salt e so, o )
4Rdd1sncLnbald HNO3
acid le he precipitatu inistubes So rorförad

Ruttdn he given izergoni aal followirng

acidic and bakt nadicles are pusert
i Aida hadick -SoCaukphatt)
(i) Rasic radicle-A Caluminium)

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iraPrapant M/to solulion f oralii acid and

wil 4 Kolp delomin he molarily ond
sbungth he ver kitn O solulior
Chumical ruauorwd> oolii acid, KmKAnO4
H2SO

niprunt haguirsd Beaker, orical fask,

bwulle, pplle i s t Lube and ursn
bwrv

Chumical sauclion
2KttnDt34So, S o , t 2/n SO, + 3H,0+ slo]

CoOH2Hp +sloj 2 Co t 3 H,oJx 5

COOH

Net eauolion
2K1,O, +3HSO4 t 5coOH > KO, + 2 n SO, +
cooH 18HO+ 1OCO
Aoni saualion i
1nO +H+ Se , + th0Jx 2
2 O >200, t 2e- xS

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Net caualion i- 2-
2Mn 16 +SGO 21n' t SH,O tloco2

dndicalor i-K1n O s a sef indicalor

nd poirl lolowrlesá lo pemonunlprk
Procedwre
eigA 1S-8g e oxalii aid eytol and dasolr
Hrem e walw ls prepane SoOml o / t o oralic
acd souliar stng Soonl muoswing fosá
2 rse_Hhe ppelle wlhM 4 0 0alic acid solulion
and piputt oul 20 ml f a a wshed
Lbralion lask
3 Rinse and fL_He bwrelle w he qiivez KMO
kolulon
4AddGntúst be laprrox 20ml pll of_dilule
HSO lo he sélian ia Llalior2 flask
5Note Hhe inilial reading of bwrwtteo
6 Heat he lask 6 0 s zo'C_andadd KTnO
sol" A from he bwrulee l l _ a pevmanert lgAt
pink aolour i p a r l e d fo he souliorr he
Lralion losk n addilion l o s t sgle oerep
of KMnO, delulion
7Note he firal ruadin2 of He brutte
Rpeat he aboue stpa4s Toes qet
Lorcodat seadngA:

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Apt Sa
Page No.

s c l t - Jhe molarily and sbwngth of qver

Tln O selulion is o:0/2 and
97S g respeclively

ucauliors
L
U he Lqupments first urse wil walor
her nst wilk humcals used.
2 Jhere should rot e any at bubble irside
Hre jet bwrulte
3 A leost 2-3tme« eading4 must Le Takan

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