OF LICL DMR. WHE ST LCR Zak bl sre Gb Ue CRE PRR ate &4 1 O Ons MET 89%) BAK, (0027) wp: 167-171'C(dec.) IR(Br.car) 1731, 1720, 1662. (0.0.28) SIENMR(CDCLs) & + 8.094d, Je8. Oz, 2H, Ar H), 7.80(G, Je7. itz, 2H, Arlt) ,7.16-7.33 m,11H, Ar), TATE, J=7. Tie, 1H, Cs” Hl) 6.2443, 1H, Cho“, 6.01 (t,J28.5llz AM, C9“) 5,87 (dd J=9,0,6, 52, IHC" = H), 5.60(G, Je7. OH, 1H. CH) ,5.51(d,J=5.8Hz, 1H, 1H), 4.93(d, JH9. Sil, 1H, CH) 4.39 ¢dd, J=10.5, 7.08.1 H), 4.26(d, J8. 3H, 1H, CooH) 4.14 (0, 8.58, 1 Hy, 3.714, 546. 8llz. 1H CH) 3.06-2.04 a, 11 H), 2.45(s,3H.Cy-Ote) , 2.18(8, 3H. C, ¢-Olc) 2.041 2(0, 19H), 1.85(8,311.Cie-Me), 1.62(8,30,C10-Me) 1 268,31), 1.1668, 311). 10.02.91) Mass (SINS) : 1090(NH)*. (0030) seibrt4 2) — ( (A-ERUY JERZY AMIE) Pe FIL) PRY NODE: (1) d-PRY ERY YY AKAN OY (920m, Anmol) EsRHRY Vy LFV (2780 mg, 2 Ommol) @HLAFL y (8 Owl) (YBAEL. YLFUTSY (5. Lml, 40am) 2YAFVTS JEN Y (10 Ong) HZ, SET 2 A NSTTREEL Te. BUST MEE PARA LINE POVAAITE (PADAVA) (2 ORL HE FETLCM—Aky KMS DUT, LEVLAF J169 5 Ome URES 0%) BBR. COTATI (6.0 Ome, Qamol ) [2 1 SABIE 1 v7 HB (2m) #imd , STS GRAIL 2. BUI REHRIS ‘LSE (Qm1) En Tt, OEE RRL LE AAI OED TI (5 0% AF PNA FORA) 1 ORL. ET ST LO BO2siy MBPEADET. A-ERUY ERY PAINS KHIR S 1 Ong RAED 496) BH (2) PRY—W (38ng, 0. O4 Amol) 2 A-E AVY SERU LY AIDINS KH (4 Ome, 0. 15) mmol) 2CH,C 1, (1 Snl) BHRL DEC (30. mg, O. 15aml) EDMAP (4, 5g) £/UA Sith C6 ORTAREL TS, RURAL BRE DEL DiI bY Ltt (5 Owl) EON A, PERNA Cts LIS, RIE HATERS 7% 27 CURR, MEE PRICE. RIN SD MIAIITE (FORMA: XH/—W=9 : DRML EMSS TLR 2k RIBS Abe CRE RAIL , MELLIN Ses (REO 6%) BR (0.031) mp: 205-209 (dec. ) IR(Brycwr!) £1740, 1710, 1639. HmEO-110865 (0032) ‘H-NMR(CDCIs) & : 8.1164, J97. Biz, 2 Ar W), 7.814, J97.8llz, 2H, Art), 7. 62-7. 38¢m, 11H, Ar), 7.21(bs,1H,C:" A), 6.295, 1, Cy -W 6. 16(t, J=7. 00 Zu lH Cis“), 5.92(dd,J-8.5,4. 1H, 1H, Cs’ “1D 5.664 lll, 1H CoM), 5.52(d, Jd. 1Hz, 1H, Cy" 4. 95(d, 95H, Cel), 4.39(dd,J=10.7.6. 8, I, GM 4 29 (4, JB. 2,1, Cyo-H), 4.18(4,J98. lz, 1, Cp, 3.T6(d,Je7 Ill, IHCe-H), 2.80-2.44¢@, 11), 2.3965, 3HLC.-O8e) 2.21 (8, 3H.G 0“) 1,89(8, 3H. o-Me) 1.6745, 38, 1.20(8,3H), 1.13(8,38). 10.033) Mass(SIMs) : 105M)". 10034) sas 20 (4 (AER PERN TY ANH ANA HS) NYS AI) PRYOR (1) 4- ERY PERU YY REN OE (920mg, Amml) pe Ka BRBEEE IY (3320ms, 20mol) 28X41 (5 0a1) te WML. PULFVTSY (5. Sm, 4 Omwl) &0 A. ASNT S OBA L 2, BERGER BFE FRAME TIL, FRIES UAH OY bY IT (OOK Ws) (A DRL BT AT LCM Aik PHS RADUT, LHVI AFBI 3.4 Ome (NEE 3 %) Bt. LOLAF IME (1000m8, 2. 77 OL) BEI PI C1: 1) RE (2 5 wl) RR LARC 7 2.1 A (2.04, 2. 7 Bio 1) ima, BATS ORAREL Ze. GREE 1 BL SEGRE (2. 7 Sal) nL Poth, REE FMR] LR LIP IL IF IB (40% KF POWA FTN) LOWML. HTSTLC B2ity MPEADET. p— (AERTS RU ZY AIRENARY ) HATES 8 One UE 2%) B4R. (2) PRIMW (3 One, 0. 03 Sam) & p— (AER YER DY IR ENARY) BEE (53mg, 0. 16mmol) CHC 1, (1 Oml) REL DCC (3 Ong, O. 1 Smol) DMAP (4, Sma) $n 22638C 6 OWSNRYEL Ae BEILIEET HEATERS DAL. DARIAN bY 7 KBE (S Om) M2, 7OOMLATHIEL A. PURE HERBS 7 RL CRE, BEE PRE LBS ALIN ISIE (Fab FA-W=92 LAE OWRL, BETS TL CHa y MDS Geb MEE PiRBAREEETL GE ACAWS Ons (WEED 5%) BABI, (0035) wm: 175-177 (ec.) TR(KBr,cmt) : 1715, 1664. (0.036 ] 1H-NMR(CDCI,) & : 8.124, J58. 382, 2H, Ar H), 8.00(d, J=8. lz, 2H, Ar), 7. 76(6, J. 38, 2H, Ar, 7.6241, 20(a, 13H, At), 7. 05(d, J°9. O82, 1H, Cs" =X.