Professional Documents
Culture Documents
BS1204 1993
BS1204 1993
BS1204 1993
Specification for
Contents
Page
Committees responsible Inside front cover
Foreword ii
1 Scope 1
2 References 1
3 Definitions 1
4 Properties of type MR adhesive: moisture-resistant and
moderately weather-resistant 2
5 Instructions for use 2
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI
6 Test requirements 2
7 Resistance to cold water 2
8 Resistance to hot water 2
9 Resistance to micro-organisms 2
10 Natural ageing of joints 2
11 Keeping qualities of components 2
12 Marking 2
Annex A (normative) Selection of test slips 3
Annex B (normative) Method of preparing gap joint test pieces 3
Annex C (normative) Method of preparing close-contact joint
test pieces 5
Annex D (normative) Method of curing and conditioning the joints 7
Annex E (normative) Method for determination of failing force 8
Annex F (normative) Method for determination of resistance
to cold water 8
Annex G (normative) Method for determination of resistance
to hot water 8
Annex H (normative) Method for determination of resistance to
micro-organisms 8
Annex J (normative) Method for determination of moisture content 9
Figure 1 — Gap joints showing method of fitting inserts 4
Figure 2 — Gap joint showing position of saw cuts 4
Figure 3 — Clamping device for five gap joints 5
Figure 4 — Close-contact joint 6
Figure 5 — Clamping device for holding five close-contact joints 6
Figure 6 — Wooden jig for locating joints in clamp 7
List of references Inside back cover
© BSI 03-1999 i
BS 1204:1993
Foreword
This British Standard has been prepared under the direction of the Adhesives
Standards Policy Committee. This edition introduces technical changes but it
does not reflect a full review or revision of the standard which will be undertaken
in due course.
Specifications and methods of test for type WBP and BR adhesives, formerly
included in BS 1204-1:1979 and BS 1204-2:1979, have been superseded by
BS EN 301 and BS EN 302-1 to BS EN 302-4.
This edition combines the previous Parts 1 and 2 which are withdrawn but covers
only type MR phenolic and aminoplastic adhesive, which is not covered in
BS EN 301.
Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
pages 1 to 10, an inside back cover and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
1)
See BS 7359 for nomenclature and sources of supply.
ii © BSI 03-1999
BS 1204:1993
1 Scope 3.3
aminoplastic resin
This British Standard specifies the technical
requirements and methods of test for type MR a synthetic resin derived from a condensation
gap-filling and close-contact adhesives based on reaction between a synthetic compound containing
synthetic resins of the phenolic and aminoplastic amino groups, e.g. urea, thiourea, melamine, or
types, with or without additional hardeners, for use allied compounds alone or in combination, with
in the manufacture of wooden assemblies. formaldehyde
Cold-setting, warm-setting and hot-setting 3.4
adhesives are covered. hardener
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI
This standard also covers the combination of resin a substance that causes or regulates the curing
and hardener when the user is required to add reaction of resins that yield rigid (hard) products. It
hardener; if the resin and hardener are sold may be supplied separately, either in liquid or in
separately, neither by itself can be said to comply powder form, or may have been incorporated with
with this standard. the resin by the manufacturer
NOTE The synthetic resin adhesives covered by this
specification are commonly manufactured in two forms:
3.5
a) liquid which may or may not require the addition, before extender
use, of hardener in liquid or powder form, or may be used with a substance, sometimes having some adhesive
a hardener separately applied;
b) powder which requires the addition, before use, of water or action, added to an adhesive to reduce cost
other liquid, with or without the addition of a separate 3.6
hardener.
cold-setting adhesive
The properties of the adhesives to which this
standard applies are determined by tests made on an adhesive which sets and hardens satisfactorily at
beechwood joints. The failing forces obtained on the temperatures of 23 °C or below under the specified
test pieces prescribed cannot be converted into conditions of use
terms of stress values measured, for example, in NOTE A cold-setting adhesive may be heated to accelerate
setting if required.
pascals.
3.7
The standard is not applicable to adhesives based on
warm-setting adhesive
resins of types other than phenolic or aminoplastic
and should not be quoted for these other materials. an adhesive which sets and hardens satisfactorily at
The standard is also not applicable to structural temperatures between 25 °C and 50 °C
adhesives of the phenolic and aminoplastic types NOTE Some warm-setting adhesives may require a minimum
temperature above 23 °C.
covered in BS EN 301.
3.8
2 References hot-setting adhesive
The titles of the standards publications referred to an adhesive which cures at a temperature of 50 °C
in this standard are listed on the inside back cover. or above
NOTE If temperatures above 90° are to be employed, it is
3 Definitions essential that the suitability of the adhesive for heating to such
temperatures, and the method of heating to be employed, are
For the purposes of this British Standard the confirmed by the manufacturer.
following definitions apply. 3.9
3.1 gap-filling adhesive
synthetic resin adhesive an adhesive used for load bearing purposes which
a composition, based on a synthetic resin of either will provide satisfactory bond strength in bond-lines
the phenolic or aminoplastic type or mixtures of up to 1.3 mm in thickness
these two types, prepared for use in accordance with 3.10
the manufacturer’s instructions spread of adhesive
3.2 the quantity of adhesive per unit bond area applied
phenolic resin to an adherend. In single spreading this quantity of
a synthetic resin derived from a condensation adhesive is applied to one surface; in double
reaction between a phenolic compound, e.g. phenol, spreading it is divided between the two surfaces to
cresol, xylenol, resorcinol, or a mixture of phenolic be joined
compounds, with an aldehyde, e.g. formaldehyde,
furfuraldehyde, or a mixture of aldehydes
© BSI 03-1999 1
BS 1204:1993
2 © BSI 03-1999
BS 1204:1993
Annex A (normative) NOTE 2 Glass paper complying with grade no. 1 of BS 871 is
recommended.
Selection of test slips A.2 Moisture content
A.1 Test slips The moisture content of the slips at the time of
A.1.1 General applying the adhesive shall be 10 ± 2.5 % when
Prepare the test slips from European determined by the method of Annex J.
beech2) 25 ± 0.25 mm wide and 3.2 ± 0.15 mm thick. NOTE The specified moisture content of 10 ± 2.5 % corresponds
with the conditions attained by wood during storage in a
Those for gap joints shall be 150 ± 1.5 mm long and normally heated room in the British Isles.
those for close-contact joints shall be 115 ± 1.5 mm
long. The growth rings may be at any angle, Annex B (normative)
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI
from 0° to 90° inclusive, relative to the face. One Method of preparing gap joint test
face of the slip should be planed, the knives being
sharp enough to provide a cleanly cut sample
pieces
without compressing or otherwise damaging the B.1 Test pieces
fibres; the other face may be planed or smoothly Prepare each test piece from two 150 mm slips of
sawn. beech as specified in Annex A.
It is essential that the slips shall be flat and free B.2 Preparation of the adhesive
from splits, knots, whorls and dote, that the angle of
Prepare and use the adhesive in accordance with the
inclination of the grain across the face of each test
instructions supplied by the manufacturer. If these
slip shall be not greater than 1 in 9, and that the
permit separate application of the resin and
grain shall not be obviously inclined to the face.
hardener, prepare the test piece by the separate
A.1.2 Inclination of grain across the face application method.
The inclination of grain across the face can be B.3 Preparation of joints
judged by the following two factors.
Prepare the joints under ordinary room conditions
a) The long lines formed by the junctions of the unless otherwise directed by the manufacturer.
growth rings which are to be seen most clearly on Coat the planed face of a test slip with adhesive over
quarter-cut slips (i.e. slips cut with the growth approximately the middle two-thirds of its length,
rings at 90° to the faces). and fit inserts of 60 + 0.0, – 1.3 mm long
b) The small rays which can be seen as dark flecks by 25 mm ± 0.25 mm wide by 1.3 ± 0.15 mm thick,
and are most prominent on slash-cut or as shown in Figure 1. Fill the resultant gap
tangentially-cut slips (i.e. slips with growth rings (approximately 30 mm long) with an excess of the
parallel to the faces). adhesive. Coat a second slip also on the planed
Slips with growth rings at other angles to the faces surface for the middle two-thirds of its length, and
show both characteristics with varying degrees of place it in position to make a joint. It is essential to
prominence. assemble the joints in a clamp, a convenient form of
which is shown in Figure 3. When a sufficient
A.1.3 Inclination of grain to the face
number of joints are in position, the clamp is
The inclination of grain to the face of the slips is screwed down “finger tight” and excess adhesive will
viewed on the edges. It is best shown by the same be squeezed out.
two factors in reverse, i.e. by the growth ring
If separate application of resin and hardener is
junctions on tangentially cut slips and by the ray
permitted by the manufacturer, normally the lower
flecks on quarter-cut slips.
face of the top slip and, if required, the lower face of
NOTE No restrictions are placed on the quality or species of the the inserts, shall be coated with hardener, the resin
veneer used for the inserts for gap test pieces. It is essential that
the thickness is 1.3 ± 0.15 mm and that the inserts are made of being applied to the upper surfaces of the bottom
veneer from a single piece. slip and inserts, and to fill the gap. A manufacturer
A.1.4 Preparation of test slips may, however, specify that the hardener is to be
Immediately before the preparation of the test piece, applied to both the top and bottom slips, instead of
lightly sand each slip on the planed side. to the top slip only, and in this case it is necessary to
NOTE 1 A suitable procedure is to give the appropriate part
coat both sides of the inserts with resin.
four double strokes parallel to the direction of the grain with a After the test joints have been cured and
flat block to which a sheet of suitable abrasive material has been conditioned (see Annex D) saw cuts shall be made as
firmly attached. Take care to hold the block flat on the slip so that
the surface is uniformly sanded and rounding of the sides of the shown in Figure 2. The resulting overlap shall
slip is avoided. be 25 ± 0.25 mm.
2)
European beech, Fagus sylvatica.
© BSI 03-1999 3
BS 1204:1993
4 © BSI 03-1999
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI BS 1204:1993
© BSI 03-1999 5
BS 1204:1993
6 © BSI 03-1999
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI BS 1204:1993
© BSI 03-1999 7
BS 1204:1993
3)
See “Handbook of Hardwoods” and “Handbook of Softwoods”, published by HMSO.
8 © BSI 03-1999
BS 1204:1993
place with material such as modelling clay to Take a representative sample of the test slips and
prevent loss of moisture. Keep the dish and contents weigh each to the nearest 0.001 g. Dry the slips in
at 25 ± 2 °C for 1 week. the oven at a temperature of 100 °C to 105 °C until
NOTE Other suitable materials used as sealants are their mass is constant.
proprietary oil-based putties. See also BS 544.
Calculate the percentage of moisture using the
H.4 Pretreatment of test pieces following formula:
Immerse five test pieces for 1 week in cold water to M1 – M0
remove any free formaldehyde or other Percentage of moisture = ----------------------
- ×100
mould-inhibiting materials from the wood. During M0
this treatment, ensure that the water has full access where
to all surfaces and that it is changed daily.
M0 is the mass (in g) of the test slip after
H.5 Procedure
heating;
Remove the cover from the dish and press the wet
test pieces into the sawdust so that their upper faces M1 is the mass (in g) of the test slip before
are level with the surface. Replace and re-seal the heating.
cover, and incubate the dish and contents Report the moisture content as the mean of the
at 25 ± 2 °C for 4 weeks. At the end of this period, results.
remove the test pieces, wash them in cold water and
NOTE Care should be taken to prevent the change in moisture
immediately test them by the method described content between the cutting of the slips and the first weighing, or
in Annex E. between removal from the oven and the subsequent weighing.
© BSI 03-1999 9
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI
blank
10
BS 1204:1993
List of references
BS 544:1969, Specification for linseed oil putty for use in wooden frames.
BS 871:1981, Specification for abrasive papers and cloths.
BS 5214, Specification for testing machines for rubbers and plastics.
BS 5214-1:1975, Constant rate of traverse machines.
BS 5214-2:1978, Constant rate of force application machines.
BS 7359:1990, Nomenclature of commercial timbers including sources of supply.
BS EN 301:1992, Adhesives, phenolic and aminoplastic, for load-bearing timber structures: classification
and performance requirements4).
BS EN 302, Adhesives for load-bearing timber structures: test methods4).
Licensed Copy: Giorgio Cavalieri, ALSTOM, 9-Mar-01, Uncontrolled Copy. © BSI
© BSI 03-1999
|
|
|
|
|
|
|
|
|
BSI Ð British Standards Institution
|
|
|
|
|
|
| BSI is the independent national body responsible for preparing British Standards. It
|
| presents the UK view on standards in Europe and at the international level. It is
| incorporated by Royal Charter.
|
|
| Revisions
|
|
| British Standards are updated by amendment or revision. Users of British Standards
|
| should make sure that they possess the latest amendments or editions.
|
|
| It is the constant aim of BSI to improve the quality of our products and services. We
|
| would be grateful if anyone finding an inaccuracy or ambiguity while using this