BGMEA University of Fashion &

Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 08

Experiment Name: Study on cotton goods with reactive dyes

Date of Experiment: 08/09/2021

Date of Submission: 15/09/2021

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:

A dye, which is capable of reacting chemically with a substrate to form a covalent dye
substrate linkage, is known as reactive dye. Here the dye contains a reactive group and this
reactive group makes covalent bond with the fiber polymer and act as an integral part of
fiber.

Objectives:
This work evaluates the effect of cellulose finishing of dyed cotton fabrics. Fabric samples
were dyed with reactive dyes possessing different reactive groups with or without metal
atoms in their structures. Enzymatic treatments were carried out with total crude cellulose.

Properties of reactive dye:

 Reactive dyes are anionic dyes, which are used for dyeing cellulose, protein and
polyamide fibers.
 Reactive dyes are found in power, liquid and print paste form.
 During dyeing the reactive group of this dye forms covalent bond with fiber polymer
and becomes an integral part of the fiber.
 Reactive dyes are soluble in water.

Recipe:
*Dye Stuff = 2 % shade
*Sequestering agent = 0.5 gm/l
*Wetting agent =1 gm/l
*Salt= 30 gm/l
*Soda= 20 gm/l
*M: L=1:30
*Temp= 50 – 90°c
*Time = 1- 1.30 hrs

Stock Solution:
Dye: 1%
Salt: 20%
Soda: 10%
Others: 5%
Recipe calculation:
Let,
Sample weight =2.50 gm
Total Liquor = Fabric weight X L [M: L = 01:30]
= 2.50 X 30
= 75 ml
A) Reactive Dye (2%) = (Fabric weight X Shade%) / stock solution%
= (2.50X2) / 1
=5mL
B) Sequestering Agent = (Total liquor X Recipe amount) / (stock solution X 1000)
= (75 X 0.5) / (0.05 X 1000)
= 0.75mL
C) Wetting Agent = (Total liquor X Recipe amount) / (stock solution X 1000)
= (75 X 1) / (0.05 X 1000)
= 1.5mL
D) Salt = (Total liquor X Recipe amount) / (stock solution X 1000)
= (75 X 300) / (0.20 X 1000)
=11.25mL
E) Soda = (Total liquor X Recipe amount) / (stock solution X 1000)
= (75 X 20) / (0.10 X 1000)
=15 mL
Required Water = Total liquor - (A+ B + C + D + E)
= 75ml - (5+0.75+1.5+11.25+15) mL
= 75ml – 33.5mL
= 41.5mL

Precaution:
The reactive dye cannot be satisfactory stripped from fiber due to covalent bond between
dye molecule and fiber. Stripping becomes necessary when uneven dyeing occurs. Time:
until desired shade is obtained.

Conclusion:
By this experiment we came to know the reactive dyes are of the least reactivity because
they take more temperature and more time for dyeing.

Reference:
BUFT Dyeing, Printing & Finishing Lab.
 BGMEA University of Fashion &
Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 09

Experiment Name: Study on dyeing jute goods with basic dye

Date of Experiment: 15/12/2021

Date of Submission: 22/12/2021

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:
Basic dye is also called cationic dyes, because in solution the basic dye
molecule ionizes, causing its colored component to become a cation or
positively charged radical. When they were first synthesized, the basic dye
was used on wool and silk, but they had very poor color fastness
properties. They were therefore displaced for this fibre by acid.

Objective:
 To jute fibre easily to dye
 To no affinity to cotton fibre.
 To write a report according to the experiment.
 To acrylic fibre is reached with basic dye.

Necessary equipment:
1. Pot.
2. Beakers.
3. Glass rod
4. Pipette.
5. Measuring cylinder.
6. Digital balance.
7. Tri-pod stand.
8. Gas burner.
9. Thermometer

Required recipe
1. Dyestuff (basic dye) ------------3%
2. Wetting agent--------------------- 0.5 g/L
3. Sequestering agent------------- 1 g/L
4. Gluber salt------------------------ 10 g/L
5. Acetic acid------------------------ 1 g/L
6. Temperature--------------------- 90 -100℃
7. Time ------------------------------- 30-50 min
8. pH----------------------------------- 4-5
9. M: L --------------------------------- 1: 20

Stock solution:
1. Dye--------1%
2. Salt--------20%
3. Soda------10%
4. Others-----5%

Recipe calculation:

Fabric weight = 4 gm
Total Liquor = Fabric weight × L [M: L = 01:20]
= 4 × 20
= 80
A. Dyestuff calculation =
𝑆𝑎𝑚𝑝𝑙𝑒 𝑤𝑒𝑖𝑔ℎ𝑡 ×𝑆ℎ𝑎𝑑𝑒% ÷ 𝑆𝑡𝑜𝑐𝑘 𝑠𝑜𝑙𝑢𝑡𝑖𝑜𝑛
=
4 ×0.03/0.01
= 12 mL
Chemical calculation =
𝑇𝑜𝑡𝑎𝑙 𝑙𝑖𝑞𝑢𝑜𝑟 ×𝑆ℎ𝑎𝑑𝑒% ÷ 𝑆𝑡𝑜𝑐𝑘 𝑠𝑜𝑙𝑢𝑡𝑖𝑜𝑛 ×1000
B. Wetting agent = 80 ×0.5 ÷ 0.05×1000
= 0.8 mL
C. Sequestering agent = 80 ×1÷ 0.05 ×1000
= 1.6 mL
D. Gluber salt = 80 ×10 ÷ 20 ×1000
= 0.04 mL
E. Acetic acid = 80 ×1 ÷ 0.05 ×1000
= 1.6 mL

Total water = 80 – (A+B+C+D+E)

= 80 – 16.04
= 63.96 mL

Curve Process:
Working procedure:
 At first take the sample, which would be dyed is weight.
 1% stock solution of dyestuff, wetting agent gluber salt and
sequestering agent and acetic acid is prepared with water.
 Required stock solution of acetic acid is added 30 times in a dye bath
is boiled at 50 ℃ for about 15 min.
 Now in dye bath required stock solution of dyestuff and wetting agent
and sample added and heated is at 70℃ and is kept for 15-20 min.
 Then sample is taken out and gluber salt solution is added and
boiled.
 After dyeing the materials is taken out and squeezed and washed
dried.

Precaution:
1. The sample should be kept uniformly in the mixture. Otherwise, non-
uniform dyeing will do.
2. Amount of chemical and water must be accurate.
3. Chemical must mix with water very well.
4. Time should be maintained as per written.

Conclusion:
Dyeing is an important experiment in textile technology. Jute is the mostly
used fibre from old ages to now. So, this experiment will do a great favor to
us in future days

Reference:
BUFT Dyeing Printing & Finishing Lab
 BGMEA University of Fashion &
Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 10

Experiment Name: Study on dyeing polyester fabric with disperse dye

Date of Experiment: 22/12/2021

Date of Submission: 29/12/2021

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:
Disperse dyes can be used with various techniques and will readily color
synthetics such as polyester, nylon, cellulose acetate, viscose, synthetic
velvets, and PVC. They can also be used to color plastic buttons and
fastenings. Their effect is less potent on polyester, due to the molecular
structure, allowing the only pastel through to medium shades. Polyester
fiber contains pores or canals within its structure which, when heated to
100°C, expand to allow particles of the dyes to enter. The expansion of the
pores is limited by the heat of the water industrial dyeing of polyester is
carried out at 130°C in pressurized equipment.

Objectives:
 To learn about dyeing process of polyester woven fabric by disperse
dye.
 To dye polyester fabric by disperse dye.
 To make a combined shade using red, yellow, blue color substances.
 To write a report according to the experiment.

Apparatus Required:
* Beakers.
* Glass Rod.
*Pipette.
* Measuring Cylinder.
*Digital Balance.
*Tri-pod stand.
*Gas Burner.
*Thermometer.
*Pot.
Process Sequence:
Collection of sample
↓
Set water level
↓
Add Acetic acid solution
↓
check pH
↓
Add dispersing agent solution
↓
Add disperse dye solution
↓
Add fabric sample
↓
Raise temperature to 130deg C
↓
Run time for 20 minutes
↓
Bath Drop
↓
Rinsing
↓
Drying
Recipe:
*Disperse Dye = 3 % shade
*Diapering Agent =1 g/L
*Sequestering agent = 2 g/L
*Acetic Acid =2 g/L
Leveling Agent =1 g/L
*Temperature =125-135*C
*Time =30-60 min
*M: L=1:20

Stock Solution:
Dye: 1%
Salt: 20%
Soda: 10%
Others: 5%

Recipe calculation:
Let,
Sample weight =1 gm
Total Liquor = Fabric weight X L [M: L = 01:20]
= (1×20)
= 20 ml
A)Disperse Dye (3%) = (Fabric weight X Shade%) / stock solution%
= (1×3)/1%
=3mL
B)Diapering Agent = (Total liquor X Recipe amount) / (stock solution X
1000)
=(20×1)/ 0.05×1000
= 2.5mL
C)Sequestering Agent = (Total liquor X Recipe amount) / (stock solution X
1000)
=(20×2)/0.05×1000
= 1.25mL
D)Acetic Acid = (Total liquor X Recipe amount) / (stock solution X 1000)
= (20×2)/0.05×1000
=1.25mL
E)Leveling Agent = (Total liquor X Recipe amount) / (stock solution X 1000)
= (20×1)/0.05×1000
= 2.5mL
Required Water = Total liquor - (A+ B + C + D + E)
= ( 20-10.5)mL
= 9.5mL

Precaution:
Avoid splashing solutions into the eyes, swallowing the materials or
prolonged skin contact.
A simple 'non-contact' approach (most people use gloves to avoid dyeing
themselves) plus normal, good, hygiene is sufficient precautions for the
occasional user.
Conclusion:
The term “disperse dye” have been applied to the organic colouring
substances which are free from ionizing groups, are of low water solu bility
and are suitable for dyeing hydrophobic fibers. Disperse dyes have
substantively for one or more hydrophobic fibers e.g. cellulose acetate,
nylon, polyester, acrylic and other synthetic fibers. The negative charge on
the surface of hydrophobic fibers like polyester cannot be reduced by any
means, so non-ionic dyes like disperse dyes are used which are not
influenced by that surface charge.

Reference:
BUFT Dyeing, Printing & Finishing Lab.
 BGMEA University of Fashion &
Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 11

Experiment Name: Study on block printing with direct dye

Date of Experiment: 29/12/2021

Date of Submission: 05/01/2022

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:
Block printing involves a block, wooden/ metal, in which a design has been
made and by dipping it on color and pressing that an fabric we get a block
print, this is called block printing method. This is perhaps the slowest
process of all the textile printing techniques. Usually a hand block is 5-6
inches in length and 2-3 inches in width. Its verity of design is decided by
the buyers and the wood worker who make those designs. The cost of
block printing set-up is very low which gives this an advantage. There are
several types’ blocks used for block printing. Such as
i. Wooden block
ii. Linoleum block
iii. Match stick blocks
iv. Blocks made of household goods like glass,
berth top and other.
v. Meter block

Objective:
 To know how to print a fabric using block
 To observe the practical knowledge about block printing
 To compare the theatrical idea with practical experiment.
 To know the dye making process of the method.
 To know how to use a block

Apparatus:
 Plastic mug
 Fabric
 Glass rod
 Measuring cylinder
 Block
 Omen
Recipe
1. Direct dye – 1.5gm
 2. TR Oil – 1gm
3. Tri sodium phosphate – 2gm
4. Thickener (Fine gum10%) – 7.5gm
5. Water as required

Working procedure:
1. At first we took a mug and spoon, washed those properly.
2. Then we measured thickener (Fine gum 10%) and put it in the mug.
3. After that mixed 100ml water with that thickener the water was added
slowly and stirred with a spoon until it was mixed perfectly and take a
paste form.
4. Then 2gm of Tri Sodium phosphate and 5gm direct dye was
transference in the mug and stirred for some time.
5. After mixing all Those, 1gm of TR oil was added and again being
stirrer to make like paste.
6. Then the fabric was spread on some papers and a wooden block with
a design was filled with printing paste
7. Then the block was put on top of the fabric and being pressed hard
for few moments
8. When the block was removed, the design was printed on this fabric.

After-Treatment:
 After printing with block, the fabric was put on the woven and left to
stream for 7-12 minutes
 Dry heat treatment was also given for 4-6 minutes
 Soaping with 0.5-1gm/1 soap to remove unfixes dye.
Sample
Conclusion:
Printing of all cotton fabric with direct dye has excellent built up
properly and maximum fixation shade is also bright. By printing with
block one can acquire practical knowledge of the method the shade
was also perfect.
 BGMEA University of Fashion &
Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 12

Experiment Name: Study on screen printing with pigment dye

Date of Experiment: 05/01/2022

Date of Submission: 12/01/2022

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:
Customarily, block printing was utilized to print textures. This cycle includes
portraying and cutting a plan into a square of wood, applying ink or color, and
stepping it onto a completed material. Square printing varies from weaving,
where examples are woven into a texture as it's made.

Objectives
 Generally, block printing was utilized to print textures.
 This cycle includes portraying and cutting a plan into a square of wood,
applying ink or color, and stepping it onto a completed fabric.
 Square printing contrasts from weaving, where examples are woven into
a texture as it's made

After treatment of block printing:

The texture, subsequent to printing is dried out in the sun. This is essential for
the fixing cycle or after treatment of printing. It is then abounded in wads of
papers to keep the color from holding fast to different layers and steamed in
boilers developed for the reason. Silks are likewise steamed this path
subsequent to printing

Procedure of block printing:

The texture to be printed is washed liberated from starch and delicate faded if
the common dark of the texture isn't wanted. On the off chance that coloring is
needed as on account of saris where borders or the body is tied and colored it
is done prior to printing. The texture is again washed to eliminate
overabundance color and dried altogether

Required recipe
√Pigment: 4m/L
√Thickener (Fine Gum 10%): 3gm
√Urea: 1gm
√Binder: 10m/L
√Fixer: 2m/a
√Water as required

Working Procedure:
 At first we took a mug and spoon washed them properly.
 Then we measured thickner 3gm ( Fine Gum 10%) and put in the mug.
 After thar mixed 100ml water with the thickner. The water was added
slowly and strirrered with a spoon until it was mixed perfectly and take a
paste form.
 Then 4m/L pigment was transferd in the mug and strirrered for sometime.
 After mixing all these 1gm urea 10m/L binder and 2m/L fixer was added
and again stirred to make the paste
 Then the fabric was spread on some papers and scree. with a specific
design was put on top of the fabric.
 Then printing paste was giveb on the surface of the screen and spread
all over the screen. using a squeeze.
 When the paste spreading was complete screen was removed and the
printed fabric was dried naturally.

In this task we have chipped away at dim the blocks must be cleaned
immediately after the printing with the help of a toothbrush, so that they are
ready for further use. The printed side of the fabric should not be exposed to
the Sun while drying. Otherwise the colors can fade

Precaution:
 All chemicals measure are taken properly.
 Temperature maintain properly.
 Amount of chemicals should be balanced and as per written in the recipe
and chemical calculation.
 While removing the container from the oven must use the gloves.
 Time and temperature should be maintained according to the recipe.
Conclusion:
Block printing involves carving the desired pattern onto a large block, covering
that design in ink or dye, and stamping it onto the fabric. While blocks could be
made from stone, they were most commonly made of wood.

Reference:
BUFT Dyeing, Printing & Finishing Lab
 BGMEA University of Fashion &
Technology (BUFT)

Lab Report

Course Code: Tex1202

Course Title: Dyeing, Printing & Finishing (Lab)

Experiment No: 13

Experiment Name: Study on stencil printing with direct dye

Date of Experiment: 12/01/2022

Date of Submission: 19/01/2022

Submitted By Submitted To
Name: Maruf Saqline Rozina Aktar

ID: 201-023-111 Lecturer

Batch: 201 Department of AMM

Group: AMM BUFT

Introduction:

Stencil printing is after used in textile industry. It has quiet an important in

the field. In this this method a design is cut according to the criteria of the
buyers them the design specifically one side of the design is dipped into
paint them being pressed on the fabric. That’s how stencil print is done. If
the pigment quality is well enough and being done according to the manner
than a remarkable outcome can be achieved.

Objective:

1. To print a material properly and practically.

2. To obscene the advantages and disadvantages of the printing
method
3. To compare the theoretical idea with practical experiment

Recipe:
Direct Dye – 1.5gm
TR Oil – 1gm

Tri sodium phosphat – 2gm

Thickener (Fine gum 10%) – 75gm

Water – As required

Working procedure:

1. At first we took a mug and spoon, washed those properly.

2. Then we measured thickener (Fine gum 10%) and put it in the mug.
3. After that mixed 100ml water with that thickener the water was added
slowly and stirred with a spoon until it was mixed perfectly and take a
paste form.
4. Then 2gm of Tri Sodium phosphate and 5gm direct dye was
transference in the mug and stirred for some time.
5. After mixing all those 1gm TR oil was added and again stirred to
make those paste ready.
6. Then the fabric was spread on some paper and a stencil with a
specific design was put on top of the fabric.
7. Then the printing paste was taken by a brush and the color was
given to the stencil.
8. When the color spreading was completely, stencil was removed and
the printed fabric was dried mutually.

sample
Conclusion:

Printing of cotton fabric with direct dye by stencil method has an excellent
build up and has maximum fixation. Shad is also bright. By this experiment
we have acquired knowledge about stencil printing process on cotton
fabric.