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    Laboratory Manual 2

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    Laboratory Manual 2

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    Sugar cane Process

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    213 views212 pages

    Laboratory Manual 2

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    amila_vithanage
    Sugar cane Process

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    BUREAU OF SUGAR | iT 1 | jp cra | | EBSES THE STANDARD LABORATORY MANUAL FOR AUSTRALIAN SUGAR MILLS VOLUME 2 C ANALYTICAL METHODS AND TABLES BUREAU OF SUGAR EXPERIMENT STATIONS BRISBANE, AUSTRALIA APRIL, 1991 ‘BSES PUBLICATIONS Published by: SES. 50 Mees Road, Indooreopl. (Qorcsiand gs PO. Box 86, Indoor, (Qatesina toss SBN 0 7242 14100 (Se) ISBN 0 72424051 8 (N01 2) Printed by Watson Ferguson and Co, Brisbane nD CONTENTS ‘Te vrous method of sah have ben groupe under headings for eso teres. Detistons ng ela products Metbod1 Calibration of polarimeter by quart plate Matod2 Pol —Deerminton nue Method Brix —Decrminaton ine by hyrometer Methods Fie — Danian ncane Method Sampling and analysis or evaluating ing tein peroemance Method Pol — Determination ln bagase by wet ‘inegraton Mainod7 Moltire— Determination in bagase and cane bya Meibod$ Tota and soluble pespute — Deterimation [Mained9 Sareh— Determination ncane es ‘Caiestion pros Maino 10 Turia — Detention nad le Method 11 Pol—Deteminton fer cae Mathod 12 Moire ~ Determination filter ake Maihod 13 Fibre — Determination in joie and mud Method 14 "Total insole sods and mud solids ‘Seen ulce and nud teas ‘Pan sage prodact and asa Mado 15 Method 16 Method 17 Math 18 Matnod20 Meth 21 Mato 2 Method 23 Method 24 ol —Determinstion npn produce is tan) ~ Determination in malas tnd cane inert by hyaromeer ‘Bes (oa sos) — Determination in su ‘ions by Abbe etacomet Suoroe — Determination a mil products by Sout polaaie “oualsls (ry sibwance) — Detention ‘nl rode Reding sapare — Determination in all [hws re jue abd pa produc bythe ‘onstat vue moan of he Lae aa Eynon method Reducing vgats — Determination in mill proc bythe Lane and Enon method ‘Total ug (er inversion)— Determination ‘ole mowifcaon ofthe Lane and Enon metod ‘Supersuraon and saturation constons — Descrnlnan nan rods Visosiy determina npn rods Matas Mato 6 Method 27 Metod29 Mato 30 Math 31 Matos 32 Method Mato 36 Mato 37 Matto 40 Faby — Deterlation in products othe fan soar ‘Ash —Determiiton nse prod yt ‘Sepesulbationetbod ‘Ash — Determination in sugar pots bythe out aipaton method Dextran — Determination ia a sugar and ‘Snr rode by the alcool haze wetod Phineas — Determination nr ga, ‘rue cae le ‘ing wl o automate polavieters Moistre — Determination in caw sugar by dying acacia presare ‘Reding sugas — Deena nam gar bythe Laneand Byron mebod “ota clour (slur inden) — Determination Affine close— Determination na suger ‘Amine ogra — Determination naw sur fd pods Filey — Deteinaion nr sae by Starch — Detain i a agar [Acluble phosphate — Determination ‘sgn bythe ail mead Passes a sie estebaton (gs) — Datereaation new gat Mean elopgation — Determination in aw ote waters fet nd leaning oaions Matos Mato Modes Mato 6 Met Method 9 Method 50 ‘Alkalinity, total aleainty and caustic ‘Ballaty — Determination a mater (Choise — Deeminaton in casi 20) (Chorite— Deerninaton in war ‘Soluble phosphate — Determination i water by theamolmebod Tot dvd sds —Eximatoninwaterby Stipe — Deteioton a water Total hardnese lean and mages) — Daeninatlon a water by EDTA tiraoa asened oxygen (D.0.)— Detrmiation in ster he aie modeaton ‘Swerve soluble sali — Determination nine ‘Sucrom® — Determination nfs by te phcnlpheric ted meta Biochemical oxygen demand (BOD) — Determinants va xt xu tt xv REFERENCE TABLES “Temperature coretons 0 reaing of bee byrne (eae! 20°) Smita for scrose (pd in je for we Inthe nd metod wih undue sous. ‘Noroal Weight of 2620 “able of factors forthe clelaton of ol pt jal fom pol eaig for we tery {End mato it unde soins aso forthe aati of sucrose accoring to lackeon aod Gills Method 2 of double plats, “Temperature conection for plain polation ‘eae i eerminaton of rte by doe {Sucrose corresponding to vais vas of (for ba normal salatons at various uaerauts, frase in Jackson and CIS Method 2f double otra 1 Poin bagase This Table isthe polinbagase (ais agate moisture) corresponding to the Dicer reading wet dsitegrator Ml Bart tps 10 parts ater when end na oo ma ube on a ug plait Tr wet ‘dno panty of 1.90. Refaive tices of sugar solons at 29°Cin ‘tne 20°C, 760 mn pres and 0 pe ee reste ami “Table of erpertre cretion for the Abe ‘eta sabre 20°C “The efratv index of pure water at vasious {emperaurey, elae toa Gum ie) “Temperature coretons to be applied to Fetutometr reading of sucrose salons of fier aa eaves rin, te dense aed socentatins of scose son a 30° corresponding 0 rene inden real ‘Selby of suo in watering weose Spe To g water According to Chris, Amt heh. "Soe, 1956 Abs of Papers. 100 Reported rinepie of Supa Solty of acre in watering ron per 100 oan (Chat). Denes of oon of cane sua a 20°C in idm Te table the ba for sana Sydrometers inating pe cent of sug at 2c) rig, apparent dense, apparent specifi roi and grams of Soro pe 10 of ‘pein. xxv xxx Celt 505 xan eal We of prema syeup eed (eween 2 7 mes after aplication of pes) a ‘trou al teperetore andere sanded ‘Stone ia Specie run of srs Cota comets masecuts Degree of supecsaturation ~ al values beng refed 1 Dens of water temperatures fom 0 to 102%. AssordiagtoM, Thine, Wis. Ath fer Physnaloch Teshlschen Rehan he 11900 Corrsons or emperatre 1 be aed tonight of mtercosalaed oobi ome (Gem of veel at 20°C. Nominal capac Sood. or vec made of soda as) Corrections for atmospheric pesure Gin) 10 feed oor subtracted fom the weet of ‘roe ontaised to obtain volume Gin) oF ‘evel at stand empertae and presre Requirements for apparatus for use ia the sub ane for pment pro. CCorectiont 10 quarts plate polarisation ‘ending forth eer ofthe ua se Coons topsarnsoas or tompeatrsof ‘making tothe ark — Gu Conresosto polarisation ortemperaturesot reading (Co Corsetons fo polarisation easing fr the ‘Sof ylanmeer tempera Milgrams of reducing sugars cequred to fede 10 Feblings Soliton (Lane and ‘Eynon mek. ‘Showing sams of product to be welged on per 100 mL of trating slution, forthe ‘cerminaton of resin sapssin product of ‘vous sore ad reducing ugar cones, Grams of eusng suas (as iver sus pet {0m of tteting solution for various sd lt nd rroseconcetatons of 255/100 aL. (Grams of rtucng spars as invert sg) Tide sting ston forvrourend pos, Andauconsconntratonsof 03 p/10 aL Proper of rate tea, aula Volume nd espa equals, Mass equivalents easy equivalents. near mesure equlales ‘Surface and are equals. Presure unas Heat, cow and and work equals et fw esas. Mecano tases sds. {Capacity of borizontal eyes tanks at varying. XXXIK Boing point ton of ug slatons and ne jes) at 760 rm pres Internationa atomic weighs, 1971 Pubes ‘by Perry and Chon, “Chemical Engines Handboot" Pith ain, PREFACE TO VOLUME 2 ‘THE STANDARD LABORATORY MANUAL FOR ‘AUSTRALIAN SUGAR MILLS ‘Volume? ofthe Laborry Map, Asia! Meth a departure rom he forma nd binding of prvons manus 1 thse an Af formats been adopted wih methods and tbls bound in ing bind wich wil pena This facta te ve of he als 4 nboraory workbook, Methods ae numbered and stared on separate sews wth page numbering within ethos. Tis Into acta he elacment of meds wih became cole In hs ny mend updting shoud beret te cri outa more roqee intra ad extra methods ued as read. ‘The production ofthis umes been underakn by a goup comping: Me PO. Ateton SES Me AG. Noble BSES Mamue GR MiGs. owe SR Moreton Skt Mr Dit Pose SRI Assistance wth wring and checking f various bas ben given by a aumber of members ofa of BSE, Suu Reach Inst nd CSR. The work fl ooo ately asked Director of Sugar Experiment Stations NOTES [NOTE 1: Change to Petar Sale [Atte Ih Session ofthe lntrnationsl Commision on Sugar Anais ICUMSA) ld in 1986, an nortan’ change was made othe definition of te Intemational Suet Scale. The new sal wes ‘Lin fore ineratiaal ul Ist 188, nd wa doped for ane pane in Quaesand forthe ‘The datin ofthe normal spr solution eas unchsnge, i. 000 grammes of pr sre weighed wih bas weighs in under normal contins (O13 WP, 30°C, 50 RED dsled pure ‘ater and made upto 10R000 cm st 20°. However, the rotation ofthis solo, messed in 8 200.00 mm tbe #20 °C with Hk of « ‘yeni a 546.227 nm has been changed, allowing pase realaton, ot #0765 dees o {777 degre. A able of rotatns at varous waver at Ov eon Angular rotation of 10°, point acum wavelength Angular ation = New mae, Previous mln, c ‘fon Veet saoa2n «am a7) Ss 000 sae Gaon, sussoor Mien Gesi6) caine Bast rs) 4, ffeive wavelength ofthe xandaré quart wag stsharineter ‘+ Mean cfestive wavelengi of spec red sai jelow Bet Readings ken sig the new sealer designate to dstingus thar fom Sn practi terme She change means hat rotations onthe new wale (2) ar 099871 of rtaons on te ld 3) see, ft hs corraion factor sane Usd tacos ld valet in'S too les Polarieters and quart plats ae now sanded a "2 by BSES. A fll isertacion on this change case found in an atic by De M.R, Plager fn the Jy 1988 sion ofthe Tteratonal Sugar Four, age 130-3. NOTE 2: CCS. Formula In ode o msn ety or cane payer change wat mide to thee. formal In eet ator of 1.0025 has ben at the form 9 tht now read: C CCS. = 1.0026 (Pol in cane — 35 Impure i Cane) DEFINITIONS or IRs ero i everence fom the truth. The word i cooly wed a death dito etwem heed ‘aise andthe "ru valu abou te "tru ale Uhl unkown Thre ae fo important catego Random Error "hn sven measurements repented hei in gee, dingecnen between the resng fia! values. AR ‘ror which individual unpredictable a random exo. Fniielong rn the sera of random cor tends omar Sytmatie Bror ‘Asptnasc eror isan vor which ests digas coh sue or simlarnesurenet anaes ad SHES sot clnited by the simple proses of serie ‘Deeinae ever are hoe which cn be crated by sone oneal proses cer horton experimen tors wich canna evo cated ae cll dtm Random econ te detrminte becuse they can be saint by application of saseal thor. Systematic ‘tree may rometme be elated ty ealtration wih a ‘hrs or by mbar epee, Preion ‘Preon ie gnc em forthe ovens of apement eta theres feat esr posed ar smal ano erst ald to have hgh reson, Depending o comstanses the precion fa prose ‘ma espe yon or moro he own ts sta (ard deviation, epeuabily and reproduc Standard Deviation “Tne sadard deviation he var root ofthe quay quia the sum of qvares of he dvations of ina ‘Sts from te mean valve ve by ope les than the umber of vse the ae ‘Note that the term se” defined a fering 0 the number nt of independent pate esiemets Fm “Te vacacs the gue ofthe standard deviation an isthe biased esate ofthe tv, But union, Sarianse shih i generally ea the Sma Reaive Standard Deviation (RSD) "Tine the magne ofthe deviation compared with he RSD x epeatabiy "Fae value st or teow wich he absolute dlference tucson te rub bed withthe ame bod ‘nent et mater wader he same contons ame ‘peor, sxe appari same laboratory and a short, Inerval of time) may be expected tole wih 9 specified ‘rbubiiy; nthe absence of other intone, he rob sy 1 938. "The 98 spent is eltd 23 whee tic tubised Ste the wihabortry weance Reprodecitty "The vale st of Dow which the absole diference ‘ese ale te rks bie with eae method (nlc et arial nde fee conn (erent hwtors fen pars iter: orto aoe [Titsent tine) ay beet witha speed ros ‘igri the acoso ter eeatons, the probity ‘The dst eproducliy i cleus a 203 whee ‘amnesia fe som of teen abr ‘asunoe andthe nthintabostoy arlaee ‘ncuty lames of how oe the et tothe tue value Atmeatuennt adobe accurate! he best vale Urmean val of ast of oberon shows no dsenble ‘dst fom he real athe amt eo sal Preclon and Acorcy ‘Messrement may epee witout eng ncaa i eration may show small caer al ough thet Bes OF ‘ean mle departs rm hee vale ‘surements may be acute without being preci thobest or mean value may not deve rom he ae al, {ow the mae of osevtions may Be wie Retrnce Beers 0985). “lnuoduction tothe Theory of sr" ‘AidoniNiaiy Publishing Ca 2nd Eon, 1958. BS s97— Pare 1973, ouden, Wad See, E. (979) "Sail Manoa fhe Aoiaon of Offa Anaya Chemis" [ASRGGT 83, Chen Tesing Sapling —Closary [RSIBS0— 1986, Chemis Ants — Intelbortony Ts Propane for setemining Presson of Anata ‘Mahod) — Galde othe Panag abd Condo w a0 METHOD 1 P. METHOD 1 CALIBRATION OF POLARIMETER BY QUARTZ PLATE CHECK SCOPE AND FIELD OF APPLICATION ‘This mebod describes procedure fr calating ‘ata de sanar. The posstar deers ne "eae coe” othe polarimete, which ores forthe elton ror ofthe potter 20°C ‘Th covron Wade to the paarmetr rend when caltg polation reul ung the Tiehods “Polration ~ Determinton In Raw ‘Scale Constions ouside the range 95° 0 100°2 {This meld detrnes the sale correction net Ios i eine ott ge aummle ire scale coroton af 100°Z (SC) ‘au10% then te ele carton a 3072 (SCs) sola be #008 PRINCIPLE OF METHOD Inia Scate Crmection ‘Sn inl sae covet is deteined it he polaister scale coetion bs nt bon (nese for an extend pri (more thn TS a9. «+ Tutienancs as been caro out on theinseumet sch hl te hae feed ealteation oe ‘Batpl:emval of th eae or adjust of te fserfernce ey eunning verge Sele Coreton Theruning vege see corcion™ isthe erage he nt ten ale cretion Setrmltons an thecal coneon apis during the normal ope thon fs nbn. Tas rate es "sooth ‘ot the nea! asics ua eal cmee ‘lon determinaonsAs he cabration of 2 pol Inter dort army ange Soden. the wrenge ‘fn sedge il asin represent he cles fiw of the planter ial the readings have bce taken within the ls 15 as Polrincters Used for Cane Payment ‘okie which reo for ean ayn In soar ‘nl should have a sal coreston teenen ~O1°Z ‘CAUSES OF CALIBRATION CHANGE ‘Thecaliation of mans! printers very stable, ‘be catratio can aormally only be afc ty ‘hanging he aligaet of the Sale ‘While th callin sabity of tomate polar ‘ses gods they are mre prose to dit han ‘Sanus poitncrs Te most commen cause dit he aglay ofthe inerfrence ier wed In ost Sulonatiscsl polaris: Tis normal ast proces seta O1°2 per ont) but can besome high a 017 per aye cad of the ese {Tere we a numberof eer seoae and epi [obloms which can cause eaibaton change rey NOTE: Changing the "REL pmber onthe “Pola ‘rool pole wl ang is calbraton {in thttore the sale svesion DEFINITIONS Qe Theerid vale of the quart latest 20%. 85 he potaranon reading (2) of the gare ate temperate ty —Thevemprtre fh quar plate (*) atthe Tine of aig ip —The ambien temperature of the polite C6; Geoed to be egal 10 in tit beth. ~The coretion to beaded to he quart plate okssuion reading 10 correct Tor" he fempeatue ofthe arte pate Go — Tae cotstin to Bonde othe polation ‘eating to covet forte temperature of the felsnmcte sc — Presse conston of he aimee a 10" {oo for terse etalon err a = tier temperature of 20°C. j—The sale corso fo Be aed when she orton ceasing () foul Whe range Bere wose. APPARATUS ‘Thermometer, lene 20 om, 1035°C, readable to one erie quart contol plate inthe ange 98°72 co ose (Goa oar! pases sal be sandar plates which Sorter ceria by BSES, Beste othe National Messerement Laboratories (SIRO, S30) Quart ter shoul be eat every re Years INSTRUMENTS. ‘The plana under ws. (Care Potrero lah tae clean be {Snes have to be moved foe Sing, sae Soule Detar when eel ht hey af ot eee {hotisy thus being anes a becom op {ahysstv wre reading wera samples fate ‘nh ugh canines stern te opal com onsite ofthe sample othe tae ican he tr fiers on sotomate poarinces ‘enya ons pr mnt) sad ae ob ‘Sex wo alow 4 ts tow of ie {oc of Poni Losi polar whee ‘uTooc behest by et atone ua) fete sbjcted to eesive viaton, ‘Toemmometr Laeton. Wilh ssl polarimeter ‘Bhcethetermomerer nthe plenaer ough r ‘Thole nar he printer Do at plac the the Toner the oups of soa planets the emperature wil above ambit and wil oot Inacte he tempertre of the quarts late. A pos tloesanair mero the plainer sae METHOD 1 F2. a am aa ‘Quarts Pate ioe he gure platen older see the elaine such tat no ested by det ‘aaton ory war a cares rom hese ‘Wit tomatic polarimeter potion neta ai Int smn ata Sr te gure platen po too fo at lest 30 minute before mensremete te ‘aid otis oder hat teach theal elas ih the thetmomter and the polcineter, PROCEDURE [A. SCALE CORRECTION DETERMINATION ‘rT AUTOMATIC POLARIMETERS Reo te oprte o e :plete o 00" Suara wedge instumeats ~ see 89) lbw the ‘dingo the empty poling to bleh et lace the quarts atin the polaris ough wit ‘mam of banding and hse the hd et ‘low the planter reading to sabe a ord the reading Oats four dings ating the uate pine tough 45" between ech rating, Ente the Tis close wearing. Serge the ou eae: fd record to he nenret 00172 Ths ithe qu ‘Dla reading. Qt erpertre Femove te quate, lore the and heck that {hepolarimer tures = 022° ig pe whet [NOTH IF AFTER A SECOND SET OF READINGS ‘THE ZERO STILL DOES NOT RETURN To = 002", A FAULT INTHE INSTRU. MENT 3 INDICATED. THE. INSTRU: MENT SHOULD RE CHECKED BY A (QUALIFIED SERVICEMAN. ‘See Sein 8 for he aclaton of cle comet, 1B SCALE CORRECTION DETERMINATION ‘Writ MANUAL POLARIMETERS laze the quart phen the prime tough with {minimum of handling and lose the Md ges. Sethe sale owed the aporonmae vate of the ‘art pie an aj the oes of hah te id and tetrad elec Rottethe elena knob tna left and gt Sith deceing mpi, Colour and intensity ofall econ of he fide ua Aways cose kd bere blac the fil Read the sale seine tthe sere 4S" for BAS Doarmeter of 001% tor Sait polarimeter cesar interpolate ben det eer resins). ‘ke two or move sigar reading ao nor ror Record the et fou rains sting he art pat 45" beroeen edn Chee and esr al for ‘a eas the st a st ofthe four readoge four readings arent win aang of 020°, take hotest of four edi, ‘Average te four ean std rcord to 001°. This {ste quar pla ane. Qt espera ty (Open the trough tnd etd the temperate to te ‘erest 01°C ad for This isthe fempeatare of Ihe quartz plat at the Une of reading. 2 sary oer temperate wih guar wedge boaters Gee 84), Remove the quarts plate and lose the i 1 obtan the 20 reading St the Sale of he ms oy 4 as arin approximately 02°72. Check the {cus of bk lesopes nd ensue that te ough Is cowed Again balance colour an ina fie ‘els and ear the renting Spy ofe the sae And repeat the balncng se rein. In this Wy, ‘eee four eating al orf the eaings cn tithinaange of 007, cara and take ner et tour edg, Aveag the fou ending and record to thenearest G1"2 Ths te pore om Pe Se Sesion 8 forthe eneiaon of cle corteton (© DETERMINATION OF AN INITIAL SCALE. CORRECTION “To deen a “na Scale Corton” at ia 20, Inoerane snl coretons ar reuited Tb ie tolerance ll ests ms Be within IN ofthe ‘serge of the rele ‘The sale coneton determinations shoul beard tore aperedof 21018 das To minnie syste She tory each of the determinations shoud be Separate by 3 prod ofa Feat ho. Ws dea taal ofthe supra who wil) Se tsing he polrimeer core cal othe oa of 20 daerminatons req. Ti partly {pecan wth mane polarimeter ‘CALCULATIONS A. CALCULATION OF A SINGLE SCALE ConRecTiON VALUE ‘helaowing rags ave been resort (Qu the gore plate reading at empertue fy CS te tempentre of the quai plate andthe ‘lacmacrat he tine of eadng (red for Scepter oy) Py —the polarimeter sero rending (manval foarte on) (Qo — ficcried vu ofthe gure late a 20°C, Clute the average quarts pst acing, Qu Dateline he even to the quart pate polis toa for thetemperstue of the guar pst Cy fom ‘le XXVI aud for ci polsimetes Sl) Catele the average tro read, Py Cor antl polaris on). Determine he cretion 1 the plasation rang for the poliineter tempuature Cy fom Tae XXIX (tl equted for cule polite wit an inerteoce ter, Noe that Calculate the scale correction at 10082 (SC), from: SC = Qu = (Qy # Gy Ce + Po Teton npinon sich an Tad wa of te at ats sr ao ied he to ovr 2c) ons cd ck SC = Qe = Qa Gy Gy) + By x A! 2. wih aus dt comps plese tem and nat a er ‘Soaton'o ho vod tna he ut pte ‘Sep etnesstr pots c temperate Hen sot pss to mestre ‘he temper wih quarts wee instrument. sulfa sae conection ude he anor 98° 0 105° Irene can be lalate fom he onan: 8, ~ 75 x sc ‘isthe polation in at which the {esrumea Is beige, Styne sale sorocon fre polation ‘eating of PZ [RL CALCULATION OF AN INITIAL SCALE ‘CORRECTION 1.7 ‘Avleat oncvdan wate core sls mst be ucrmined (4-116 and 8186). alelae the ‘erage sale coreton from al ul 8 Decioe the rent which furthest from the ‘Sse srg ele creon ths es sme than 2-087 fromthe average al otto, hen ‘hmatei from the stand vcleulat te aerage cal coreton 9) Repent Bul a elt ain oleae fers METHOD 1 fous than 20 reas remaining, the fre eer nuns sould be mate “Tu aeag of ot 20 tolerance sale cretion ‘erations the inital we correction for he CALCULATION OP THE RUNNING AVERAGE SCALE CORRECTION “Tee “Running Average Scale Correo it dtr ‘oy elaating the average he st tn ae tein deermintions ono the en velar wish ae we calculate he Zing sage mae cretion shoal be mre han 1S dy ol. ride oma at ast one ete natn per iy. Howey al en aes should not etalon on te on I a sate coverton determination ix more than dt from the eure running average wal or ‘tonto te dtermioton shuld be repented. (herepetdtranaton rao ot af lero hen the plaints be cece and nna sae ‘Srrton oul the Be enabled [SCALE CORRECTION DETERMINATION ORK SHEFY (Method 1) Anat a B 2 3 2 o 2 doe QP ring % QP. Temp. etre. y= 4 a rains z z % Ave eo rain, Pe on ECA 1s eae ‘QP. Cerified Yue Os z (QP, Raang, Oe 2 Cotesia Cycle XXVD z Cmrstan Cs (ale XXIX) z 2a ein, Po a ‘EALCULATE THE SCALE CORRECTION AT 1007 FROM EQUATION: Sn Oe (Oy + Ga + Cy) * Pe SE = Oe = Oe 2 se> METHOD 1 Pa. WORKED EXAMPLE SCALE CORRECTION DETERMINATION ‘WORK SHEET (Metea ‘Quits Plate Na 487 Anat UR, Smart Dae 29485 Polritr Manual B & S READINGS CALCULATIONS ‘QP. racngs b Ree ‘QP. Cen Valve 5890 $9.08 % $00 ‘Ae OP. ang, Ox 98.98% QP. Raatng, Quy 598 QP. Teme. 2asTe Cention Gq Cable XXVD 0012 Parmeter ey ‘Cetston C9 Cale XXIX) aed ar reais @ -007 @ snas “ooo 6 2a rdin. Pe 00s uw wo aa 33 a6 Fa au a METHOD 2 PA. METHOD 2 POL — DETERMINATION IN JUICE SCOPE AND FIELD OF APPLICATION ‘This method tas ten azopte ofl within the ‘esr sugar ings Tt comple wih the ‘Roum ofthe Regsnon of Spar Cane Pros [Rises forthe ana of Istexpresed ie fer payment for cane delve wo ll ‘Thetmehod i appisblseot the detention of po inal ter Cae and male PRINCIPLE, ‘ramp of thee clarified by ding ba ead tat pode (whch coagulate celled impuris nd remove some color alowed by fraton. The ol ofthe died solton ead in polarinett ‘She f sandard ngs in = tga pounce Ith le fom cert ane anna bead ty bend neat powder, soliton of lad tasters head (ere Reagent wed. diay aorsory apart and lassware and Shear Polarimeter, All ease polit for fist ‘Sted Jc asi for sae pave purposes aus be ouified for ane inthe. Abtraian Sugae Industry by BSES. Automate spar polarimeter ould conform to he Australia Standard IST (Quarts Contr! Plates, Qui cono aes us be (franc fy BSES or bythe Navonal Mesut {aborts (SIRO Syte) ‘obi tn 210m log and cover hss con Forming with ICUMSA (979), Subject spestin- ‘Sim Awana oe conus ple can bee. ‘ottubes shoal be serce by BSES. Ice cm, lati or eal ‘Stem ter fanned ss or plastic 25 cm da {oom apa ‘iter pape, Waan No, 31 oF enualnt ‘Cod ter bath fot noted fori ers ub) REAGENTS ‘ise lend atte ponder (Horo Dry Lend, having the flowing spesitstions Base Lend (ar POO) ot ess han 386 ‘oa Lead (os POO) ot et has 258 Bas assure (2 at 10") noe eeaing 155 ‘gin sOmL wats): not ecening 20% Inslale M {Sig in 10) ma. of 108 sei) not exenting 2055 Finens hough 25 riser 08 trough 125 42 Hee Regent Ssition A" Disve $00 + 01g sodium box (ae water and ue 1 rie ina ‘amet is isle 00 adnate in wats aod dite to 1 ire i Volumen tk, “Ty check th eget egal Volumes of suns ‘Nand and mest the plo he med slow {ithe pH abo 7.0, sation A dted unl be relat mined tla gves a pH below 10 Suey ‘dad i bitoni, comet pison. esos who ‘cg ato yd oe ng Po shuld Sve an ona lod tou ol hospital of ‘cspanal bealh autores, ate somaners Lael contigs in which ‘sy lead soliton’ or com pounds i noreé or el, Sie the same ad ao peso ‘Avoid ageing lead: Awaye wash hands ‘orouphy “fore catog ‘Awe wat a as and ‘pots beta dst when Sanding. Powe. Do not ‘ink ro borioy sas vo abrorting lad = Dey bad th band towel, ot Iboratorylaseare tomel Wear glove ed pro ible Rep led eget and Tend olson say fom Display presatone On laboratory notes board ‘atte duce voting wit 108% gucous mages shale Tow th eo we eal water Sot Teal atenon Dispos of ead wate: Pace ll water contiing fy led engin psc bake wih all filled with ery sodas (odin carbonate) pond ‘The bucks sould ne © Sih ig a and be Ste hed “Posed ‘ane Asumalatad ead ‘ste shoal be coed {oan autorbed eae mate 0 CALIBRATION OF THE POLARIMETER ‘The panera est cried gut Pine Ave coreston Srmied and apple 0 Sohn B 6 HOD 2 P2. the potato reading of the st sample. Refer t0 ‘he metod for "PolarinetrCalbraton by Quarts Pte Check Altenatiely the cllation of the puree shuld be ated och thatthe eae forestion i isgiieat. A ICE CLARIFICATION foros cool he ae to rom epee in 2 ‘pl wna ath a oon asthe sapien ‘Traer 150.200 mo 4 dey 250" oling ask on. rmadiatey athe minimum quaniy of dry lead ede fo lay the Jule. For nora ues out 10 _/200 mL dy edi suet or aces hat ae

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