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Chem 2 Prac 28 Rida
Chem 2 Prac 28 Rida
of Pharmacy, Akola
D.Pharm – II Year
Experiment No. 28
Title: To Prepare and submit computerized report of Expt. No. D8 (Any one
compound from D1 to D10) By Systematic Qualitative Analysis.
A) PELIMINARY TEST
Sr
Test Observation Inference
No.
A) Colour Yellow-Orange
Nitro Anilines
B) Odour Phenolic
Phenol
Solubility Behaviour
C) 1) Solubility in Water Insoluble Insoluble
2) Test with Litmus Acid Acids or Phenol
Conclusion: On basis of the test performed above and with reference to the handbook the
given organic compound / drug is:
1)Aromatic
2)Unsaturated
3)Acid
B) DETERMINATION OF PHYSICAL CONSTANT
Conclusion: The boiling of the given organic drug or compound was found to be 182℃
C) DETERMINATION OF ELEMENT
Sr
Test Observation Inference
No.
Test for Nitrogen: 3-4 ml filtrate + Solid
A) No blue green colour "N" absent
FeSO4 Heat, to boil with Conc. H2SO4
Test for Halogen: 5ml filtrate + dil. H2SO4 Boil no white colour is
C) "Cl" absent
+ add few drops of dil. HNO3 add AgNO3 soln produced
Conclusion: The given organic drug or compound was found to contain phenol [−𝑂𝐻]
functional group.
Result: The given organic compound was having 182℃ bp, O, H elements and [−𝑂𝐻]
functional group.
Therefore, with reference to literature, the organic compound may be Phenol.
E) CONFERMATORY TEST
Sr
Test Observation Inference
No.
Structure:
[Phenol]
OH
Category: Antiseptic
Therefore, the given compound with code D8 is confirmed.
Phenol
SIGNATURE OF ANALYST
(RIDA FATEMA)
ROLL NO. 34
DATE: __/__/____